1001 West Saint Paul Ave.

, Milwaukee, WI 53233
Telephone: 414-273-3850 • 800-231-8327
Fax: 414-273-4979 • 800-962-9591
Website: http://www.sigma-aldrich.com
Aldrich is a member of the Sigma-Aldrich family E-mail: aldrich@sial.com

AL-210 TechnicalBulletin
VerSA-Flow™ Can and Drum Dispensing Systems
Aldrich VerSA-Flow dispensing systems provide convenient methods for transferring and dispensing laboratory and
development scale quantities of solvents, fine organics, and other liquids from various Aldrich containers using the
equipment and techniques described in this bulletin.

Iin. NPT threaded

plugs for accessories
PFA fitting with FEP solvent pick-up tube
Iin. i.d. hose barb
VerSA-Flow cap
Gas inlet

UN approved container Double-containment

is completely recyclable design for safe
shipping and storage

HDPE liner for

Liquid-level
permeation protection
indicator (optional)

Cutaway view of an 18L poly-lined steel can with low-flow

VerSA-Flow dispenser cap and optional liquid-level indicator.

TABLE OF CONTENTS

Container Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
VerSA-Flow Dispenser Selection Guide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Specifications for VerSA-Flow Dispensers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-4
Optional VerSA-Flow Dispenser Configurations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Handling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Low-Flow Pressure-Transfer Procedures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-8
High-Flow Pressure-Transfer Procedures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9-12
Installing a Liquid-Level Indicator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Reading the Liquid-Level Indicator . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
VerSA-Flow Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13-15
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

CONTAINER SPECIFICATIONS

VerSA-Flow dispensers are available to fit the Aldrich cans and drums shown in Figure 1. Table 1 provides specifications
for the containers. All of these containers are one-way, disposable units, and when empty, may be recycled or utilized
for waste solvent collection with the appropriate VerSA-Flow cap.

CAUTION! These containers are suited only for low-pressure (2-4psi) transfer techniques. Read and closely follow
the pressure-transfer procedures described in this bulletin, regardless of the quantity needed or the chemical
transferred. Since many of the products packaged in these containers are hazardous, they must be handled while
using appropriate personal protective equipment. See the Equipment section of the Aldrich Handbook for a com-
plete listing of chemically resistant gloves, aprons, goggles, face shields, and respirators.

Figure 1
Aldrich Containers

18L Poly-Lined Can 20L Steel Can 25L Steel Can and 50L, 100L,
200L Poly-Lined Drums

Table 1
SPECIFICATIONS FOR ALDRICH CONTAINERS
Overall dim.
Container Type Capacity Cat. No. H x diam. (in.) Plug Size
Poly-lined steel can 18L 16.25 x 11.75 2in. buttress thread
Carbon steel can 20L 14.5 x 11 2in. NPT thread
Stainless steel can 25L 20.75 x 10.75 2in. NPT thread
Poly-lined steel drum 50L Z55,343-3 26.25 x 14.25 2in. NPT thread
Poly-lined steel drum 100L Z55,344-1 30 x 18.5 2in. NPT thread
Poly-lined steel drum 200L Z55,346-8 36 x 23.5 2in. NPT thread

2
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

VERSA-FLOW DISPENSER SELECTION GUIDE

VerSA-Flow dispenser options for the various Aldrich containers are shown in Table 2. Figure 2 provides specifica-
tions for each dispenser type. Figure 3 shows other configurations of the VerSA-Flow pressure-delivery caps which
are available on request.

Table 2
DISPENSER OPTIONS BY CONTAINER TYPE
Container Type Applications Cat. No.
Poly-lined steel can, 18L, 2in. buttress thread
A. Hand pump* Low-flow dispensing Z52,906-0
B. Economy pressure-delivery cap* Low-flow transfer, waste solvent collection Z52,902-8
Can thread adapter, 2in. NPTF to buttress *Required for above pump and cap Z52,903-6
C. Low-flow pressure-delivery cap Low-flow transfer/dispensing Z54,381-0
D. High-flow pressure-delivery cap High-flow transfer Z55,318-2

Steel cans, 20L, 25L, and poly-lined steel drums, 50L, 100L, and 200L, 2in. NPT thread
A. Hand pump Low-flow dispensing Z52,906-0
B. Economy pressure-delivery cap Low-flow transfer, waste solvent collection Z52,902-8
C. Low-flow pressure-delivery cap Low-flow transfer/dispensing Z54,573-2
D. High-flow pressure-delivery cap High-flow transfer Z54,579-1

