Escolar Documentos
Profissional Documentos
Cultura Documentos
Technical Bulletin A2
Aremcos high temperature ceramic and graphite adhesives are unique formulations for bonding, potting and sealing ceramics, composites, graphite, metals, quartz, and semiconductors for applications to 3200 F (1760C). TYPICAL APPLICATIONS
Electrical Halogen Lamps Heaters Igniters Fiberoptics Resistors Solid Oxide Fuel Cells
Instruments & Sensors Gas Chromatographs High Vacuum Components Liquid Metal Inclusion Counters Mass Spectrometers Oxygen Analyzers Strain Gauges Semiconductors Temperature Probes
Mechanical Ceramic Honeycombs Ceramic Textiles Graphite Blocks Refractory Insulation Sagger Plates Thread-Locking
Ceramabond 685-N bonds ceramic honeycomb to infrared heater.
PART NO. 503 552 569 670 671 835-M 835-MB 813-A 865 600-N 668 677 551-RN 669 571 632 618-N 516 685-N 835 885 890
FILLER
PRINCIPAL USE Dense Ceramics; Alumina-to-Alumina Solid Oxide Fuel Cells; Low CTE Metals
Ceramabond 835-M bonds halogen lamp.
C-C, C-M, Quartz Heaters, Igniters, Resistors, Sensors Al2O3 C-C, C-M C-C, C-M, M-M Ceramic Textiles, Thread-Locking Ceramic Textiles, Thread-Locking
C-C, C-M, Quartz Halogen Lamps C-C, C-M, Quartz Halogen Lamps C-C, C-M AlN C-C, C-M C-C, C-M Al2O3 SiO2 C-C, C-M C-C Graphite MgO Mica SiO2 Tundish Nozzles Probes & Sensors;Thermal Conductivity Refractory Repair Oxygen Sensors, Heaters Refractory Board
Ultra-Temp 516 bonds thermocouple to quartz tube. Ceramabond 503 coats heater used to 1700 C.
Graphite, Carbon Reducing/Vacuum Atmosphere Graphite C-M, M-M Mica C-C, Quartz C-C, C-M Oxidizing Atmosphere Heaters, Induction Coils, Sensors Mica Heaters Porous Ceramics, Quartz Tubes Thermocouples, Semiconductor Wafers Gasketing, Heaters, Igniters Halogen Lamps Zirconia, Solid Oxide Fuel Cells Crucibles, Heaters, Sagger Plates
M-M = Metal-to-Metal
ZrO2
SiC
C-C
C-M = Ceramic-to-Metal
*C-C = Ceramic-to-Ceramic
P.O. Box 517, 707-B Executive Boulevard, Valley Cottage, NY 10989 (845) 268-0039 FAX: (845) 268-0041 E-mail: aremco@aremco.com Website: www.aremco.com Rev. 02/13 7
Handling
Curing
8 503 569 Ceramabond Al2O3 White White 1 Paste 2.15 - 2.30 3000 (1650) 4.2 (7.6) N/A 569-T Water 50-90 40-90 6 1-4 200, 2 200, 2 200, 2 200, 2 1-4 1-4 1-4 6 6 6 40-90 40-90 40-90 50-90 50-90 50-90 50-90 40-90 6 1-4 200, 2 Water Water Water Water 670-T 671-T 813-A-T 835-M-T N/A N/A N/A N/A 4.3 (7.7) 4.3 (7.7) 4.0 (7.2) 4.0 (7.2) 3.8 (6.8) 100 : 60-80 835-MB-T Water 50-90 40-90 6 1-4 200, 2 + 350, 2 + 500, 2 136 27 Excellent Excellent Good
Abbreviations N/A Not Applicable N/M Not Measured
Tradename
Ceramabond
Major Constituent White 1 53,000 73,000 2,500 - 5,000 1.80 - 1.95 3000 (1650) 1.90 - 2.20 3000 (1650) 4.3 (7.7) N/A 552-T Water 50-90 40-90 6 1-4 200, 2 + 500, 2 173 52 Excellent Excellent Good Excellent Good Good Good Excellent 38 60 57 138 142 182 1 White
No. Components
Viscosity, cP
2.35 - 2.55
Temperature Limit, F (C )
3000 (1650)
CTE, in/in/F x 10-6 (C) N/A 503-T Water 50-90 40-90 6 <= 1 200, 2 + 500, 2 + 700, 2 171 60 Good Fair
4.0 (7.2)
Thinner
Solvent
Application Temperature, F
Storage Temperature, F
Moisture Resistance
Alkali Resistance
Acid Resistance
Excellent
Footnotes Tested using a torque wrench after bonding a pre-oxidized 1/2"-13 nut and bolt and final curing at 1000 F. Properties were evaluated after curing at 700 F for 2 hours. Graphi-Bond 551-RN is also offered in a two-part, resin and powder, system called 551-RN-X for international shipments of 1 gallon or more. Graphi-Bond 551-RN also demonstrates a lap-shear strength of 770 psi. Ceramabond 571 ranges for viscosity and specific gravity reflect a powder-to-liquid mix ratio that ranges from 1-to-1 to 1.5-to-1.
