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Measurement profile
400
300
100
20
40
7/7/2014 2:52:26 PM
XRD Analysis
UMP 2.raw
UMP
60
2-theta(deg)
-1-
Analysis date
Sample name
File name
Comment
200
[1], d=7.111(6), 2-theta=12.437(10)
Intensity (cps)
Analysis Results
General Information
Measured time
Operator
6/9/2014 12:34:15 PM
administrator
50
-50
80
Measurement conditions
XG
Goniometer
Attachment
K-beta filter
Incident monochromator
Receiving monochromator
Counter
Cu/30 kV/15 mA
-
-2-
1 deg/min
0.02 deg
2/
10-80 deg
-
Formula
Al2 Si2 O5 ( O H )4
Figure of merit
0.6861116897989547
ICDD
582001 (ICDD)
Phase name
Kaolinite-1A
Formula
Al2 Si2 O5 ( O H )4
Space group
1 : P1
ICDD
582001 (ICDD)
-3-
Intensity (cps)
300
2-theta (deg)
12.437(10)
17.78(4)
19.87(2)
21.32(7)
24.918(14)
26.700(14)
35.00(3)
36.05(3)
38.436(12)
200
0
20
d (ang.)
7.111(6)
4.984(12)
4.464(5)
4.164(14)
3.570(2)
3.3361(18)
2.561(2)
2.4894(18)
2.3401(7)
40
Height (cps)
235(15)
23(5)
57(8)
41(6)
190(14)
101(10)
44(7)
34(6)
41(6)
Kaolinite-1A,Al2
Al2Si2
Si2O5
O5((O
O H)4,
)4,(-1
(-2-3
0 1)
Kaolinite-1A,
Kaolinite-1A,
Al2 Si2
O5
O H( H
)4,
(1 -1(-1
2) 1)
Kaolinite-1A,
Al2O5
Si2((O
O5
OH
Kaolinite-1A,
Al2 Si2
H )4,
(-2)4,
1 1) 3 1)
Kaolinite-1A,
Al2 Si2
O H( )4,
0 3)
Kaolinite-1A,
Al2O5
Si2( O5
O H(0)4,
(-2 0 2)
Kaolinite-1A,
(O
H-3
)4,2)(1 3 1)
Kaolinite-1A,
Al2 Si2Al2
O5 Si2
( O O5
H )4,
(-1
(0 4 0)
Kaolinite-1A,
2)
Kaolinite-1A, Al2
Al2 Si2 O5
O5 ( O
OH
H )4, (-1
(2 031)
Kaolinite-1A, Al2 Si2 O5 ( O H )4, (0 -2 3)
Kaolinite-1A, Al2 Si2 O5 ( O H )4, (-2 2 2)
Kaolinite-1A,
0 3)
Kaolinite-1A, Al2
Al2 Si2 O5
O5 ( O
OH
H )4, (-2
(1 -3
2)
Kaolinite-1A, Al2Si2
Si2 O5( O
( O H)4,
)4, (1-432)
2)
Kaolinite-1A,
Kaolinite-1A, Al2
Al2 Si2 O5
O5 ( O H
H )4, (0
(-1 -3 3)
Kaolinite-1A,
Al2
(0
4 32)3)
Kaolinite-1A,
Al2Si2
Si2O5
O5((O
OHH)4,
)4,
(-1
(-2)4,
-2(1
3)-2
Kaolinite-1A,
O )4,
H
Kaolinite-1A,
Al2Al2
Si2Si2
O5O5
( O( H
(-1
-1
4)3)
Kaolinite-1A, Al2 Si2 O5 ( O H )4, (0 0 4)
Kaolinite-1A,
Al2 Si2
O5
(O5
O H( O
)4,H(0)4,2 (-1
0) 1 0)
Kaolinite-1A,
Al2
Si2
Kaolinite-1A,
Al2Al2
Si2Si2
O5O5
)4,
(1 (-1
1
Kaolinite-1A,
O)4,
H (-1
)4,
Kaolinite-1A,
Al2
Si2
O5
((OO(HH
1 0)
1)-1 1)
Kaolinite-1A,
Al2
Si2
O5
(
O
H
)4,
(0
-2
Kaolinite-1A, Al2 Si2 O5 ( O H )4, (0 2 1) 1)
Kaolinite-1A, Al2 Si2 O5 ( O H )4, (0 0 2)
Kaolinite-1A,
Al2Al2
Si2Si2
O5O5
( O( O
H )4,
(1 (-1
1 1)0 2)
Kaolinite-1A,
H )4,
Kaolinite-1A,
Al2
Si2
O5
(
O
H
)4,
(-1
-1
2)
Kaolinite-1A, Al2 Si2 O5 ( O H )4, (-1 1 2)
100
400
400
200
60
80
2-theta(deg)
Peak list
Int. I(cpsdeg)
128.2(18)
9.5(6)
55(11)
52(9)
114(2)