FIGURE 2 - SPECIFICATIONS FOR VERSA-FLOW DISPENSERS

A. Tapper pressure dispenser

Simple pumping action pressurizes container to dispense solvent. Fits Aldrich cans and
drums with 2in. NPT threads. Pump can be adapted to 2in. buttress threads with optional
thread adapter Z52,903-6.
• Machined PBT body and piston with PTFE wiper
• 30in. L PTFE solvent pick-up tube and On/Off spigot
• Built-in pressure-relief valve
• Spigot with M in. o.d. outlet tube

Pump with 2in. NPT thread Z52,906-0

Thread adapter, 2in. NPTF to 2in. buttress threads Z52,903-6

B. Economy pressure-delivery cap

For low-flow pressure-delivery of solvents and for waste solvent collection using Aldrich
cans and drums with 2in. NPT threads. Solid machined PBT body. Use at <5psi max.
• Flow rate: approx. 1L/min at 4psi
• Includes 10ft x Iin. o.d. FEP tubing, adjustable depth through compression fittings on cap
• Can be adapted to 2in. buttress threads with optional thread adapter Z52,903-6

Cap with 2in. NPT thread Z52,902-8

Thread adapter, 2in. NPTF to 2in. buttress threads Z52,903-6

3
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

FIGURE 2 - SPECIFICATIONS FOR VERSA-FLOW DISPENSERS (CONTINUED)

C. Low-flow pressure-delivery cap

For low-flow pressure-delivery of solvents from Aldrich cans and drums with 2in. NPT
threads or 2in. buttress threads. Precision machined, two-piece, PBT cap with special
threading that permits the removal of the cap without disconnecting solvent and gas
lines when changing containers.
• Flow rate: approx. 1 L/min at 4psi
• Includes 10ft x Iin. o.d. FEP solvent pick-up tubing, adjustable depth through
compression fitting on cap
• Iin. i.d. gas hose connection
• Extra 90° PFA elbow with Iin. o.d. compression fittings for connecting pick-up
tubing to cap in low-clearance applications
• Two additional Iin. NPT threaded holes with plugs permit the addition of a liquid-
level indicator, vent line, or sparge/delivery tube assemblies
• Built-in pressure-relief valve vents automatically in case of excessive pressure (5psi max.)
• Optional Kin. o.d. compression fittings for HPLC tubing
Cap with 2in. NPT thread Z54,573-2
Cap with 2in. buttress thread Z54,381-0

D. High-flow pressure-delivery cap

For high-flow pressure-delivery of solvents from Aldrich cans and drums with 2in. NPT
threads or 2in. buttress threads. Precision machined, two-piece, PBT cap with special
threading that permits the removal of the cap without disconnecting solvent and gas
lines when changing containers.
• Flow rate: approx. 5 to 6 L/min at 4psi
• Includes 8ft x Lin. i.d. FEP solvent pick-up tubing, adjustable depth through
compression fitting on cap
• On/Off spigot
• Iin. i.d. gas hose connection
• Built-in pressure-relief valve vents automatically in case of excessive pressure (10psi max.)
Cap with 2in. NPT thread Z54,579-1
Cap with 2in. buttress thread Z55,318-2

FIGURE 3 - OPTIONAL VERSA-FLOW DISPENSER CONFIGURATIONS

A. Low-flow cap with quick-disconnect fitting for

flexible gas-inlet tubing.

B. Low-flow cap with Kin. o.d. FEP sparge and solvent

pick-up tubes each with 2 micron SS filters. For
delivery of solvents directly to HPLC instruments.

C. Low-flow cap with Kin. o.d. FEP sparge and solvent

pick-up tubes each with 2 micron SS filters and liquid-
level indicator. For delivery of solvents directly to
HPLC instruments.

A B C

4
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

HANDLING

The user of VerSA-Flow dispensers should be a fully qualified and experienced laboratory or chemical technician or
production worker. User should be aware of the hazardous nature of many of the products that may be dispensed
with these systems. The material safety data sheet (MSDS), which is provided with each Aldrich chemical product,
must be read and understood by the user prior to the installation or use of VerSA-Flow dispensers.

