Winter 2014 Chemistry 14CL Laboratory Schedule and Assignment (Last Day To Drop Impacted class; January 17)

SAFETY GLASSES AND LAB APRONS OR LAB COATS MUST BE WORN IN THE LABORATORY. FAILURE TO DO SO WILL RESULT IN DISMISSAL FROM THE LABORATORY 1 Experiment Videotape2 Reading3 1: Check-in, Pipet Calibration (1) 8: pH titration of an amino acid (2) ) (Handout) Determination of iron in Vitamin (1) (Handout) Spectrophotometric M p. F95-F102 Extraction (#3132) IR (#3139) Safety (#5805) Use of a Pipet M p. 2-27; p 42-44 AJ p. 579-609; B p. 1034-1048 B p. 533 ; M 429

Date 1/7 - 8 1/9-15 1/16-17

Postlabs Due Date4 NONE 1/21 & 22 1/23 & 24

1/21-24 1/28-29 1/30-31 2/4-7 2/11-12 2/13-14 2/18-19 2/20-21

7a: Extraction of Caffeine (2) 7b: Spartan Infrared spectroscopy (1) 7a: Analysis of Caffeine (1) Titrimetric Analysis of Vitamin C (2) (Handouts) 6: Aldol condensation (1) Molecular Modeling (1) Isolation of Chlorophyll and Carotenoid Pigments from Spinach (Handouts) (1) Characterization of Pigments isolated from Spinach (1) 15: 13C NMR and DEPT Spectra (1) 10: Oxidation of Borneol to Camphor (1) (handouts) 9: Distillation & Gas chromatography (1) 10: Analysis of Camphor (1) Lab Clean-up (Attendance is required)

M p.113 - 124 B Ch. 12 & 14; M 277-300 M p. 221-235; p. 277-300; 434-437 AJ p. 633-642; p. F 95-F 102

One postlab for 7a refer to due date shown below 2/6 & 7 2/6 &7 2/13 & 14 2/25 & 26 2/25 & 26 One postlab for Spinach 2/27 & 28

Melting Point Determination (#3138) Column Chromatography (#3133) Thin layer Chrromatography

M p.174-182 B 28-43 & 682-685; AJ Chapter 3 M p. 235-256, p. 432 B p.532-538

2/25-26 2/27-28 3/4- 5 3/6-7 3/11-12

M p.371-396; B p. 498-500 M p. 56-71; AJ p. 633-638; Distillation (#3134) GC (#3134) M p. 145-177 M p. 256-272 M p. 277-300; AJ p. 633-638;

2/25 & 26 refer to due date shown below 3/11 & 12 3/13 & 14

3/13-14

Review for Final

(Attendance is required)

1) Chemistry Experiments for Life Science Majors, Second Edition, A.A. Russell, Burgess Publishing Company. 2) Instructional Media Library, Powell 270 or on the WWW (http://www.oid.ucla.edu/Webcast/Chemistry/index.html) 3) Mohrig (Organic Techniques) = M, Brown (Organic chemistry) = B, Atkins and Jones, The Quest for Insight, 2nd Edition = AJ. 4) Pre-lab reports (if any) are due at the beginning of the lab period; observations and data are due at the end of the lab period in which the data are taken; post-lab reports are due at the beginning of your regularly scheduled lab period one week after the experiment is finished. NO WORK WILL BE ACCEPTED AFTER 4:00 P.M. Friday, 3/14/2014