Sl No

Category Items

FSSAI LAB PARAMETERS for IMPORTED FOOD & METHODS FOR STANDARDIZATION Parameters limit as per Method of analysis FSS Regulations followed Chemical parameters i) Moisture % by wt ii)Total milk protein,% by wt iii)Milk fat % by wt iv) Total ash % by wt v)Ash insoluble in Dil HCl,%by wt vi)Added colour 1) Stablizers Sodium Pottassium & calcium Chloride INS 331,INS 332, INS 333 Sodium Pottassium and Calcium cabonateINS 500 (i), INS 501 (i), INS 170(i) potassium and Calcium Sodium Citrate Calcium salt of Orthophospheric Acid, Calcium salt of poly phosporic Acid Potassium Salt of Orthophospheric Acid Potassium salt of Poly phospheric Acid, salt of Orthophospheric Acid Sodium Sodium salt of polyphospheric Acid
2)Lecithins INS 322 2)2.5 gm/Kg MAX Bioelectrochemistry and Bioenergetics Volume 47, Issue 1, November 1998, Pages 2538Chemical codex Chemical codex DGFS manual Chemical codex

1 Milk & Milk Products Processed Baby Food Milk powder

i)Not more than 4.5 ii) Not less than 12.0 iii) Not less than 18.0 iv) not more than 8.5 v)not more than 0.1 absent

DGHS/IS 11623:1986 (R2003) DGHS DGHS DGHS DGHS DGHS

2 g/ kg singly or 3 g /kg in combination max.

Chemical codex

3)Sodium,Potassium,Calcium Citrate 4) BHA 5) Citric Acid with Sodium HydogenCarbonate and / or Calcium Cabonate 6)Phosphoric Acid with Sodium Hydrogen Carbonate and /or Calcium Carbonate

3)2.5 gm/Kg MAX 4)100 ppm MAX 5) 500 ppm MAX

6) 500 ppm MAX

Chemical codex

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Pesticide 1) Aldarin,Daldarin 2) Chlordane 3) DDT 4) Fenitrothion 5) Heptachlor 6) Hexa chloro cycle

( Initial screening for major pesticide groups is preffered)

1)0.15 ppm (on fat basis) AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 IS 14587: 2000 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52 AOAC 18th edition 970.52

Not more than

2)0.05 ppm 3) 1.25 ppm 4) 0.05ppm 5) 0.15 ppm 6) 0.02 ppm 7) 0.02 ppm 8)0.01ppm 9)0.5ppm 10)0.02ppm 11)0.01ppm 12)0.01ppm 13)0.1ppm 14)0.1ppm 15)0.05ppm 16)0.01ppm 17)0.01ppm 18)0.05ppm 19)0.01ppm 20)0.01ppm 21)0.05ppm 22)0.05ppm 23)0.05ppm Heavy Metal i)0.05 ppm ii)0.2ppm iii) 5 ppm iv)0.1ppm

7) CHLORINE VINPHOS 8) Chlorpyrifos 9) 2,4 D 10) Ethion 11) Monocrotophos 12) Paraquat Dichloride 13) Carbendazine 14) Benomyl 15) Carbofuran 16) Cyper methrin 17) Edifenphos 18) Fenthion 19) Fenvalerate 20) Thenthoate 21) Phorate 22) Pirimiphos-Methyl 23)Trichlorfon Heavy Metal i) Arsenic ii) Lead iii) Tin iv) Cadmium

AOAC 986.15 AOAC 972.23 AOAC 980.19 AOAC 986.15

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Melamine Aflatoxin M1 Microbiological parameters i) Bacterial Count per gm ii) Coliform Count/g. iii)Yeast & mold/g. iv) Salmonella/g. v) Shigella/g. v)E-Coli/g. vi) Staphylococcus aureas/g. Antibiotics and drug residue

absent 0.5 ppb 10000cfu absent absent absent absent absent absent As recommended by FSSAI NMT 36.0% NLT 32.0% NMT 50,000 cfu/gm <10 cfu/gm absent

ISO/TS 15495/ IDF/RM 230:2010 LCMS/MS AOAC 18th edition Chap.49 APHA/FDA-BAM-2001 APHA/IS:1622:1981/FDA-BAM-2001 APHA/IS 5403:1999/FDA-BAM-2001 APHA/FDA-BAM-2001 APHA/FDA-BAM-2001 APHA/FDA-BAM-2001 APHA/FDA-BAM-2001

Cheese*

Moisture Fat (ODB) Total Viable Count Coliform Salt of Sodium,Potassium,Calcium salts of Mono/Di-Poly phosphates Colours 1) Curcumin 2) Riboflabin 3) Beta Carotene 4) Carotene 5) Annatto extract Preservative 1)Sorbic Acid and its sodium photasium, calcium salts 2)Nisin

DGHS. Manual /ISO 5534|IDF 4:2004 DGHS Manual/IS: 2785: 1979 FDA-BAM-2001 /APHA FDA-BAM-2001 /APHA Chemical codex/DGHS manual

1)NMT 100 ppm 2)NMT 100 ppm 3)NMT 100 ppm 4)NMT 100 ppm 5)10-50 ppm

DGHS/IS:2446-1980 DGHS Manual DGHS Manual DGHS Manual DGHS Manual

1)NMT 3000 ppm 2)12.5 ppm

DGHS Manual/AOAC, 18th Edn. 2005, 974.10 DGHS Manual

Microbiological Parameters* as per PFA(see the note below)

Total Plate Count* Coliform * E.Coli* 50,000 / gm Max absent in 0.1 gm absent in 1 gm IS 5402 : 2007 FDA-BAM-2001 /APHA FDA-BAM-2001 /APHA

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Salmonella/25gm* Staphylococcus aureus* Yeast & Mould* Listeria monocytogenes * Anerobic spore count* Heavy Metals 1)Lead 3)Arsenic 4)Tin 6)Cadmium

absent in 25 gm absent in 1 gm absent in 1 gm absent in 1 gm absent in 1 gm 100/gm 1) NMT 2.5 ppm 2)NMT1.1 ppm 3)NMT 250 ppm 4)NMT 1.5 ppm

FDA-BAM-2001 /APHA FDA-BAM-2001 /APHA FDA-BAM-2001 /APHA FDA-BAM-2001 /APHA FDA-BAM-2001 /APHA

IS 12074-1987 reaff 1998 IS 11124-1984 reaff-1995 AOAC 966.16, AOAC 984.27, AOAC 985.35, ICP AOAC 966.16, AOAC 984.27, AOAC 985.35, ICP, AAS AOAC 966.16, AOAC 984.27, AOAC 985.35, ICP, AAS DGHS Manual

7)Mercury

5) NMT 1ppm

Pesticides Residue 2 Refractive index at 40 C or

BDL

Fat Oils & Fats Crude Palm Oil

1.4491-1.4552
35.5-44.0

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/AOAC 18th Edn., 2005, 920.157 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/AOAC 18th Edn. 2005, 933.08 DGHS/IS 548 (I),1964 Rffmd , 2006

Butyro Refractometer reading at 500C

Melting Point (Open tube capillary slip method) Iodine value(Wij's Method) Saponification value Unsaponifiable matter Acid Value

Not more then 37 C 45-56 195-205 Not more then 1.2%

10.0 Max.

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Flash Point (Pensky Marten Closed Cup Method) Added Colouring matter Added flavouring matter Test for mineral oil by HOLD Test for Argemone oil Test for Cotton Seed Oil Test for Sesame oil Refractive index at 40 C Crude Sunflower Oil

Not less then 250C Absent Absent Absent Absent Absent 15 Red Units Max

DGHS/IS1448 (P-20) 1998 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS MANUAL/IS: 548 Part II, 1976 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006

1.4610-1.4680

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006

62.4 to 64.7 NMT 4 118-141 188-194

Butyro Refractometer reading at 50 C

Acid Value Iodine value(By Wij's Method Saponification value Flash Point (Pensky MartenClosed Cup Method) Test ForSesame Oil Mineral Oil by TLC Cotton Seed Oil(Halphen Test) Argemone Oil Peroxide value

BIS METHOD

Above 250 C
IS1448 (P-20) 1998

15 Red Units Max Absent 10red unit max Absent

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS MANUAL/IS: 548 Part II, 1976 AOAC 18th Edn, 2005, 965.33 41.1.16

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Rapseed Oil (mustard oil)

Iodine value (Wij; Method) Polybromide Test Acid Value BTT Test(acetic acid method) Refractive Index (at 40 C) Saponification value Argemone Oil

96 - 112 Negative NMT 6%

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS MANUAL/IS: 548 Part II, 1976

