Engineering Management Support, Inc.: West Lake OU-1

ENGINEERING MANAGEMENT SUPPORT, INC.
West Lake OU-1
STANDARD LEVEL IV
REPORT OF ANALYSIS
WORK ORDER #13-04053-0R
May 6, 2013
EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

OAK RIDGE, TN
TABLE OF CONTENTS
SECTION
DESCRIPTION
PAGE
Chain of Custody & pH Check Sheet
0004
II
Sample Acknowledgement
0012
III
Case Narrative
0015
IV
Analytical Results Summary
0019
Analytical Standards
0023
VI
Quality Control Sample Results Summary
0047
VII
Laboratory Technician's Notes
0056
VIII
Analytical Data (Isotopic Uranium)
0082
IX
Analytical Data (Isotopic Thorium)
0146
Analytical Data (Radium-226)
0210
XI
Analytical Data (Radium-228)
0269
XII
Barium-133 Analytical Tracer Data
0286
Last Page Number
0322
STANDARD OPERATING PROCEDURE
MP-001, Rev. 12
Effective. 10131112
Page 14 of 14
Sample Receiving
Eberline Services - Oak Ridge laboratory

LABORATORY DATA SUPPORT CHECKLIST
MP-001-3
1_J_-_0_4_0_5_3_____
Eberline Services Work Order # _ _ _
The checklist items listed below are to be initialed by appropriate staff upon completion/verification.
Date for Partial
Initials
Date
Initials
Checklist Items
Sample Log-In
Data Compilation
First Technical Data Review
Second Technical Data Review
Data Entry/Electronic Deliverable
Case Narrative
Electronic Deliverable Proof
SampleS\AJralyzed within Holding Time
Yes?
Lf:-..J..o.? I
QA/QC Aeview
Client in Possession of Data
ct
: or Har.d Coov
Invoiced by Laboratory
Date/Initials
Technical/Clerical Corrections, Signatures Needed, Problems, Etc
Date pa ckage approved by:
Laboratory Manager
Copy No. _ _ __
Date
Radiochemistry Services
SECTION I
CHAIN OF CUSTODY
&
pH CHECK SHEET
13-04053
Ebullne Servtcas
Chain of Custody Record

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601 Scalboto Road

oak Ridge, TN 37830
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Chain of Custody Record

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601 Sealbolo Road
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EBERLINE
....
SERVICES
Oak Ridge Laboratory
Internal
Work Order#
13-04053
Chain of
Lab Deadline
4/30/2013
Custody
Analysis
Water
Sample Matrix
Sample
Fraction
Comments
UUISO - Level 4
HP 210/270
Detector Activity
Storage
Location
Initia IS
Date
Fxns 04, 06 & 08 are TOTAL

Fxns 05, 07 & 09 are DISSOLVED
Location (circle one)

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EBERLINE
SERVICES
Internal
Work Order#
13-04053
Chain of
Custody
Lab Deadline
4/30/2013
Analysis
ThiSO - Level 4
Water
Sample Matrix
HP 210/270
Detector Activity
Sample
Fraction
Comments
04
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EBERLINE
SERVICES
Internal
Work Order#
13-04053
Chain of
Custody
Lab Deadline
4/30/2013
Comments
Analysis
Ra226 - Level 4
Water
Sample Matrix
Sample
Fraction
HP 210 I 270
Detector Activity
Storage
Location
04
40
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EBERLINE
SERVICES
Internal
Work Order#
Chain of
Custody
Lab Deadline
Analysis
Sample Matrix
Sample
Fraction
Comments
13-04053
4/30/2013
Ra228 - Level 4
Water
HP 210/270
Detector Activity
Storage
Location

Date
Location
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Printed: 4/9/2013 2:24 PM
G61fi
Printed: 4/9/2013 2:03 PM
Page 1 of 1
Internal Work Order
(Volumes, pH, & CPM)
SERVICES
ClientiD
DUP
0
0
0
04
PZ-305-AI TOT I'
LCS
BLANK
Comments
# Btls
01
02
03
PZ-305-AI DIS"'
WA
, ,Conlainer Numtier,
1
07
DUP 03 DIS'
09
DUP 04 TOT/
DUP 04 DIS
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13-04053
Sample Receiving Report
E:EJ E~RJ...,1NE
VolumeiU
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MP-001, Rev 5
Effective: 11/22/02
JJ
SECTION II
SAMPLE ACKNOWLEDGEMENT
GG12
Client Name
Contract/PO
Engineering Management Support, Inc. West Lake ou-1j

I'
Project Name
ClientWO
West Lake OU-1
West Lake OU-11
---
lnternaiiD
Client ID
Project Type
Date Received
Environmental
04/09/2013
28
Sample Disp
Lab Deadline
Internal Deadline
04/30/2013
05/06/2013
. ...
..
Required Turnaround Days
13-04053
I.
Sample Date
Matrix
Storage
,,
II
~ 3
04/09/13
WA
GGLO
05/07/2013
01
LCS
02
BLANK
04/09/13
WA
GGLO
03
DUP
04/09/13
WA
GGLO
04
PZ-305-AI TOT
04/05/13 15:58
WA
GGLO
OS
PZ-305-AI DIS
04/05/13 15:58
WA
GGLO
06
DUP 03 TOT
04/05/13 00:00
WA
GGLO
07
DUP 03 DIS
04/05/13 00:00
WA
GGLO
08
DUP 04 TOT
04/05/13 00:00
WA
GGLO
09
DUP 04 DIS
04/05/13 00:00
WA
GGLO
0
0
0
0
0
0
0
0
0
0
0
Totals Per Analysis (non QA samples)
Invoice
E.ae:B~lNE:
SERVICES

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice
Sam pie Log In Report
Voice: (865) 481-0683

Fax:
(865) 483-4621
Paul V. Rosasco, P.E.
Report Data
Engineering Management Support, Inc
7220 West Jefferson Avenue, Suite 406
7220 West Jefferson Ave, Suite 406
Lakewood, CO 80235
Lakewood, CO 80235
303-640-3426
Engineering Management Support, Inc.
Fax
Voice
303-940-3426
Fax
Contact
Lyn Fitzgerald
Voice
303-601-4255
Fax
Cil!)
jl!tw~t.
t)
Printed: 4/9/2013 2:24PM
STANDARD OPERATING PROCEDURE
MP-001, Rev. 12
Effective. 10131112
Page 13of 14
Sample Receiving
Eberline Services -Oak Ridge laboratory

SAMPLE RECEIPT CHECKLIST
MP-001-2
1_3_-_0_4_0_5_3_
WORK ORDER# _ _
SAMPLE MATRIX/MATRICES:
(CIRCLE ONE OR BOTH)

(fouEoUS)
NON-AQUEOUS
(CIRCLE EITHER YES, NO, OR N/A)

WERE SAMPLES
Received in good condition?
If aqueous, properly preserved
G)
Present on outside of package?
10
Unbroken on outside of package?
Present on samples?
N/A
WERE CHAIN OF CUSTODY SEALS
Unbroken on samples?
Was chain of custody present upon sample receipt?
Ki?)
(~YJ
IF THE RESPONSE TO ANY OF THE ABOVE IS NO, A DISCREPANT SAMPLE RECEIPT REPORT
(DSR) HAS BEEN ISSUED.
REMARKS: ________________________________________________________
SIGNATURE:
CopyNo. ________
c::KnJ.Aioru Ca,UtuV
DATE:
~ftl /13
Radiochemistry Services
SECTION III
CASE NARRATIVE
EBERLINE ANALYTICAL CORPORATION
601
SCARBORO ROAD
37830
(865) 481-0683
(865) 483-4621
OAK RIDGE, TENNESSEE

PHONE
FAX
EBS-OR-35528
May 7, 2013
Lakewood, CO 8023 5
CASE NARRATIVE
Work Order# 13-04053-0R
SAMPLE RECEIPT
This work order contains three water samples received 04/09/2013. All samples were analyzed as total
and dissolved for Isotopic Uranium, Isotopic Thorium and Radium-226/228.
CLIENTID
LABID
PZ-305-AI TOT
PZ-305-Al DIS
DUP03 TOT
DUP 03 DIS
DUP 04 TOT
DUP 04 DIS
13-04053-04
13-04053-05
13-04053-06
13-04053-07
13-04053-08
13-04053-09
ANALYTICAL METHODS
Isotopic Uranium and Isotopic Thorium were analyzed using Method HASL 300, 4.5.2. Radium-226 was
analyzed using EPA Method 903.0. Radium-228 was analyzed using EPA Method 904.0.
Laboratory qualifiers are as follows:
J-
Indicates a situation where the result minus the error is less than the detection limit but greater
than zero.
U-
Indicates a situation where the result minus the error is less than or equal to zero.
ANALYTICAL RESULTS
Combined Standard Uncertainty is reported at 2-sigma value.
Page 1 of3
i-616
ANALYTICAL RESULTS CONTINUED