In general, VerSA-Flow pressure-delivery caps should be used at low pressure (2-4psi) using a pressure-regulated nitrogen
supply. During nitrogen pressure-transfers, the flowing liquid can generate a static charge. Therefore, metal cans and
drums and receivers must be connected to a suitable ground. See the VerSA-Flow Accessories section for various lengths
of flat braided bare cable with copper clips at each end which makes a convenient grounding strap.

LOW-FLOW PRESSURE-TRANSFER PROCEDURES

CAUTION! Due to the hazardous nature of many chemicals packaged in Aldrich steel cans and drums, the user
must exercise caution to prevent inhalation of chemical vapors or direct contact with skin during system set up
and transfer. During pressure-transfer procedures it is recommended that operators wear appropriate personal
protective equipment such as chemically-resistant gloves, goggles, splash apron, full face shield plus any addi-
tional protective equipment as required. See the Equipment section of the Aldrich Handbook for a complete list-
ing of these items. The operator should be a fully qualified and experienced laboratory or chemical technician or
production worker.

18L POLY-LINED CANS

Step 1.
Place the container in a secure and upright position in a safe and well
ventilated area. If the product is to be delivered by weight, secure the
container on an appropriate scale.

Step 2.
Remove the protective metal shipping cover on the can.

Step 3.
Remove the 2in. plug from the inner poly container with a plug wrench 18L Poly-Lined Can
and set aside for re-use after transfer.
Solvent
delivery
Step 4.
Separate the top cap from the lower cap by turning the center nut Compression
counterclockwise. Observe the Viton® O-ring within the lower part of fitting
Gas in Top cap
the cap assembly and use care to ensure that it remains in position dur-
Center nut
ing the next step.
Lower cap
Step 5.
Install the lower cap in the poly container opening by carefully turning O-ring

cap clockwise, then tighten securely by hand. Make sure that the cap is 2in. buttress
thread
threaded into container opening properly to avoid cross-threading Solvent pick-
(damaging) the container threads. up tube

Step 6.
Install optional one-hole metal can cover, aligning hole with cap bottom
installed in Step 5. Note: Check local fire codes to determine if use of
cover is required in your laboratory.

5
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

Low-Flow Pressure-Transfer Procedures - 18L Poly-Lined Cans (continued)

Step 7.
Adjust the depth of the FEP solvent pick-up tubing by loosening the compression fitting on the top cap and pushing
the tubing to a length that just reaches the bottom of the container. Hand tighten the compression fitting to secure
the tubing position. Carefully lower the solvent pick-up tubing into the container and install top cap into lower cap
(installed in Step 5) by turning the center nut on the top cap clockwise, then tighten center nut securely by hand. Use
care during installation of top cap to prevent cross-threading.

OPTION:
A 90° PFA elbow with Iin. o.d. compression fittings is supplied
90° PFA elbow FEP tubing
with the cap. It can be used for connecting the solvent pick-up
tubing to the cap in low-clearance applications. To use the elbow,
make sure the FEP solvent pick-up tubing depth is properly adjust- Nut
Ferrules
ed as above, then cut the tubing about one inch above the com-
pression fitting on the top cap. Connect the elbow to the cut end
using the ferrules and nut. Connect FEP tubing to the other elbow
end as shown in the diagram to continue the delivery line to the
reaction vessel or storage flask.

Step 8.
Run the open end of solvent pick-up tubing to a receiving vessel or flask. Note: Torion™ tubing adapters provide
a convenient, closed system connection of tubing to reaction vessels and storage flasks. Alternatively an On/Off
spigot may be attached to the end of the tubing for dispensing. See the Accessories section for a listing of these
products. If a spigot is installed, turn it to the Off position.

Step 9.
Connect Iin. i.d. flexible gas line tubing to the hose barb on the top cap. CAUTION! Do not clamp or wire
the gas line tubing to the hose barb. The hose barb allows the gas tubing to safely pop off in the event of
excessive over-pressure during transfer. Connect the other end of the gas line tubing to a pressure-regulated
(2-4psi) nitrogen supply.

Step 10.
Check that all cap connections are hand tight, including the two solid Iin. NPT plugs (if present). Teflon® tape
may be used to seal NPT threads if necessary.

