LCI - LABORATRIO DE CROMATOGRAFIA INSTRUMENTAL - UFPE

ANLISE DE LEOS E GORDURAS - COMPOSIO EM CIDOS GRAXOS

Planilha 1 - Composio Centesimal (rea%)
QUADRO 1 - reas cromatogrficas
Procedimento: Informe as reas no Quadro 1. No Quadro 2 so encontrados os teores, em % rea.

INSTRUES:
1)

Espao reservado para colar os dados cromatogrficos. Coloque

o cursor na clula azul e cole (Ctrl+V).

2)

Em seguida, copie as reas (verde) e cole na clula da linha 28

correspondente ao nmero de sua amostra, no QUADRO 1.

3)

finalmente, leia no QUADRO 2 a composio centesimal da

amostra.

QUADRO 1: REAS CROMATOGRFICAS

IDENTIFICAO DA AMOSTRA
ram1
ram2
ram3
ram4
C6:0
0.0
0.0
0.0
0.0
C8:0
0.0
0.0
0.0
0.0
C10:0
0.0
0.0
0.0
0.0
C11:0
0.0
0.0
0.0
0.0
C12:0
0.0
0.0
0.0
0.0
C14:0
0.0
0.0
0.0
0.0
C14:1
0.0
0.0
0.0
0.0
C15:0
0.0
0.0
0.0
0.0
71.87
C16:0
0.0
0.0
0.0
0
0
0
0
C16:1
22.75
21.17
21.27
0
C17:0
43.9
41.14
38.89 158.195
C18:0
0
0
0
0
C18:1
61.62
55.365
53.23 217.635
C18:2
0
0
0
33.57
C18:3
C20:0
0.0
0.0
0.0
0.0
C18:1(OH)
0.0
0.0
0.0
0.0
TOTAIS
128.3
117.7
113.4
481.3
CIDO

ram5
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
87.98
0
0
181.68
0
247.12
31.415
0.0
0.0
548.2

ram6
7
8
9
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
79.02 544.79 528.23 545.66
0
0
0
0
0
0
0
0
172.22
911.6 958.54 928.07
0
0
0
0
236.31 1624.9 1652.2 1698.3
0
0
0
0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
487.6 3081.3 3138.9 3172.1

ram5
0.0
0.0
0.0
0.0

ram6
0.0
0.0
0.0
0.0

QUADRO 2 - COMPOSIO CENTESIMAL (rea%)

CIDO
C6:0
C8:0
C10:0
C11:0

CONCENTRAES POR AMOSTRA

ram1
ram2
ram3
ram4
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0

7
0.0
0.0
0.0
0.0

8
0.0
0.0
0.0
0.0

9
0.0
0.0
0.0
0.0

C12:0
C14:0
C14:1
C15:0
C16:0
C16:1
C17:0
C18:0
C18:1
C18:2
C18:3
C20:0
C18:1(OH)
TOTAIS

0.0
0.0
0.0
0.0
0.0
0.0
17.7
34.2
0.0
48.0
0.0
0.0
0.0
100.0

c16
Mdia CP1
Mdia CP2 15.7
Mdia CP3 17.2
Mdia CP4 16.2
Mdia CP6 16.2

0.0
0.0
0.0
0.0
0.0
0.0
18.0
35.0
0.0
47.0
0.0
0.0
0.0
100.0
c17
18.2

0.0
0.0
0.0
0.0
0.0
0.0
18.8
34.3
0.0
46.9
0.0
0.0
0.0
100.0

0.0
0.0
0.0
0.0
14.9
0.0
0.0
32.9
0.0
45.2
7.0
0.0
0.0
100.0

c18:0 c18:2
47.3
34.5
33.8
46.3
29.8
53.0
28.0
49.6
35.6

48.2

0.0
0.0
0.0
0.0
16.0
0.0
0.0
33.1
0.0
45.1
5.7
0.0
0.0
100.0
c18:3
4.2
6.2

0.0
0.0
0.0
0.0
16.2
0.0
0.0
35.3
0.0
48.5
0.0
0.0
0.0
100.0

0.0
0.0
0.0
0.0
17.7
0.0
0.0
29.6
0.0
52.7
0.0
0.0
0.0
100.0

0.0
0.0
0.0
0.0
16.8
0.0
0.0
30.5
0.0
52.6
0.0
0.0
0.0
100.0

0.0
0.0
0.0
0.0
17.2
0.0
0.0
29.3
0.0
53.5
0.0
0.0
0.0
100.0

ENTAL - UFPE

res, em % rea.

colar os dados cromatogrficos. Coloque

cole (Ctrl+V).

eas (verde) e cole na clula da linha 28

ro de sua amostra, no QUADRO 1.