ISOTOPIC URANIUM
Samples were filtered to disassociate dissolved and total fractions. Volumetric aliquots from dissolved
fractions were acidified with HN03 All samples were prepared by mixed acid digestions as appropriate.
Uranium was selectively extracted by ion exchange. Uranium was eluted, micro-precipitated and
mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy
using energy specific regions of interest for Uranium-234, Uranium-235 and Uranium-238. Chemical
recovery was determined by the use of a Uranium-232 tracer. Activity of the Uranium-232 tracer was
determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Uranium analyses. Chemical recovery was acceptable for
all samples. The Uranium-234, Uranium-235 and Uranium-238 method blank demonstrated acceptable
results. Results for the Uranium-234, Uranium-235 and Uranium-238 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Uranium-234 and Uranium-238 laboratory control sample demonstrated an
acceptable percent recovery.
ISOTOPIC THORIUM
fractions were acidified with HN0 3 . All samples were prepared by mixed acid digestions as appropriate.
Thorium was selectively extracted by ion exchange. Thorium was eluted, micro-precipitated and
mounted on micro-porous filter media. Sample activities were then determined by alpha spectroscopy
using energy specific regions of interest for Thorium-228, Thorium-230 and Thorium-232. Chemical
recovery was determined by the use of a Thorium-229 tracer. Activity of the Thorium-229 tracer was
determined by alpha spectroscopy using an energy specific region of interest.
Samples demonstrated acceptable results for all Thorium analyses. Chemical recovery was acceptable for
all samples. The Thorium-228, Thorium-230 and Thorium-232 method blank demonstrated acceptable
results. Results for the Thorium-228 duplicate demonstrated an acceptable relative percent difference and
normalized difference. Results for the Thorium-230 and Thorium-232 duplicate demonstrated a high
relative percent difference; however, normalized difference is within acceptable limits for the analytical
technique. Results for the Thorium-228, Thorium-230 and Thorium-232 laboratory control sample
demonstrated an acceptable percent recovery.
RADIUM-226
fractions were acidified with HN03 . All samples were prepared by mixed acid digestions as appropriate.
This was followed by selective sulfate precipitations of the Radium. Samples were then mounted by
semi-micro-precipitations onto micro-porous filters. Samples were counted by alpha spectroscopy using
an energy specific region of interest for Radium-226. Chemical recovery was calculated by the use of a
Barium-133 tracer, which was determined by HPGe gamma spectroscopy.
Samples demonstrated acceptable results for all Radium-226 analyses. Chemical recovery was acceptable
for all samples. The Radium-226 method blank demonstrated acceptable results. Results for the Radium226 duplicate demonstrated a high relative percent difference; however, normalized difference is within
acceptable limits for the analytical technique. Results for the Radium-226 laboratory control sample
Page 2 of3
S&17
ANALYTICAL RESULTS CONTINUED

RADIUM-228
Following alpha spectroscopy analysis of Radium-226, Barium/Radium Sulfate precipitates were
redissolved and allowed for sufficient ingrowth of the Actinium-228 daughter. After ingrowth, Actinium228 was selectively precipitated. Precipitates were filtered and beta emissions for Actinium-228 were
then counted on a gas proportional counter. Chemical recovery was determined by the use of a Barium133 tracer, the activity of which was determined by HPGe gamma spectroscopy and an elemental Yttrium
carrier by gravimetric measurements. The product of these two recoveries was used to calculate chemical
yield.
Samples demonstrated acceptable results for all Radium-228 analyses. Chemical recovery was acceptable
for all samples. The Radium-228 method blank demonstrated acceptable results. Results for the Radium228 duplicate demonstrated a high relative percent difference; however, normalized difference is within
acceptable limits for the analytical technique. Results for the Radium-228 laboratory control sample
CERTIFICATION OF ACCURACY
I certify that this data report is in compliance with the terms and conditions of the Purchase Order, both
technically and for completeness, for other than the conditions detailed above. Release of the data
contained in this hard copy data package has been authorized by the cognizant project manager or his/her
designee to be accurate as verified by the following signature.
M.R. McDouga I
Laboratory Manager
Date: 5/7/2013
Eberline Analytical wants an
' rages your feedback regarding our performance providing radioanalytical services. Please
visit http://www.cberlincserviccs.com/clicnt.htm to provide us with feedback on our services.
Page 3 of3
SECTION IV
ANALYTICAL RESULTS SUMMARY
fiilS

Lakewood, CO 80235
Client Sample ID
Q:)
~:;!;'
f')
Lab Sample ID
Analysis Date/Time
Analvte
LCS13-04053-01
LCS13-04053-01
LCS13-04053-01
LCS13-04053-01
LCS13-04053-01
LCS 13-04053-01
LCS13-04053-01
LCS13-04053-01
13-04053-01
13-04053-01
13-04053-01
13-04053-01
13-04053-01
13-04053-01
13-04053-01
13-04053-01
04/25/2013 14:47:23
05/01/2013 09:51:05
04/24/2013 11 :56:35
04/24/2013 11 :56:35
04/24/2013 11 :56:35
04/24/2013 08:57:26
04/24/2013 08:57:26
04/24/2013 08:57:26
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
BLANK13-04053-02
BLANK13-04053-02
BLANK13-04053-02
BLANK 13-04053-02
BLANK13-04053-02
BLANK 13-04053-02
BLANK13-04053-02
BLANK13-04053-02
13-04053-02
13-04053-02
13-04053-02
13-04053-02
13-04053-02
13-04053-02
13-04053-02
13-04053-02
04/25/2013 14:47:25
05/01/2013 09:51:05
04/24/2013 11 :57:05
04/24/2013 11 :57:05
04/24/2013 11:57:05
04/24/2013 08:57:27
04/24/2013 08:57:27
04/24/2013 08:57:27
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP 03 TOT DUP

DUP 03 TOT DUP
PZ-305-AI TOT DUP
PZ-305-AI TOT DUP
PZ-305-AI TOT DUP
PZ-305-AI TOT DUP
PZ-305-AI TOT DUP
PZ-305-AI TOT DUP
13-04053-03
13-04053-03
13-04053-03
13-04053-03
13-04053-03
13-04053-03
13-04053-03
13-04053-03
04/25/2013 14:47:20
05/01/2013 09:51:06
04/24/2013 11 :57:06
04/24/2013 11 :57:06
04/24/2013 11 :57:06
04/24/2013 08:57:56
04/24/2013 08:57:56
04/24/2013 08:57:56
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
13-04053-04
13-04053-04
13-04053-04
13-04053-04
13-04053-04
13-04053-04
13-04053-04
13-04053-04
04/25/2013 14:47:22
05/01/2013 09:51:06
04/24/2013 11 :57:07
04/24/2013 11 :57:07
04/24/2013 11 :57:07
04/24/2013 08:57:57
04/24/2013 08:57:57
04/24/2013 08:57:57
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
TOT
TOT
TOT
TOT
TOT
TOT
TOT
TOT
~EBERLINE
SERVICES
Final Report of Analysis

Date: 5/7/2013
Page 1 of 3
Project: West Lake OU-1

SDG: 1304053
Received: 04/09/2013
Matrix: Water
Method
Result
Error
MDA
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
10.49
9.95
6.21
5.40
5.82
7.52
0.61
8.23
1.16
1.12
0.92
0.82
0.87
1.06
0.22
1.14
0.14
1.52
0.10
0.08
0.07
0.07
0.10
0.07
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.00
0.56
0.04
0.14
0.00
0.06
0.07
0.08
0.00
0.59
0.06
0.09
0.03
0.06
0.07
0.06
0.05
1.20
0.11
0.08
0.08
0.09
0.07
0.06
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.49
1.21
0.21
0.47
0.15
0.44
0.04
0.55
0.23
0.61
0.13
0.18
0.10
0.20
0.07
0.22
0.14
1.17
0.14
0.09
0.08
0.12
0.10
0.13
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
1.13
3.02
0.24
0.26
0.19
0.69
0.09
0.79
0.37
0.66
0.13
0.13
0.11
0.27
0.11
0.29
0.16
1.10
0.13
0.11
0.08
0.14
0.16
0.09
I EBERLINE
ANALYTICAL CORPORATION
601 SCARBORO ROAD OAK RIDGE, TN 37830
865/481-0683
FAX 865/483-4621
Qualifier
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
u
u
u
j
u
u
u
j
j
j
j
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
Analysis Date/Time
Analyte
13-04053-05
13-04053-05
13-04053-05
13-04053-05
13-04053-05
13-04053-05
13-04053-05
13-04053-05
04/25/2013 14:47:35
05/01/201312:01:55
04/24/2013 11 :57:08
04/24/2013 11 :57:08
04/24/2013 11 :57:08
04/24/2013 08:57:58
04/24/2013 08:57:58
04/24/2013 08:57:58
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP 03 TOT
DUP 03 TOT
DUP 03 TOT
DUP 03 TOT
DUP 03 TOT
DUP 03 TOT
DUP 03 TOT
DUP 03 TOT
13-04053-06
13-04053-06
13-04053-06
13-04053-06
13-04053-06
13-04053-06
13-04053-06
13-04053-06
04/25/2013 14:47:31
05/01/201312:01:55
04/24/2013 11 :57:09
04/24/2013 11 :57:09
04/24/2013 11 :57:09
04/24/2013 08:57:59
04/24/2013 08:57:59
04/24/2013 08:57:59
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
DUP 03
DUP 03
DUP 03
DUP 03
DUP 03
DUP 03
DUP 03
DUP 03
13-04053-07
13-04053-07
13-04053-07
13-04053-07
13-04053-07
13-04053-07
13-04053-07
13-04053-07
04/25/2013 14:47:33
05/01/2013 12:01 :56
04/24/2013 11 :57:10
04/24/2013 11 :57:10
04/24/2013 11 :57:10
04/24/2013 08:58:00
04/24/2013 08:58:00
04/24/2013 o8:58:00
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
13-04053-08
13-04053-08
13-04053-08
13-04053-08
13-04053-08
13-04053-08
13-04053-08
13-04053-08
04/25/201314:47:27
05/01/2013 12:01 :56
04/24/2013 11 :57:25
04/24/2013 11 :57:25
04/24/2013 11 :57:25
04/24/2013 08:58:01
04/24/2013 08:58:01
04/24/2013 08:58:01
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
PZ-305-AI
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DIS
DUP 04 TOT
DUP 04 TOT
DUP 04 TOT
DUP 04 TOT
DUP 04 TOT
DUP 04 TOT
DUP 04 TOT
DUP 04 TOT
I!~
;;,
..,,)
~
Method
Lab Sample ID
Client Sample ID
2J
~EBER!,....INE