Step 11.
Slowly turn on nitrogen supply to pressurize the container and cause solvent to begin flowing out of the pick-up
tubing and into the receiving vessel. Note: if an On/Off spigot is used, open spigot slightly to allow trapped gas
in the tubing to escape, then open spigot fully to dispense solvent. The built-in pressure-relief valve will auto-
matically vent if gas pressure exceeds 5psi. This is normal and prevents the buildup of unsafe pressures inside con-
tainer. Adjust nitrogen supply to a lower pressure (2 to 4psi) and continue transfer.

Step 12.
When the solvent transfer is complete, turn off nitrogen gas and allow remaining solvent in the pick-up tubing
to drain. Disconnect gas line tubing. Carefully remove cap assembly from the can and place into a fume hood to
dry. Avoid solvent contact with skin or breathing vapors when handling the cap assembly and tubing.

Step 13.
Replace the 2in. plug into the inner poly container and tighten with a plug wrench. Remove the metal one-hole
cover and install the protective metal shipping cover on the can.

Step 14.
Discard the empty can or use for the collection of waste solvents. The economy VerSA-Flow cap, Z52,902-8, is well
suited for waste solvent collection from instruments or reaction vessels.

6
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

Low-Flow Pressure-Transfer Procedures - 20L, 25L Steel Cans and 50L, 100L, and 200L Poly-Lined Drums

CAUTION! Due to the hazardous nature of many chemicals packaged in Aldrich steel cans and drums, the user
must exercise caution to prevent inhalation of chemical vapors or direct contact with skin during system set up
and transfer. During pressure-transfer procedures it is recommended that operators wear appropriate personal
protective equipment such as chemically-resistant gloves, goggles, splash apron, full face shield plus any addi-
tional protective equipment as required. See the Equipment section of the Aldrich Handbook for a complete list-
ing of these items. The operator should be a fully qualified and experienced laboratory or chemical technician or
production worker.

20L, 25L STEEL CANS AND 50L, 100L, AND 200L POLY-LINED DRUMS

Step 1.
Place the container in a secure and upright position in a safe and well
ventilated area. If the product is to be delivered by weight, secure the
container on an appropriate scale.

Step 2.
Remove the 2in. plug from the container with a plug wrench and set
aside for re-use after transfer.

Step 3.
Separate the top cap from the lower cap by turning the center nut
counterclockwise. Observe the Viton® O-ring within the lower part of the 25L Steel Can and 50L,
20L Steel Can
cap assembly and use care to ensure that it remains in position during 100L, 200L Poly-Lined Drums

the next step.

Step 4.
Install the lower cap in the container opening by carefully turning cap Solvent
delivery
clockwise, then tighten securely by hand. Make sure that the cap is thread-
ed into container opening properly to avoid cross-threading (damaging) Compression
fitting
the container threads. If container thread damage is suspected due to
Gas in Top cap
cross-threading, remove the cap and wrap the threads of the lower cap
Center nut
with several turns of Teflon® tape, then reinstall as above.
Lower cap
Step 5.
2in. NPT O-ring
Adjust the depth of the FEP solvent pick-up tubing by loosening the com- thread
pression fitting on the top cap and pushing the tubing to a length that
just reaches the bottom of the container. Hand tighten the compression Solvent
pick-up
fitting to secure the tubing position. Carefully lower the solvent pick-up tube
tubing into the container and install top cap into lower cap (installed in
Step 4) by turning the center nut on the top cap clockwise, then tighten
center nut securely by hand. Use care during installation of top cap to
prevent cross-threading.

OPTION:
A 90° PFA elbow with I in. o.d. compression fittings is supplied with the
cap. It can be used for connecting the solvent pick-up tubing to the cap in 90° PFA elbow FEP tubing
low-clearance applications. To use the elbow, make sure the FEP solvent
pick-up tubing depth is properly adjusted as above, then cut the tubing Nut
Ferrules
about one inch above the compression fitting on the top cap. Connect the
elbow to the cut end using the ferrules and nut. Connect FEP tubing to the
other elbow end as shown in the diagram to continue the delivery line to
the reaction vessel or storage flask.

7
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

Low-Flow Pressure-Transfer Procedures - 20L, 25L Steel Cans and 50L, 100L, and 200L Poly-Lined Drums (continued)

Step 6.
Run the open end of solvent pick-up tubing to a receiving vessel or flask. Note: Torion™ tubing adapters provide
a convenient, closed system connection of tubing to reaction vessels and storage flasks. Alternatively an On/Off
spigot may be attached to the end of the tubing for dispensing. See the Accessories section for a listing of these
products. If a spigot is installed, turn it to the Off position.