23.0 C to 27.5 C 1.4646-1.4662 168 to 177 Negative

Rapseed Oil (mustard oil) low erucic acid

Total fatty acid Acid Value Iodine value (Wij; Method) BTT Test(acetic acid method) Refractive Index (at 40 C) Saponification value Argemone Oil Unsaponifiable matter

NMT 2% erucic acid NMT 0.6% 105-126

Fatty acid profie using GLC /AOAC 18th ed., 41.1.28 (969.33) & 41.1.29 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS MANUAL/IS: 548 Part II, 1976 DGHS/AOAC 18th Edn. 2005, 933.08

NMT 19.0 C 1.465-1.467 182-193 Negative NMT 20 G/Kg

Acid Value Crude Degummed Soyabean Oil Iodine value (Wij; Method)

NMT 2.5% 120-141

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006

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Crude Degummed Soyabean Oil

Refractive Index (at 40 C) or Butyro Refractometer reading at 40 C Saponification value Unsaponifiable matter Phosphorous Argemone Oil 1.4649-1.4710 58.5 to 68.0 189-195 NMT 1.5% NMT 0.02% Negative DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/AOAC 18th Edn. 2005, 933.08 A.O. C. S. (1989), Official Method Ca 12-55 DGHS MANUAL/IS: 548 Part II, 1976

RBD Pamoline

1) Refractive Index at at 40 C 2)Iodine value(WijsMethod ) 3) Saponification value 4)Cloud Point 5)Unsaponifiable matter 6)Acid Value 7)Moisture

1.4550-1.4610 54-62 195-205 Not more than 18C Not more than 1.2% Not more than 0.5 Not more than 0.1%

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006
DGHS/AOAC 18th Edn. 2005, 933.08

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS-1448(P-20) 1998 DGHS/ A.O.C.S (1989) Official Method Ca 3b.- 87

8) Flash Point (Pensky Marten Closed Not less than 250C Cup Method) 9)Hexane Not more than 5ppm Test for a) Sesame oil (Baudouin test) b) Mineral oil (TLC) Negative Negative

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006

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C) Cotton seeds oil (Halphen test) d)Argemone oil by TLC e)Castor oil by TLC

Negative Negative Negative

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 Adulterants and contaminants in Foods ICMR (1990) Page 14/DGHS DGHS Method using GLC Method using GLC Method using GLC Method using GLC Method using GLC/AOAC 983.15/2002 Method using GLC

f) Tri-ortho cresyl phosphate by TLC Negative

Proply gallate,ethyl gallate,Octyl gallate,Dodecyl gallate or mixture thereof Hydrooxy Anisole(BHA) Butylated

Not more than 100ppm Not more than 200ppm

Any Combination of proply gallate Not more than 200ppm and BHA Ascorbyl palmitate/ stearate singly or Not more than 500ppm in combination Resin Guinace Not more than 100ppm TBHQ Not more than 200ppm

Isopropyl citrate mixture/Phosphoric Not more than 100ppm acid/Monoglyceride citrate(Singly or in combination) Dimethyl polysioxane singly or in combination with silicon dioxide Not more than 10ppm

IS 548 (Part 1) :1964 (R 2006)

Olive oil

Refractive index at 40 C B.R.Reading at 40 C Saponification Value Iodine Value

1.4600-.14630 51.0-55.6 184-196 75-94

DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006

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Unsaponifiable matter, % by mass Acid Value Bellier Turbidity Temperature, C Test for presence of mineral Oil Test for presence of syntheticOil soluble Colour Test for presence of Argemone Oil Test for presence of sesame Seed Oil Test for presence of Cotton Seed Oil

NMT 1.5% NMT 6.0

DGHS/AOAC 18th Edn. 2005, 933.08 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (I),1964 Rffmd , 2006 DGHS/IS 548 (II),1964 Rffmd , 2006 DGHS MANUAL/IS: 548 Part II, 1976 DGHS/IS 548 (II),1964 Rffmd , 2006 DGHS/IS 548 ,1964 Rffmd , 2006 DGHS/IS 548 ,1964 Rffmd , 2006 DGHS/IS 548,1964 Rffmd , 2006 DGHS MANUAL/IS: 548 Part II, 1976

NMT 17 C Absent Absent Absent Absent Absent

Test for presence of Olive Pomace Oil Absent Test for presence of Semi Siccative Oil Absent Argemone Oil Negative

3 Fresh Fruits & vegetables Physical parameters All fresh rotting Fruits
Rodent contamination Added colouring matter

absent Absent Absent

Visual Examination DGHS Manual DGHS Manual Hexane Method Visual Examination DGHS/AOAC 18th Edn. 2005, 970.52 DGHS/AOAC 18th Edn. 2005, 970.52 DGHS/AOAC 18th Edn. 2005, 970.52 DGHS/AOAC 18th Edn. 2005, 970.52

Added vax coating absent Mould Nil Pesticide ( Initial screening for major pesticide groups is preffered) Not more than 1)Dodine 1) 5.0 ppm 2)Thiophenatemethyl 2) 5.0 ppm 3)Fenarimol 4)Hexaconazone 3) 5.0 ppm 4) 0.1 ppm

Page 9

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5)Dithion 6)Difenoconazole 7)Propineb Pesticides 1)Chlordane 2)Dicofol 3)Dimethoate 4)Endosulfane 5)Fenitroteione 6)Inorganic Bromide 7)Hexachlorocycle-Hexane 8)Malathione 9)Parathione 10)Parathione Methyl 11)Phosphamidon Residue 12)Pyrethrins 13)Chlorobenzilate 14)Chlorpyrifos 15)Chloropyrifos 16)Ethion 17)Formothion 18)Monocrotohos

5) 0.1 ppm 6) 0.01 ppm 1.0 ppm NMT 1) 0.1 ppm 2) 5.0ppm 3) 2.oppm 4) 2.0ppm 5) 0.5ppm 6) 30.0ppm 7) 1.0 ppm 8)4.0ppm 9)0.5ppm 10)0.2ppm 11)0.2ppm 12)1.0ppm 13)1ppm 14)0.5ppm 15)2.0ppm 16) 2.0ppm 17) 1.0ppm 18)1.0ppm

DGHS/AOAC 18th Edn. 2005, 970.52 DGHS/AOAC 18th Edn. 2005, 970.52 DGHS/AOAC 18th Edn. 2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

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19)Paraquat Dichloride 20)Phosalone 21)Dichlortrichlorfon 22)Thiometon 23)Carbendazin 24)Benomyl 25)Captan 26)Carbofuran 27)Copper Oxychloride 28)Ethylene Bis-Dithiocarbamates 29)Phorate 30) 2,4 D

19) 0.05ppm 20) 5.0ppm 21) 0.1 ppm 22) 0.5 ppm 23) 5.0 ppm 24) 5.0 ppm 25) 15.0 ppm 26) 0.10 ppm 27) 20 ppm 28) 3.0 ppm 29) 0.05 ppm 30) 2 ppm

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn.

2005, 970.52

DGHS MANUAL/AOAC 18th Edn. 2005, 970.52/USEPA 8141 A DGHS MANUAL/AOAC 18th Edn.
2005, 970.52/USEPA 515.1

4 Sugar Raw Sugar

Colour Extraneous matter Dirt, Filth & Iron fillings Sulphor Di-oxide content Colouring matter Moisture Total Sugar (Expressed as Sucrose) Metal contaminant 1)Lead 2)Copper 3)Arsenic 4)Tin 5)Zinc 6)Cadmium 7) Mercury 200 ppm, Max 0.1% max absent 150 ppm max absent 1.5% by wt max not less than 90% 1) NMT 5 ppm 2)NMT 30 ppm 3)1.1PPM 4)NMT 250 ppm 5)NMT 50 ppm 6)NMT 1.5 ppm 7) NMT 1ppm ICUMSA GS 2/3-9-1994,ICUMSA 210-1998 DGHS Method DGHS Method DGHS Method DGHS Method DGHS Method DGHS Method
DGHS/AOAC 972.23

DGHS
DGHS/AOAC 986.15 DGHS/AOAC 980.19

DGHS
DGHS/AOAC 986.15

DGHS/ AOAC 977.15

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5 All fish and fish products All extraneous matter to be absent Fish & Fish Physical Examination Ash insoluble in Dil HCl (on dry basis) 0.1%max products Acidity of extractedfat (as oleic acid) Sugar Starch Added Colour Histamine TVN 1.5%max present present Only permitted colour up to 40mg/100g & 10/100 g as per codex 3mg/100gm max

DGHS

DGHS DGHS DGHS DGHS DGHS Journal of Chromatography A.1032 (2004); 79-85 J. Sci. Fd. Agric. (1955), 6:207-217

Shigella/25gm Salmonella/25gm Total plate count /gm E-Coli / gm Staphlococcusaureus /gm Vibrio Chloerae /25gm Vibrio Parahaemolyticus/25g Listeria monocytogenes Clostridium perfringes Metal contaminants Mercury

