CCB 2073 Jan 2014

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CCB 2073
ANALYTICAL CHEMISTRY

LABORATORY MANUAL (PREFACE)

DR. YEONG YIN FONG

UNIVERSITI TECHNOLOGI PETRONAS

Department of Chemical Engineering

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TABLE OF CONTENTS
1) General Information 2) Objectives 3) Laboratory Location 4) Laboratory Safety 5) Pre-Experiment Preparation 6) Format Report Writing 7) Report Grading 8) Laboratory Time Schedule 9) Group List 3 4 4 4 5 6 9 10 11

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Lecturers: Dr. Yeong Yin Fong Office: 04-03-13 Phone: 05-3687564 Email: yinfong.yeong@petronas.com.my

CCB 2073 Jan 2014 Objectives

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The main objective of the Analytical Chemistry Laboratory is to adapt the students in analyzing experimental data. It is important for the students to understand the theories they study in lecture and in their textbooks. In addition, laboratory experimentation provides opportunity to the students to learn how to write clear and concise scientific reports. It will be a strong emphasis in this course to

get the student familiarized with the analytical equipment.

Laboratory Location: Experiments 1-5 will be conducted at the following laboratories, respectively: Experiments 1 2 3 4 5 Laboratory Location 05-00-06 04-02-09 05-00-06, 05-00-09 05-00-08 05-00-06, 04-02-09

Laboratory Safety Safe practices in the laboratory are of high importance. The general rules and regulation in the laboratory while conducting experiments are as follows:

Personal Protective Equipment (PPE) All students are COMPULSORY to wear lab-coat and covered shoes all the time in the laboratory. Safety goggle and gloves are necessary when handling chemical reagents.

CCB 2073 Jan 2014 General Rules of Safety and Precautions 1. Food or drinks are not allowed in the laboratory.

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2. Familiarized with the location of the safety equipment such as eye wash, shower and fire extinguishers. 3. Pay full attention to all instructions presented by the instructor. Do not conduct any unauthorized experiment. Consult instructor if something is not clear. 4. Avoid contact your skin with chemicals. If contact does occur, wash the area contacted thoroughly with water. Report all accidents to the instructor immediately. 5. Consult instructor before dispose any waste chemicals. 6. Use all heating and electrical equipment carefully to avoid any burns and shocks. 7. NEVER handle broken glassware with your hands. 8. After the experiment is completed, turn off all equipment and clean your area.

Pre-Experimental Preparation A proper planning is crucial before carry out any of the experiment. Students will not be granted
extra time to complete the laboratory. Students are required to read the procedure and theory of the experiment carefully before arriving at the laboratory. It is important to prepare a brief outline (or flow-chart) before start of experiment and to organize the format of the data section before coming to the laboratory so that you will only need to record your data and observations during the experiment.

CCB 2073 Jan 2014 Format Report Writing (Group Report)

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As part of post-laboratory exercise, all the groups are required to submit laboratory report for each of the experiment. The format and content of the report are as follows:

Cover Page Experimental number and title, Name for all the group members, date of the experiment and report submission deadline. For example:

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CCB 2073 ANALYTICAL CHEMISTRY LABORATORY REPORT

Semester Jan 2014
Experiment 1: Gravimetry Gravimetric Analysis of a Chloride Salt Group No: 1 Members: 1) 2) 3) 4)

Date of Experiment: Report Submission Deadline:

Department of Chemical Engineering

CCB 2073 Jan 2014 Introduction

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Write a brief statement or a paragraph to describe the objective of the experiment and the method used. State the purpose of the experiment.

Experimental Procedure
A brief description of the experiment steps and a drawing of the apparatus should be included.

Data and Observations Report all the measurements or data collected during the experiment, including the units of the data. The use of table or graph is suggested. For the experiments 3-6, attach the spectra, graphs, charts or other data that produced during the experiment.

Calculation and Discussion Calculations: If the experiment involves calculation, perform a sample analysis of the data that was collected during the experiment prior to calculation. Use an appropriate equation. Discussion: Include an interpretation of the data that you observed and understand the data. Explain how the data fit your hypotheses. If not, discuss why. Include also possible sources of error. Refer to the Questions section which may help to guide your discussion of the data.

Questions Questions are provided in the manual and all assigned questions are answered in this section.

Conclusions Report the outcome of the experiment.

CCB 2073 Jan 2014 Report Grading

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The laboratory contributes overall 20% of the total grading in this course. Therefore, a student must complete all of the assigned laboratory work including report submission. All groups are required to submit five reports, 100% will be allocated for each of the report based on the following criteria: preparedness, cleanliness, following safety rules, following instructions, taking notes during laboratory report attendance (0 % for those absent)

The report must be completed and submit to Lecturer within 1 week, by the next scheduled
laboratory date. Late submission of your report will be met with a 10% deduction.