Step 7.
Connect I in. i.d. flexible gas line tubing to the hose barb on the top cap. CAUTION! Do not clamp or wire
the gas line tubing to the hose barb. The hose barb allows the gas tubing to safely pop off in the event of
excessive over-pressure during transfer. Connect the other end of the gas line tubing to a pressure-regulated
(2-4psi) nitrogen supply.

Step 8.
Check that all cap connections are hand tight, including the two solid I in. NPT plugs (if present). Teflon® tape
may be used to seal NPT threads if necessary.

Step 9.
Slowly turn on nitrogen supply to pressurize the container and cause solvent to begin flowing out of the pick-
up tubing and into the receiving vessel. Note: if an On/Off spigot is used, open spigot slightly to allow trapped
gas in the tubing to escape, then open spigot fully to dispense solvent. The built-in pressure-relief valve will
automatically vent if gas pressure exceeds 5psi. This is normal and prevents the buildup of unsafe pressures
inside container. Adjust nitrogen supply to a lower pressure (2 to 4psi) and continue transfer.

Step 10.
When the solvent transfer is complete, turn off nitrogen gas and allow remaining solvent in the pick-up tubing
to drain. Disconnect gas line tubing. Carefully remove cap assembly from the can and place into a fume hood to
dry. Avoid solvent contact with skin or breathing vapors when handling the cap assembly and tubing.

Step 11.
Replace the 2in. plug into the container and tighten with a plug wrench. Discard the empty container or use for the
collection of waste solvents. The economy VerSA-Flow cap, Z52,902-8, is well suited for waste solvent collection from
instruments or reaction vessels.

8
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

HIGH-FLOW PRESSURE-TRANSFER PROCEDURES

CAUTION! Due to the hazardous nature of many chemicals packaged in Aldrich steel cans and drums, the user
must exercise caution to prevent inhalation of chemical vapors or direct contact with skin during system set up
and transfer. During pressure-transfer procedures it is recommended that operators wear appropriate personal
protective equipment such as chemically-resistant gloves, goggles, splash apron, full face shield plus any addi-
tional protective equipment as required. See the Equipment section of the Aldrich Handbook for a complete list-
ing of these items. The operator should be a fully qualified and experienced laboratory or chemical technician or
production worker.

18L POLY-LINED CANS

Step 1.
Place the container in a secure and upright position in a safe and well
ventilated area. If the product is to be delivered by weight, secure the
container on an appropriate scale.

Step 2.
Remove the protective metal shipping cover on the can.

Step 3.
Remove the 2in. plug from the inner poly container with a plug wrench 18L Poly-Lined Can
and set aside for re-use after transfer.
Solvent
Step 4. delivery
Separate the top cap from the lower cap by turning the center nut
counterclockwise. Observe the Viton® O-ring within the lower part of the Compression
fitting
cap assembly and use care to ensure that it remains in position during
the next step. Gas in Top cap
Center nut
Step 5. Lower cap
Install the lower cap in the poly container opening by carefully turning O-ring
cap clockwise, then tighten securely by hand. Make sure that the cap is 2in. buttress
threaded into container opening properly to avoid cross-threading thread
Solvent
(damaging) the container threads. pick-up
tube
Step 6.
Install optional one-hole metal can cover, aligning hole with cap bottom
installed in Step 5. Note: Check local fire codes to determine if use of
cover is required in your laboratory.

Step 7.
Adjust the depth of the FEP solvent pick-up tubing by loosening the com-
pression fitting on the top cap and pushing the tubing to a length that
just reaches the bottom of the container. Hand tighten the compression
fitting to secure the tubing position. Carefully lower the solvent pick-up
tubing into the container and install top cap into lower cap (installed in
Step 5) by turning the center nut on the top cap clockwise, then tighten
center nut securely by hand. Use care during installation of top cap to
prevent cross-threading.

Step 8.
An On/Off spigot is attached on the end of the solvent pick-up tubing for
dispensing into a reservoir or reaction vessel. Check that spigot is in the
Off position.

9
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

High-Flow Pressure-Transfer Procedures - 18L Poly-Lined Cans (continued)

Step 9.
Connect I in. i.d. flexible gas line tubing to the hose barb on the top cap. CAUTION! Do not clamp or wire
the gas line tubing to the hose barb. The hose barb allows the gas tubing to safely pop off in the event of
excessive over-pressure during transfer. Connect the other end of the gas line tubing to a pressure-regulated
(2-4psi) nitrogen supply.

