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IV B.Tech I Semester Regular Examinations, November 2008
ANALYTICAL INSTRUMENTATION
(Electronics & Instrumentation Engineering)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
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1. What are the applications of pH analyzer and Conductivity meter? Explain with
examples. [16]
2. (a) With a neat sketch explain the analysis of Nitric Oxide using CO Laser.
(b) Discuss Laser-Opto Acoustic Detector for the detection of nitric oxides. [8+8]
7. Discuss in detail the various salient features of the detectors used in mass Spec-
trometers. [16]
8. (a) Discuss the variation of count rate with voltage using suitable counter.
(b) What is the dead time of the counter? Explain. [10+6]
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Code No: R05411001 Set No. 2
IV B.Tech I Semester Regular Examinations, November 2008
ANALYTICAL INSTRUMENTATION
(Electronics & Instrumentation Engineering)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
⋆⋆⋆⋆⋆
2. (a) What are the applications of IR gas analyzer? Briefly discuss any one of them.
(b) Name an analyzer for detecting Hydrocarbons and explain it. [8+8]
6. Describe the basic design difference between a spectrometer for absorption mea-
surements and emission studies. [16]
7. Explain in detail the construction and working principle of single focusing mass
spectrometer. [16]
8. (a) What is a scintillator? Give examples and discuss the salient features of
scintillation counter.
(b) Explain in detail with a neat diagram the construction and working principle
of scintillation counter. [6+10]
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Code No: R05411001 Set No. 3
IV B.Tech I Semester Regular Examinations, November 2008
ANALYTICAL INSTRUMENTATION
(Electronics & Instrumentation Engineering)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
⋆⋆⋆⋆⋆
3. (a) Draw the circuit of Amplifier circuit used with Chromatograph and explain.
(b) Draw and explain the differential Flame Ionization Detector. [8+8]
4. What do you mean by Dissolved Oxygen? Name and explain a method to measure
it. [16]
6. Explain in detail with schematic, the Fourier transform infrared spectroscopy. [16]
7. (a) Define sensitivity of an instrument and discuss the various operation tech-
niques for sensitivity enhancement.
(b) Compare the conventional NMR and the Fourier transform NMR spectroscopy.
(c) Explain about the relaxation process in NMR spectroscopy. [8+4+4]
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Code No: R05411001 Set No. 4
IV B.Tech I Semester Regular Examinations, November 2008
ANALYTICAL INSTRUMENTATION
(Electronics & Instrumentation Engineering)
Time: 3 hours Max Marks: 80
Answer any FIVE Questions
All Questions carry equal marks
⋆⋆⋆⋆⋆
2. (a) With a neat sketch explain the analysis of Nitric Oxide using CO Laser.
(b) Discuss Laser-Opto Acoustic Detector for the detection of nitric oxides. [8+8]
3. (a) Define
i. Adsorption
ii. Absorption
iii. Ion Exchange Chromatography.
(b) What do you mean by Chromatogram? Draw a typical Chromatogram and
explain the different terms in it. [2+2+4+8]
5. Discuss the various arrangements used for recording the infrared spectra. [16]
7. State the principle of NMR. With neat diagram, explain about the constructional
details and working of a NMR spectrometer. [16]
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