Absent Absent Not more than 5,00,000/g Not more than 20/g Not more than 100/g Absent Absent absent in 25 gm Absent

USFDA BAM/APHA USFDA BAM/APHA USFDA BAM/APHA USFDA BAM/APHA USFDA BAM/APHA USFDA BAM/APHA USFDA BAM/APHA USFDA BAM/APHA USFDA BAM/APHA

0.5 ppm max

AOAC 18th Edn.2005; Chapter-09, 9.02.23; 977.15/AOAC 988.11 AOAC 18th Edn.2005; Chapter-09, 9.01.09; 999.11

Cadmium

1.5 ppm max

Pesticides 1)Carbaryl 2)Endosulfan 3)Hexachlorocycle Hexane and its isomers 4)Quinolphos

Not more than 1) 0.2 ppm 2) 0.2 ppm 3) 0.25 ppm 4) 0.01 ppm

AOAC 18th Edn.2005;970.52 AOAC 18th Edn.2005;970.52

AOAC 18th Edn.2005;970.52 AOAC 18th Edn.2005;970.52

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Antibiotic &OtherPharmacologicallyActive substance A) Tetracycline

Categories of antibiotics to be tested

1) 0.1 ppm max

AOAC 18th Edn.2005; Chapter-23, 23.01.07; 986.15 AOAC 18th Edn.2005; Chapter-23, 23.01.07; 986.15

B)Oxytetracyline

2) 0.1 ppm max

C) All Nitrofurans including 1) Furaltadone 2) Furazoliddone 3) Furylfuramide 4) Nifuratel 5) Nifuroxime 6) Nifurprazine 7) Nitrofurnatoin 8) Nitrofurazone D)Chloranphelicol

1) Absent 2) Absent 3) Absent 4) Absent \5) Absent 6) Absent 7) Absent 8) Absent D) Absent

JAOAC; 1994; 77(2), 344-350

Petz, 1983, Z.LebUnters. Forsch (176),(289-293); J.AOAC

1990 (73), 813-16 &Central Institute of Fisheries

Technology Training Manual; Page No: 07-09,14,15

E)Sulphonamide Drugs (Except Approved Sulfadinethoxine, Sulfabrononethazine and Sulfsethoxypyridazine Sulphalethoxazole

Sulphamethizole

E)Absent

J.A.O.A.C Int. (1994) 77 (3) 558-564 Absent Absent Absent

Sulphadiazine 6 Meat and Meat Products Frozen Meat Total Plate Count E.coli Staphylococcu s aureus Clostridium botulinm and Clostridium perfringes Yeast & Mould Salmonella Listeria monocytogenes Heavy metals

100000 /gm max 100/gm max 100/gm max 30/gm max 1000 /gm max absent in 25 gm absent in 25 gm

IS 5887 (P-1):1976 IS 5887 (P-8):2002 IS 5887 (P-4):1999 IS 5887 (P-4):1999 IS 5887 (P-3):1999 IS 14988 (Part 1):2001 USFDA BAM/APHA

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1)Lead 2) Tin Vetenary drugs Preservatives Sodium nitrite Canned meat ( Canned Luncheon/Cann ed Cooked Ham/ Canned Chopped Meat/ Canned Chicken/ Canned Mutton and Goat Meat Total fat content a)Product with binder i)Canned Chopped Meat ii)Canned Luncheon Ham b)Product without binder i)Canned Chopped Meat ii)Canned Luncheon Ham Total Plate Count E.coli Staphylococcus aureus Clostridium botulinm and Clostridium perfringes Salmonella Listeria monocytogenes Incubation at 37 C for 10 days and 55 C for 7 days Heavy metals 1)Lead 2) Tin
Veterinary drugs**

1) 2.5 ppm max 2)250 ppm max As recommended by FSSAI 200 ppm, max

IS 14988 (Part 1):2001 AOAC 985.16

IS 5402:2002 IS 5887 (P-1):1976/IS:5960 (Part-3)1970 (R-2005)

30 % max 35% max 25 % max 30 % max 1000 /gm max absent in 25 gm absent in 25 gm absent in 25 gm absent in 25 gm absent in 25 gm No change in container

IS 5887 (P-1):1976 IS 5887 (P-8):2002 IS 5887 (P-4):1999 IS 5887 (P-4):1999 USFDA BAM/APHA USFDA BAM/APHA APHA# 4th Edn. 2001, 61.51

1) 2.5 ppm 2)250 ppm

drugs as listed by FSSAI should be screened

AOAC 972.23/AOAC 999.11 - 2000 AOAC 985.16

Depending upon the drug any

Preservatives Sodium nitrite

as per persecribed limits

200 ppm, max

DGHS Manual IS 5402:2002

7 Dry Fruits Almond

Extraneous Veg matter Insect Fragments Rodent hair &Excreta

NMT 1.0% absent absent

DGHS Manual DGHS Manual DGHS Manual DGHS Manual DGHS Manual DGHS Manual

Added colour absent Acidity of Extracted fats as expressed NMT 1.25% as oleic acid Mould Affected absent

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Aflatoxin Total

30 ppb max

ELISA (J.European Food Research Tech; 210; 213-215; 2000) /AOAC 18th edition Chap.49

Pesticides &Residues 1)Chlorienvinphos 2)Chlorobenzilate 3)Ethion 4)Carbendazim 5)Benomyl 7 Nuts & Rasines

1) 0.05 shell free basis max 2) 0.2 shell free basis max 3) 0.1 shell free basis max 4) 0.10 ppm max 5) 0.10 ppm max

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL

Cashew Nuts/Raw cashew Nuts

Extraneous Veg matter Insect Fragments Rodent hair &Excreta Added colour Acidity of Extracted fats as expressed as oleic acid Mould Affected Aflatoxin Total

NMT 1.0% absent absent absent NMT 1.25% absent 30 ppb max

Visual Examination Visual Examination DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL ELISA (J.European Food Research Tech; 210; 213-215; 2000) /AOAC 18th edition Chap.49

Pesticides &Residues 1)Chlorienvinphos 2)Chlorobenzilate 3)Ethion 4)Carbendazim 5)Benomyl

1)0.05 shell free basis max 2)0.2 shell free basis max 3)0.1 shell free basis max 4)0.10 ppm max 5)0.10 ppm max

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL

8 Poppy seeds

Poppy seeds Physical Examination

Moisture Added colouring matter Extraneous matter Non volatile ether extract on dry basis Not more than 11% Absent Not more than 2% Not less than 40%

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL

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Presence of mould Insect Total Afflatoxin Rodent hair & Excreta Damaged by discoloured unit Salmonella/ 25gms 9 Cereals &Pulses

Negetive Absent 30 ppb max Absent Absent Absent

DGHS MANUAL Visual Examination AOAC 18th edition Chap.49 DGHS MANUAL DGHS MANUAL APHA# 4th Edn. 2001, 37.123 to 37.126

Black Matpe/Green Peas/Chick Peas/Toor/Gre en Moong/Red Lentils

Moisture(Loss in weight determined as specified) Argemone Seeds Khesari Dal Foreign Matter 1)Mineral matter 2) Organic matter Damaged grain Insect damaged byweevilled grain Other Edible grain Insect Microscopic Examination Rodent hair & Excreta Total Afflatoxin Presence of mould Test for added colour Test for mineral oil Uric Acid Pesticide 1) Aldrin 2) Dieldrin 3)Carbaryl 4)Chlordane 5)Diazinone 6)Dichlorvos 7)Fenitrothion 8)Heptachlor 9)HCN

14.0% Max. Nil Nil 1% by wt Max. i) 0.25% Max. ii) 0.10% Max 5.0% Max. 6.0% Max. 4.0% Max. Absent Characterstic feature Absent 30 ppb max Negetive Absent Negetive

DGHS MANUAL Visual Examination Refraction(DGHS)/ Chromatography Refraction DGHS Refraction DGHS Refraction(DGHS) Refraction(DGHS) Refraction(DGHS) Refraction(DGHS)/IS: 4333: (Part-I): 2002 Visual Examination DGHS MANUAL DGHS MANUAL AOAC 18th edition Chap.49 DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL/I.S 4333 Not
DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52

100ppm ( Initial screening for major pesticide groups is preffered) 1) 0.01 ppm 2) 0.01 ppm 3) 1.5 ppm 4) 0.02 ppm 5)0.05 ppm 6)1.0 ppm 7) 0.02 ppm 8) 0.01 ppm 9) 37.5 ppm