Step 10.
Check that all cap connections are hand tight. Teflon® tape may be used to seal NPT threads if necessary.

Step 11.
Slowly turn on nitrogen supply to pressurize the container. Note: Open the On/Off spigot slightly to allow trapped
gas in the tubing to escape, then open spigot fully to dispense solvent. The built-in pressure-relief valve will auto-
matically vent if gas pressure exceeds 10psi. This is normal and prevents the buildup of unsafe pressures inside
container. Adjust nitrogen supply to a lower pressure (2 to 4psi) and continue transfer.

Step 12.
When the solvent transfer is complete, turn off spigot and nitrogen gas. Open spigot to allow remaining solvent
in the pick-up tubing to drain. Turn spigot off. Disconnect gas line tubing from cap. Carefully remove cap assem-
bly from the can and place into a fume hood to dry. Avoid solvent contact with skin or breathing vapors when
handling the cap assembly and tubing.

Step 13.
Replace the 2in. plug into the inner poly container and tighten with a plug wrench. Remove the metal one-hole
cover and install the protective metal shipping cover on the can.

Step 14.
Discard the empty can or use for the collection of waste solvents. The economy VerSA-Flow cap, Z52,902-8, is well
suited for waste solvent collection from instruments or reaction vessels.

10
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

High-Flow Pressure-Transfer Procedures - 20L, 25L Steel Cans and 50L, 100L, and 200L Poly-Lined Drums

CAUTION! Due to the hazardous nature of many chemicals packaged in Aldrich steel cans and drums, the user
must exercise caution to prevent inhalation of chemical vapors or direct contact with skin during system set up
and transfer. During pressure-transfer procedures it is recommended that operators wear appropriate personal
protective equipment such as chemically-resistant gloves, goggles, splash apron, full face shield plus any addi-
tional protective equipment as required. See the Equipment section of the Aldrich Handbook for a complete list-
ing of these items. The operator should be a fully qualified and experienced laboratory or chemical technician or
production worker.

20L, 25L STEEL CANS AND 50L, 100L, AND 200L POLY-LINED DRUMS

Step 1.
Place the container in a secure and upright position in a safe and well
ventilated area. If the product is to be delivered by weight, secure the
container on an appropriate scale.

Step 2.
Remove the 2in.plug from the container with a plug wrench and set
aside for re-use after transfer.

Step 3.
Separate the top cap from the lower cap by turning the center nut coun- 20L Steel Can 25L Steel Can and 50L,
terclockwise. Observe the Viton® O-ring within the lower part of the cap 100L, 200L Poly-Lined Drums

assembly and use care to ensure that it remains in position during the
next step.
Solvent
delivery
Step 4.
Install the lower cap in the container opening by carefully turning cap
clockwise, then tighten securely by hand. Make sure that the cap is
Compression
threaded into container opening properly to avoid cross-threading fitting
(damaging) the container threads. If container thread damage is sus-
Gas in
pected due to cross-threading, remove the cap and wrap the threads of Top cap
Center nut
the lower cap with several turns of Teflon® tape, then reinstall as above.

Lower cap
Step 5.
Adjust the depth of the FEP solvent pick-up tubing by loosening the com- 2in. NPT thread O-ring
pression fitting on the top cap and pushing the tubing to a length that
Solvent
just reaches the bottom of the container. Hand tighten the compression pick-up
fitting to secure the tubing position. Carefully lower the solvent pick-up tube

tubing into the container and install top cap into lower cap (installed in
Step 4) by turning the center nut on the top cap clockwise, then tighten
center nut securely by hand. Use care during installation of top cap to prevent cross-threading.

Step 6.
An On/Off spigot is attached to the end of the pick-up tubing for dispensing into a reservoir or reaction vessel.
Check that spigot is in the Off position.

Step 7.
Connect I in. i.d. flexible gas line tubing to the hose barb on the top cap. CAUTION! Do not clamp or wire
the gas line tubing to the hose barb. The hose barb allows the gas tubing to safely pop off in the event of
excessive over-pressure during transfer. Connect the other end of the gas line tubing to a pressure-regulated
(2-4psi) nitrogen supply.

