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By: Jack H. Berg are present in the plat- onto a filter surface, is
WHY FILTER? 1 President of Serfilco ing tank, or 300 to 450 not a filter aid. The
I
oz. per 100 sq. ft. in a diatomaceous earth is
surface filter. That is the filter aid and any
n an article I wrote
INDUSTRY 2 over 18# to 27#, powder, such as car-
EVENTS
awhile back for the P.F.
which goes to waste bon, is a solid which is
Directory based on ‘tell
treatment every time to a filter, a solid which
it like it is’ opinions, I
the filter is serviced, lowers solids holding
NEWS & 3 feel that I may have
NOTES sometimes once or capacity; hence fre-
missed a most impor-
twice a week, some- quent servicing. Not
tant fact in regards to
times less if cleaning is just because the flow
FROM THE 6 organic removal and
less frequent, plus so- rate has been lowered,
FORUM filtration. Other authors
lution loss. but because the car-
suggest 1½ oz. of filter
bon, acting like a filter,
aid plus up to 3 oz. of The fact, which may
FINISHING 9 plugs up and fails to
powdered carbon on be overlooked, is that
SPOTLIGHT adsorb the organic im-
their disc filters for filters remove insolu-
purities.
continuous organic re- ble solids - carbon ab-
THE LAST 15 moval and filtration. sorbs organics which During many of my
WORD That’s up to 3 – 4.5 oz are in solution. The talks around the world,
total solids to remove powdered carbon, I’ve opened with a re-
what solids or organics which is pre-coated mark indicating that
you no longer have to filter your particle retention and flow rates sulfate nickel for record masters
plating solution. The reaction I to assure the solution was free in what looked like a simple
see is “Why does this speaker of solids. waffle iron.) This is an example
tell us we no longer have to fil- of being able to prevent solids
Many years ago, I authored an
ter our plating solutions?” It is from entering the chamber if
article which Products Finishing
simple – No dirt (solids) in, no filtration was done at 100% of
editor emeritus, Ezra Blount,
dirt out. flow rate, and the filter media
typed as I dictated, entitled The
was chosen to be non-migrating
Another time, a special part to Case for Coarse Filtration at
and at a level of particle reten-
be plated had to be done in a High Turnover Rates (PF 1964).
tion to match the desired result.
solids free solution. So an in- It was based on the Hydraulic
strument which monitors solids Handbook, which states that at This brings us to explain the dif-
was purchased to signal when 14 turnovers per hour, all of the ference between nominal filter
the part could enter the tank. solution would have passed over media, which stops certain size
Of course, the instrument didn’t the filter at least once. It didn’t solids according to its density
assure the plater that during the recognize dead areas in a tank which could offer 85 – 95% as-
time of deposition the solution of plating solution. surance that no particles larger
stayed free of solids from the air than the rated media would re-
It also depended on no addi-
(or anodes, or migrated filter tain, and absolute rating indicat-
tional solids from entering the
media). I feel that the money ing a 100% of certain size parti-
plating tank while deposition
spent on the instrument should cles were stopped. The use of
was taking place, (which condi-
have been used on a filter and any filter media does not assure
tion would occur when plating
Page 5
VOLUME 1, ISSUE 7
that the presence of different and solids to be disposed of. With the use of filters, coa-
size particles aren’t in the plat- Previous articles have empha- lescers, and carbon on solutions
ing solution, but when media sized the choice to “Work Back- from the soak to the plating
and flow rate (turnover) are put wards.” This reduces the solids, tank, the plater may expect to
together, than a predictable de- which may reach the plating so- have eliminated up to 90% of
gree of clarity can be accom- lution. Therefore, the final rinse solids from entering the plating
plished. before plating is a good oppor- solution. This could make it pos-
tunity to stop particulates, which sible for his plating filter to last
The plating of memory drums
from surface tension have trav- ten times longer between servic-
for electronic applications some-
eled from the cleaner to the ing. Did we completely eliminate
times employs 40 – 50 turn-
etch and finally arriving at the the filter on the plating solution?
overs per hour at .1 micron ab-
plating station. No, but with the steps of pre-
solute particle retention from
vention in place, we have
non-migrating membrane me- Attention to prevention could
greatly reduced the need.
