Fatigue behavior of glass-ceramics, glassinfiltrated alumina, and zirconia (Y-TZP) for dental applications Paulo Francisco Cesar, PhD

Associate Professor University of So Paulo School of Dentistry Department of Biomaterials and Oral Biology

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paulofc@usp.br

Outline:

1.1. Fatigue of ceramic materials (Slow Crack Growth). 1.2. Load application modes: static, dynamic, cyclic. 1.3. Cyclic fatigue: types of laboratorial tests. 1.4. Fatigue parameters (stress corrosion coefficient, n).

1.1. Fatigue of ceramic materials (Slow Crack Growth)

Stresses below the critical level (< KIc)

Strong effect of humidity

http://youtu.be/U9GbhHFaTmk

1.2. Load Application modes

Static
Dynamic Cyclic

Gonzaga et al. J Biomed Mater Res B Appl Biomater. 2011, 99(2):247-57 Gonzaga et al. Dent Mater. 2011, 27(4):394-406

Cyclic fatigue

Callister, 2007

Cyclic fatigue

Presence of artificial saliva, Temperature and pH variations, Stress level and frequency similar to in vivo situation.

1.3. Cyclic fatigue: types of laboratorial tests

S-N curves
Cycling at a fixed stress level

Stair-case approach
Step-stress approach

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 S-N Curve

Stress Amplitude

Number of cycles Learnengeneering.org

 Cycling at a fixed stress level

500 N

160 N
Studart et al. Biomaterials. 2007, 28(17):2695-705.

 Cycling at a fixed stress level

Fatigue parameters obtained by cycling at a fixed stress level

Studart et al. Biomaterials. 2007, 28(17):2695-705.

 Stair-case approach

900

Stress (MPa)

850 800 750

10^2 102 10^3 103 104 10^4 105 10^5

700
650 600
-1 9 19 29

Specimen order

39

49

59

69

79

Amaral, M.; Cesar, P.; Valandro, L.; Lohbauer, U., 2013

 Stair-case approach

Silicatization (Rocatec)
Stress (MPa)

Glass film Control

Amaral, M.; Cesar, P.; Valandro, L.; Lohbauer, U., 2013

 Step-stress

 Step-stress
R eliaSoft A LT A 7 - www.R eliaSoft.com

400

Stress vs Time
Stress Profile

340

S t re ss (M Pa )

280

220

160

100

40871

81741

Time (cycles)

163482

204353

Borba et al. Dent Mater, 2013, doi: 10.1016/j.dental.2013.05.009

1.4. Fatigue parameters (stress corrosion coefficient, n)

log fracture stress (MPa)

1 day

1 yr 10 yrs

Log time to failure (MPa/s)

Fracture stress (MPa)

2.1. Residual stress level predicted by finite element analysis (Thermal stress analysis). 2.2. Residual stresses calculated by the hole-drilling technique.

2.1. Residual stress level predicted by finite element analysis (Thermal stress analysis).

2.1. Residual stress level predicted by finite element analysis (Thermal stress analysis).

Meira et al. Dent Mater, 2013, 29(5):594-601

 Minimum principal stress (s 3 )

Meira et al. Dent Mater, 2013, 29(5):594-601

 Maximum principal stress (s1)

Meira et al. Dent Mater, 2013, 29(5):594-601

Belli R, Dent Mater. 2013; 29(2):181-90

Belli et al., J Mech Behav Biomed Mater. 2013; 21:167-77

2.2. Residual stresses calculated by the hole-drilling technique COFECUB project

Comit Franais d'Evaluation de la Coopration Universitaire et Scientifique avec le Brsil
- Title: Residual stress in veneering ceramic on YTZP, alumina and ZTA frameworks.

- Authors: K. Fukushima, M. Sadoun, P. Cesar, A. Mainjot.

- Aknowledgements: Grace de Souza, H. Yoshimura, H. Goldenstein, Jean-Pierre Attal.

2.2. Residual stresses calculated by the hole-drilling technique

 Hole-drilling technique

Mainjot et al. Dent Mater. 2011; 27(5):439-44

 Hole-drilling technique

 COFECUB Project: Univ. Paris-Descartes (Paris 5)

Fukushima et al., 2013 - COFECUB

Y-TZP

Alumina

ZTA

Fukushima et al., 2013 - COFECUB

Fukushima et al., 2013 - COFECUB

3.1. Reinforcement of dental porcelain with alumina particles. 3.2. Addition of carbon nanotubes to Y-TZP.

3.1. Reinforcement of dental porcelain with alumina particles

PhD project: Reinforcement of dental porcelain with alumina (mono and pollycristal)
PhD Student: Marina Kaizer Advisor: Rafael Moraes In colaboration with: Paulo Cesar

Univ. Federal de Pelotas

Kaizer, 2013

Kaizer, 2013

Kaizer, 2013

 Reinforcement of dental porcelain with alumina (mono and pollycristal)

Control

Polly

Polly+Sil

Mono

Mono+Sil

Kaizer, 2013

3.2. Addition of carbon nanotubes to Y-TZP

PhD Project: Development of the nanocomposite Y-TZP / MWCNT-COOH for dental applications Student: Lucas Hian da Silva Co-advisor: Rubens Tango Advisor: Paulo Cesar In collaboration with the Institute for Nuclear and Energetic Research (IPEN): Dolores Lazar Walter Usui Walter Yoshito

 Carbon Nanotube (CNT)

Yu et al., 2000; Ando, 2010

 MWCNT fuctionalized

Lucas Hian da Silva, 2013

3.2. Addition of carbon nanotubes to Y-TZP

Y-TZP conventional

Y-TZP/MWCNT

Lucas Hian da Silva, 2013

Thank you!

paulofc@usp.br
Paulo Francisco Cesar, PhD
Associate Professor University of So Paulo School of Dentistry Department of Biomaterials and Oral Biology

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