Step 8.
Check that all cap connections are hand tight. Teflon® tape may be used to seal NPT threads if necessary.

11
AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

High-Flow Pressure-Transfer Procedures - 20L, 25L Steel Cans and 50L, 100L, and 200L Poly-Lined Drums (continued)

Step 9.
Slowly turn on nitrogen supply to pressurize the container. Note: Open the On/Off spigot slightly to allow trapped
gas in the tubing to escape, then open spigot fully to dispense solvent. The built-in pressure-relief valve will auto-
matically vent if gas pressure exceeds 10psi. This is normal and prevents the buildup of unsafe pressures inside
container. Adjust nitrogen supply to a lower pressure (2 to 4psi) and continue transfer.

Step 10.
When the solvent transfer is complete, turn off spigot and nitrogen gas. Open spigot to allow remaining solvent
in the pick-up tubing to drain. Turn spigot off. Disconnect gas line tubing from cap. Carefully remove cap assem-
bly from the container and place into a fume hood to dry. Avoid solvent contact with skin or breathing vapors
when handling the cap assembly and tubing.

Step 11.
Replace the 2in. plug into the container and tighten with a plug wrench.

Step 12.
Discard the empty container or use for the collection of waste solvents. The economy VerSA-Flow cap, Z52,902-8,
is well suited for waste solvent collection from instruments or reaction vessels.

INSTALLING A LIQUID-LEVEL INDICATOR

Liquid-level indicators are available as options for low-flow pressure-delivery caps for 18L poly-lined cans and 50L
poly-lined drums. Please inquire about indicators for other container sizes.

Step 1.
The stainless steel pipe is installed in the threaded hole on the under-
Level indicator wire
side of the top cap. Remove the threaded plug for this hole on the top
cap by turning the plug counterclockwise.
Top cap
Step 2. Center nut
Separate the top cap from the lower cap by turning the center nut coun-
terclockwise. Observe the Viton® O-ring within the lower part of the cap
Lower cap
assembly and use care to ensure that it remains in position.

Step 3.
Move the stainless steel pipe upwards through the lower cap, then care-
fully push the loop of the level indicator wire up through the threaded Stainless steel pipe
hole in the top cap so that it extends above the cap.

Step 4.
Carefully install the pipe into the threaded hole on the underside of the
Float
top cap by turning pipe clockwise until hand tight. Note: Check that
pipe is vertically aligned in the threaded hole prior to turning. If pipe is
misaligned during the turning process, cross-threading will occur and
the pipe will not be straight in the cap.

Step 5.
Slide center nut upwards onto top cap, then slide the lower cap
upwards to meet center nut. The assembly is now ready to install into
container.

Step 6.
Go to STEP 4 of the LOW-FLOW PRESSURE-TRANSFER PROCEDURES
to complete installation of the cap assembly.

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AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

READING THE LIQUID-LEVEL INDICATOR

The liquid-level indicator consists of a 316 SS pipe with a float that is magnetically coupled to a color-coded wire
that provides a visual indication of the liquid level in a container. The float drops with the liquid level in the con-
tainer and pulls the color-coded wire along as it does so. The blue to yellow to red bands on the wire indicate the
time to change out a container as they approach the top of the cap.

It is good practice to perform a manual check of the liquid level by lifting the wire upwards until it disconnects from
the float, then lowering the wire until it reconnects. One can actually “feel” the connect or disconnect with the float
through the wire. This practice ensures an accurate reading in the event the float becomes stuck or disconnects from
the wire.

VERSA-FLOW ACCESSORIES

Automatic shut-off quick-disconnects

Well suited for gas line connections to VerSA-Flow caps. Fittings are spring-loaded, locking,
and made of PP with 316 SS springs and EPR seals. When pulled apart, both sides seal quickly
and automatically. For I in. i.d. flexible rubber and PVC tubing. Max. pressure: 90psi at 70ºF. A.
Working temp.: 32 to 230ºF (air/water).
Product Name Bore (in.) For tubing i.d. (in.) Cat. No.
A. Coupling Insert I I i.d., flexible Z12,654-3
B. Coupling Body I I in. NPTM thread Z12,645-4
B.

