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Engr. E. G. Ronquillo MTM.3.07
FINENESS: Specific Surface, sq.cm/gm Residue on #200 Sieve. % % Fineness 1600 min. 10 max. 90 min.
TIME OF SETTING: GILMORE TEST a. Initial Set, minutes b. Final Set, hours 60 min. 10 max
SOUNDNESS: Autoclave Expansion, % Pat Test 0.50 max No Sign of Volume Change
COMPRESSIVE STRENGTH, MORTAR CUBE, psi 1 day in moist air, 2 days in water 1 day in moist air, 6 days in water 1 day in moist air, 27 days in water 1,200 min. 2,100 min. 3,500 min.
Lost on Ignition, % Insoluble Residue, % Sulfur Trioxide, % Magnesium oxide, % Sodium and Potassium Oxide, %
3.00 max. 0.75 max 3.00 max 5.00 max. 0.50 max
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Engr. E. G. Ronquillo MTM.3.07
PROCEDURE:
1. Place a 50-gram sample of cement on the No. 200 sieve with pan attached. 2. Start sieving and continue until the residue looks clean. This will take about 5 minutes. 3. Place cover on sieve and remove pan. Tap gently the sides of sieve to dislodge dust adhering to the sieve and brush the underside of the sieve. 4. Continue sieving until no more than 0.05 gram passes through in one minute of continuous sieving. 5. Brush thoroughly both sides of sieve. Get the weight of residue by weighing the sieve with residue (cement retained) on it.
CALCULATION:
% Residue = W2 x 100 W1 Where: W2 = weight of residue W1 = weight of original sample = 50 grams And, % Fineness = 100% - % Residue
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Engr. E. G. Ronquillo MTM.3.07
MATERIALS TESTING LABORATORY COLLEGE OF ENGINEERING AND ARCHITECTURE HOLY ANGEL UNIVERSITY
LAB. EXERCISE NO. :________________ TITLE: ____________________________ DATE PERFORMED: ________________ DATE SUBMITTED: _________________
DATA SHEET: a. Weight of # 200 Sieve + Residue, gm b. Weight of # 200 Sieve, gm c. Weight of Residue, W2, gm (a) - (b) d. Weight of Original Sample, W1, gm e. % Residue f. % Fineness
SPECIFICATION FOR % FINENESS FOR TYPE I PORTLAND CEMENT = 90% TEST RESULT FOR % FINENESS = _____________ Therefore, CEMENT ___________ MEETS REQUIREMENT ___________ DOES NOT MEET REQUIREMENT
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Engr. E. G. Ronquillo MTM.3.07
PROCEDURE:
1. Fill the Le Chatelier flask with water-free kerosene to a point on the stem between the zero and 1 ml. - mark. 2. Immerse the flask in a constant temperature water bath maintained at room temperature for a sufficient time interval before making any reading. 3. Take initial reading. 4. Put the 64-gm. cement sample into the flask. 5. Stopper the flask and roll in an inclined position until no air bubbles rise to the surface. 6. Immerse in temperature bath and then take final reading.
CALCULATION:
Gs = Wc Rf - Ri Where: Gs = Wc = Rf = Ri = specific gravity of cement weight of cement in grams final reading in ml. initial reading in ml.
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Engr. E. G. Ronquillo MTM.3.07
MATERIALS TESTING LABORATORY COLLEGE OF ENGINEERING AND ARCHITECTURE HOLY ANGEL UNIVERSITY
LAB. EXERCISE NO. :________________ TITLE: ____________________________ DATE PERFORMED: ________________ DATE SUBMITTED: _________________ NAME:_____________________ CLASS CODE:_______________ GROUP NO.: ________________ RATING: ___________________
DATA SHEET:
1 2
Specific Gravity
GOVERNMENT SPECIFICATIONS FOR SPECIFIC GRAVITY OF TYPE I CEMENT Gs = 3.10 3.15 TEST RESULT: _________________ Therefore, ____________ CEMENT MEETS REQUIREMENT ____________ CEMENT DOES NOT MEET REQUIREMENTS
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Engr. E. G. Ronquillo MTM.3.07
APPARATUS:
Vicat Needle Graduated Cylinder Balance Glass plate Trowel Mixing tray
PROCEDURE:
1. Make 500-gm. of cement sample into a mound and form a crater in the center. 2. Pour a measured quantity of water into the crater. Within 30 sec. turn the outer edge into the center with a trowel. Allow another seconds for the absorption of water. 3. Mix the material with gloved hands for 1-1/2 minutes in a continous kneading, mixing and squeezing operation. 4. Form the paste into a ball and toss it from one hand to the other 6 times, the hand being kept 6 in. apart. 5. Press the ball in the larger end of the conical ring of the Vicat needle, filling the ring completely with the paste. Remove excess paste with palm of hand. 6. Place the conical ring with its larger end resting on the glass plate. Remove excess paste at smaller end with one stroke of the trowel. 7. Center the mold under rod of Vicat apparatus, with end of plunger in contact with surface of paste. 8. Determine the penetration 30 seconds after release of plunger. The paste is of normal consistency if the penetration is 10 mm. 9. Repeat procedure with different amounts of water until normal consistency is obtained. Use fresh cement for each trial.