Component Retention

Area

C6:0
C8:0
C10:0
C11:0
C12:0
C13:0
C14:0
C14:1
C15:0
C16:0
C16:1
C17:0
C18:0
C18:1
C18:2
C18:3
C20:0
C18:1(OH)

0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
814.65
0
0
1838.7
0
2476.4
0
0.0
0.0

0.7
0.9
1.4
1.666
2.5
0.0
3.7
3.9
4.2
5.0
5.2
5.8
6.7
6.8
7.1
7.5
8.0
12.0

C16:0
C18:0
C18:2

ADRO 2 a composio centesimal da

10
11
12
13
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
785.84 854.34 800.26 757.83
0
0
0
0
0
0
0
0
1321.8 1515.4
1385 1582.6
0
0
0
0
2393.8 2641.7 2437.4 2251.3
300.16 326.09 303.86
0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
4801.5 5337.6 4926.5 4591.7

10
0.0
0.0
0.0
0.0

11
0.0
0.0
0.0
0.0

12
0.0
0.0
0.0
0.0

13
0.0
0.0
0.0
0.0

14
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
792.305
0
0
1783.77
0
2304.46
0
0.0
0.0
4880.5

14
0.0
0.0
0.0
0.0

15
16
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
130.9
0.0
0.0
0.0
0.0
814.65 4093.2
0
0.0
0
0.0
1838.73
980.9
0
5994.7
2476.43 13594.3
0 1192.7
0.0
0.0
5129.8
25986.7

15
0.0
0.0
0.0
0.0

16
0.0
0.0
0.0
0.0

17
0.0
0.0
0.0

18
0.0
0.0
0.0

19
0.0
0.0
0.0

0.0
130.9
0.0
0.0
4093.2
0.0
0.0
980.9
5994.7
13594.3
1192.7

0.0
130.9
0.0
0.0
4093.2
0.0
0.0
980.9
5994.7
13594.3
1192.7

0.0
130.9
0.0
0.0
4093.2
0.0
0.0
980.9
5994.7
13594.3
1192.7

25986.7 25986.7 25986.7

17
0.0
0.0
0.0
0.0

18
0.0
0.0
0.0
0.0

19
0.0
0.0
0.0
0.0

0.0
0.0
0.0
0.0
16.4
0.0
0.0
27.5
0.0
49.9
6.3
0.0
0.0
100.0

0.0
0.0
0.0
0.0
16.0
0.0
0.0
28.4
0.0
49.5
6.1
0.0
0.0
100.0

0.0
0.0
0.0
0.0
16.2
0.0
0.0
28.1
0.0
49.5
6.2
0.0
0.0
100.0

0.0
0.0
0.0
0.0
16.5
0.0
0.0
34.5
0.0
49.0
0.0
0.0
0.0
100.0

0.0
0.0
0.0
0.0
16.2
0.0
0.0
36.5
0.0
47.2
0.0
0.0
0.0
100.0

0.0
0.0
0.0
0.0
15.9
0.0
0.0
35.8
0.0
48.3
0.0
0.0
0.0
100.0

0.0
0.5
0.0
0.0
15.8
0.0
0.0
3.8
23.1
52.3
4.6
0.0
0.0
100.0

0.0
0.5
0.0
0.0
15.8
0.0
0.0
3.8
23.1
52.3
4.6
0.0
0.0
100.0

0.0
0.5
0.0
0.0
15.8
0.0
0.0
3.8
23.1
52.3
4.6
0.0
0.0
100.0

0.0
0.5
0.0
0.0
15.8
0.0
0.0
3.8
23.1
52.3
4.6
0.0
0.0
100.0

4.416
7.383
8.35

814.65
1838.7
2476.4

20
0.0
0.0
0.0

21
0.0
0.0
0.0

0.0
130.9
0.0
0.0
4093.2
0.0
0.0
980.9
5994.7
13594.3
1192.7

0.0
130.9
0.0
0.0
4093.2
0.0
0.0
980.9
5994.7
13594.3
1192.7

25986.7 25986.7

20
0.0
0.0
0.0
0.0

21
0.0
0.0
0.0
0.0

0
0
0
0

0.0
0.5
0.0
0.0
15.8
0.0
0.0
3.8
23.1
52.3
4.6
0.0
0.0
100.0

0.0
0.5
0.0
0.0
15.8
0.0
0.0
3.8
23.1
52.3
4.6
0.0
0.0
100.0