551-RN 669 Graphi-Bond Ceramabond Mica Tan 1 40,000 60,000 1.80 - 1.90 3000 (1650) .33 (.59) N/A 618-N-T Water 50-90 40-90 6 1-4 200, 2 + 500, 2 + 700, 2 156 77 Excellent Good Good Water 50-90 40-90 6 <= 1 200, 2 + 500, 2 + 700, 2 73 40 Good Good Good Good 890-T N/A 2.4 (4.4) 4.1 (7.4) N/A 516-T Water 50-90 40-90 6 1-4 200, 2 + 500, 2 + 700, 2 188 50 Good Excellent Good 3000 (1650) 3200 (1760) 1.70 - 1.75 2.15 - 2.30 35,000 55,000 40,000 70,000 5,000 20,000 1.85 - 1.95 3000 (1371) 4.5 (8.1) N/A 685-N-T Water 50-90 40-90 6 1-4 200,2 1 1 1 1 Off-White Blue-Gray Tan Tan Tan 1 20,000 40,000 2.25 - 2.35 3000 (1371) 4.0 (7.2) N/A 835-T Water 50-90 40-90 6 <= 1 200,2 SiO2 SiC ZrO2 - ZrSiO4 Ceramabond Ceramabond Ceramabond Ceramabond Ceramabond Ceramabond 571 632 618-N 890 516 685-N 835
885 Ceramabond
Tradename AlN Grey 1 1 Paste 1.45 - 1.50 5400 (2985) 3200 (1760) 7.0 (12.6) 1.0:1.0 - 1.5:1.0 571-T Water 50-90 40-90 6 1-4 200,2 4.1 (7.4) N/A Ethanol Ethanol 40-90 30-75 6 1-4 265,4 + 500,2 200,2 75 91 22 Excellent 30 26 Excellent Good Good Excellent Good Good 105 1-4 6 40-90 50-90 Water 669-T N/A 4.2 (7.6) 1400 (760) 1.45 - 1.50 1.90 - 2.20 20,000 40,000 Paste 1 Black
Ceramabond
Major Constituent
Color
Tan 1 10,000 20,000 2.65 - 2.70 3200 (1760) 4.0 (7.2) N/A 885-T Water 50-90 40-90 6 <= 1 500,2
No. Components
Viscosity, cP
1.95 - 2.15
Temperature Limit, F (C )
3000 (1650)
CTE, in/in/F x 10-6 (C) N/A 865-T Water 50-90 40-90 6 1-4 200, 2 + 350, 2 + 500, 2 187 27
1.5 ( 2.7)
Thinner
Solvent
Handling
Application Temperature, F
Storage Temperature, F
Curing
Excellent
Alkali Resistance
Acid Resistance
Footnotes Tested using a torque wrench after bonding a pre-oxidized 1/2"-13 nut and bolt and final curing at 1000 F. Properties were evaluated after curing at 700 F for 2 hours. Graphi-Bond 551-RN is also offered in a two-part, resin and powder, system called 551-RN-X for international shipments of 1 gallon or more. Graphi-Bond 551-RN also demonstrates a lap-shear strength of 770 psi. Ceramabond 571 ranges for viscosity and specific gravity reflect a powder-to-liquid mix ratio that ranges from 1-to-1 to 1.5-to-1.