Page 16

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10)Hydrogen Phosphide 11)Inorganic Bromide 12)Malathion 13)Phosphamidon 14)Pyrethrins 15)Chlorienvinphos 16)Chlorpyrfos 17)Ethion 18)Monocrotophos 19)Praquat Dichloride 20)Trichlorfon 21)Thiometon 22)Carbendazin 23)Benomyl 24)Carbofuran 25)Decamethrin/Deltamethrin 26)Fenthion 27)Dithiocardamates 28)Phenthoate 29)Phorate 30)Pirimiphos-Methyl 31)Oxydemeton methyl 32) 2,4, D 10 Insect Red Lentils/Green Argemone Seeds Khesari Dal moongs Foreign Matter 1)Mineral matter 2) Organic matter Damaged grain Insect damaged by weevilled grain Other Edible grain Microscopic Examination Rodent hair & Excreta Moisture(Loss in weight determined as specified)

10) Nil 11)25 ppm 12) 4 ppm 13) 0.05 ppm 14) Nil 15) 0.02 ppm 16) 0.05 ppm 17) 0.025 ppm 18) 0.025 ppm 19) 0.1 ppm 20) 0.05 ppm 21) 0.025 ppm 22) 0.5 ppm 23) 0.5 ppm 24) 0.1 ppm 25) 0.5 ppm 26) 0.1 ppm 27) 0.20 ppm 28) 0.05 ppm 29) 0.05ppm 30)5.0ppm 31)0.02ppm 32) 0.01 ppm Nil Nil absent Max 1% by wt NMT 0.25 % by wt NMT 1.0% by wt NMT 5% by wt NMT 6% by count NMT 3% by wt Characterstic feature Absent NMT 14% by wt

DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52 DGHS MANUAL/AOAC 18th Edn. 2005, 970.52

Refraction(DGHS) Visual Examination Visual Examination/ chromatography Refraction(DGHS) Refraction DGHS Refraction DGHS Refraction(DGHS) Refraction(DGHS) Refraction(DGHS)/IS: 4333: (Part-I): 2002 Visual Examination DGHS MANUAL DGHS MANUAL

Page 17

Sheet1

Presence of mould Test for added colour Test for mineral oil Total Aflatoxin Uric Acid

Absent Negetive Absent 30 ug/kg 100ppm

DGHS MANUAL DGHS MANUAL TLC METHOD

AOAC-993.16, 2000/AOAC 18th edition Chap.49/ AOAC-993.16, 2000

DGHS MANUAL

Pesticide residue ( Initial screening for major pesticide groups is preffered) Not more than DGHS/AOAC 18th Edn. 2005, 970.52 1) Aldrin 1) 0.01 ppm Max DGHS/AOAC 18th Edn. 2005, 970.52 2) Dieldrin 2)0.01 ppm DGHS/AOAC 18th Edn. 2005, 970.52 3)Carbaryl 3)1.5 ppm DGHS/AOAC 18th Edn. 2005, 970.52 4)Chlordane 4)0.02ppm DGHS/AOAC 18th Edn. 2005, 970.52 5)Diazinone 5)0.05 ppm DGHS/AOAC 18th Edn. 2005, 970.52 6)Dichlorvos 6)1.0ppm DGHS/AOAC 18th Edn. 2005, 970.52 7)Fenitrothion 7)0.02ppm DGHS/AOAC 18th Edn. 2005, 970.52 8)Heptachlor 8)0.01ppm DGHS/AOAC 18th Edn. 2005, 970.52 9)HCN 9)37.5ppm DGHS/AOAC 18th Edn. 2005, 970.52 10)Hydrogen Phosphide 10)Nil DGHS/AOAC 18th Edn. 2005, 970.52 11)Inorganic Bromide 11)25ppm DGHS/AOAC 18th Edn. 2005, 970.52 12)Malathion 12)4ppm DGHS/AOAC 18th Edn. 2005, 970.52 13)Phosphamidon 13)0.05ppm DGHS/AOAC 18th Edn. 2005, 970.52 14)Pyrethrins 14)Nil DGHS/AOAC 18th Edn. 2005, 970.52 15)Chlorienvinphos 15)0.02ppm DGHS/AOAC 18th Edn. 2005, 970.52 16)Chloriopyrfos 16)0.05ppm DGHS/AOAC 18th Edn. 2005, 970.52 17)Ethion 17)0.025ppm DGHS/AOAC 18th Edn. 2005, 970.52 18)Monocrotophos 18)0.025ppm DGHS/AOAC 18th Edn. 2005, 970.52 19)Praquat Dichloride 19)0.1ppm DGHS/AOAC 18th Edn. 2005, 970.52 20)Trichlorfon 20)0.05ppm DGHS/AOAC 18th Edn. 2005, 970.52 21)Thiometon 21)0.025ppm DGHS/AOAC 18th Edn. 2005, 970.52 22)Carbendazin 22)0.5 ppm DGHS/AOAC 18th Edn. 2005, 970.52 23)Benomyl 23)0.5 ppm DGHS/AOAC 18th Edn. 2005, 970.52 24)Carbofuran 24)0.1 ppm DGHS/AOAC 18th Edn. 2005, 970.52 25)Decamethrin/Deltamethrin 25)0.5 ppm DGHS/AOAC 18th Edn. 2005, 970.52 26)Fenthion 26)0.1 ppm DGHS/AOAC 18th Edn. 2005, 970.52 27)Dithiocardamates 27)0.20 ppm DGHS/AOAC 18th Edn. 2005, 970.52 28)Phenthoate 28)0.05 ppm DGHS/AOAC 18th Edn. 2005, 970.52 29)Phorate 29)0.05 ppm DGHS/AOAC 18th Edn. 2005, 970.52 30)Pirimiphos-Methyl 30)5.0 ppm DGHS/AOAC 18th Edn. 2005, 970.52 31)Oxydemeton Methyl 31)0.02 ppm

Page 18

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11 Salt &Spices inclusive Dry Fruits Nuts/Betel Nuts/ Curry powder/masala powder 1% by wt Extraneous matter Saffron Floral waste NMT 10% BY WT Moisture and volatile matter at 103 NMT 12% C Total Ash on Dry basis NMT 8% by wt

DGHS Manual DGHS Manual

DGHS/AOAC Chapter 43 17th Edn. 986.21/IS: 5453 P-II: 1996 Reaff. 2001

DGHS/AOAC Chapter 43 17th Edn. 941.12/IS: 5453 P-II: 1996 Reaff. 2001 DGHS/AOAC Chapter 43 17th Edn. 941.12/IS: 5453 P-II: 1996 Reaff. 2001 DGHS Manual DGHS Manual

Ash insoluble in Dil HCl on dry basis

NMT 1.5 % by wt

Solubility in cold water on dry wt NMT 65% by wt basis Bitterness expressed as direct reading NLT 30% by wt of absorbance of picrocrocin at about 257 nm on dry basis Safranal expressed as direct reading NLT 20%-NMT 505 by wt of absorbance of 330 nm on dry basis Colouring strength expressed as direct NLT 80% by wt reading of absorbance of 440 nm on dry basis Total Nitrogen on dry basis NMT 2.0% by wt Crude Fibre on dry basis Added colour/ Artificial Colour Microbiological parameters 1)Salmonella NMT 6% BY wt Absent 1)Absent in 25 gm
free from fungal growth

DGHS/I.S 5453 ( PartII) - 1966

DGHS Manual

DGHS/AOAC Chapter 43 17th Edn. 920.173/IS: 5194-1996 DGHS Manual DGHS Manual APHA METHOD/USDA BAM Visual Examination DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL

Split cassia

Physical Examination Extraneous matter Moisture Total Ash(on dry wt basis) Ash in soluble in Dil HCl on dry basis Volatile oil content(V/w) Insect Rodent hair &excreta

1%MAX 12% max 5%max 1%max

2.0 % Min.

Absent Absent

Page 19

Sheet1

Added colouring matter Coumarin Microbological parameters 1)Salmonella absent in 25 gm Pesticides & Residues 1)Inorganic Bromide

Absent

DGHS MANUAL

Absent in 25 gm 1) 400 ppm max

APHA METHOD AOAC Method 986.21 Visual Examination DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL/A.O.A.C 17th edn , 2000 Official Method 970.55 Visual Examination DGHS MANUAL Visual Examination DGHS MANUAL DGHS MANUAL Visual Examination APHA METHOD Visual Examination DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL/AOAC 962.17 Visual Examination Visual Examination Visual Examination DGHS MANUAL Visual Examination DGHS MANUAL USDFA BAM/APHA

Cloves

Physical Examination Extraneous matter Moisture Tendrils,Mother Cloves Khokar Cloves Volatile oil content Headless cloves Insect Fragments Rodent hair &Excreta Insect damaged cloves Added colouring matter Damaged/discoloured cloves MicrobiologicalAnalysis 1)Salmonella absent in 25 gm Extraneous matter % w/w Moisture % w/w Total ash in dry basis Ash insoluble in Dil HCl on dry basis % w/w Volatile oil content on dry basis Mould growth Insect damaged matter % w/w Live & dead insects insect fragments Rodent contamination Nutmeg in Mace % w/w Added colouring matter Microbiological parameters 1)Salmonella /25 gm

1.0% Max.

