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REAGENTS 1. 2. 3. Zinc Carbonate Solution. 10% Diammonium Hydrogen Phosphate. Dilue Ammonia Solution.
REACTIONS Zn+++HPO4++NH4ZnNH4PO4+H+ 2ZnNH4PO4Zn2P2O7+2NH3+H2 OBSERVATION Weight of the empty crucible = 32.02gm CALCULATION Weight of the empty crucible Weight of the empty crucible + ppt Weight of ppt (Zn2P2O7) = 32.23-32.02 Molecular Weight of Zn2P2O7 Amount of Zn in Zn2P2O7 (0.21)304gm of Zn2P2O7 contains 25ml of Zinc Salt Solution contains 1000ml of Zinc Salt Solution contains RESULT The amount of Zinc is found to be 3.59 gm. = 32.02gm = 32.23gm = 0.21gm = 304gm = 130gm = (130/304)0.21gm of Zinc = 0.089gm = 0.089gm of Zinc = (0.089/25)1000gmof Zinc =3.59gm of Zinc
DISCUSSION
The object of our experiment is to determine the quantity of Zinc as Zinc Pyrophosphate by gravimetric analysis. MECHANISM Mechanism is categorized in the following steps.
Chemical Processes Industries Inorganic II Course # 501 The crystals are then burn in a crucible slowly to remove water of crystallization and then strongly which causes the decomposition of crystals i.e. the pyrolysis process occur and we obtain a compound called Zinc Pyro Phosphate the word pyro indicating that this compound is obtained through the pyrolysis process (i.e. decomposition by heating ) 2ZnNH4PO4Zn2P2O7 + 2NH3 + H2 REFERENCE Ferman Inorganic Analysis