31.4(12)
26.7(18)
13.6(13)
19(2)
-4-
FWHM(deg)
0.431(9)
0.33(4)
0.66(11)
1.00(15)
0.506(12)
0.280(12)
0.44(4)
0.33(4)
0.36(4)
Size
194(4)
252(32)
129(21)
84(13)
168(4)
305(13)
196(16)
261(29)
246(28)
Phase name
Kaolinite-1A, (0,0,1)
Unknown,
Kaolinite-1A, (0,2,0)
Kaolinite-1A, (1,1,-1)
Kaolinite-1A, (0,0,2)
Kaolinite-1A, (1,1,1)
Kaolinite-1A, (2,0,-1)
Kaolinite-1A, (1,-3,-1)
Kaolinite-1A, (2,0,-2)
39.34(3)
45.47(5)
62.32(6)
76.9(3)
2.2882(18)
1.993(2)
1.4888(12)
1.239(4)
17(4)
35(6)
39(6)
3.3(18)
25(3)
24.5(12)
20.5(11)
5.7(14)
0.98(16)
0.50(5)
0.38(5)
1.6(3)
-5-
90(15)
182(19)
255(35)
67(11)
Kaolinite-1A, (1,3,1)
Kaolinite-1A, (2,0,-3)
Kaolinite-1A, (3,3,-1)
Unknown,
Background
Data
Function name
param0
param1
param2
param3
param4
param5
param6
param7
param8
param9
param10
param11
param12
param13
param14
param15
param16
node0
node1
node2
node3
node4
node5
node6
node7
node8
node9
node10
node11
node12
node13
-6-
UMP 2
B-spline
13.40700321021733
18.0031852965251
-3.232632501915734
21.98833764246207
46.21134101656693
4.949476948295137
24.11769534335532
32.97160400155261
1.157635881719851
25.46587843796416
4.034675928233191
38.32556858199003
10.02922263200282
17.88430462620008
19.72161543365654
14.1720221782605
12.33193360005924
10
15.32
20.64
25.96
31.34
35.54
39.74
43.94
48.16
52.04
55.92
59.8
63.74
70.7
Common Parameter
Kaolinite-1A
node14
80
Function name
param0
param1
param2
s
U
V
W
A0
A1
etaL0/mL0
etaL1/mL1
etaH0/mH0
etaH1/mH1
h
k
l
March coefficient
Peak shift
Scale factor
FWHM
Asym. factor
Extinction coefficient
Preferred orientationMarch-Dollase
-7-
Structure parameters
Data set name
File name
UMP 2
Phase Name
Rwp
0
Element
Rp
0
Re
0
Occupancy
S
0
-8-
Temperature factor
Chi^2
0
Maximum shift/e.s.d.
0
Lattice constants
Angular correction
No correction
Use External standard parameters
Use internal standard data
Analysis results
File name
UMP 2
a (ang.)
5.143205
b (ang.)
8.930718
c (ang.)
7.391349
alpha (deg)
91.697502
beta (deg)
104.836304
gamma (deg)
89.831703
Phase name
Kaolinite-1A
a (ang.)
5.143205
b (ang.)
8.930718
c (ang.)
7.391349
alpha (deg)
91.697502
beta (deg)
104.836304
gamma (deg)
89.831703
1
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
UMP 2
UMP 2
Data set
a
b
c
-9-
Crystallinity
File name
Crystallinity (%)
CrystallinityGraph.emf
- 10 -
Crystallite size(ang.)
Strain (%)
Phase name
Crystallite size(ang.)
Strain (%)
CSSGraph.emf
- 11 -
RIRGraph.emf
- 12 -
- 13 -
QCGraph.emf
- 14 -
QCGraph.emf
- 15 -
QCGraph.emf
- 16 -
Stress
Stress constants
Analytical conditions
Analysis results
StressGraph.emf
- 17 -