CALCULATION:
N. C. = V X 100% W Where: N. C. = normal consistency V = volume of water used in cc. W = weight of cement sample = 500 gm.
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Engr. E. G. Ronquillo MTM.3.07
MATERIALS TESTING LABORATORY COLLEGE OF ENGINEERING AND ARCHITECTURE HOLY ANGEL UNIVERSITY
LAB. EXERCISE NO. :________________ TITLE: ____________________________ DATE PERFORMED: ________________ DATE SUBMITTED: _________________
DATA SHEET:
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Engr. E. G. Ronquillo MTM.3.07
APPARATUS:
Gillmore Needle Graduated Cylinder Balance and set of weights Glass plate Trowel Mixing tray
PROCEDURE:
1. Prepare a cement paste of normal consistency (Test 4 - C). 2. Make a pat about 3 in. in diameter, 1/2 in thick at the center with a flat top and tapering to a thin edge on a glass plate. 3. Store the pat in a moist closet with a temperature of 230 C and test at intervals. 4. Determine the time of setting by applying the needles lightly on the surface of the pat. The cement shall be considered to have acquired its initial set when the pat will bear the 1/4 lb. needle without appreciable indentation. The final set is when the pat will bear the 1-lb. needle without appreciable indentation.
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Engr. E. G. Ronquillo MTM.3.07
MATERIALS TESTING LABORATORY COLLEGE OF ENGINEERING AND ARCHITECTURE HOLY ANGEL UNIVERSITY
LAB. EXERCISE NO. :________________ TITLE: ____________________________ DATE PERFORMED: ________________ DATE SUBMITTED: _________________
DATA SHEET:
TIME OF SETTING Initial Set, min., (b) - (a) Final Set, hrs., (c) - (a)
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Engr. E. G. Ronquillo MTM.3.07
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Engr. E. G. Ronquillo MTM.3.07
MATERIALS TESTING LABORATORY COLLEGE OF ENGINEERING AND ARCHITECTURE HOLY ANGEL UNIVERSITY
LAB. EXERCISE NO. :________________ TITLE: ____________________________ DATE PERFORMED: ________________ DATE SUBMITTED: _________________
DATA SHEET: OBSERVATIONS: ( ( ( ( ( ) Cracking ) Checking ) Disintegration ) Distortion ) No sign of volume change
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Engr. E. G. Ronquillo MTM.3.07
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Engr. E. G. Ronquillo MTM.3.07
MATERIALS TESTING LABORATORY COLLEGE OF ENGINEERING AND ARCHITECTURE HOLY ANGEL UNIVERSITY
LAB. EXERCISE NO. :________________ TITLE: ____________________________ DATE PERFORMED: ________________ DATE SUBMITTED: _________________
DATA SHEET:
TRIAL NO. Weight of Cement Sample, gm. Weight of Sand, gm. FLOW DETERMINATION a. Water Used, ml b. Initial Diameter, in. c. Final Diameter, in. d. Flow, %, [(c) - (b)]/ (b) x 100%
COMPRESSIVE STRENGTH DETERMINATION a. b. Cross-sectional area, mm2 Total load in N for 3 1st Cube 2nd Cube 3rd Cube c. Compression Strenght, Mpa Age in Days 7 28
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Engr. E. G. Ronquillo MTM.3.07