CCB 2092 Unit Operation Lab I

September 2013

CCB 2092 Unit Operation Laboratory I

September 2013 Laboratory Course Outline
1. General Information & Course Administration

Credit Unit
Coordinators 1.

: 2 (Core Engineering subject)

Room 05-03-36, Block 5 05-368 7611 tazliazizan@petronas.com.my Room 05-03-24, Block 5 05-3687616 Maziyar.sabet@petronas.com.my

Mohammad Tazli bin Azizan (MTA)

2.

Dr. Maziyar Sabet (MS)

Lab Instructors 1. 2. 3. 4. 5. 6. 7. Ahmed Ali Baig (AAB) Omer Eisa Babiker Abdelgadir (OE) Rizwan Safdar (RS) Zahid Majeed (ZM) Tauqeer Abbas (TA) Muhammad Zulfiqar (MZ) Fareeda Che Mat ahmed1dec@gmail.com omar22eisa@yahoo.com engr_chem@hotmail.com zahidfdb@gmail.com tauqeerabbas@ciitlahore.edu.pk zulfiqar_rehmani@hotmail.com Unique.utp@gmail.com

Laboratory Technologists 1. 2. 3. 4. 5. Azriha Bt. Anuar (AA) Khairul Afizan B. Saidin (KAS) M. Azfarnur B. Mat Juri (MA) Mohd. Shahafizan B. Zulkifli (MSZ) Muhammad Fairis B Arifin (MFA) Room 03-02-012 azriha_anuar@petronas.com.my Room 03-00-008 khairulafizan@petronas.com.my Room 04-00-14 azfarnur_juri@petronas.com.my Room 03-00-008 mshahafizan_zulkifli@petronas.com.my Room 04-00-14 fairis.arifin@petronas.com.my Room 03-01-009 suleiman_hakimi@petronas.com.my ext 7540 ext 7586 ext 7540 ext 7586 ext 7541 1

6.

Suleiman Hakimi B. Zainal Abidin (SH)

CCB 2092 Unit Operation Lab I

September 2013

2.

Course Learning Outcome (CLO)

At the end of this course, you should be able to demonstrate the practical skills and the understanding of knowledge on chemical engineering unit operations focusing on Fluid Flow, Transport Processes and Process Heat Transfer.
3. Laboratory Delivery Lab Session:

a)

Group 1 12: Thursdays 3.00-7.00 pm Replacement (14/02/2014) :Friday 3.00 pm 7.00 pm

b) c) d) e) f)

You will be divided into groups of 4 to 5 students. You will carry out experiment sessions and group projects in the semester. Lab will be done as per schedule (Refer to the schedule for details). In case of lab falls on the public holiday, lab will be replaced on similar day in the afternoon session in some other week. In case of equipment breakdown, experiments will be replaced with another experiment. However, cases below will apply: If equipment breakdown is more than half of the experiment requirement, the student must proceed with the available results. If equipment breakdown less than half of the experiment requirement, the experiment must be replaced with other available experiment/equipment.

4.

Laboratory Assessment

Assessment Task Lab Report + Job Safety Analysis (JSA) Form Group Project Report Lab Oral Presentation / Viva Voce Lab Test TOTAL

Mark 45% (40% + 5%) 10% 15% 30% 100%

Assessment Type Group Group Individual Individual

CCB 2092 Unit Operation Lab I

September 2013

5. a)

Report Submission There will be TWO (2) types of report and submission as in the followings: Type
th

Experiment 1 , 2 , and 4 3
rd st nd

Report due One week after lab session 24 March 2014 Week 13

Submit to Coordinator Coordinator Coordinator

Remarks Both, hardcopy and softcopy of the report MUST be submitted.

to 8

th

Short Report Long Report Long Report

Group Project b) c)

Contents of the report and length: please refer lab manual. Submit report on time. Late submission will result in mark deduction: 1 day late 5 marks deducted. > 2 days late no marks.

d)

Softcopy shall be emailed to the Coordinator. The filing name format: YYYYMMDD-GXXEXPXX. Example: Group 1, Exp 1, Date 1/10/2012, the file name should be typed as: 20121001-G01-EXP01

6.

Laboratory Module Content

FLUID FLOW & TRANSPORT PROCESSES Experiment 1 2 3 4 5 6 7 8 9 Properties of Fluid Fluid Friction Fluid Statics Pipe Network Cavitation Compressible Fluid Flow Pressure Drop in Packed Bed Fluid Mixing Multipump Location 04.00.13 04.00.13 04.00.13 04.00.13 04.00.13 04.00.13 04.00.13 04.00.13 04.00.13 Lab Instructor OE OE ZM ZM MZ MZ AAB AAB ZM Lab Technologist MA / MFA MA / MFA MA / MFA MA / MFA MA / MFA MA / MFA MA / MFA MA / MFA MA / MFA

PROCESS HEAT TRANSFER Experiment 10 11 12 13 14 15 Plate Heat Exchanger Shell and Tube Heat Exchanger Heat Transfer in Agitated reactor Cross Flow Heat Exchanger Double Pipe Heat Exchanger Multi-Heat Exchanger System Location 03.00.06 03.00.06 04.00.16 04.00.16 03.00.06 03.00.06 Lab Instructor RS RS/ FCM TA TA RS/ FCM RS Lab Technologist MSZ / KAS / SH MSZ / KAS / SH AA / MFA AA / MFA MSZ / KAS / SH MSZ / KAS / SH 3

CCB 2092 Unit Operation Lab I

September 2013

7.

