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Experiment 1. The Synthesis of D !"Phenyl#lycine an$ Its Optical %esol&tion Total Scores: 100 points
1-1 Total Points %ecei+e$ () 1-2 1) 1-3 () 1-4 ) 1-5 3* ' 1**
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1-1
Weight of benzoylformic acid used: Weight of fritted glass funnel: After complete dryness: Product weight + fritted glass funnel:
g/
[Weigh on a balance that reads to the nearest centigram ( ! "g#$! Weight of %&'(phenylglycine obtained: Chemical yield: ) g
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1-2 +urn in the sample (in the ,ial with blue label#! -ignature of student: -ignature of the lab assistant: [+he organization committee will weigh an appropriate amount of sample ( ! "g# for ". /01 spectroscopic analysis!$ Step (. Enantiomeric resol&tion of D !"phenyl#lycine 4y 253"camphors&lfonic aci$ 6253"CSA7 1-3 Confirmed and signed by lab assistant g g/
g/
After complete dryness: Product weight + fritted glass funnel: g g/ [Weigh on a balance that reads to the nearest centigram ( ! "g#$! Weight of the resol,ed phenylglycine (+#(C-A salt: Chemical yield: ) g
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1-4 %raw the correct absolute stereochemical structure of the isolated phenylglycine!
1-5 -pecific rotation of the enantiomeric phenylglycine (+# C-A salt (to be determined by the organization committee# +urn in the sample (in the ,ial with pin2 label#! -ignature of student:
-ignature of the lab assistant: [+he organization committee will weigh an appropriate amount of sample ( ! 33 4 ! 53g# for measurement of optical purity!$
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77-econd column is for duplicates! 2-2 A! Write the electrolysis e@uation that would help you confirm that an un2nown sample is ?nCl8!
;! Write one e@uation that shows how to clean the deposit of ?n on the electrode (limited to the items pro,ided in this tas2#!