12.0% max 2% max 2% max 17% min 2%max Absent Absent NMT 2.0 by wt Absent Absent Absent in 25 gm NMT 0.5% NMT 10.0% NMT 4% NMT 0.5% NLT 7.5% Absent NMT 1.0% Absent Absent NMT 1.0% absent 1)Absent in 25 gm

Mace

Garlic Powder

Extraneous Matter Moisture

NMT 0.5% NMT 5%

DGHS MANUAL DGHS MANUAL

Page 20

Sheet1

Garlic Powder
Total ash Acid Insoluble ash Volatile organic Sulphur compound on dry basis Peroxidase Test Added colouring matter Salmonella Afflatoxin Metal Contaminants 1) Lead 2) Copper 3) Arsenic 4) Tin 5) Zinc 6) Cadmium 7) Mercury 1) 10 ppm MAX 2) 30 ppm MAX 3) 5 ppm MAX 4)250 ppm MAX 5) 50 ppmMAX 6)1.5 ppm MAX 7) 1 ppm MAX AOAC 18th Ed. 975.03 AOAC 18th Ed. 975.03 IS 2088 1983
AOAC 18th Edn. 2005, 985.16, 980.19

NMT 5% NMT 0.5% NLT 0.3% Negative Absent absent in 25 gm

30 ppm MAX

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL USDFA BAM/APHA
ELISA (J.European Food Research Tech; 210; 213-215; 2000) /AOAC 18th edition Chap.49

AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03 AOAC 18th Ed., 977.15

13 Additives Ammonium bicarbonate INS 503 (ii)

End use certificate is required

Assay Chloride Sulpher compounds Pb(mg/Kg) Specification 99.02 % -100.5% specification 0.003%Max 0.007% max 5 mg/kg max Food Chemical codex Food Chemical codex Food Chemical codex Food Chemical codex

Phosphoric Assay Acid INS 338 Fluride

Pb(mg/Kg) As(mg/Kg)

Not less than as per label declaration 10 mg/kg Max 5 mg/kg max 3 mg/kg max

Food Chemical codex/IP 1985 Food Chemical codex Food Chemical codex Food Chemical codex

Monosodiu m Glutamate INS 621

Purity Chloride Loss on Drying % by Lead

Specification 98.05 % -101.5% Max 0.2 % Max 0.5 % Max 10 mg/Kg

Food Chemical codex Food Chemical codex Food Chemical codex Food Chemical codex

Page 21

Sheet1

Penta cake

Non permitted food colours

P2O5:

absent 30 % max Satisfactory

Insect infectation

Mould growth
P2O5

Absent 30 % max

Enzyme

Enzyme activity Additives Mould growth

As per enzyme characterstics as per label declaration Absent

14 Thermally processedFruits &Vegetables products Tomato paste/ Physical Examination Chemical Parameters Tomato Added colouring matter powder
Total soluble Solids (w/w) Container filled Colour Added-non permitted Insects

Absent 25.0 % min NLT 90% of net wt of container Negative Absent

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL APHA/USDA BAM APHA/USDA BAM

Alkalinity test Microbiological Parameters

1)Total plate count 1) < 50 /ml 2)Incubation at 37 C for 10 days and 2)No change in pH 55 C for 7 days 3)Direct mould count
Preservatives

<40% positive field

AOAC 16.17.01/USDA BAM/AOAC 965.41

DGHS/AOAC 994.11

1)Benzoic Acid

1) 750 ppm 25.0 % min

1.0% Min.

Tomato sauce

Total soluble solid salt free basis (m/m) Acidity as acetic Acid Container filled Alkalinity test
A) Microbiological Parameters

DGHS MANUAL DGHS MANUAL DGHS MANUAL

NLT 90% of net wt of container

Page 22

Sheet1

1) Total plate count

<10, 000

USFDA BAM/APHA < 40% Positive field examined <125 per 1/60 cmm
AOAC 18th Edn. 2005, 16.17.01

2)Mould count 3)Yeast &spores Preservatives & acidifying agents Fumeric Acid Sorbic Acid&its Sodium,Calcium Pottasium salt Benzoic Acid& its Sodium Potassium Salt or both

USFDA BAM/APHA

0.3% Max 1000 ppm Max 750 ppm Max

DGHS MANUAL DGHS MANUAL DGHS MANUAL

15 Thermally processed Fruits & Vegetablesproducts / Fruit Juice

Grape Juice

Chemical Parameters

1) Total soluble Solid 2) Acidity (as citric Acid) 3)Colour Added-non permitted

Min 9% Max 3.5% Absent

AOAC 932.12

DGHS DGHS/Journal of Food Technology, 1966, 1, 63-72. Official Methods of Analysis of the Associate of Official Agricultural Chemists, 7th Edition. 34.2, 34.29.
Test as per added sweetner

Added sweeteners (g/kg) Pesticides

as per the reulations 2.3.6 FSSAI below detectable limits as in FSSI regulations

DGHS MANUAL DGHS DGHS/AOAC 983.16/AOAC 994.11 DGHS

IS 2088 1983 AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03

Preservatives Sorbic acid and its sodium, potassium 500 ppm max or calcium Benzoic Acid 600 ppm max Sulpher dioxide Heavy Metal: 1) Arsenic 2)Lead 3) Tin 4) Zinc 5)Copper Bacteriological Parameters 1)Total plate count 350 ppm max 0.2 ppm max 1 ppm max 250 ppm max 5 ppm max 5 ppm max 50 cfu/ml

USFDA BAM/APHA

Page 23

Sheet1

2)Coliform Count 3)Yeast &Mould CFU/ml 16 Fruit Drinks

Absent 2 cfu /ml

USFDA BAM/APHA USFDA BAM/APHA

Fresh Mango Chemical parameter 1)Total soluble Solid Fruit Drink

2)Acidity (as Citric Acid) 3) Colour Added-non-permitted

1) NLT 10% 2)Max 3.5% 3)Absent

DGHS MANUAL DGHS MANUAL DGHS MANUAL

Fruit juice content

not less than 10%

Heavy metals Lead Bacteriological parameters 1)Total plate count 2)Yeast &Mould cfu/ml 3)Coliform Count 1)50 cfu/ml 2) absent 3)2cfu/ml USFDA BAM/APHA USFDA BAM/APHA USFDA BAM/APHA 1.0 mg/kg

AAS/AOAC 18th Ed. 975.03

Concentrated Physical appearance TSS Fruit/ Vegetable Acidity (as citric acid) juice (Juice Concentrate)
Colour (Non-permitted)
Synthetic color Poncea 4R

pulpy, turbid/ clear Not less than double the contents of original juice as in FSSAI regulations

visual examination DGHS Manual DGHS Manual/AOAC 18th Edn. 2005, 950.15, 942.15

Min 10%

absent
100 ppm max

1)Total plate count 2)Yeast &Mould cfu/ml 3)Coliform Count Lead

Benzoic acid

1)50 cfu/ml 2) absent 3)2cfu/ml 2.0 mg/kg

1500 ppm

DGHS Manual DGHS Manual USFDA BAM/APHA USFDA BAM/APHA USFDA BAM/APHA
AAS/AOAC 18th Ed. 975.03 DGHS/AOAC 994.11

Page 24

Sheet1

17 Sweets & Confectioneries inclusive Chewing gum Chewing Gum Gum

Moisture Sulphated ash % Acid insoluble Ash % Reducing Sugar (calculated as Dextrose) Sucrose
Added sweeteners (g/kg)

NLT 12.5% NMT 3.5% NMT 9.5% NMT 2.0% NLT 4.5% NMT 70.0%
as per the reulations 2.3.6 FSSAI

IS 6747 : 1981/DGHS Manual DGHS Manual/IS: 6287 1971 DGHS Manual/IS: 6287 1971 DGHS Manual/IS: 6287 1971 DGHS Manual/IS: 6287 1971 DGHS Manual/IS: 6287 1971
Test as per added sweetner

Sachharine(Sodium) Aspertame Acesulphame k Sodium,Potassium,BenZoate/Benzoate Acid Sulphur Dioxide Sorbic Acid & its Calcium,Sodium & salts Added Colour Titanium Dioxide Mineral Oil erythrosine L- Tartaric Acid

NMT 3000ppm NMT 10000ppm NMT5000ppm NMT 1500ppm NMT 2000ppm NMT 1500ppm Only permitted colour NMT 10000 ppm NMT 0.2% 100 ppm max NMT 3000 ppm