Date: 5/7/2013
Page 2 of 3

SDG: 1304053
Matrix: Water

Lakewood, CO 80235
Result
Error
MDA
0.27
0.11
1.54
0.11
0.10
0.08
0.11
0.09
0.09
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.01
0.13
0.06
0.44
0.15
0.59
0.16
0.76
0.05
0.10
0.06
0.18
0.11
0.21
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.73
0.73
0.16
1.47
0.06
0.59
0.05
0.82
0.26
0.77
0.10
0.36
0.06
0.19
0.06
0.23
0.17
1.56
0.10
0.09
0.09
0.07
0.08
0.06
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.21
0.90
0.03
0.08
-0.01
0.97
0.10
0.79
0.15
0.68
0.05
0.07
0.03
0.28
0.10
0.25
0.14
1.36
0.09
0.07
0.07
0.09
0.14
0.11
0~
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
0.79
1.98
0.29
0.33
0.28
0.28
0.11
0.36
0.11
1.31
0.08
0.07
0.08
0.12
0.15
0.13
0.72

865/481-0683
0.72
0.14
0.15
0.13
0.16
0.12
0.18
FAX
865/483-4621
Qualifier
Units
u
u
pC~
~~
pC~
~~
pC~
pC~
~~
pC~
~~
~~
pC~
pC~
~~
pC~
pC~
~~
~~
pC~
~~
~~
pC~
~~
pC~
~~
pC~
pC~
~~
pC~
pC~
~~
~~
~~

Lakewood, CO 80235
Client Sample ID
DUP 04 DIS
DUP 04 DIS
DUP 04 DIS
DUP 04 DIS
DUP 04 DIS
DUP 04 DIS
DUP 04 DIS
DUP 04 DIS
;;,
t~~
!'\)
11'1,)
Lab Sample ID Analvsis Date/Time
Analvte
14:47:29
12:02:02
11 :57:26
11 :57:26
11 :57:26
11 :55:55
11:55:55
11 :55:55
Radium-226
Radium-228
Thorium-228
Thorium-230
Thorium-232
Uranium-234
Uranium-235
Uranium-238
13-04053-09
13-04053-09
13-04053-09
13-04053-09
13-04053-09
13-04053-09
13-04053-09
13-04053-09
j/JEBERLINE

SDG: 1304053
Matrix: Water
SERVICES
04/25/2013
05/01/2013
04/24/2013
04/24/2013
04/24/2013
04/24/2013
04/24/2013
04/24/2013
Method
E903.0
E904.0
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
HASL 300,
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2
4.5.2

Date: 5n/2013
Page 3 of3
Result
Error
MDA
0.27
0.53
-0.01
0.05
0.05
0.31
0.08
0.32
0.16
0.74
0.04
0.06
0.06
0.14
0.08
0.14
0.11
1.53
0.09
0.09
0.08
0.09
0.09
0.07

865/481-0683
FAX
865/483-4621
Qualifier
u
u
u
u
u
Units
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
pCi/1
SECTIONV
ANALYTICAL STANDARDS
, ...
'
OA/OC REVIEWED CERTIFICATE OF CALIBRATION

~q(lnitialsA ALPHA STANDARD SOLUTION
Date
Radionuclide:
Half Life:
(4.468
Catalog No.:
Source No.:
.....
0.005) x
OR2778
P.O.No.:
Reference Date:
January 11995
12:00 PST.
Contained Radioactivity: (Total U) 8.016 p.Ci
Contained Radioactivity: (Total U) 297 kBq
10"9 years
7338
479-50
Description of Solution
a. Mass of solution:
b. Chemical form:
c. Carrier content:
TMAEBERLINE
Customer:
U-238NAT
..~ . ~ ....
. ,. .
.........
,...
65.2896 gin a 50 ml flame sealed ampoule

Uranyl Nitrate in H20
None
Approximately 1.3202
d. Density:
Radioimpurities
,: "~
Refer to attached technical data sheet
.-~
Radioactive Daughters
Refer to attached technical data sheet
Radionuclide Concentration
(Total U) 0.1228
Method of Calibration
....
I'Cilg.
:;..;:.'
Activity calculations are based upon known specific activity and mass .
.:;
. ....
,..
...
.:~.:
Uncertainty of Measurement
a. Systematic uncertainty in instrument calibration:
b. Random uncertainty in assay:
c. Random uncertainty in weighing(s):
d. Total uncertainty at the 99% confidence level:
3.0%
0.0%
2.0%
3.6%
NIST Traceability
This calibration is implicitly traceable to the National Institute of Standards and Technology.
Leak Test(s)
See reverse side for Leak: Test(s) applied to this source.
Notes
:, ..
:.~
!.":.
1. Nuclear data were taken from "Table of Radioactive Isotopes, edited by Virginia S. Shirley, 1986.
2. IPL participates in an NIST measurement assurance program to et.tablish and maintain implicit traceability for a number of nuclides,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
"' .::'
e(J.Iv~
YCONTROL
!:
:.
~~ .:
:.;:
i
'
:.
"
C?euv1h31k t~f
Date Signed
..,:
ISOTOPE PRODUCTS LA BORATORIES
: ..
3017 N. SAN fERNANDO
BLVD.
BURBANK, CALIFORNIA
91504
818 8437000
818 843 6168
!:_:: .. ,_,.:
,..
FAX
., ...
:!
'":;.
<"""
. ':'
::.;.
.. '
~ ~ ..
..;;
;"'
........ ,;:-....
~ I;:_J;I ~R l, IN I
E;
QUALITY CONTROL PROGRAM

MP-009
S~Rvaee:$
Rev.8; 11/01/03
Title: Radioactive Reference Standards Solutions & Records
EBERLINE SERVICES -OAK RIDGE LABORATORY
RADIOACTIVE REFERENCE SOLUTIONS
PRIMARY DILUTION RECERTIFICATION
MP009
.9/6/2012 O:OOJ
CURRENT DATE!
SOLUTION #I < ' , U;;a> ..
I
Half Life, Daxs
1.632E+121
SOLUTION REFERENCE #IIPL 479~50

Principal Radlonuclide
Half Life, Years
2
~~; ~u . .l
l'<.4.466E+09l
Radionuclide l.:23~~2~o;..:~u
Certified Activity </8:016E+OO iJ.CI
Certified Concentration L.:<>, :. , iJ.Ci per gram
Ampoule /Solution Gross
Empty Ampoule
Solution Net
Total Activity In Ampoule
Reference Date!. 'd/111'99'5
. >'.
97,6400
32:5020
65.1380
'8.0160
Chemical Composition of Standard Solution

l~ranY.Fn~r~te.Jrfdil'4e.HNQi ; :. : ::\:>):
Dilution Instructions:
o:ool
Weight, Grams
Weight, Grams
Weight, Grams
J.tCi
; / , .......c
,c.
.''
Dilution Solvent Used
I1MHN()3 \
.. ..
...
..... ,.:.\:..
Dilute to a volume of! 1000.00 ...jmlllillters

Certified Total Activity ofl
. 8:0160iiJ.Cl
Which Eauals
1.780E+07ldpm at the date listed above
This activity concentration is based on the original

And after dilution the activity of this solution is I 1.77955E+04ldpm/m&-eterence date listed above. All activities are corrected
to the date and time of analysis by the laboratory data
processing software.
Expiration Date:! Seetember6, 2013
rVerified & Approved By