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Date 11 Feb 2014 13 Feb 2014 4 Mar 2014 6 Mar 2014 11 Mar 2014 13 Mar 2014 25 Mar 2014 27 Mar 2014 1 Apr 2014 3 Apr 2014 8 Apr 2014 10 Apr 2014
Note: -

Day Tuesday Thursday Tuesday Thursday Tuesday Thursday Tuesday Thursday Tuesday Thursday Tuesday Thursday

Laboratory Time Schedule (Subjected to Change) Exp. 1: Exp.2: Exp. 3: Time Location Gravimetry FT-IR UV-Vis 1 5 pm 05-00-06 G1-G7 11 am 3 pm 05-00-06 G8-G14 1 5 pm 11 am 3 pm 1 5 pm 11 am 3 pm 1 5 pm 11 am 3 pm 1 5 pm 11 am 3 pm 1 5 pm 11 am 3 pm 04-02-09 (Exp. 2) 05-00-06, 05-00-09 (Exp. 3) 05-00-08 (Exp. 4) 05-00-06, 04-02-09 (Exp. 5) Oral Presentation G1-G7 To be confirmed G8-G14 G1-G4 G8-G11 G5-G7 G12-G14 G5-G7 G12-G14 G1-G4 G8-G11

Exp. 4: GC

Exp. 5: HPLC

G1-G4 G8-G11 G5-G7 G12-G14

G5-G7 G12-G14 G1-G4 G8-G11

All students will be divided into 14 groups, G1-G14 There are 4 students in each group (please refer to the Group List)

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Group List
Group Student Name ALI ABDULLAH BAQDHIMH BARASHAID G1 JOANNA RUTH A/P THANGA RAJ NORHIDAYU BINTI JAMAL SITI NUR FATIHAH BT MOHD SHAIB THARRANI ALI ABDULLAH SALEH AL-YAFEAI KANAPATHY MOHANAN NUR ATHIRAH AYUB SYIFAA BINTI ZUKHRI MOHD LUQMAN HANIS BIN MOHD GHAZALI AMIRA NURAIN BINTI RAMDAN KESHVEENI KUANASEALAN SHAAVESH KUMARAN A/L PARAMESWARAN TAN WEI YEIN ANDERSON JOSEPH LAI CHUN HOE SARA GALAL ELDIN ELTAHIR MUSTAFA CHIEW CHEE SENG ASHWIN PAL SINGH LOW WEI JIN OLA YAHIA OSMAN MOHAMED UMMU ATHIRAH ELIAS AZLAN BIN RAMALI MOHAMED RIZWAN BIN RAFEEK OMAR MABKHOT MUHSEN MUBARAK VAAGHISEN A/L DEVAN VIMMAL A/L DESIGA VINAYAGAM MUHAMMAD AMIRUL FARIS BIN SABRI PANNIR SELVAM A/L MURUGIAH VANISHA KUMAR A/P PARAM KUMAR ID 0016667 0016933 0018666 0018656 0015861 0017036 0018672 0016998 0018634 0016134 0018624 0016716 0016703 0016780 0016740 0016751 0020474 0016779 0016990 0016863 0020479 0016186 0018645 0017021 0015719 0016761 0016853 0018678 0016768 0018695

G2

G3

G4

G5

G6

G7

CCB 2073 Jan 2014 Group G8 Student Name TON KAR YAN MUHAMMAD FIRDAUS BIN AZNAN PANG ZHEN HONG CHEN SWEE KEAT

P a g e | 12 ID 0018653 0016182 0018709 0018604

G9

CHONG CHAO SIAN MUHAMMAD HAIQAL BIN ROSLI PHUMPHAIRIN LIONG VINOD KANNA A/L KOBAL DINESHKUMAR A/L G.RAMACHANDRAN MUHAMMAD HILMI BIN AHMAD KUJAJI RABEA SALEH RABEA BIN SOWAD VIVENDRAN A/L KRISHNAN MOORTHY EE MING FERN MUHAMMAD ILYASA SAFFIQ BIN ARIFFABILAH OLA ABDALGAWI ALI OSMAN WALTER PAULO AZIZE TAJU GURJIT KAUR A/P RANJIT SINGH MUHAMMAD NAZRIN BIN AHMAD FARID SEK CHUN HEI WAN AMIRAH BINTI WAN AMERI HESHAM SAEED SALEM AL-GARIRI NG JIA PING NUR NADIAH MUSTAPHA YAKESHWARAN A/L KENISHAN ILYA AMANINA BINTI MAHMUD NIK NUR IZZATUL IKMAL BINTI MUHD NOR SITI NORIAYANA BINTI ROSLI ARASH YAZDANI

0018619 0016890 0018707 0016776 0016799 0018774 0016673 0016891 0016869 0018720 0020478 0016562 0016741 0018727 0016749 0018632 0016669 0018668 0016431 0016715 0018660 0018699 0018644 0017043

G10

G11

G12

G13

G14