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  • Lillio 2014 10a50 V8N3 PDF

    Enviado por

    Gabriel Miguez
    15 visualizações2 páginas
    The document reports results from an x-ray powder diffraction scan of a sample using a diffractometer. It lists the experimental parameters used for the scan including the scan range, step size, and scan time. It provides information on the x-ray source including the anode material and wavelengths. A graph shows the diffraction pattern with intensity on the y-axis and position on the x-axis. A table lists the peaks detected with information on position, height, width and d-spacing.

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    Lillio-2014-10a50-V8N3.pdf

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    The document reports results from an x-ray powder diffraction scan of a sample using a diffractometer. It lists the experimental parameters used for the scan including the scan range, step size, and scan time. It provides information on the x-ray source including the anode material and wavelengths. A graph shows the diffraction pattern with intensity on the y-axis and position on the x-axis. A table lists the peaks detected with information on position, height, width and d-spacing.

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    © All Rights Reserved
    Baixe no formato PDF, TXT ou leia online no Scribd
    Sinalizar o conteúdo como inadequado
    15 visualizações2 páginas

    Lillio 2014 10a50 V8N3 PDF

    Enviado por

    Gabriel Miguez
    The document reports results from an x-ray powder diffraction scan of a sample using a diffractometer. It lists the experimental parameters used for the scan including the scan range, step size, and scan time. It provides information on the x-ray source including the anode material and wavelengths. A graph shows the diffraction pattern with intensity on the y-axis and position on the x-axis. A table lists the peaks detected with information on position, height, width and d-spacing.

    Direitos autorais:

    © All Rights Reserved
    Baixe no formato PDF, TXT ou leia online no Scribd
    Sinalizar o conteúdo como inadequado
    de 2

    Backupn

    Page 1

    12/23/2014

    Muestra V8N3
    Diffractometer system=XPERT-PRO
    Start Position [2Th.]
    10,0100
    End Position [2Th.]
    49,9900
    Step Size [2Th.]
    0,0200
    Scan Step Time [s]
    2,0000
    Anode Material
    Cu
    K-Alpha1 []
    1,54060
    K-Alpha2 []
    1,54443
    K-Beta []
    1,39225
    K-A2 / K-A1 Ratio
    0,50000
    Generator Settings
    40 mA, 40 kV

    Main Graphics, Analyze View:


    Counts
    Lillio-2014-10a50-V8N3-dic

    400

    100

    0
    20

    30

    40

    Position [2Theta] (Copper (Cu))

    Peak List:
    Pos. [2Th.] Height [cts]
    11,0025
    59,85
    13,7479
    78,57
    17,1784
    287,94
    20,4094
    57,02
    22,0148
    108,99
    26,0070
    289,59
    26,7269
    78,90
    28,0381
    515,20
    29,9309
    91,20

    FWHM Left [2Th.]


    0,1181
    0,0984
    0,1181
    0,0590
    0,0984
    0,1771
    0,1181
    0,1574
    0,0984

    d-spacing []
    8,04168
    6,44138
    5,16197
    4,35151
    4,03768
    3,42623
    3,33555
    3,18247
    2,98539

    Rel. Int. [%]


    7,87
    10,33
    37,85
    7,50
    14,33
    38,06
    10,37
    67,72
    11,99

    Backupn

    31,3130
    32,7562
    33,3107
    33,7767
    34,6896
    35,4138
    35,8966
    37,6517
    38,2134
    40,1513
    41,4385
    41,9921
    43,3192
    43,9572
    44,8521
    45,6548
    47,3873
    48,3386
    48,7673

    Page 2

    760,77
    133,00
    38,37
    27,78
    445,56
    52,41
    89,14
    45,36
    18,03
    50,47
    81,05
    71,76
    11,81
    28,60
    74,48
    41,83
    137,87
    84,56
    88,84

    0,1771
    0,1181
    0,1181
    0,1181
    0,1968
    0,1181
    0,1574
    0,1574
    0,2362
    0,1181
    0,1574
    0,2165
    0,2362
    0,3149
    0,2362
    0,1574
    0,1574
    0,0787
    0,2362

    12/23/2014

    2,85670
    2,73407
    2,68981
    2,65376
    2,58598
    2,53475
    2,50175
    2,38907
    2,35524
    2,24592
    2,17908
    2,15163
    2,08874
    2,05989
    2,02086
    1,98718
    1,91849
    1,88293
    1,86738

    100,00
    17,48
    5,04
    3,65
    58,57
    6,89
    11,72
    5,96
    2,37
    6,63
    10,65
    9,43
    1,55
    3,76
    9,79
    5,50
    18,12
    11,11
    11,68

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