QCApproval
~
1'-~ ~.
~rn (
"
\I
Date:
9126/2012 0:00
Date:
1tUtl'"2-
~~~~0!1;1 QUALITY CONTROL PROGRAM

MP.009
Rev.8; 11/01/03
EBERLINE SERVICES- OAK RIDGE LABORATORY

RADIOACTIVE REFERENCE STANDARD SOLUTIONS
SECONDARY DILUTION RECERTIFICATION
MP-009
Solution Reference#IIPL479~50
Principal Radionuclide
Half Llfe1 Years
2~;~238u
Referenee Date
-,;_.
<
u~aa
. t
Radionucllde of lnteresd :- ~~ 23~~ ~U J

Parent Solution Conc.I1~7796E+04 dpm/ml
Chemical Comeosltlon of Standard Solution
">
Half Life1 Da~s

. . t.632E+12I
''4~4sae~o91
Iuranty Nitrat~ trJ tJI HN03.. < ..
9/6/2012 0:00J
DateL
Solution#(
.. >
11111995 o:oo
.. . . I
I1M.HNo; ..
.I
..
SECONDARY VOLUMETRIC DILUTION

Vol. Parent Solution: -~ :. :.";. : .. 4:0000 ml
Total Activity: . 7.1182E+04 dpm
. . 1000:00 ml
Final Volume:
:"
Final Activity Concentration:!

reference date listed above. All activities are
corrected to the date and time of analysis by the
hahnrJ tory data processing software.
NOTES:
Isotopic Distribution as:
U-238 Atom % 48.239
U-235 Atom % 2.25
U-234 Atom%= 49.501
All values +/- 3.6%
=
=
7.1182E+011 dpmlml
U-238 = 71.182 dpm/ml X 0.48249 .. 34.345 dpm/ml

U-235 = 71.182 dpmlml X 0.0225 1.602 dpmlml
lJ..238 = 71. 182 dpm/ml X 0.49501 = 35.236 dpm/ml
Expiration Date:l Septemr6, 2013

Isotopic ratios from manufacturer's data sheet
f\
~~.
Verified & Approved y
QCApproval
1,---....
5tl1l.Alll
1 1\
"
Date:
9/26/2012 0:00
Date:
!IUP/rz-
~-".'":
.. ..:."?!!
.RECORD COPY
Tracer Solution for Environmental Analysis & Disequilibrium Studies
,:
Product Description & Measurement Certificate

Product code: UDPl 0050
Batch Number. 921232/67
Description
Principal radionuclide:
Daughter Nuclide:
Measurement
Reference date:
Radioactive concentration U-232
which is equivalent to
01 March 2000
6. 739E+03 becquerels per gram of solution
1.821E-Ol microcuries per gram of solution
Volume of solution
Total activity ofU-232
which is equivalent to
5.035 millilitres
3.61E+04 becquerels
9.76E-ol microcuries
Accuracy
Radionuclidic
Purity
uranium 232 (U-232)

Th-228
Method ofmeasurement (see reverse of this certificate)

Random uncertainty is: 0.7%
Systematic uncertainty: 0.5%
Overall uncertainty in the radioactive concentration quoted above: I. 7%
Overall uncertainty is defined on the reverse of this certificate.
Any radioactive impurities measured are listed below, expressed as percentages
of the activity of the principle radionuclide at the reference date .
Th-228 and daughter activity removed 2 Feb 2000
U-232 daughters activity will increase with time. By alpha 88% U-232, 12% daughters on 1/3/00
Isotopic
Purity
'T'"ne isotopic composition, exprP.ssed as atom per cent at the reference date .
l~Ot measured
Chemical
Composition
Calculated weight ofU-232, 4.42E-08 grams, as 2M HN03 solution in a flame sealed glass vial.
This Tracer solution has been produced 'carrier free'.
Physical
Data
Recommended half life of uranium 232: 6.980E+Ol years

Principle energies of alpha emissions (MeV): 5.263 31. 7%, 5.320 68.00/o
Branching ratio for alpha emission: 100%
Calculated specific activity of uranium 232: 8.167E+05 Bq per microgram U-232.
Remarks
For safety information and notes to ensure correct usage by all persons handling this radio~ive Tracer
solution please read the instructions accompanying the package.
AEA Technology operates a quality management system which has been independently audited and
approved to ISO 900 l.
Approved
Signatory
Project Ref. AE231S
Roger Wiltshire
Prepared and characterised in the UK, for world wide distribution by Isotrak, AEA Technology, QSA.
Trkcert.wps 10103/00
AEA Techmlogy is the trading name of AEA Technology pic

MP.009
Rev.8; 11/01/03

PfflMARYD~UTIONRECERTIRCATION
MP009
IHal~~~b~;1j
c.~:=l ~~~:O:l,,.CI
Certified Concentration
< <
'
IHalf Life,
Refarence
~ft~E+04I
oatel. .3/112ooOO:Ool
JJ.CI per gram
Ampoule /Solution Gross~

. ; ... . . . Weight, Grams
Empty Ampoule . . .. . ... Weight, Grams
Solution Net . . .. . Weight, Grams
0.9760 J.LCI
Total Activity in Ampoule
Dilute to a volume off'
Certified Total Activity off
I2MHNOq
" " ... 3 ....
-;....
. -.:,,.
:.. :..:,_.
....,
1000.00 >.fmilliliters
... . 0.9760fJJ.CI
Which Eauals
j 2.167E+06fdpm at the date listed above
And after dilution the activity of this solution Is I2,167E+03fdpm/ml

reference date listed above. All activities are corrected
Expiration Date:f December 7, 2013
Date:
Date:
12/13/2012 0:00
eji3//':J/
ii
~EE!~!NE I QUALITY CONTROL PROGRAM

MP..IJ09
EfltVICC::&
Rev.a: 11/01/03
Title: RadiOactive Reference Standards Solutions & Records

SECONDARY DILUTION RECERTIF/CA TION
MP-009
Solution Reference # AEA!Amersham 921232/67
Principal Radionucllde
Half Life, Years
232
.
0 . I
1.. 7.200E+01l
121712012 0:001
Date I
Solution #I . < u~1oa
I
...
Radlonuclide of lnteresj .;~~u

Parent Solution Cone. <2.167E+03: ldpm/ml
Half Life, DaX!
I ... . . . 2.630E+04]
Reference Datel : .....
Chemical Come2sitlon of Standard Solution

. .... ..:.. . < ... ... ..
l2!f2U(N03)e:in"2M HNOs
3/112ooo
:o:oo I
.I
;
j2MHNO:..:
..
.. 3 . :.. \
: .:~
:..:
. .. . ,..
_
,.

Vol. Parent Solution:
Total Activity:
Final Volume:
.. 10.0000 ml
2.1670E+04 dpm
... 1000~00 ml
2.1670E+01Idpm/ml

laboratory data processing software.
NOTES:
Expiration Date:l December 7. 2013
C"~
l\
~
r~~tl tJAJl< ~\
Verified & Approved By
QC Approval .
..t
---
Date:
Date:
12113/2012 0:00
laf1t2::
r
RTIFICATE OF CALffiRATIOfl.\\f ~ ,9"1,

LPHA STANDARD SOLUTION" rue' it"Get\\\\\\
TMA EBERill..,,~,\\ \.~
Th-230
Customer:
(7 .54 0.03) x 10"4 years
7230
Source No.:
P.O.No.:
TI4944
Reference Date:
November 1 1991
Contained Radioactivity:
1.036
388-116
Desaiption of Solution
5.0042
\\\\~
12:00 PST.
14Ci.
grams.
b. Chemical form:
Th(N03)4 in O.lN HN03
c. Carrier content:
d. Density:
None added
1.0016
Radioimpurities
See attached technical data sheet
See attached technical data sheet
0.207
J4Cilgram.
Weighed aliquots of the solution were assayed using a liquid scintillation counter.
c. Random uncertainty in weigbing(s):
2.0%
0.5%
0.2%
2.7%
NIST Traceability
Notes
1. Nuclear data wete taken from "Table of Isotopes", Sevendt Edition, edited by Virginia S. Shirley.
2. IPL participates in an NIST measurement assurance program to establish and maintain implicit
traceability for a number of nuclides, based on the blind assay(and later NIST certification) of
Standard Reference Materials. (As in NRC Regulatory Guide 4.15)
ISOTOPE PRODUCTS LABORATORIES

1800 No. Keystone Street.,
Burbank, California 91504
818 843 - 7000
2J
E
~
EJ E RLI N._t;;
SERVO<>$
I QUALITY CONTROL
PROGRAM
MP-009
Rev.S; 11/01/03
EBERLINE SERVICES OAK RIDGE LABORATORY

MP-009
Solution Reference# IPL ~116 :
Half Life, Years
j7054oE+041
Radlonucllde of lnteres............~""
Parent Solution Conc.L.;..;.;::;.;;.::.::....:.=;.;.;;;;.(dpm/ml

Vol. Parent Solution: < Ao;oooo ml
Total Activity: 2,2999E+04 dpm
Final Volume: . > :fOOO~OO ml
Final Activity Concentration:!.
2.2999E+01ldpmlml

NOTES:
Expiration Date:
Recertified
Date:
Date:
QCApproval
Date:
March 4, 2014
3121/2013 0:00
j~t'~
~t;~.-\(1/
&831

MP-009
Rev.8; 11/01/03

MP009
CURRENT DATE I
3/412013 O:OQJ
SOLUTION REFERENCE #r:-:IP=t..-:::3~8=a.:.~t1':":6l"'"'....,:. ,. .... :.-.:,-:.........-.. . . . .,.,.. SOLUTION #l < . Th~t.' .< >I
2
. :iltfh 'I
Half Life, Years
Half Life, Days

2:754E+07l
I i t540E+'c>4l
, ... . .....
Radionuclide L}~lltinurn
Certified Activity \'-'t;036Et(l0 JA.CI
Certified Concentration 1 ' . : '\ ::. < ' J.&Ci per gram
Reference Date!
. .
'11/1)199to:ool
Ampoule /Solution Gross .. . < 9.2660 Weight, Grams

Empty Ampoule I\< 4:6218 Weight, Grams
Solution Net
. 4~6442 Weight, Grams
Total Activity In Ampoule .. 1.0360 1-1Ci
Dilute to a volume ofl
Certified Total Activity ofl
tooo;oo:
1.0360\~J.Ci
>I milliliters
Which Eauals
2:300E+06l dpm at the date listed above

This activity concentration Is based on the original
And after dilution the activity of this solution is I 2.300E+03Idpmlml reference date listed above. All activities are corrected
Expiration Date:
Date:
Date:
March 4, 2014
3/21/2013 0:00
--~;.....;..;...;..;......;;...__
;/'J-1 fr 3 _ _
-7~-,f-1-...__
&ii32
1h-8
CERTIFICATE OF CALffiRATION
ALPHA STANDARD SOLUTION
TMA EBERLINE
Customer:
VH1632
P.O.No.:
Reference Date:
November 1 1993
12:00 PST.
(fh-232) 0.0933
~i.
(Th-232) 3.45
kBq.
Radionuclide:
Th-232
HalfLife:
(1.~05 0.006) x 10"10 years
Catalog No.:
7232
Source No.:
435-104-2
b. Chemical form:
c. Carrier content:
d. Density:
11.9712 g (in a 10 ml flame sealed ampoule)

Th(N03)4 in water
None added
Approx. 1.21
g/ml
@20~C.
None detected (other than daughters).
Radioimpurities
Ra-228, Ac-228, Th-228, Ra-224, Rn-220, Po-216, Pb-212, Bi-212,Po-212, Tl-208
(Th-232) 0.00779
~-tCilg.
Activity calculations are based upon known specific activity and mass.
3.0%
0.0%
2.0%
3.6%
NIST Traceability
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data \Vere iat:en from "'rable ofR.adioactive Isotopes", edited by Virgiiua S. Shirley, . l986.
2. IPL partic~tes in an NIST measurement assurance program to establish and maintain implicit traceability for a number of nucli~,
based on the blind assay (and later NIST certification) of Standard Reference Materials (As in NRC Regulatory Guide 4.15).
QUALITY CONTROL
AltiV . <L ! "! 9 "$
Date Signed
1800 North Keystone Street
818 843 - 7000
ii33

MP-009
Rev.8; 1/10/03
TiUe: Radioaclive Reference Standards Solutions & Records

PRI~RYD~UTIONRECERTIRCATION
MP009
CURRENT DATEf > 10/9120120:001
SOLUTION REFERENCE #r:-:1P::-:,J;:=:.:.4"""'S"""S::.=.t04=.
' ...=}2"""." ". ...~=," ".;:-i" "<e"-" '-.:.;:,;~y;~:U
SOLUTION #177?0?;
tn~''':'.J'" /\'1
Principal Radlonucllde
Half Life, Years
Half Life, Days
.':?~?TR.??tft{l
nuAj::4o5.E't'iol
>
;
5.132E+12l
Radionuclidel :,;;:7':':':'::\T":':I:fu'j:
Certified Activity ):'i.i/91$3()E:i!Qt J.LCi
Certified ConcentrationF~'>'If'ii J.LCi per gram
Ampoule /Solution Gross X::>!1Si$t5 Weight, Grams
Empty Ampoule 3;y;;:;;6.~929El Weight, Grams
Solution Net.; 11;9119 Weight, Grams
Total Activity in Ampoule <: ,Q:osas J.LCi
Dilute to a volume ofl<h':'lOOO:OO\<'>Imllllllters
Certified Total Activity ofl.
;: Oi0933lJJ.Ci
Which Eauals
I' ' :: :2;071E+o5ldpm at the date listed above
And after dilution the activity of thl$ $Oiution l$1 '2;071 E+02Idpmlml

Expiration Date:l
Otober9,:2013
Date: _ _10/9/2012 0:00
.;..;;:;;.:=;.;.;;;;..~.;..
Date: _..~., /~
,J,I....._'I_ _
I f
(EBERI...lh!E
SttRVICI;.S
PROGRAM
I QUALITY CONTROL
MP-009
Rev.B; 1110/03
TIUe: Radioactive Reference Standards Solutions & Records

MP-009
Solution Referenee t#IIPL 436~1~2
Half Llfe1 Years
us&232Th
.....
Datel . 11/9/2012 O:OOj

Solution #I <. Tthab ' I
Half Life1 Da~s
I . . 5.132E12l
I r.4osE1ol
Radlonuclide of Interest[ 2284 ~Ttl ..

Parent Solution Conc.L ' 2:07E+02 ' dpm/ml
Reference Date
Chemical Come2!1tlon of Standard Solution
1Th(N03)4 in 1% HN03
<
<
.. . ..
I<
.f111i1993:o:oo I
I
j1% Nitric Acid'
. I

Vol. Parent Solution: ... . soo;oooo ml
Total Activity: 1.0365E+05 dpm
Final Volume: . 1000;00' ml
1.0356E+02Jdpm/ml

NOTES:
Expiration Date:
Vorif~ed&Approved ~ ~
QCApproval
-~jJJ
~\t'llt t[j""'
vvr
v
~v
Date:
Date:
I . October 9, 2013 I
1119/2012 0:00
1\
t.,_ I 1'1I
Isotope Products
Laboratories
An Eckert & Ziegler Company
7J, l8
24937 Avenue Tibbitts

Valencia, California 91355
Tel 6613091010
Fax 6612578303
CERTIFICATE OF CALIBRATION
ALPHA STANDARD SOLUTION
Radio nuclide:
Half-life:
Catalog No.:
Source No.:
Th-229
7340 160 years
Customer:
P.O. No.:
Reference Date:
(Th-229 only)
7229
867-54
EBERLINE SERVICES
00009633
15-Jan-02 12:00 PST

1.013
JlCi
37.48
kBq
Physical Description:
A.
B.
C.
D.
Mass of solution:
Chemical form:
Carrier content:
Density:
5.0147 g in 5 ml flame-sealed ampoule

Th(N03)4 in 0.1 M HN03
10~9 Th/mL
1.0016 g/ml @ 20C.
Radioimpurities:
None detected (daughters in equilibrium)
Radionudide Concentration:
0.2020
!JCVg,
kBq/g
7.474
Method of Calibration:
This source was prepared from a weighed aliquot of solution whose activity in !JCi/g was determined
using gamma ray spectrometry.

193.5 keV
Peak energy used for integration:
Branching ratio used:
0.0441 gammas per decay
Uncertainty of Measurement:
A. Type A (random) uncertainty:
B. Type B (systematic) uncertainty:
0.7%
3.0%
C. Uncertainty in aliquot weighing:

D. Total uncertainty at the 99% confidence level:
0.0%
3.1%
Notes:
- See reverse side for leak test(s) performed on this source.
- IPL participates in a NIST measurement assurance program to establish and maintain implicit traceability
for a number of nuclides, based on the blind assay (and later NIST certification) of Standard Reference
Materials (As in NRC Regulatory Guide 4.15).
- Nuclear data was taken from IAEA Technical Report Series No. 261.
- This solution has a working life of 5 years.
Quality "Control
Date Signed
IPL Ref. No.:
867-54
- - - - - - - - - - - - - - - - - - 1509001 CERTIFIED - - - - - - - - - - - - - - - - - -
Medical Imaging Laboratory

24937 Avenue Tibbitts
Valencia, California 91355
Industrial Gauging Laboratory

&&36

MP..009
Rev.8; 1/10103


MP009
CURRENT DATEl.
SOLUTION REFERENCE #I...11P__L_S_67-~54,..,._ -_--..,..--.....,
SOLUTION #I
Half Life, Years

7.340E+03I
<
11/9/2012 0:001
Th~18
.
I
Half Life, Days

2.681E+06I
. ~ I
I .. .
RadlonucHdol ', , !29"fii ;<
Reference Date
I . 1h5/2002o:ool
Certified Activity . f.013E+OO ~CI

Certified Concentration ; > ~CI per gram
<
Ampoule /Solution Gross, . . 8.7752 Weight, Grams

Empty Ampoule
3. 7591 Weight, Grams
Solution Net
5.0161 Weight, Grams
Total Activity In Ampoule
1.0130 ~CI
229fh(NO')'iri 0.'1MHNo? . ...

. . . ....3 4 .. . ..... :.! . .
1
. ..
..
.. .. .
.... . I
Dilute to a volume ofl .1000.00 !milliliters

Certified Total Activity of! -.1.0130I~Ci
Which Eauals
2~249E+06!dpm at the date listed above

And after dilution the activity of this solution is 1 2.249E+03jdpm/ml reference date listed above. All activities are corrected
Expiration Date:l 'October 9, 2013 ]
~----=d~=~~~---
Verified & Approved By __

QC
Approvat_~+--~A~~-----~...w.A~UQ.IIU~v-1.,-N_ __
'--""
Date:
Date:
__
__
11/9/2012 0:00
_,;,....;..___,;,.
u/rz/tz...
--:.:t,.......,,
.......___
~EB.ERL.!NE I QUALITY CONTROL PROGRAM

MP.009
5E.RVICS
Rev,7; 9129199
Title: Radloacuve Reference Standards SolUtions & Records

MP-009
Solution Reference# IPL86.7;.s.4 .
Half Life, Years
2
~hl
7.34oE+o31
11/9/2012 0:001
Date[
Solution #I . . . Th~18a
I
Half Life, Daxs
2.681E+oal
Radionucllde of lnte:j . .. ~
Parent Solution Cone. 2.25E+03 ldpm/ml
Reference Date!.: .. 1/15/2002 O:Oo
Chemical Comf!2!1tlon of Standard Solution
jTH(NOs)41n 0.1 MHN03
.. .. .... . . > . . . .. . ..
I
I
jo.1MHNO
... ... . . 3 .
SECONDARY VOLUMEmiC DILUTION

Vol. Parent Solution:
Total Activity:
Final Volume:
10.0000 ml
2.2490E+04 dpm
1000.00 ml
2.2490E+01Idpmlmt

NOTES:
Expiration Date:l
QC
~~~
Approval~'
J L
---::"""
~~
"'V__
October 9, 2013
Date:
11/9/2012 0:00
Date:
ult~L-zr i
j}attonal 3Jn~tttute of
i>tanbatb~
& ~ecbnologp
<ttrttftcate''
:
..
-~:
.-i.L7.:
Standard Reference Material 4251C