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL AOAC, 18th Edn. 2005, 973.36/DGHS DGHS MANUAL DGHS MANUAL DGHS MANUAL

Jelly Candy Drops/Fox Blackcurrant Tin

Physical Examination Sulphated Ash on salt freebasis Ash insoluble in Dil HCl Added Colour (permitted) Titanium Dioxide talc Mineral Oil Added Colour (non-permitted) Artificial Sweeteener) 1)Aspertame 2)Acesulphame k 3)Saccharin Sodium

NMT 2.5% NMT 0.2% NMT 100ppm 10000ppm 0.2%Max 0.2%Max Absent NMT 1)1000ppm 2)5000ppm

DGHS Manual AOAC 18th Edn. 2005, 900.02 DGHS MANUAL DGHS MANUAL AOAC, 18th Edn. 2005, 973.36/DGHS chemical codex DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL

Page 25

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Preservatives 1)Benzoic Acid,Sodium and Pottasium Benzoate 2)Sulphur Dioxide 3)Sorbic Acid and its Calcium,Sodium,Pottasium salts(Calculated as Sorbic Acid) Heavy Metals 1)Lead 2)Copper 3)Arsenic 4)Tin 5)Zinc 6)Cadmium Erythrosine 18 Bakery products

3)3000ppm 1)1500ppm 2)2000 ppm 3)2000ppm

DGHS MANUAL DGHS MANUAL DGHS MANUAL

1)NMT 2 ppm 2)NMT 5 ppm 3)NMT 1ppm 4)NMT 5 ppm 5)NMT 5 ppm 6)NMT 1.5 ppm 100 ppm max

AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03

IS 2088 1983

AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03 DGHS MANUAL

Food Aid Biscuits

Standrads as per FSSAI

Acid insoluble Ash in Dil HCl (on dry Max. 0.1% wt basis) Acidity of extracted fat (as Oleic acid) Max. 1.5% Added colouring matter Nature of Fat Salt (as Sodium Chloride) absent As per declaration of ingredients As per declaration of ingredients

IS 1011-1992 DGHS MANUAL DGHS MANUAL DGHS MANUAL/IS:7874 (Part 2)1975 Reaffirmed 2004

Emulsifying Agents 1)Sucroglycerides INS 474 2) Di-Acetyl Tartaric Acid esters of Mono and Di-glycerides Flour Treatment Agent 1)Benzoyl Peroxide Synthetic colour 1)Ponceau 4 R Artificial sweetners(Singly) 1)Asparatame 2)Acesulphame K

Emulsifying Agents 1)1000 ppm 2)10000 ppm Flour Treatment Agent 1)40 ppm Max

GC-FID/GC-MS Food Additives and Contaminants Food chemical codex

DGHS MANUAL

1)100 ppm Max(singly or in combination) Artificial sweeteners 1)2200ppm 2)1000 ppm

Page 26

IS: 12711:1989 IS: 12711:1989 DGHS MANUAL

Sheet1

3) Sucralose Leavening agents Ammonium carbonate

3)750 ppm 500 ppm max

DGHS MANUAL DGHS MANUAL

19 Fruits & vegetables product Moisture content Dates

Ash insoluble in Dil HCl Blemished/damaged unit Extraneous matter Insect Fragments/insect Rodent hair &excreta Added colouring matter Aflatoxin Microbiological parameters 1)Total plate count 2)Clostridium botulinium Preservatives 1) Sulphur Dioxide,Sodium/Pottassium/Calcium Sulphide/bisulphide metasulphite expressed as SO2 20 Beverages

30%max 0.1%max 5%max 1% max Absent Absent Absent 30ppm 1)NMT 40,000/gm 2) Absent in 25 gm/ml 1) Only SO2 max 50gm/ Kg

DGHS MANUAL/AOAC 934.06 DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL AOAC 18th edition Chap.49 USFDA BAM/APHA USFDA BAM/APHA DGHS MANUAL

Instant Coffee
Standrads as per FSSAI 2.10

Moisture(on dry basis) Total Ash(on dry basis)

4.0%Max
DGHS MANUAL/IS 2791 - 1998

12 % Max
DGHS MANUAL/IS 2791 - 1998

Caffeine content (on dry basis) Solubility in boiling water

Solubility in cold water at 16 2 C Test of Chicory Insects Fragments Rodent hair & excreta Added colouring matter
Heavy Metals:

NLT 2.8% Dissolved readily in30 secs with moderate stiring Soluble with moderate stirring in 3 minutes Absent Absent Absent Absent 30 ppb Max

DGHS MANUAL//AOAC 18th Ed., 925.16 DGHS MANUAL/IS 2791 - 1998 DGHS MANUAL/IS 2791 - 1998

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL

AAS/AOAC 18th Ed. 971.20

Cu (in ppm)

Page 27

Sheet1

Pb (in ppm) As (in ppm) Pesticides 1) Ethephon 2) Monocrotophos

2.5 ppb Max 1.1 ppb Max 1) 0.10 ppm Max 2) 0.1 ppm Max

AAS/AOAC 18th Ed. 971.20 IS 2088 1983

DGHS MANUAL DGHS MANUAL

Indian Black Total Ash determined on tea dried to NLT 4% and NMT 8% a constant wt at 100 Deg C Tea
Standrads as per FSSAI for tea 2.10 Total Ash soluble in boiling distilled water Ash insoluble in HCl Extract obtained by boiling dry tea( dried at constant wt at 100 Deg C) with 100 parts of distilled water for one hour under reflux Alkalinity of water soluble ash expressed as KOH (m/m) Crude Fibre(determined on tea dried to a constant wt at 100 Deg C Rodent hair &excreta Microscopic Examination Iron filling Pesticides & Residues 1)Dicofol 2)Quinolphols 3)Glyphosphate 4)Glufosinate-ammonium 5) Propargite 6) Fenzaquin Metal Contaminants 1) Mercury 2) Copper 3) Lead NLT 45% of Total Ash
1.0 % Max

DGHS MANUAL DGHS MANUAL

DGHS MANUAL

DGHS MANUAL

32.0% Min

DGHS MANUAL
1.0% 3.0%

DGHS MANUAL/IS: 10226: 1972

16.5% Max.

absent Tea structure only absent 1) 5.0 ppm 2) 0.01 ppm 3) 1.0 ppm 4) 0.01 ppm 5) 10.0 ppm 6) 3.0 ppm 1)1 ppm 2)150 ppm 3)10 ppm on dry matter

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL AOAC 18th Ed., 977.15
AAS/AOAC 18th Ed. 971.20 AAS/AOAC 18th Ed. 971.20

Page 28

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21 Proprietary Food Test parameters: as per the category Fruit of food / label declaration infusion Orange spice
Proprietary food : check list of ingradients and see for whether it falls under which category or it needs product approval and then go for analysis

Physical parameters

Microbiological testing Salmonella /25mg Mould Growth Added colouring matter Preservative Additives Afflatoxin Metal contaminant 1)Lead 3)Arsenic 4)Tin 6)Cadmium 7) Mercury

Proprietary Food (Need for product approval and Testing as per label declaration)

permitted colour As per label/category As per label/category & Permitted as per FSSAI regulations only 30 ppb max

IS 12074-1987 reaff 1998

IS 2088 1983 AOAC 18th Edn. 2005, 985.16, 980.19

AAS/AOAC 18th Ed. 975.03 AOAC 18th Ed., 977.15

22

Koka Instant Test parameters: as per the category of food / label declaration Noodles

Added colour Preservative

Additives

permitted colour As per label/category As per label/category & Permitted as per FSSAI regulations only 30 ppb max

DGHS MANUAL

Afflatoxin Metal contaminant

Page 29

Sheet1

Proprietary Food (Nee

1)Lead 3)Arsenic 4)Tin 6)Cadmium 7) Mercury Test parameters: as per the category of food / label declaration

IS 12074-1987 reaff 1998

IS 2088 1983 AOAC 18th Edn. 2005, 985.16, 980.19

AAS/AOAC 18th Ed. 975.03 AOAC 18th Ed., 977.15

Porridge Mix Added colouring matter

Permitted colour only

Microbiological testing Salmonella Mould Growth Preservative

Additives

Afflatoxin

As per label/category As per label/category & Permitted as per FSSAI regulations only 30 ppb max absent
Visual Examination/USFDA Technical Bulletin No: 5 Macro Analytical Procedures Manual, Chapter: 5

