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Contents Characterization of Plastic Packages—4 The characterization process is comprised of only eight steps.—4 Acid Choice:—4 Acid Temperature: ––5 Determine Correct Fixturing: —5 Determine Pulse or Reciprocating:—5 Determine Heat-up Time:—6 Determine Etch Volume:—6 Rinse Time:—7 Etch Time:—7 3 .
If decapsulation is not sucessfull with nitric acid. sample etch characterization. Much less metal damage. Lowest grade that will decapsulate plastic packages. the next step would be trying the six mixed ratios. For this ﬁrst step any deﬁnition gasket that has an opening that is 50% of the size of the package may be used to determine the correct acid type to be used. Characterization is the process of determining the correct etch recipe and ﬁxturing to successfully decapsulate a plastic package. The following paragraphs will explain how each of the steps are performed and can be optimized for a successful decapsulation. Acid Choice: Every package has an optimum acid for decapsulation. Common Acids Used For Decapsulation: TYPE 90% Fuming Nitric 98% Fuming Nitric Red Fuming Nitric 96 to 98% Sulfuric 20% Fuming Sulfuric USES Least expensive. Lowest grade that will decapsulate Hi-Temp packages. Efﬁcacy has not been tested. Much less metal damage. The ﬁrst rule in determining the acid type is to start with Fuming Nitric Acid. Least expensive. Faster Etch Rate. The characterization process is comprised of only eight steps. The lower the temperature the less chance of thermal stress being introduced to the sample. New users and veterans alike share one common dilemma. If decapsulation is still not sucessfull ﬁnally use either 98% Sulfuric or 20% Fuming Sulfuric Acid. Faster Etch Rate. The ﬁrst thing to remember is: All plastic packages follow the same characterization process no matter what type of package you are trying to decapsulate. 4 .Characterization of Plastic Packages This guide will show you in simple steps the art of characterizing and opening virtually any plastic package for decapsulation. 1) Determine Correct Acid Type 2) Determine Temperature 3) Determine Fixturing 4) Choose Pulse / Reciprocating 5) Determine Heat-up Time 6) Determine Acid Volume 7) Determine Etch Time 8) Determine Rinse Time While everyone ultimately follows these eight steps. Nitric acid uses the lowest temperature of all of the acid types usable in the system. Will work in the system. using the eight steps in the correct order greatly reduces the time of characterization. Wider temp range.
Recriprocating etch does not work with applications using only fuming sulfuric acid. Whenever possible the use of a pocket gasket will optimize the ﬁxturing creating a precice location and cavity deﬁnition in a single gasket. When nitric acid is use for decapsulation the etch will be isotropic. mixed acid. or put simply the higher the temperature the faster the etch. Reciprocating works with nitric acid. Therefore the correct temperature would be high enough to have a fast etch rate with no metal loss. while pulse will produce a more rounded side wall. the larger the hole is going to be. The temperature range should be between 30 and 50°c in order to protect the metalization. Determine Pulse or Reciprocating: The choice of pulse or reciprocating etch determines the relative angle of the side wall.Determine Etch Temperature: The basic rule for determining the temperature is as follows: The closer the etch temperature is to the boiling point of the acid the more reactive the acid will be. but the metal will be preserved. and device to be etched. Any leaks will be visible in the waste line. Standard starting temperatures are: HNO3 75 to 80c Mixed 80 to 90c H2SO4 225 to 250°c In packages where unpassivated metals are used. the correct ﬁxturing can be chosen. With an isotropic etch the deﬁnition gasket hole must be slightly smaller than the die size. Any leak in any of the mating surfaces will render reciprocating inoperable. a different technique is required. Reciprocating requires an excellent seal between the etch head. Sulfuric acid etches from the center outwards and therefore a gasket that is slightly larger than the die size is required. The higher the temperature the more likely there may be metal damage. 5 . In other words the deeper the package. The etch rate will be much slower. gasket. This can be seen because the waste acid will appear to be slowly moving toward the waste bottle while there is no pump operation. Conversly. The deﬁnition gasket is determined by the acid type used for decapsulation. Use Pulse Etch only with fuming Sulfuric Acid applications. Determine Correct Fixturing: Once the acid type and temperature have been determined. and non-fuming sulfuric applications. This also applies to mixed acid to a lesser extent. A reciprocating etch will produce a relatively straight side wall.