Barium-13~ Radioactivity Standard
This Standard Reference ~at~rial {SRM) consists of radioactive barium-133. cJ;Uoride, non':":radioactive barium
chloride, and hydrochloric acid diSsolved in 5 mL of distilled water. The solution is contain~d in a flamesealed NIST borosilicate-glass ampoule. The SRM is intended for the calibration of ionization' chambers and
solid-state gamma-ray 1spectrome1fY .systems.
Radiological Hazard
The
ampoule contains barium-133 with total activity of approximate~ 2.5 MBq. Barium-133 decays
.by electron capture and during *e decay process X-rays and g~a;rays with energies from 4. tp 400 keV are
emitted. Most of these photons escape from the SRM ampoule and can represent a radiati9n hazard.
Approximate unshielded dose rates at several distances (as of the reference time) are given in note [a]*.
Appropriate shielding and/or distance should be m;ed to minimize, personnel exposure., ,The ,SRM $hould be
}~Se!;l only by persons qualified to han?Ie radioactiv~ material.
'
SRM.
'a
Chemical Hazard
The SRM ampoule c~:mtain~,hydr~chloric acid (HO) with a concentration of 1 mole per liter,.o(.water. The
solution is corrosive and represents a health hazard if it comes in contact with,. eyes or skin. If. the ampoule
is to be opened to transfer the solution, the recommended procedure is given on page 2.
ampoule should
be opened only by person,s qualified to handle both radioactive material and strong R;cid solution.
The
Storage and Handling

The SRM should be stored and used at a temperature between 5 and 65 C. The solution in an unopened
ampoule should remain stable and homogeneous until at least June 2004.
The ampoule (or any subsequent container) should always be clearly marked as containing radioactive
material. If the ampoule is transported it should be packed, marked, labeled, and shipped in accordance with
the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous
good (hazardous material) both because of the radioactivity and because of the strong acid.
Preparation
This Standard Reference Material was prepared in the Physics Laboratory, Ionizing Radiation Division,
Radioactivity Group, J.M.R Hutchinson, Group Leader. The overall technical direction and physical
measurements leading to certification were provided by LL. Lucas of the Radioactivity Group and D.B. Golas,
Nuclear Energy Institute Research Associate.
The support aspects involved in the preparation, certification, and issuance of this SRM were coordinated
through the Standar<! Reference Materials Program by N.M. Trahey.
Gaithersburg, Maryland 20899
October 1994
Thomas E. Gills, Chief

Standard Reference Materials Program
*Notes and references are, on pages ~ and 6.