Seasoning powder

Physical characterstics& Insects infestation

Rodent hair & Excreta Calcium and MagnesiumCarbonate Mould growth Added colour Saffron Sulphor Di-oxide Modified Starch Salmonella Afflatoxin HCN Metal contaminant 1)Lead 2)Copper

absent 2% max
absent absent

DGHS Manual Visual Examination DGHS Manual DGHS Manual DGHS Manual DGHS Manual USFDA BAM/APHA/IS 5402 : 2002
ELISA (J.European Food Research Tech; 210; 213-215; 2000) /AOAC 18th edition Chap.49

100 ppm Max NMT 1500 ppm 0.5 % of final food for consumption absent in 25 gm
30 ppm MAX

NMT 5 ppm 1) NMT 2.5 ppm 2)NMT 30 ppm

IS 548: 1976 Reaff. 2006 (P-II) IS 12074-1987 reaff 1998 AAS/AOAC 18th Ed. 975.03

Page 30

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3)Arsenic 4)Tin 5)Zinc 6)Cadmium 7) Mercury Pesticides Residue

3)1.1PPM 4)NMT 250 ppm 5)NMT 50 ppm 6)NMT 1.5 ppm 7) NMT 1ppm BDL

IS 2088 1983 AOAC 18th Edn. 2005, 985.16, 980.19

AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03 AOAC 18th Ed., 977.15 DGHS Manual

23 Thermally processed vegetables products ( Canned vegetables) 50% of net wt of contents Ice Cool Baby Drained wt.

AOAC 968.30

Corn(whole) (canned)
Added Colour(Non-permitted colour) absent Salt Flat sour organism,CFU/gm Staphylococcus aurerus/25gm Salmonella & Shigella/25gm Clostridium botalinum/25gm E.Coli/gm Yeast & Mould count/gm Vibrio Cholera/25gm Total plate count/gm pH after incubation at 37 C for 10 days and pH after incubation at 55 C for 5 days Firming Agents 1)Calcium Chloride INS 509 Thickening Agent 1)Aerobic gum(Vegetable gum) INS 414 Present Absent absent absent absent absent absent absent 120 No change in pH DGHS Manual DGHS Manual DGHS Manual APHA METHOD APHA METHOD APHA METHOD APHA METHOD APHA METHOD APHA METHOD APHA METHOD APHA METHOD

1)0.80% max

Food chemical codex/ DGHS Manual

1)10 gm/kg max

Food chemical codex/ DGHS Manual

Mushroom

Container filled Drain weight 1) Liquid pack 2) Solid pack 3) Mushroom packed in sauce Flat sour organism,CFU/gm

NLT 90% of net wt of container 1) 50 % of net wt. of contents 2) 70 % of net wt. of contents 3)25 % of net wt. of contents Absent

DGHS Manual AOAC 968.30

USFDA BAM/APHA METHOD

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Staphylococcus aurerus/25gm Salmonella & Shigella/25gm Clostridium botalinum/25gm E.Coli/gm Yeast & Mould count/gm Vibrio Cholera/25gm Total plate count/gm pH after incubation at 37 C for 10 days and pH after incubation at 55 C for 5 days Tin

absent absent absent absent absent absent No change in pH

USFDA BAM/APHA METHOD USFDA BAM/APHA METHOD USFDA BAM/APHA METHOD USFDA BAM/APHA METHOD USFDA BAM/APHA METHOD USFDA BAM/APHA METHOD 120 USFDA BAM/APHA METHOD APHA METHOD

250 ppm Max

AOAC 18th Edn. 2005, 985.16, 980.19

25 Flavouring Substances Mix orange Testing parameters as per label declaration Flavour Colour Limit to be checked as per end use Artificial Swteener Preservatives Limit to be checked as per end use

DGHS MANUAL DGHS MANUAL DGHS MANUAL

26

Macoroni products Pasta

Physical Examination Moisture % Total Ash % Acid insoluble Ash %(Dil in HCl) Nitrogen % Faecal Streptococci
Added colour

free from insects, dirt NMT 12 % by wt NMT 1.0 % on dry basis NMT 0.1% by wt NLT 1.7 % on dry basis Absent
Absent

Visual Examination DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL USFDA BAM/APHA METHOD DGHS MANUAL

27

Pop corn

Physical Examination Insects Argemone Seeds Khesari Dal Mineral matter (as defined) Nil Nil Nil NMT 0.25% Visual Examination Visual Examination Visual Examination Visual Examination

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Organic matter (as defined) Damaged grain (as defined)

NMT 1.0% NMT 5.0%

By Refraction By Refraction

28 Vegatable products/ CANNED VEGETABLES Peroxidase Frozen

negative < 40, 000/ gm 30 ppb Max

By Refraction IS:4333 (P-2)-2002 AOAC 18th edition Chap.49

Vegetable
Total Plate Count Toal Aflatoxin (B1, B2, GI& G2) UG/KG

29 Swteening Agent

Honey Standrads as per FSSAI

Specific gravity Moisture Total Reducing Sugar i) for Carbia colossa and Honey dew Sucrose i) for Carbia colossa and Honey dew Fructose-glucose ratio Ash Acidity Fiehe's Test i) Hydroxy Methyl furfural,mg/kg Foreign matter (Extraneous matter), Fragments of insects Monosodium glutamate

NLT 1.35 NMT 25% I)NLT 65% II)NLT 60% NMT 5% by mass NMT 10% by mass NLT 0.95% NMT 0.5 % NMT 0.2% Negative NMT 80 absent absent absent

LCMS/MS IS: 4941: 1994 IS: 4941: 1994 /DGHS MANUAL IS: 4941: 1994 /DGHS MANUAL DGHS MANUAL

IS: 4941: 1994 IS: 4941: 1994 IS: 4941: 1994 IS 4941:1994, IS: 4941: 1994 DGHS MANUAL DGHS MANUAL IS: 4941: 1994

30 Beverages

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Alcoholic

1)Total fat content Alcoholic content Total Acid as Tartaric Acid expressed in terms of 100 Ltrs of absslute alcohol Volatile Acid as Acetic Acid Expressed in terms of 100 Ltrs of absl alcohol Chloral Hydrate Paraldhyde Tranquilizer
Ethyl Alcohol Ash content Residue on evaporation Total Acidity Volatile Acidity Fixed Acidity Esters Higher Alcohols Aldehydes Methyl alcohol Sulphur dioxide Copper Iron Arsenic Lead Caramel (Qualitative) Furfural Color pH Residue on evaporation

As per BIS specifications for different categories

BIS satandards

IS: 3752: 2005

IS: 3752: 2005

IS: 3752: 2005

IS: 3752: 2005 IS: 3752-2005, SP-18 (P10)-1984 IS: 3752: 2005 IS: 3752: 2005 IS: 3752: 2005 IS: 3752: 2005 IS: 3752: 2005 IS: 3752: 2005 IS: 3752: 2005 IS: 3752: 2005/AOAC 18th Edn. 2005, 972.11 IS11124: 1984 Reaff 2004/ AOAC 18th Edn. 2005, 990.28 APHA3030D, 3030J: 1992/IS: 3752: 2005/AOAC 18th Edn. 2005, 985.35 APHA3030D, 3030J: 1992/IS: 3752: 2005IS: 3752: 2005 APHA3030D, 3030J: 1992/IS: 3752: 2005IS: 3752: 2006 APHA3030D, 3030J: 1992/IS: 3752: 2005IS: 3752: 2007 AOAC, 18th Edn. 2005, 948.07 IS: 3752: 2005 DGHS Manual IS: 3752: 2005 IS: 3752: 2005 DGHS Manual

added colour suspended or sediment particle

Artificial Sweetner

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Sedative Sulphor Di-oxide(According to nomenclature of the product) Methyl Alcohol

31

Non Alcoholic Beverages

Standrads as per FSSAI

145 ppm max

Caffeine Estergum Quinine salts as quinine sulphate

IS 3077 - 1998/DGHS

100 ppm max 100 ppm max 1)700ppm max 2)300 ppm max 3)300 ppm max 4) 100 ppm max 120 ppm 2.5 ppm 30 ppm 1.1 ppm 5 ppm max Not more than 50 cfu/ ml Absent in 100 ml Not more than 2.0 cfu / ml
30 ppm MAX

Artificial sweetners(Singly) 1)Asparatame 2)Acesulphame K 3) Sucralose 4)Saccharin Sodium Benzoic acid Heavy Metal: Lead, mg/kg copper, mg/kg Arsenic, mg/kg Zinc, mg/kg Total Plate Count, cfu/ml Coliform count/gm Yeast and mould count Afflatoxin

DGHS DGHS DGHS DGHS DGHS AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03 IS 2088 1983 AAS/AOAC 18th Ed. 975.03 USFDA BAM/APHA/IS 5402 : 2002 USFDA BAM/APHA/IS 5402 : 2002 USFDA BAM/APHA/IS 5403 : 1991 ELISA (J.European Food Research Tech; 210; 213-215; 2000) /AOAC 18th edition Chap.49