DESIGN GUIDELINES
General design criteria for bonding with ceramic and graphite adhesives are similar to those for epoxies and other organic adhesives. Main considerations include the coefficient of thermal expansion, joint design, glue line thickness, and operating environment.
APPLICATION PROCEDURES
Surface Preparation
Smooth surfaces are difficult to bond and should be etched, abrasive blasted or oxidized, then cleaned thoroughly prior to application. Aremcos Corr-Prep CPR2000 is recommended for etching metals. Porous substrates should be pre-coated with a binder to prevent separation and absorption of the adhesive binder. Add a -T to the part number (ex. 503-T) to designate the product thinner.
Mixing
One-part adhesives tend to settle and should be mixed thoroughly prior to use. Refer to Tech Bulletin A12 for information about Aremcos Model 7000 Pneumatic Mixer. Mix ratios for twopart adhesives are shown in the Property Chart. Viscosity may be adjusted by thinning up to 20% by weight.
Application
Apply a thin coat of adhesive to each surface using a brush, spatula or dispenser. Using a clamp or similar tool, maintain a uniform glue line of 2-8 mils (200-500 microns) by applying even pressure across the assembly. Wipe away excess material prior to drying. Refer to Tech Bulletin A12 for optional dispensing tools
Model 7000 Mixer
Joint Design
Most adhesives offer relatively poor tensile-shear strength, so it is important to design a joint that will distribute the mechanical stress by maximizing the length of the glue line as shown in this illustration.
Curing
Refer to the Property Chart for specific curing instructions for each product.
Operating Environment
These adhesives offer excellent chemical, electrical and ultra high thermal resistance, and do not outgas under high vacuum.The main limitations are (a) relatively low mechanical strength and (b) slight porosity after curing. Contact Aremco for suggestions about how to reduce porosity and produce gas-tight seals.
Graphi-Bond 551-RN seals sensor in carbon brushes.
10
11
CERAMICS
METALS
12
Material 503 Al2O3 AlN SiC x x x x x x x x x x x x x x x x x x x x . x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x x Graphite MgO Mica SiO2 x x Al2O3-SiO2 ZrO2 - ZrSiO4 552 569 670 671 813-A 835-M 835-MB 600-N 668 677 865 551-RN 669 571 632 618-N 890 516 685-N 835
CTE F ( C)
885
x x x x x x x x
x x
x x
x x x
x x x
x x x
x x
x x
Alumina Alumina-Silica Aluminum Nitride Beryllia Boron Carbide Boron Nitride Borosilicate Glass Calcium Silicate Ceramic Textile Cordierite Graphite Macor Mica Mullite Quartz Refractory, Dense Refractory, Light Weight Sapphire Silica Silicon Carbide Silicon Nitride Steatite Zirconia Zirconia Silicate Aluminum Brass Cast Iron Copper Inconel Molybdenum Nickel Nickel-Iron Platinum Silicon Silver Stainless (300 Series) Stainless (400 Series) Steel (1010) Tantalum Titanium Tungsten x x x x x x x x x x x x x x x x x x x x x x x x
4.4 (7.9) 1.8 (3.2) 1.5 (2.7) 4.1 (7.4) 2.6 (4.7) 4.2 (7.6) 1.8 (3.2) 3.0 (5.4) 1.1 (2.0) 4.3 (7.7) 5.2 (9.4) 4.7 (8.5) 3.0 (5.4) 0.30 (0.54) 4.2 (7.6) 0.31 (0.56) 2.9 (5.2) 1.8 (3.2) 4.0 (7.2) 5.7 (10.3) 4.0 (7.2) 15.0 (27.0) 10.2 (18.4) 5.9 (10.6) 9.3 (16.7) 6.4 (11.5) 2.9 (5.2) 7.2 (13.0) 2.6 (4.7) 4.9 (8.8) 1.6 (2.9) 10.6 (19.1) 9.6 (17.3) 6.2 (11.2) 6.5 (11.7) 3.9 (7.0) 5.8 (10.4) 2.5 (4.5)
x x x x x
= Preferred x = Applicable
Refer to Price List for availability of sample kits and complete order information.
Aremco Products makes no warranty express or implied concerning the use of this product. The user assumes all risk of use or handling whether or not in accordance with directions or suggestions, or used singly or in combination with other products.