Timetable

EXPERIMENT / DATE
Group 1
ST

ND

RD

TH

TH

TH

TH

TH

23/01 30/01 06/02 13/02

14/02 20/02 27/02 06/03 13/03 20/03 27/03 03/04 10/04 (R)

1 2 3 4 5 6 7 8 9, 10 11 12 Briefing CNY Leave / Group Project Assignment

1 2 3 4 5 6 7 8 10 11 12 13

9 3 6 5 7 8 1 2 12 13 14 11

6 5 7 8 10 11 12 13 1 2 3 4

8 7 1 2 12 13 14 10 3 4 5 6

2 8 4 9 13 12 10 11 5 6 1 14

10 11 12 14 2 1 9 3 6 7 13 8

12 13 14 11 3 4 2 6 8 10 7 5

14 13 10 8 5 7 11 9 6 1 Test 2 Group Project Report Submission 4 12 Poster / Oral Presentation

Fluid Flow & Transport Processes Process Heat Transfer

CCB 2092 Unit Operation Lab I

September 2013

8.

Grouping

GROUP 1 12: Thursdays, 11.00 am 3.00 pm

ALI ABDULLAH SALEH AL-YAFEAI AMIRA NURAIN BINTI RAMDAN GROUP 1 AZLAN BIN RAMALI CHEN SWEE KEAT DINESHKUMAR A/L G.RAMACHANDRAN FERNANDO JUMA MUZONDE NIK NUR IZZATUL IKMAL BINTI MUHD NOR MUHAMMAD AMIRUL FARIS BIN SABRI TAN WEI YEIN PANNIR SELVAM A/L MURUGIAH ALI ABDULLAH BAQDHIMH BARASHAID NUR ATHIRAH AYUB GROUP 3 MUHAMMAD HAIQAL BIN ROSLI PANG ZHEN HONG VAAGHISEN A/L DEVAN OLA YAHIA OSMAN MOHAMED SITI NORIAYANA BINTI ROSLI MUHAMMAD ILYASA SAFFIQ BIN ARIFFABILAH LAI CHUN HOE VINOD KANNA A/L KOBAL 0017036 0018624 0018645 0018604 0016799 GROUP 7 ANDERSON JOSEPH ILYA AMANINA BINTI MAHMUD MOHAMED RIZWAN BIN RAFEEK ASHWIN PAL SINGH KANAPATHY MOHANAN HESHAM SAEED SALEM AL-GARIRI NORHIDAYU BINTI JAMAL GROUP 8 MUHAMMAD FIRDAUS BIN AZNAN TON KAR YAN SHAAVESH KUMARAN A/L PARAMESWARAN 0016740 0018660 0017021 0016990 0018672

0014617 0018699 0018678 0016780 0016768

0016669 0018666 0016182 0018653 0016703

GROUP 2

0016667 0016998 0016890 0018709 0016761 GROUP 9

OLA ABDALGAWI ALI OSMAN NUR NADIAH MUSTAPHA MUHAMMAD HILMI BIN AHMAD KUJAJI SEK CHUN HEI VIMMAL A/L DESIGA VINAYAGAM OMAR MABKHOT MUHSEN MUBARAK SITI NUR FATIHAH BT MOHD SHAIB GROUP 10 WALTER PAULO AZIZE TAJU LOW WEI JIN VIVENDRAN A/L KRISHNAN MOORTHY

0020478 0016431 0018774 0016749 0016853

0020479 0018644 0018720 0016751 0016776

0015719 0018656 0016562 0016863 0016891

GROUP 4

CCB 2092 Unit Operation Lab I

September 2013

OSAMA AHMED BAKRI SYIFAA BINTI ZUKHRI GROUP 5 CHONG CHAO SIAN VANISHA KUMAR A/P PARAM KUMAR YAKESHWARAN A/L KENISHAN RABEA SALEH RABEA BIN SOWAD MUHAMMAD NAZRIN BIN AHMAD FARID GROUP 6 CHIEW CHEE SENG GURJIT KAUR A/P RANJIT SINGH

0015679 0018634 0018619 0018695 0016715 GROUP 11

PHUMPHAIRIN LIONG UMMU ATHIRAH ELIAS EE MING FERN THARRANI KESHVEENI KUANASEALAN SARA GALAL ELDIN ELTAHIR MUSTAFA NG JIA PING

0018707 0016186 0016869 0015861 0016716

0016673 0018727 GROUP 12 0016779 0016741

0020474 0018668 0018726 0016933

MUHAMMAD LUQMANUL HAKIM BIN KAMARULZAMAN JOANNA RUTH A/P THANGA RAJ

CCB 2092 Unit Operation Lab I

September 2013

9. a) b) c) d) e) f) g) h) i)

