fl Designation: 8 764 - 94
Sedo:
Determination of Indi
(STEP Test)?
oR cay
Standard Test Method fbi: 20/10,
Simultaneous Thickneks and El
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1. Scope
1.1 This test method closely estimates the thickness of
individual layers of a multilayer nickel deposit and the
electrochemical potential differences between the individual
layers while being anodically stripped at constant current
density.29
1.2 This standard does not purport to address all of the
safety concems, if any. associated with its use. It is the
responsibility of the user of this standard to establish appro.
priate safety and health practices and determine the applica-
bility of regulatory limivacions prior to use.
2. Referenced Documents
21 ASTM Standards:
B504 Test Method for Measurement of Thickness of
Metallic Coatings by the Coulometric Method®
1D 1193 Specification for Reagent Water?
3. Summary of Test Method
3.1 This procedure is a modification of the well-known
coulometric ‘method of thickness testing (Test Method
3504). It is also known as the anodic disolution or
electrochemical stripping method
3.2 Coulometric thickness testing instruments are based
fon the anodic dissolution (stripping) of the deposit at
Constant current, while the time is measured to determine
thickness. As commonly practiced, the method employs a
small cell that is filled with an appropriate electrolyte, and
the test specimen serves as the bottom of the cell. To the
bottom of the ceils attached a rubber or plastic gesket whose
opening defines the measuring (stripping, anodic) area, If a
metalic cell is used, the rubber gasket also electrically
insulates the test specimen from the cell. With the specimen
as the anode and the cell or agitator tube as the cathode, a
constant direct current is passed through the cell until the
"This etn i nde the jursiction ef ASTM Commie BA on Metalic
a iacpanie Coatings and is the dest rerponitlty of Suscommites B04 tooo
Gener Fest Meds
Curent elon approved Jan 15, 198 Published Apri 1988. Orinally
Pubisbed a Bed ~26 ast previous eon B04
2 Far Gocuon of hist sr Harbulah EP Simataneous Tikes and
Ecrochemiea| Potenah Determination a Undidunl Lape Ia Mute
Nike Deposta” Plating and Suface Finishing, Vl 67. No 2 Febary (80.
84
2S, Paenk 4310.90. Asignee The Chrys Coro, Mitland Fark, 34h
‘ Aanusl Bok of ASTM Standards, ot 02.05
¥ anmasl Book f ASTM Sionares Val i
nickel layer is dissolved. A sudden change in voltage between
the electrodes occurs when a different metalic layer stats to
dissolve
3.3 Each different metal or species of the same metal
requires a given voltage (electrochemical potential) to keep
the current constant while being stripped, As one nickel layer
is dissolved away and the next layer becomes exposed, there
will be a voltage change (assuming a constant current and
difference in the electrochemical characteristics of the {wo
nickel layers). The clapsed time at which this voltage change
‘occurs (relative to the start of the test or previous voltage
change) is a measure of the deposit thickness,
3.4 At the same time, the amplitude ofthe voliage change
can be observed, That is, the ease (or difficulty) wth which
fone layer can be dissolved or stripped with reference to
another layer can be compared. The lower the voliage
needed the more active the metal or the greater the tendency
to corrode preferentially toa more noble metal adjacent 10 it
3.5 Where the metallic layers are of such a similar nature
that change of the stripping voltage is small, there can be
problems in detecting this change ifthe voltage between the
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