Device only takes 40 sec to heat up adding 20 sec to etch time. First Device: Everything except the etch head is cold. The color of the waste material will determine the correct volume. Third device is almost over etched. Pumping Acid without Etching 20 Sec.Determine Heat-up Time: Heat-up time is the amount of time that is required to preheat the device to match the etch temperature selected. place the device on a hot plate at 85% of programmed temperature for 30 minutes to ensure that the 120 second Heat-up Time will start the etch process at Etch Time 1. Program Settings Heat-up Time 20 Sec. If it is very dark brown and not moving freely the volume is too low. Sulfuric acid requires a higher volume. Device takes 60 sec to heat up. Second Device: Entire Etch area is warmer. For this example. Etch Time 60 Sec. If the waste acid is dark brown and moving freely the volume is still too low. Efﬁcient and reproducible etching will not occur until the part is at the same temperature as the acid. 6 . If it is dark brown and not moving freely the volume is too low. Device only takes 20 sec to heat up adding 40 sec to etch time. If the waste acid is brown and moving freely the volume is correct. Third Device: Entire Etch area is Hot.* * Note: For all devices that have a heat sink. As a general rule when using nitric acid start with a volume of 3 ml/min. The diagram below shows what is occuring and how to correct the problem. Having too low of a volume requires a longer etch time than necessary. Programming of the heat-up time is dependent upon the temperature of the entire heat exchanger assembly and safety cover. If the waste acid is light brown to clear the volume is too high. Etch Time 40 Sec. The reactivity of a given acid is determined by the chemistry and by Etch Temperature. Heat-up Time 20 Sec. which reduces as the waste acid moves away from the etch head. Therefore if the color of the waste acid is light brown to clear the volume is correct. Etch Time 20 Sec. Correct Setting Heat-up Time 120 Sec. Etch Time 60 Sec. Etching takes 20 sec. The volume is determined differently when using nitric or nitric/sulfuric mixes when compared to sulfuric acid although both share a similar characteristic in that they each have waste material carrying capacity based on the reactivity and heat of the acid. Heat-up Time 20 Sec. Determine Etch Volume: The etch volume is the amount of acid used in ( ml/min ) that is programmed in the etch time. By using 120 seconds of Heat-up Time almost all devices will start the etch process at Etch Time 1. Having too high of a volume wastes the acid. Heat-up Time 20 Sec. Etch Time 20 Sec. The carrying capacity of the acid is inﬂuenced by the temperature of the acid. the ﬁrst device opens correctly. Common indication of incorrect Heat-up Time: Decapsulation of ﬁrst device opens correctly. Pumping Acid without Etching 40 Sec. Fourth or ﬁfth device requires a reduction in etch time. Second device opens a little more than expected.
Nitric. Rinse Time: The rinse time serves two functions. For example if the package is very slightly over etched. Next add all of the etch times together and subtract 3 seconds for each time the package was etched. Examine the package opening. or No Rinse for Sulfuric packages. As the Elite Etch has active pressure monitoring. there is little likelyhood of damage to the system during the purge process due to clogging of the system. ( The subtraction of the 3 seconds is to account for the rinse time. or Sulfuric. If the die is not exposed. or No Rinse for Nitric packages. is to make very small changes to the etch cavity. If the package is dirty or very slightly under etched. increase the rinse time in order to make the cavity perfect. for all other packages 60 seconds works well as a starting time. The operator has the choice of Nitric. Sulfuric. decapsulate the package again using the above base etch time. Continue to re-decapsulate the package changing the etch time to a shorter etch time only when you reach a decapsulation point at which it seems probable that an additional time increment (10 seconds or 60 seconds) will over etch the package. The ﬁrst is to clean the part with cold acid and ﬂush the part and waste line before nitrogen ﬂush. This back pressure will increase the efﬁciency of the acid by holding the acid on the device for a longer period of time. and very important function. The easiest way to determine the etch time is to run a sample of the package for a short period of time. ) Run another sample package using the calculated etch time and make minor corrections as necessary. The Elite Etch operates with a waste cooling system which increases the back pressure to the heat exchancer.Etch Time: The etch time is the amount of time ( in seconds ) that the device is actually being etched. reduce the rinse time to make the cavity perfect. This is especially true of parts that are opened using 20% Fuming Sulfuric Acid where the etch rate may be up to ﬁve times faster than other systems. Start the characterization with the rinse time set to 12 seconds which is the middle of the programmable range. The second. These are your base etch times. 7 . Sulfuric.MIxed or No Rinse for Mixed acid packages. Examine the package again. If the rest of the recipe is characterized you can make small changes to perfect the etch. For SO and TSOP packages start with 10 seconds.
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