References de Nevers, N., Fluid Mechanics for Chemical Engineers, 3 Ed., McGraw-Hill, 2005. McCabe W.L., Smith J. C. and Harriot P., Unit Operations of Chemical Engineering, th 7 Ed., McGraw-Hill. 2005. Cengel, Y. A. and Cimbala, J. M., Fluid Mechanics: Fundamentals & Application, McGraw-Hill, 2006. th White, F. M., Fluid Mechanics, 5 Ed., McGraw-Hill, 2005. th Geankoplis, C.J., Transport Processes and Separation Process Principles, 4 Ed. Prentice Hall. 2003. th Mott, R.L., Applied Fluid Mechanics, 6 Ed. in SI Units, Pearson-Prentice Hall. 2006. th Holman, J. P., Heat Transfer, 8 SI Metric Ed., McGraw-Hill, 2001. Hewitt, G. F., Shires, G. L. and Bott, T. R., Process Heat Transfer, CRC Press, 1993. th Green D. and Perry R.H., Chemical Engineers' Handbook, 8 Ed., McGraw Hill, 2007.
rd

10.

Program Outcomes
PO7 Understand the impact of professional engineering solutions in societal and environmental contexts and demonstrate knowledge of and need for sustainable development PO8 Apply ethical principles and commit to professional ethics and responsibilities and norms of chemical engineering practice

PO1 Apply knowledge of mathematics, science, engineering fundamentals and an engineering specialization to the solution of complex chemical engineering problems PO2 Identify, formulate, research literature and analyze complex chemical engineering problems reaching substantiated conclusions using first principles of mathematics, natural sciences and engineering sciences PO3 Design solutions for complex chemical engineering problems and design systems, components or processes that meet specified needs with appropriate consideration for public health and safety, cultural, societal, and environmental considerations PO4 Investigate complex chemical engineering problems using research based knowledge and research methods including design of experiments, analysis and interpretation of data, and synthesis of information to provide valid conclusions PO5 Utilize modern engineering and IT tools to evaluate complex chemical engineering activities

PO9 Communicate effectively on complex chemical engineering activities with the engineering community and society

PO10 Function effectively as an individual, and as a member or leader in diverse teams and in multidisciplinary settings

PO11 Recognize the need for, and have the preparation and ability to engage in independent and life-long learning in the broadest context of technological change PO12 Demonstrate knowledge and understanding of engineering management, business acumen and entrepreneurship in multidisciplinary environments

PO6 Apply reasoning informed by contextual knowledge to assess societal, health, safety, legal and cultural issues and the consequent responsibilities relevant to professional engineering practice

CCB 2092 Unit Operation Lab I

September 2013

PROGRAM OUTCOMES (PO)

DELIVERY METHODS Lab Oral Presentation / Viva Voce

ASSESSMENTS Lab Oral Presentation / Viva Voce 3

Laboratory Reports

Laboratory Session

CCB 2092 UNIT OPERATION LAB 1

Group Project Report

Group Project

Lab Test

COURSE LEARNING OUTCOMES Demonstrate the practical skills and the understanding of knowledge on chemical engineering unit operations focusing on Fluid Flow, Transport Processes and Process Heat Transfer.

10

11

12

Lab Test 4 8

PO10

PO11

PO12

PO1

PO2

PO3

PO4

PO5

PO6

PO7

PO8

PO9

CCB 2092 Unit Operation Lab I

September 2013

11. a) b) c) d)

Attendance You must attend all lab sessions. In case of absentees due to illness, a valid Medical Certificate must be submitted to the Lab Coordinator. In the case of other commitment (student activities, family matters, etc) an authorization letter from the relevant personnel/family member is required. In case of emergency or any unavoidable circumstances that you cannot attend the lab session, you are required to inform the Lab Coordinator prior to the event. This needs to be supported by a letter.

e)

Your lab session WOULD NOT BE REPLACED due to absenteeism. However, you will still be graded for the lab report, ONLY when a supporting document is given to the Lab Coordinator. You must also attend the Viva Voce session at the convenience of the Lab Instructor.

f)

Without any supporting document due to absenteeism, you will not be getting any marks for the lab assessment.

12. a) b)

Attire Properly attired. Wearing your lab coat is a MUST. Other personal protective equipment (PPE, such as goggles, safety helmet, ear plugs, ear muff, etc) will be provided. These clothing are not allowed in the laboratory: national costumes (baju kurung, cheongsam saree, etc), jubah, skirts (short or long), sarongs, shorts, sandal, slippers and uncovered shoes) while conducting experimental work. You ARE NOT ALLOWED TO PROCEED with your laboratory work if you fail to do that.

c) d)

For those who are wearing tudung or hijab, and with long hair, you are required to keep them neat. Besides the lab instructor, the technical assistants have the authority to ask you to leave the lab if you do not adhere to the above regulations.

13. a) b) c)

Safety in Laboratory Please abide to all safety rules and regulations in the laboratory. Please be aware on the laboratory safety signs indicated in the lab. You must fill the Job Safety Assessment Form (JSA) BEFORE conducting the experiment. The JSAF must be approved by the respective personnel and submitted with the lab report.