QCP-009
Rev.8; 11/10103
TIUe: Radioactive Reference standards Solutions & Records

PRIMARYD~UTIONRECERTIRCATION
QCP009-1
CURRENT DATEL
9/201201.2 0:001
SOLUTION REFERENCE #r:"tii::':".:IS=:r~<S~RM~
.....~4~.25::"!1~C~)~:. "1""
..;.,....,\...,.':"""'.\I
SOLUTION #F> i' ?~;aa~:Ci'\ /;"c:il
Half Life, Years
Half Life, Days
J~aarfoitF\1
!. . . ~.s2ee+oal
In :1:b48.gt6il
Radlonuclide ~ '~B'~i;iUmH:
Certified Activity H2;::!Z
J.LCI
Certified Concentration ' ~t:31:6E+01; J.LCi per gram
Ampoule /Solution Gross };:?,.i9lat Weight, Grams
Empty Ampoule '~?~~Di';i:4t2$82 Weight, Grams
Solution Net '. > 5;0499 Weight, Grams
66~5577 J.LCi
Dilute to a volume otb':/.A.OOO:oo:):;:.jmllllliters
Certified Total Activity of!

A d
66.5577IJ.LCi
Which Eauals J' . 1A78E:f08)dpm at the date listed above
d.l t
h
1
1
er 1 u ton t e activity of this solution is 1,478E+ dpmlml reference date listed above. All activities are corrected
aft

Expiration Date: I 5ept$mper 20, 2013J
r
QCApproval
"'
.6tttMu1"
____,---..:
~~.
._.,
Date:
9/27/12
Date:
,I'2.,+z
Rev.B: 11/10103

Date
Solution#
Half Life, Years
1.048E+01l
9/20/12
B~a
Half Life, Days
Reference Date I
... . 911/1993 0:00 I
l1MHct..
.. ..
.I

Vol. Parent Solution: . > .. < 25:0000 ml
Total Activity:
3.6950E+06. dpm
Final Volume: : > 1000;00 ml
NOTES:
3.6950E+03ldprnlml

Expiration Date: September 20, 2013
Date: _ _ _9-./-27~/1..;.;;2--.__
Date: _ _'f....,{t_?-+/....
t Z....____
Radionuclide:
Half Life:
Catalog No.:
TMA EBERLINE
Customer:
VH1888
P.O.No.:
Reference Date:
February 1 1994
12:00 PST.
Contained Radioactivity: (Ra-226) 1.001 p.Ci.
Contained Radioactivity: (Ra-226) 37.0 kBq.
Ra-226
1600
Source No.:
b. Chemical form:
c. Carrier content:
d. Density:
7 years
7226
453-26
5.1864 g (in a 5 m1 Flame Sealed Ampoule)

Ra(N03)2 in 1 N HN03
None added
1.0318
Radioimpurities
None detected(other than daughters)
Rn-222, Po-218, At-218, Pb-214, Bi-214, Po-214, Tl-210, Pb-210, Bi-210, Po-210 and Tl-206.
Radionuelide Concentration
(Ra-226)
0.1929
p.Cilg.
Weighed aliquots of the solution were assayed using gamma spectrometry:
Energy peak(s) integrated under: 186 keV.
0.0351
gamma rays per decay.
Brancbitlg ratio(s) used:
3.4%
3.1%
0.2%
4.6%
NISTTraceability
Leak Test(s)
See reverse side for Leak Test(s) applied to this source.
Notes
1. Nuclear data were tabrt ftom "Table of Radioactive lsoropes, edited by VIrginia S. Shirley, 1986.
_
2. IPL participates in an NIST measurement assurance program to eStablish and maintain implicit traceability for a num~r of nuclides,
- --- based on:tlle liliiiinlssaHaiid later NIS'NertificationfofSfiiiidiffii-Rcference Materiiillf{As-in NRC Reguliltory-Guide 4; rs): ---
QUALITY CONTROL
/iA,. 3 199 tt
I
Date Signed
818 843 - 7000

MP009
Rev.8; 11/01/03


MP009
CURRENT DATEI
. 11/9/2012 O:OOj
SOLUTION REFERENCE #I~IP~L~4~5"""'3-=26~.........~-...,.,....,.
.-......,J
SOLUTION #I ... . .. . .. Ra.:.s . .. I
22
Half Life, Years
~Radium 1
Half Life, Days
1:aooe+oal
Radionuclide ~~R$dium :
Certified Activity 1.0.0.1 E+oo ,1
. J.LCi per gram
Reference Datel. . > 2/1]1994
O:ool
Ampoule /Solution Gross~.

. ..... . . . We~ght, Grams
Empty Ampoule .. . ... : .. Wetght, Grams
Solution Net
.
Weight, Grams
1.0010 J.LCI
j1MHN03
Dilute to a volume ofl . 1000:00 . !milliliters
Certified Total Activity ofj
1;0010IJ.LCI
Which Eauals
. 2.222E+06Idpm at the date listed above
And after dilution the activity of this solution lsi 2.222E+03ldpmlml
Verified & Approved

QC
By_~--~----t---:-1-..._~-~--
Approval_-\~c:'"".':P.aAl~.;loC..l~:.;::l:...l...._ _ _~..::::;;.__

Expiration Date:
I November 9, 2013 I
Date:
___ ___
11/9/2012
........;
Date:---"~
f,t+J~If'Z..__
I '
4:E_.. E.R1;,~~ I QUALITY~~OLPROGRAM

Rev.8; 11/01/03
Tille: Radioactive Reference Standards Solutions & Records

Date!. t1/9/2Q12 O:OOj

Solution #l)~/-;i,>URa't5b:c;'.''' :1
MP009
Solution Reference# IPL45~26:!'::/. ... :-.. ,,; : ::'/1
Half Life, Years
r~~~aafum-::1
1~,:.12b6o'E+o31
Radlonucllde of Interest _,;,~RadiumS:'.!

Parent Solution Cone. [;/?2~2'E03J<Idpmlml
. . ..,.i(.,.o"'
...... . _. ,;: ..,... 1"~;1Ag"4
- .t .;:~~, ......
v; .. o, l
te !::':'!/S:>2
Refe renee 0 a..,
Dilution Solve,rt Used

SECONDARYVOLUMEnVCD~UTION
Vol. Parent Solution: ~>{';;20YOOOO ml

Total Activity: . '4.4440E+04 dpm
Final Volume: ;::
ml
S!looo:oo.
NOTES:
I ' . '
Final Activity Concentration:

4.4440E+01Idpmlml
Expiration Date:l November 9, 20131
verified & Approved
a~-~
QC Approval
IJJJ 1 i I/ ~
V'~
Date:
11/9/2012 0:00
Date:
''
/f'z./I 1k
RA-\\
ANALYTICS
1380 Seaboard Industrial Blvd.

Atlanta, Georgia 30318 U.S.A.
Phone (404) 352-8677
Fax (404)352-2837
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
62680-416
Ra-228 5 mL Liquid in Flame Sealed Vial
This
standard
radionuclide
source
was
prepared
gravimetrically from a calibrated master solution.
The
master solution was calibrated using a germanium gamma
spectrometer system.
Radionuclide purity and calibration were checked using a
germanium gamma spectrometer system. The nuclear decay rate
and assay date for this source are given below.
ANALYTICS maintains traceability to the National Institute
of Standards and Technology through Measurements Assurance
Programs as described in USNRC Reg. Guide 4.15, Revision 1.
ISOTOPE:
Ra-228
ACTIVITY (dps) :
2.585 E3
HALF-LIFE:
5.75 years
CALIBRATION DATE:
November 7, 2001 12:00 EST
TOTAL UNCERTAINTY*:
4.0%
SYSTEMATIC:
3.0%
RANDOM:
1. 0%
*99% Confidence Level

Impurities: y-impurities (other than decay products) <0.1%
5.07198 grams 0.1M HCl solution with 50 ~g/g Ba carrier.
P 0 NUMBER
9508, Item 1 (Part #4339A)
SOURCE PREPARED BY:
. . . . . . . ~.
M. D.
Q A APPROVED:
urr1e, Rad1ochem1st

MP-009
Rev.B; 1/10/03

RECERTIFICATION
MP009
Radionuclide it:};;;'Kf;'<',Riit~h1V.(~
Certified Activity ;~;?e~~Eii02. f.l.CI

fJ.CI per gram

Ampoule /Solution Gross ~tJi:;;k~'.f}~49.a2 Weight, Grams
Empty Ampoule ,;WW:\~'~r4.6.~5. Weight, Grams
Solution Net . : :5:000'7: Weight, Grams
Total Activity in Ampoule '(( ~Oi0699 JJ.Ci
Chemical Com osition of Standard Solution
Certified Total Activity ofj;:. .
0/0699lt.tCi
Which Eauals
'''t:1;5.S1E+oqldpm at the date listed above
And after dilution the activity of thh~ solution is I<~1:551E+02 Idpmfml
This ac;tivity concentration is based on the original

Expiration Date:!> iApril12;'2013>
Date:
4/16112
-------
Date:------Date: _""'"'"LJ:~/-'-1-..~/~~-k---
SECTION VI
QUALITY CONTROL SAMPLE RESULTS SUMMARY
Eberline Services
Analysis Control Chart
Printed: 4/25/2013 S:3S AM