dia. Compare the above to 1-2 eliminate 80-90% of such solids,
turnovers per hour at even 5 and when a separate chamber You now have a system of filtra-
micron retention from a media containing granular carbon is tion and separate purification in
which migrates, and you see used to recirculate on the place which will pay dividends
why your plating may some- etchant and pre-rinse, another from less solution contamina-
times have rough areas of de- problem is avoided. This leaves tion, less solids to hazardous
posit. the organic breakdown products waste, less labor for servicing
as the only other need for car- and, as we’ve said before,
Frankly, I have always favored
bon on the plating solution. “unattended filtration” and puri-
some type of cartridge which,
This in turn can be reduced by fication, from day-to-day and
after a first flush, is no longer
switching from air for agitation month-to-month. Talk to your
allowing fibers to migrate. I also
to pumps with eductors to cre- chemical supplier; he knows the
favor cartridges because they
ate the necessary movement of value of getting rid of solid or
are available for use on slimy
the ions for faster plating with- organic contamination, as it ap-
alkaline solutions with coarse
out causing breakdown of the plies to service requirements.
windings. (Platers of alkaline
brightener chemical. Talk to your customer as well;
zinc used them because their
he knows the value of more uni-
cleaning was inadequate and One recent report indicated that
form deposits with improved
the coarse filter held more solids a plater could plate up to 33%
ductility. And finally, talk to your
– sometimes 6-8 wks. between faster at higher amps without
production staff; they know the
services.) Other solutions which burning. It made it possible for
value of less rejects.
crystallize, such as acid zinc or his company to bring in more
nickel, would usually use 5 to 15 parts from his customer without
micron, but even certain nickel the need to increase his need Article reprinted, courtesy of:
applications may find that a 50 for another automatic machine.
Jack H. Berg
micron at high turnover rates A further benefit of controlling
President
will provide good results. the amount of solids in the plat-
SERFILCO, Ltd.
ing rank and the level of organic
Now, what about ‘no filter on 2900 MacArthur Dr.
impurities is that captured plat-
the plating tank’ - why not? Be- Northbrook, IL 60062
ing solutions dripping from parts
cause the filter media needs Ph: 847-509-2900
in a 'dry sump' may be added
neutralizing of the plating solu- Fax: 847-559-1995
back to the plating tank without
tion, all steps should be taken to sales@serfilco.com
the fear that you are building up
minimize the amount of media www.serfilco.com
the level of organic impurities.
Page 6
FINISHING TALK
Posted on October 11, 2006 24 hours or more. I'm certainly no plater, but
could a Woods strike be used instead?
Our August installment of From the Forum is a
discussion between members William S, Cap- Labrat
tain Tripz, Dedalus, Labrat, Skelton, and
The most successful nickel reactivation process
DustinGebhardt on the topic of nickel plating
I have used is the cyanide activation process.
over an item that has already been nickel plated.
Used cathodically, the make up is 8 opg Potas-
Feel free to add your thoughts to their ongoing
sium Cyanide, 8 opg Potassium Hydroxide
discussion by visiting the forums at
(Caustic Potash) and water to operating level.
www.finishingtalk.com/community and choosing
I normally reactivate for 5 minutes, cyanide
the “Decorative Plating” forum. For more ‘From
copper flash (no rinse between), rinse well,
the Forum’ discussions, check out our internet
television show, Finishing Talk Live, where hosts then into bright nickel.
Paul Fisher and Paul Skelton bring the boards to I have heard of other methods that worked
life! well that you may want to experiment with:
www.finishingtalklive.com cathodic activation in 30% hydrochloric acid;
Woods nickel strike (Nickel Chloride, Hydro-
chloric Acid, water) for 1-2 minutes, very quick
William S
rinse, and into bright nickel.
