The graphic below express the calibration curve, which relates concentration and conductivity:

0.1
0.09
0.08

Concentration,g/L

0.07
0.06
0.05
0.04

Conductivity

Concentration

6.41

0.013

7.12

0.021

7.54

0.031

7.71

0.045

0.01

7.81

0.051

8.02

0.06

8.32

0.072

8.85

0.08

8.91

0.091

0.03
y = 0.0327x - 0.2049
R = 0.9468

0.02

6.5

7.5

Conductivity, mS/cm

8.5

9.5

Measurement Points
Time(min)
0
0.5
1
1.5
2
2.5
3
3.5
4
4.5
5
5.5
6
6.5
7
7.5
8
8.5
9
9.5
10
10.5
11
11.5
12
12.5
13
13.5
14
14.5
15
16
17
18

Conductivity
Concentration
=
(mS/cm)
(g/L)

8.5
0.07305
0
0
8.22
0.063894 0.015974 0.031947
8.19
0.062913 0.031457 0.031457
8.17
0.062259 0.046694 0.03113
8.14
0.061278 0.061278 0.030639
8.11
0.060297 0.075371 0.030149
8.09
0.059643 0.089465 0.029822
8.06
0.058662 0.102659 0.029331
8.04
0.058008 0.116016 0.029004
8.01
0.057027 0.128311 0.028514
7.99
0.056373 0.140933 0.028187
7.96
0.055392 0.152328 0.027696
9.94
0.120138 0.360414 0.060069
7.91
0.053757 0.17471 0.026879
7.89
0.053103 0.185861 0.026552
7.87
0.052449 0.196684 0.026225
7.85
0.051795 0.20718 0.025898
7.83
0.051141 0.217349 0.025571
7.8
0.05016 0.22572 0.02508
7.78
0.049506 0.235154 0.024753
7.76
0.048852 0.24426 0.024426
7.74
0.048198 0.25304 0.024099
7.72
0.047544 0.261492 0.023772
7.7
0.04689 0.269618 0.023445
7.68
0.046236 0.277416 0.023118
7.65
0.045255 0.282844 0.022628
7.64
0.044928 0.292032 0.022464
7.62
0.044274 0.29885 0.022137
7.6
0.04362 0.30534 0.02181
7.58
0.042966 0.311504 0.021483
7.57
0.042639 0.319793 0.02132
7.55
0.041985 0.67176 0.041985
7.52
0.041004 0.697068 0.041004
7.48
0.039696 0.714528 0.039696

Reactor Volume(L)

13.8

Inlet Flow(L/h)

40

Residence Time (h)

0.345

Ideal Residence Time

(min)
Non ideal Residence
Time(min)
Deviation(%)

20.7
32.8
58.6

According to the t =(tiCiti)/( Citi) formula (Chemical Reaction

Engineering, Octave Levenspiel), the experimental value for the residence time
is 32,8min. The difference between the experimental and ideal value is 63%.

19
20
21
22
23
24
25
26
27
29
31
33
35
37
39
41
43
45
50
55
60
65
70
75
80
85

7.45
7.42
7.39
7.37
7.35
7.32
7.29
7.27
7.25
7.21
7.17
7.14
7.1
7.07
7.05
7.02
7
6.97
6.92
6.88
6.85
6.82
6.8
6.78
6.76
6.76

0.038715
0.037734
0.036753
0.036099
0.035445
0.034464
0.033483
0.032829
0.032175
0.030867
0.029559
0.028578
0.02727
0.026289
0.025635
0.024654
0.024
0.023019
0.021384
0.020076
0.019095
0.018114
0.01746
0.016806
0.016152
0.016152

0.735585
0.75468
0.771813
0.794178
0.815235
0.827136
0.837075
0.853554
0.868725
1.790286
1.832658
1.886148
1.9089
1.945386
1.99953
2.021628
2.064
2.07171
5.346
5.5209
5.7285
5.88705
6.111
6.30225
6.4608
6.8646
80.96242

0.038715
0.037734
0.036753
0.036099
0.035445
0.034464
0.033483
0.032829
0.032175
0.061734
0.059118
0.057156
0.05454
0.052578
0.05127
0.049308
0.048
0.046038
0.10692
0.10038
0.095475
0.09057
0.0873
0.08403
0.08076
0.08076
2.465918