Page 1 of 2
Ana~
Run
UUISO
WO
13-04053
Activity U[lits . .
----i-__ J\hquot_Units____ _
pCi
Client Name
Laboratory Control Sample

Analyte
U-234
Normalized
Difference
0.99
0.46-
U-23S
csu
LCS
Measured
92.54%
1
I
Uncert.
Expected
I 15.7S% I 100.00%
-".~. 103.S3o/c ~
--~---~~
LCS
Expected
Measured
15.57%
l
--------t-
3.60%
100.00%
Known
Error
Known
S.13E+OO
2.93E-01
Result
csu
7.52E+OO : 1.19E+OO
.. --- -----1------t----+-- -- --
3.60%
7.92E+OO
2.S5E-01 I S.23E+OO I 1.2SE+OO
Standard
10
U-Sa
Standard
ACT(dpm)
Standard
Error
3.52E+01
3.60E+OO
Standard
Added (g)
5.12E-01
--- ----------,---------- -----+-!
U-Sa
3.44E+01
3.60E+OO
5.12E-01
Matrix Spike
Analyte
Normalized
Difference
MS Actual
%Rec
Expected
MS Result
Expected
MS Uncert
Actual
Actual
MSCSU
Sample
Result
Sample
csu
Sample
Aliquot
Standard
ID
Standard
ACT(dpm)
Standard
Error%
Standard
Added(g)
RepRPD
Rep NO
-I
Replicate Sample
Analyte
QCSummary
Original
Result
Original
6.S5E-01
2.72E-01
LCS Relative
Bias
LCS%R
LCSND
4.41E-01 ! 1.99E-01
0.93
OK
OK
NA
OK
5.52~~01 -rl--2.26E-01
1.04
OK
OK
NA
OK
NA
OK
Replicate
Result
csu
I
U-234
1.42
43.27
Replicate
csu
MS%R
MSND
U-23S
1.2S
35.S1
7.93E-01
2.91E-01
-------t--------, -- - - - t - - - - + - - - - - + - - U-235
;,;,
;;~
ti:
(1:)
Version
0.72
70.15
9.36E-02
1.13E-01
4.50E-02
6.90E-02
OK
OK
Eberline Services
Printed: 4/25/2013 8:38AM

Page 2 of 2
wo
,6.~tivit
UUISO
13-04053
Aliquot Units
I.}nits
pCi
Replicate Sample RPD
LCS % Recovery
130.00
L------t--- ---~1
40.00
120 00
35 00
110.00
100.00
90 00
7000
30_00
25 00
20 00
80.00
15 00
10 00
+-------------------r-----------:---------,
U-234
U-238
_L_____
73.16
111.92
92.54
80
_:::--- Mean
100
120
-UCL
Client Name
5.00
84.66
123.00
103.83
0 00
Lower E.~!?~
Upper Error
~_1)-----+
-
U-234
52.31
34.22 - - - -~-- -
U-238
U-235
42.70
28.92
116.21
------24.09
4327
. . __________
35.81
.
_j_5 ______ .. -- .-3_5________
-CL
Normalized Difference
3.50
l' _ _ _ __
3.00 +--------~
2.50
--
-----~------ --~--------
i - - - - - ---
2.00 + - - - - - - - - - - - - - - - - - - - - - - - - - - ---------
m
t!;~
f:Ji
lt.~)
Version
No Matrix Spike
-------70.15
35
-----
Eberline Services
Printed: 4/25/2013 8:33AM

Page 1 of 2
wo
Analysis
Run
Activity Units
Client Name
13-04053
ThiSO
pCi

Analyte
Nonnalized
Difference
TH-228
1.89
TH-230
'
TH-232
1.28
LCS
Expected
17.53%
1oo.oo%
,;,7%
19.58%
112.94%
17.36%
: 120.46%
,;--1
i
csu
Measured
LCS
Measured
I
I
Uncert.
Expected
Known
3.60%
5.15E+OO
100.00%
2.70%
5.48E+OO
1.48E-01
5.40E+OO
1.06E+OO
Th-1b
100.00%
3.60%
5.15E+OO
1.86E-01
5.82E+OO
1.01E+OO
Th-8b
Sample
Aliquot
Standard
ID
Known
Error
Standard
csu
Result
I 1.86E-01 ! 6.21 E+OO i 1.09E+OO
10
Standard
ACT(dpm)
Th-8b
I 1.04E+02 I
Standard
Error
I
1
Standard
Added (g)
3.60E+OO
I 1.11E-01
2.35E+01
2.70E+OO
5.17E-01
1.04E+02
3.60E+OO
1.11E-01
Matrix Spike
MSActual
%Rec
Normalized
Difference
Analyte
Replicate Sample
Normalized
Difference
Analyle
TH-228
~'t.ll
Ul
Q)
RPD
Original
Result
Original
csu
Replicate
Result
Replicate
csu
LCS R_elative
B1as
LCS % R
1.35E-01
2.14E-01
1.30E-01
1.20
57.20
2.62E-01
1.39E-01
4.72E-01
1.91 E-01
0.99
OK
1.12E-01
1.51E-01
9.78E-02
1.13
OK
TH-232
0.58
25.49
1.95E-01
LCSND
_OKTaK
2.37E-01
1.74
I
'
10.31
I
I
Version
QCSummary
0.24
TH-230
G~
Standard
Added(g)
MS%R
MSND
RepRPD
RepND
NA
OK
OK
NA
OK
OK
NA
OK
Eberline Services
Printed: 4/25/2013 8:33AM

Page 2 of 2
wo
Analysis
Run
Activity Units
Client Name
13-04053
ThiSO
pCi
LCS % Recovery
130 00
40.00
120.00
- - - - - - UCL
35.00
110.00
30.00
100.00
25.00
20.00
90 00
15.00
80.00
70.00
- - - - - - - LCL
Lower Error
Upper Error
10.00
L------~-------,--------:;:;:;--;;;;-;:;-----T----lifM~----TH-228
TH-230
TH-232
%R
99.33
141.60
120.46
80
100
-LCL
---Mean
-U~C~L~--+----~.~--=----I<:U
76.39
120.95
98.67
80
100
120
5.00
91.98
133.89
112.94
80-------1
100
120=---------1
+--------------,----------------,--------------,
TH-228
TH-230
TH-232
70.07
33.24
13.34
Lower Erro'-t--~ -~
f.LI
44.33
17.73
Uooer Error
10~1
S7 20
25.49
--c~L=-----1-----~--=-------~--RPD
~0
~5
35
0.00
3.50 , - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 3.001
2.50
E,
il~
u~
.....
Version
+------
- - - -
- - - -
No Matrix Spike
Eberline Services
Printed: 4/26/2013 9:07AM

Page 1 of 2
WO
- ------+---
Ra226
13-04053
Run
__ ~-~ctivity: Units
Client Name
Aliquot Units~------
pCi
Analyte
RA-226
Matrix Spike
Analyte
Normalized
Difference
MSActual
%Rec
Expected
MS Result
Expected
MS Uncert
Actual
MSResult
Actual
MSCSU
Sample
Result
Sample
csu
RA-226
ilili"
"'
U1
I'\)
Version
Standard
ID
Standard
ACT (dpm)
Standard
Error%
Standard
Added(g)
RepRPD
RepND
NA
OK
QCSummary
Replicate Sample
Analyte
Sample
Aliquot
Normalized
Difference
RPD
Original
Result
Original
1.19
38.96
7.33E-01
3.02E-01
csu
Replicate
Replicate
LCS Relative
Result
csu
Bias
4.94E-01
2.52E-01
1.02
LCS%R
LCSND
OK
OK
MS%R
MSND
Eberline Services
WO
Printed: 4/26/2013 9:07AM

Page 2 of2
Analrsis
Run
"-----~T
13-04053
Ra226
'I
~ctivity
Units_______ ~
pCi
LCS % Recovery
13000
=oof
110 00
10000
t
t
:::: t
'
30 00
25 00
oo
RA-226
5 00
130.47
100
120
-UCL
f -_
80
~~ea_n
t
,. ,
73.60
102.04
%R
...,..,_ -::LCL
~:::I+
I
l
---0~;:~ ~~~; j
woot
oooot
70
Client Name
Aliquot Units
ooo[-
Low._e__, Errorf
_l)pper Error I
RPD
---CL
-,.,,~%
--35
No Matrix Spike
3.50
3.00
2.50
2.00
1.50
000
3
W
~1,
tJ1
(,,,)
Version
--- I
I
Eberline Services
Printed: 5/1/2013 2:56PM

Page 1 of 2
WO
Analysis
Run
13-04053
Ra228
Activity Units
.l~~g(JotUnits.---+
pCi
Client Name

Analyte
Normalized
Difference
LCS
Measured
csu
Measured
LCS
Expected
Uncert.
Expected
25.30%
100.00%
5.10%
I
I
Known
Known
Error
Result
csu
Standard
10
9.95E+OO
2.52E+OO
Ra-11
Sample
Aliquot
Standard
ID
Standard
ACT (dpm)
Standard
Error
Standard
Added (g)
I 3.90E+01
5.10E+OO
I 5.13E-01
RA-228
0.72
'
110.34% [
t~
9.01E+OO
4.60E-01
-+--
Matrix Spike
Analyte
Normalized
Difference
Actual
MS CSU
Sample
Result
Sample
CSU
Replicate Sample
Analyte
RA-228
en
tn
tl~
t::~
Version
Standard
ACT (dpm)
Standard
Error%
Standard
Added (g)
RepRPD
RepND
NA
OK
QCSummary
Normalized
Difference
RPD
Original
Result
Original
csu
Replicate
Result
Replicate
csu
LCS Relative
Bias
LCS%R
II
LCSND
0.91
49.16
7.34E-01
7.87E-01
1.21E+OO
6.65E-01
1.10
OK
OK
MS%R
I
I
MSND
Eberline Services
Printed: 5/1/2013 2:56PM