I am looking for a process that you can plate
Skelton
bright nickel over bright nickel, without peeling
I can speak from experience that its part "how
problems. Any help would be great. Thanks.
you hold your mouth" and the rest following
Captain Tripz process procedure. Plating over a passive
You could use a cyanide activator. Same prin- nickel coating can be much compared to that
ciple as when dummying a bright nickel tank of plating over stainless steel, which is a me-
with previously used dummies. Activate with thodical process, but simple all in the same.
cyanide activator to keep chunks from slough- You have one of two choices and can incorpo-
ing off the dummies into the solution. Just rate one into the other’s process if it makes
make sure you are equipped to deal with the sense for the other processes you are per-
cyanide waste treatment. forming.
www.finishingtalk.com/community
Page 9
VOLUME 1, ISSUE 7
Syracuse, NY
I recently participated in a week 60,000) than be hit by a lightning parent and caretaker of over
long leadership training program bolt). 12,000 standards. It was origi-
in Seattle, Washington – home of While I was educating myself on nally formed in 1898 by a group
rainy days, a gargantuan volcano the fascinating history of the of scientists and engineers seek-
named (appropriately enough) Space Needle, I came across a ing to standardize the steel used
Mt. Rainier, and of course, that reference to a very familiar or- in rail road track fabrication – ap-
world famous architectural nov- ganization. The ASTM (American parently there were a lot of rail
elty, the Space Needle. I had very Society for Testing and Materials) breaks in those days. As time
little time to go sightseeing during mentions in its 1998 publication A went on, it developed the Com-
my trip; nevertheless, I did have Century of Progress, the impact mittee A01 which oversees stan-
the opportunity to see the struc- that its structural steel specifica- dards for Steel, Stainless Steel
ture I’ve come to know only at a tions had on “some of the most and Related Alloys and has a
distance through shows like Fra- prestigious and demanding con- membership of 800 industry pro-
sier and the Austin Powers mov- struction projects of the postwar fessionals and experts. Today,
ies. I know it’s a bit cliché – I era” – including the legendary ASTM standards cover both fer-
guess the inner tourist in me just Space Needle. An excerpt from rous and nonferrous metals, in-
couldn’t be mollified until I took the section entitled ASTM in the cluding steel, copper, aluminum
the 60 story elevator ride up to Postwar Economy, reads: and many others.
the observation deck. The organization is also active in
“Seattle’s Space Needle, a soaring
After my trip, I decided to do a bit 600-foot steel tower that was the standardization of metal fin-
of research into the design and built for the 1962 World’s Fair, ishes. In fact, it is a focus of the
construction of the structure, and featured three sets of tapered ASTM Committee A05 on Metallic-
I found quite a bit of fascinating steel legs made according to Coated Iron and Steel Products.
information about the tower. It Standard A 36. The standard de- Over the past hundred years, the
turns out that it was built to be a scribed a new type of hardened committee has developed “over
focal point at the 1962 World’s carbon steel that could handle 70 specifications and test meth-
Fair in Seattle, and the final ele- extreme design stresses. An ods that help protect iron and
vator car was installed only a day ASTM publication reported that steel products against corrosion
before the grand opening. During the Space Needle had “less than by the use of metallic coatings, as
the Fair (which ran from April 21 3-inch maximum sway at the top; well non-metallic coatings” (ASTM
to October 21) 20,000 people per it is designed for heavy seismic & the Metals Industry: Partners in
day traveled up to the observa- loads and wind gusts. The greater Long Term Success).
tion deck. And if safety was ever strength of A 36 steel permitted Over the years, I come to see
a concern to those early visitors, higher design stresses, welded more and more just how inter-
they would probably be relieved fabrication, and cost savings.” connected everything is in this
to know that the structure was
I wonder if the Space Needle world. Odd how a trip to the
built to withstand Category 5 hur-
would have been there for me to Space Needle can connect you to
ricane-force winds (around 200
visit if the standards for the hard- over a century of history—even
mph), and earthquakes up to a
ened carbon steel had not been in though the structure itself is less
9.5 magnitude. It also has 25
place? What else has been stan- than 50 years old.
lightning rods, for those of you
dardized by the ASTM?
who are scared of death by light-
ning (which is pretty rare, actu- Presently, the ASTM develops
ally; statistics say that in the U.S. standards for many industries,
there is only a 1 out of 700,000 including the metals industry,
chance of being struck by light- with which it has a long history. It
ning in a given year. To put that turns out that the ASTM is the
in perspective, you are more oldest and most dominant stan-
likely to be legally executed (1 in dard organization in the United
States, and to date is the proud
PRST/STD
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Rutherfordton, NC 28139
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