31 Dehydrated Fruits & Vegetables products Onion Moisture Seasoning powder Total ash on dry basis

5.0 % Max by weight

DGHS MANUAL/AOAC (934.06)

5.0 % Max by weight

DGHS MANUAL

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Standrads as per FSSAI for onion powder

Ash insoluble in dil HCl

0.5 % Max by weight

IS:5403-1999/IS 13846-1993

Peroxidase Total Plate Count, cfu/ml Sulphur dioxide Heavy metals Lead Arsenic 32 Processed Vegetables

Negative < 40,000/ gm 2000 ppm max 10 ppm on dry matter 2.0 ppm max

IS 1797:1985(Reaff.2001) IS 1797:1985(Reaff.2001) DGHS MANUAL DGHS MANUAL/ DGHS MANUAL/

Olives in Brine
Standrads as per FSSAI for table olive

Sodium Chloride in Brine ( hermetically sealed container) Sodium Chloride in Brine ( non hermetically sealed container) Test for Added colour pH for Brine ( in hermetically sealed container) pH for Brine ( in non hhermetically sealed container) Acidity of Brine as lactic acid ( Brine wih natural lactic fermentatin) damaged matter Foreign matter Insect damaged unit Acidifing agents Citric Acid L Tartaric acid Lactic acid Antioxidants L- ascorbic acid Preservatives 1) Sulphor Dioxide,Sodium/Pottassium/Calcium Sulphide/bisulphide metasulphite expressed as SO2

5.0 % min 6.0 % min

IS 2860-1995 IS 2860-1995

Absent 4.0 % max 4.5 % max 0.4 % min

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL

2.0 % Max Not more than 1 unit/ kg 2.0 % Max 15 gm/Kg max 15 gm/Kg max 15 gm/Kg max 0.2 gm/Kg max 1.5 gm/Kg max only SO2

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL Visual Examination

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Benzoic acid/sodium/potassium Benzoate expressed as Benzoic acid Ferrous gluconate Ferrous lactate Mono sodium glutamate Sodium Alginate xanthan gum Calcium chloride 33 Flavouring agents Flavour granules Physical Examination Insect Fragments Damaged/Discoloured unit Moisture Insectdamaged matter Iron filling Rodent hair &Excreta Solubility 34 Cereals & cereal products Wheat flour Moisture Total ash ash insoluble in HCL Gluten on dry basis Alcoholic acidity (as H2SO4)

1 gm/Kg max

DGHS MANUAL

0.15 gm/Kg max of total iron 0.15 gm/Kg max of total iron 5 gm/Kg max 5 gm/Kg max 3 gm/Kg max 1 gm/Kg max as calcium ions in stuffed end products

DGHS MANUAL DGHS MANUAL DGHS MANUAL Magnetic Examination Visual Examination DGHS MANUAL

DGHS MANUAL

NMT 14% NMT 1% NMT 0.1% NLT 7.5%

DGHS MANUAL/IS 1009 - 1994 DGHS MANUAL/IS 1009 - 1994 DGHS MANUAL/IS 1009 - 1994 DGHS MANUAL/IS 1009 - 1994 DGHS MANUAL/IS 1009 - 1994/IS: 1009 1979 & AACC 10th Edn. 38 - 10 DGHS MANUAL IS:4333 (P-2)-2002 USDFA BAM DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL

Rodent hair & Excreta Improver 1)Benzoyl paroxide 2)Potassium Bromate 3)Ascorbic Acid Fungal /Mould Growth Insect Infestation Rodent hair &Excreta

NMT 1.2% absent in 25 gm 1)NMT 40 ppm 2)NMT 20 ppm 3) NMT 200 ppm Absent Absent

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Papad
(proprietary product)

Moisture

IS 2639-1999

Added colouring matter Preservative

Nil

DGHS MANUAL

as per label declaration

Aflatoxin Fat

NMT 30 ppn as per label declaration

AOAC 18th edition Chap.49

35 Culiminary pastes & other sauces( other than tomato and soya) Other sauces TSS Salt free basis (m/m) 1) Chilli Sauce 2) Fruit/Vegetable Sauce 3) Culinary paste/Sauce 4) Ginger paste Acidity % ( as acetic acid) 1) Chilli Sauce 2) Fruit/Vegetable Sauce 3) Culinary paste/Sauce 4) Ginger paste Added colour Preservatives Benzoic acid 1)Lead 2)Copper 3)Arsenic 4)Tin 5)Zinc 6)Cadmium 7) Mercury Yeast and mould count 36 Carbonated Beverages/sweatned carbonated beverages NLT 8% NLT 15% NLT 8% NLT 3%

DGHS MANUAL

DGHS MANUAL NLT 1% NLT 1.2% NLT 1% NLT 1% 1)2% Max absent
750 ppm

DGHS MANUAL
DGHS/AOAC 994.11

1) NMT 2.5 ppm 2)NMT 30 ppm 3)1.1PPM 4)NMT 250 ppm 5)NMT 50 ppm 6)NMT 1.5 ppm 7) NMT 1ppm
positive in not more than 100 counts/ gm

AOAC 18th Ed. 975.03 AOAC 18th Ed. 975.03 IS 2088 1983
AOAC 18th Edn. 2005, 985.16, 980.19

AAS/AOAC 18th Ed. 975.03 AAS/AOAC 18th Ed. 975.03 AOAC 18th Ed., 977.15
APHA METHOD

Sweetened Carbonated Beverage

145 ppm max

Caffeine JAOAC Vol 71, 5, 1988, p-934-937

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Standrads as per FSSAI

100 ppm max

Estergum Quinine salts as quinine sulphate

DGHS MANUAL DGHS MANUAL

JAOAC Vol 71, 5, 1988, p-934-937 JAOAC Vol 71, 5, 1988, p-934-937

100 ppm max 1)700ppm max 2)300 ppm max 3)300 ppm max 4) 100 ppm max 120 ppm 10 ppm 30 ppb Max 1.1 ppm Max 5 ppm Max Not more than 50 cfu/ ml Absent in 100 ml Not more than 2.0 cfu / ml

Artificial sweetners(Singly) 1)Asparatame 2)Acesulphame K 3) Sucralose 4)Saccharin Sodium Benzoic acid Lead, mg/kg Copper, mg/kg Arsenic, mg/kg Zinc, mg/kg Total Plate Count, cfu/ml Coliform count/gm Yeast and mould count

DGHS MANUAL
JAOAC Vol 71, 5, 1988, p-934-937 AOAC, 18th Edn. 2005, 994.11 AOAC 999.11 - 2000 IS:3752:1988

IS 2088 1983
AOAC-986.15
APHA METHOD APHA METHOD APHA METHOD

37 Seasoning powder Dried Ginger Extraneous matter,% by mass powder

Standrads as per FSSAI for Mixed Masala Moisture

Absent

Visual Examination/USFDA Technical Bulletin No: 5 Macro Analytical Procedures Manual, Chapter: 5

NMT 12%

DGHS MANUAL

Total ash (on dry basis), % by mass i)Unbleached ii)Bleached Calcium as calcium oxide (on dry basis),% by mass i)Unbleached ii)Bleached Volatile oil, (on dry basis) % vol/wt Water soluble ash on dry basis Acid insoluble ash on dry basis Alcohol(90%v/w) soluble extract on dry basis Cold water soluble axtract on dry basis

8% max 12% max

DGHS MANUAL DGHS MANUAL

1.1 % max 2.5 % max 1.5% min 1.7% min 1% max 5.1% min 11.4% min

DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL DGHS MANUAL

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Added colouring matter Total plate count Salmonella Afflatoxin

Absent 40,000 /gm max absent in 25 gm 30 ppb max

DGHS MANUAL APHA METHOD APHA METHOD ELISA (J.European Food Research Tech; 210; 213-215; 2000) /AOAC 18th edition Chap.49 APHA METHOD

Mould

Absent

Kindly note:

* *

1. As discussed in meeting, group of Veterinary drugs for testing in Meat and Meat products yet to be

decided. 2. Table 2 in APPENDIX B of FSSAI regulations dealing with MIcrobiological parameters of Milk and Milk products mention the microbiological limits at production stage by the industry. Therefore as in FSSAI, regulations no defined limits are written for Microbiological analysis of Milk and Milk Products so the parameters and limits written for Cheese samples are those as were followed under PFA, act . Manuls/Metho ds of analysis Important links DGHS Manual http://www.mohfw.nic.in www.aoac.org AOAC methods BIS Methods www.bis.org.in APHA methods www.apha.org/
Department Directorate General of Health Services, Ministry of Health & Family WelfareAssociation of Official Analytical Chemists BUREAU OF INDIAN STANDARDS American Public Health Association

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