Can and drum adapters

Adapters are precision machined PBT. A.
Adapter Threads Application Cat. No.
A. Buttress 2in. NPT to buttress Adapt NPT threads with 18L Z52,903-6
poly-lined steel cans
Buttress Spare thread adapter, Z54,386-1
for cap Z54,381-0
B. Bottle-top GL 32 to 2in. NPT Mount Optifix® dispensers Z52,904-4
to Aldrich 20L steel cans
Bottle-top GL 45 to 2in. NPT Mount Ceramus® dispensers Z52,905-2
to Aldrich 20L steel cans
B.

Torion™ tubing adapters

The Torion connection ensures an airtight seal between rigid wall transfer tubing and reaction vessel.
For a complete listing of these adapters, see the Equipment section of the Aldrich Handbook or visit
the Aldrich Glassware Catalog on-line at www.sigma-aldrich.com/glassware.

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AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

VerSA-Flow Accessories (continued)

Compression tubing fittings

Adapts rigid wall tubing of various sizes to VerSA-Flow caps. Fitting includes nut with ferrules and PBT
bushing with Iin. NPTM thread.
For tubing o.d. (in.) Cat. No.
K Z54,385-3
P Z54,458-2
I Z51,437-3

VerSA-Flow threaded plug

Solid threaded plug, PBT, Iin. NPTM. Z51,436-5

Liquid-level indicators
316 SS pipe and float with color-coded (blue-yellow-red) indicator wire for visual determination of
liquid level inside of container.
For container Cat. No.
18L poly-lined steel can Z54,378-0
50L poly-lined steel drum Z54,379-9

Sparge/solvent delivery assembly

2 micron SS filter, compression tube fitting and bushing with Iin. NPTM thread, 30in. x Kin. o.d. FEP
tubing. For direct dispensing of solvents from 18L poly-lined steel cans to HPLC instruments.
Z54,382-9

Pump N’ Pour adapter Z55,775-7

NPTM, 2 in.

Metal drum pump Z55,536-3

Fits 5 gal. can, FM approved

Zinc plated pump Z55,780-3

Zinc plated pump adapter Z55,781-1

One-hole metal cover with locking ring

For 18L poly-lined steel cans. Z55,319-0

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AL-210 VerSA-Flow™ Can and Drum Dispensing Systems

Ground wires
Flexible wire prevents sparking of static electricity generated by the transfer of flammable liquids.
Description Cat. No.
3ft L, w/2 copper alligator clips Z19,786-6
3ft L, w/2 hand clamps Z19,790-4
6ft L, w/2 copper alligator clips Z15,030-4
10ft L, w/Iin. terminal and hand clamp Z19,791-2

On/Off spigot
Teflon® body, with compression fitting for Iin. o.d. rigid wall tubing. Z55,320-4

O-rings, Viton®
2in. Buttress thread O-ring Z55,327-1
Inner O-ring for lower VerSA-Flow cap Z55,329-8

Plug wrench
For roundhead plugs only. 12in. L with offset handle. Non-sparking alloy. Z12,923-2

SNOOP® gas-leak detector

8oz bottle. Z27,391-0

Teflon® sealing tapes

Excellent for sealing NPT fittings. In 520in. rolls.
Width (in.) Cat. No.
I Z14,881-4
F Z10,438-8
1 Z22,188-0

Tubing
O.d. (in.) I.d. (in.) Cat. No.
Teflon® FEP rigid wall tubing
K O Z51,533-7
I K Z28,023-2
I P Z28,024-0

Latex rubber vacuum tubing

M I Z25,585-8

Ceramus® is a registered trademark of Hirschmann Laborgerate GmbH & Co.

Optifix® is a registered trademark of Walter Graf u. Co. GmbH & Co.
SNOOP® is a registered trademark of Swagelok Co.
Teflon® is a registered trademark of E.I. Du Pont de Nemours & Co., Inc.
Torion™ is a trademark of J. Bibby Science Products
VerSA-Flow™ is a trademark of Sigma-Aldrich Biotechnology LP.
Viton® is a registered trademark of Du Pont Dow Elastomers, LLC

FORM: AL-210 We are committed to the success of our Customers, Employees and Shareholders
1/2003
through leadership in L i f e S c i e n c e , H i g h Te c h n o l o g y and S e r v i c e .
© 2003 Sigma-Aldrich Co. Printed in the USA. Aldrich is a member of the Sigma-Aldrich family. Aldrich warrants that its products conform to the information contained in this and other
Aldrich publications. Purchaser must determine the suitability of the product for its particular use. See reverse of invoice of packing slip for additional terms and conditions of sale.

15