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Lins – SP
2009
AVALIAÇÃO DO TEOR DE HIPOCLORITO DE SÓDIO EM ÁGUA
SANITÁRIA: Execução e validação de metodologia
RESUMO
Seletividade (especificidade).
Precisão.
Exatidão
Robustez.
RESULTADOS E DISCUÇÕES
Concentração Teórica / %
y = 1,031x + 0,030
5,00 R² = 0,999
4,00
3,00
2,00
1,00
0,00
0,00 1,00 2,00 3,00 4,00 5,00 6,00
Concentração Real / %
CONCLUSÃO
ABSTRACT
Used in certain cases and for different purposes, sodium hypochlorite is frequently
found in bleach, especially in Brazil. But with the growing illegal production became
possible because the consumer is being harmed. The aims of this work aims was the
implementation and validation of the NBR-9425 - ABNT - Sodium hypochlorite -
Determination of active chlorine. For the development and validation, calibration
curve was constructed in a range of concentration from 0.5% to 5.0%. Was evaluated
all the necessary requirements for validation: selectivity, linearity, precision,
accuracy, detection limit, quantification limit and ruggedness. After the validation,
samples of bleaches sold clandestinely in the Lins region were evaluated. The results
showed the non-conformity with the decree n ° 89/94 , which defaults to the content of
2.00% w / w 2.5% p / p. This work showed that validation tool is adequate and
proved that the technique is sensitive to low concentrations of sodium hypochlorite,
showing yet that the results of the tests performed allow an evaluation of specific
parameters as ensuring the implementation of the method and reliability of analytical
results.
ORIENTADOR: