Department: Quality Assurance Issue Date: 01.03.06 Su !

ect

DOC. No. : AV/QA/SOP/026 Page No. : Page 1 of 2 Revision No. & Date : (00)-01.03.06

Operating Proce"ure #or $elting Point Apparatus.

Revisi Revis on No. ed Pages 00 0

REVISIONS Revision Description Original Issue

Date of Revision 01.03.06

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Department: Quality Assurance Issue Date: 01.03.06 Su !ect

DOC. No. : AV/QA/SOP/026 Page No. : Page 2 of 2 Revision No. & Date : (00)-01.03.06

Operating Proce"ure #or $elting Point Apparatus.

(.) *.) +.)

Purpose: -o !ro$#.e !roce.ure to o!erate Melt#ng Po#nt a!!aratu". Scope : -/e !roce.ure #" a!!l#ca0le for t/e o!erat#on of Melt#ng Po#nt a!!aratu". Responsi ility 1OD Qual#t&. QC C/em#"t De#inition: Melt#ng Po#nt A!!aratu"+ -/e #n"trument u"e. to mea"ure t/e melt#ng !o#nt of t/e mater#al"/!ro.uct". Proce"ure: (. )n"ert t/e tem!erature "en"#ng !ro0e #n t/e /ole !ro$#.e. on t/e -eflon co$er "ame a" for t/e .eterm#nat#on" of melt#ng !o#nt". *. A large /ole #" !ro$#.e. on t/e -eflon co$er. )t #" f#tte. 2#t/ a -eflon cor3. emo$e t/#" cor3. %#ll t/e 0o#l#ng !o#nt" tu0e nearl& /alf 2#t/ t/e l#4u#. to 0e te"te. for 0o#l#ng !o#nt. )n"ert t/e 0o#l#ng !o#nt tu0e #n t/e /ole of t/e -eflon co$er5 2/#c/ #" f#tte. 2#t/ cor3. 6ee.le"" to "tate t/at 0efore #n"ert#ng t/e tu0e #t #" 2ell 2#!e. from out"#.e 2#t/ a clean !#ece of clot/. +. )n"ert a melt#ng !o#nt ca!#llar& conta#n#ng t/e l#4u#. to 0e te"te. #n t/e 0o#l#ng !o#nt tu0e. -/e melt#ng !o#nt ca!#llar& "tan." #n t/e 0o#l#ng !o#nt tu0e 2#t/ #t" o!en en. .o2n2ar. an. "eale. en. u! "#.e .o2n. ,. 1eat t/e "#l#con o#l 0at/ "lo2l& #n t/e "ame 2a& a" for f#n.#ng melt#ng !o#nt" an. 2atc/ t/e tem!erature. -. A" "oon a" t/e 0o#l#ng !o#nt of t/e l#4u#. #" reac/e. a fa"t an. cont#nuou" "tream of 0u00le "een com#ng out from t/e #n$erte. ca!#llar& tu0e. 6ote t/e tem!erature at t/#" "tate. -/#" tem!erature #" t/e 0o#l#ng !o#nt of t/e l#4u#. un.er te"t. Documentation: -/e re"ult" recor.e. 0& Melt#ng !o#nt a!!aratu". Re#erence: )n /ou"e te"t !roce.ure Manual" of Melt#ng !o#nt a!!aratu".

,.)

-.)

..) /.)

Compile" %y Document Controller

Approve" %y Management e!re"entat#$e

'C(ASS)%)*D+ )nternal ,"e Onl& '

Aut&ori'e" y %actor& Manager