Page 2 of 2
WO
Analysis
Run
Activity Units
13-04053
Ra228
pCi
Aliquot Units
Client N..=a'-'m'-'e'---------------i
LCS % Recovery
130.00
40.00
120 00
35.00
11000
30.00
100.00
25.00
20.00
90.00
15.00
80.00
10.00
RA-228
10.00
---Mean
-
5.00
79.94
140.74
110.34
80
100
-UCL
o.oo
-
+
-
LowerError
Upper Error
RPD
-CL
RA-228
67.49
30.83
49.16
35
3.50 , - - - - - - - - - - - - - - - - - - - - - - - - - - -
3.00
2.50
- - - -
-----
+- -
2.00f------------------------------1.50
i;!)
;!~
u~
(.Jl
Version
+-
No Matrix Spike
SECTION VII
LABORATORY TECHNICIAN'S NOTES
ISOUNOTES
Printed: 4/19/2013 9:25AM
2J
~ I;:: 1:3
Page 1 of 1
E . R L.., I N E
SERVICES
Work Order Analysis Notes
I
#
Date
Dept
04/19/13 09:24
PREP
User
JBARNARD
I
I
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
www.eberlineservices.com
Internal Work Order
Analysis Code
Run Number
13-04053
UUISO
1
Notes
ALIQUOT ED AND FILTERED THE DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
Printed: 4/23/2013 4:47PM
Page 1 of 1
EE3ERLINI::
13-04053
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
SERVICES
UUISO
1
Date
Dept
04/19/13 09:24
PREP
JBARNARD
ALIQUOTED AND FILTERED THE DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
04/23/13 16:47
CHEM
JDEMELAS
Added concentrated HCI to sample beakers and heated to. dryness; Added 20 ml BN HCL to samples and
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 mi8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 mi8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml BN HCI- 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of O.SN HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
User
Notes
~HiSS
Printed: 4/24/2013 5:30AM
Page 1 of 1
i
2J
E:: E3 E:RLI~E
~
SERVICES
Date
Dept
04/19/13 09:24
PREP
~2- --""
User
JBARNARD
.....
.....
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
13-04053
,_
Analysis Code
Run Number
UUISO
1
Notes
AU QUOTED AND FILTERED THE DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
----~.-
04/23/13 16:47
CHEM
JDEMELAS
Added concentrated HCI to sample beakersand heated -io dry-ness; Added 26mfBNHCLto-samples_a_ncr .
transferred to new, labeled C-Tubes, rinsing with 8N HCI to bring volume to 35 ml; Preconditioned resin
columns with 35 ml 8N HCI; Centrifuged samples and loaded onto columns; Rinsed C-Tubes with 20 mi8N
HCI, centrifuged as needed and loaded onto columns; Rinsed columns with 35 ml 8N HCI- 0.1 N NH41, 35 ml
of 6.5N HCI- 0.04N HF, and 10 ml of 6.5N HCI; Eluted Uranium with 50 ml of O.SN HCI into clean, labeled 100
ml beakers; Dried-down samples on hotplate; Dissolved samples in -10 ml of concentrated HCI; Transferred to
new, labeled C-Tubes with Dl H20. Set samples aside for later precipitation and filtering.
04/24/13 05:30
CHEM
RMARTZ
ADDE[:i"0~1ML NEODYMHJM-CARRIER, 0.3 ML TiTANOUS CHLORIDE, & 1 ML HF TO C-TUBES; LET SET

SIT IN ICE BATH FOR ONE HOUR. SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE
THEN ADDED SAMPLES; WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES
FROM C-TUBES, REMOVED FILTERS, LET DRY IN DESSICATOR, THEN SENT SET TO COUNT ROOM .
Eberline Analytical
Printed: 4/24/2013 5:31AM

Page 1 of 1
Analysis Code
UUISO
Reagents Used in an Analysis

Reagent
ID
Reagent
Name
Run
Reagent
Concentration
JDEMELAS
JDEMELAS
JDEMELAS
Solution
Reagent Grade
iii61
0~f
_ ~I /PL-tr-:t
_.{2
--~~ (//1)///t
tlh Jj, I-.
rifvt.~ ..,
VI\JtlJ,Il
l(f'u.l,r
VninJ
-..
l//IMJ.~
Vt~,,~
f)
~
~~rff;._ fi~-t~
../JA.f;:t:
L ,
tu!J/t/!J 0<-
l/t"1')
H~ uf2-li#!v\,r ,7\
'~Lto.r-{41-tJ, 1,-\ ~ _, ~L.
f?o'lbrrl(}tt,,:"J~ 'icvPf!
I 10
1.( ) ;
.4..1
~~
I '7 lf'iJQ14-IJ.,
~~
l"}oL(o}-.,At"J)
t~"u-,'f
'
A-U-i
t'"?o"toMA.l "
~ ~~
~l-t.
.
~
nr'lt..,
12K~
ffi..'S1...,_
Ol.f!L_
f)[ 0
l_tf)
I
In ""~e~>
I { J'(,
19
.J.
_Uj_.__
-::2_.1_
fi
--~
H- ; '-
"'-
/1.1(
I .I I~ 'U!..... ,
-J.'-~- -a..r~
ti.Yt. t.Jt-~1\:
-JA. .v-.....
u '--'~-
l ....cn....~.--
L-t~
- , '-r"'-
CA.&..-~
~;~y--4-.
..[
./
'-L-
c._.;
c...-l.,.../
7l.r..- ~
--t-~~~~-~-+~~-~--t---~--+-~--t------~--+--
------+'--~--~~-~~~--~--~~---~------+~--~+---
--------------r-~~~~~~-+~~----+~~---1--~----+---~-r--
---------------r~~--~--~~+-----~--~4------~---~~~-------+--------+-~-----+------+-----+------+--
i
!
---~~--------~-----~--~--T--~----r---,
!
-------------If------------+-------------------.-----
-~--
----------t---------------t--------t------
ISOTHNOTES
Printed: 4/19/2013 9:24AM
Page 1 of 1
~EBER~LNE
~
SERVICES
#
1
Date
Dept
04/19/13 09:24
PREP
User
JBARNARD
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
13-04053
T hIS Q
~-~~~~~~~~~~-----~--~-----11
Run Number
Notes
Printed: 4/23/2013 4:48PM
Page 1 of 1
}!JI;:BERLINE
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
SERVICES
Date
04/19/13 09:24
04/23/13 16:48
Dept
PREP
CHEM
User
JBARNARD
l
I
13-04053
Analysis Code
Notes
- - - - - - ----------------JDEMELAS
lntemal Work Order
---------------
------;-
Added concentrated HN03 to sample beakers and heated to dryness; Added 20 ml 8N HN03 to samples and
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; Eluted
Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15m I. Set samples aside for later precipitation and filterino.
Printed: 4/24/2013 5:31 AM
Page 1 of 1
~
E.E:3.E::R.I,.IN E
~
SERVICES
Date
04/19/13 09:24
,,,,, 2 '"
Dept
PREP
User

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
;-~~
13-04053
ThiSO
..
,,,.,, .........., ...... ' ..-~---
Run Number
. .......... .
~~~~-~~41
Notes
JBARNARD
ALl QUOTED AND FILTERED THE DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERSPRESERVED SAMPLES WITH HN03 AND DRIED SAMPLES DOWN
64i23h3il3:48''f-''"c:::H--::E~M:--+--"J'''"D'"Ec::M~:E=-c-LAS' - '' Added concentrated HN03 to sample beakers and heated to drynes-s; Added20mi'8N'HNo:ftosam'piesancf
transferred to new, labeled C-Tubes, adding 8N HN03 to bring volume to 35 ml; Preconditioned resin columns
with 50 ml 8N HN03; Centrifuged samples as needed, and passed through columns; Rinsed C-Tubes with 20
ml 8N HN03; Centrifuged rinsates and loaded onto columns; Rinsed columns with 40 ml 8N HN03; Eluted
Thorium with 50 ml of 8N HCI into clean, labeled 100-ml beakers; Dried-down samples on hotplate; Dissolved
samples in -10 ml of concentrated HCI; Transferred to new, labeled C-Tubes with deiononized water, bringing
volume to -15m I. Set sa~-~-<;JSi_<!El.!9!)~~1Jl.recipitatiqr:~~_cLf~t~J.IJ.9~---------.,.:--c=~=-c==-ll
ADDED 0.75 ML 0.1MG/ML CERIUM CARRIER & 1 ML HF TO C-TUBES & LET SET SIT IN ICE BATH FOR
ONE HOUR; SET UP FILTERS BY ADDING ALCOHOL & CARBON SUBSTRATE THEN ADDED SAMPLES;
WHEN SAMPLES WERE THROUGH FILTERS, ADDED 10 ML Dl H20 RINSES FROM C-TUBES,
REMOVED FILTERS LET DRY IN DESSICATOR THEN SENT SET TO COUNT ROOM.
ii67
Eberline Analytical
Printed: 4/24/2013 5:31AM

Page 1 of 1
Internal Work Order
Analysis Code
Run
ThiSO
;."~''"'""'''''''~~-
Date
Recorded
4/19/2013
I
!-~~~~~~~~~~
4/23/2013
.. I
.........~+.. ~8_N~
Reagent Grade
,_,
'
8N
..+--""'''''
Reagent Grade
.. . .
Solution
~'~~-~~VW~m.m
JDEMELAS
iT JDEMELAS
14/23/20131
i 4/23/2013
'~ WNmm~""=w~-W~ A-=~'~"'."'"'kccc't'A~,.w"'"''~~N~VN'""""'~="
I . .JDEMELAS
'
.. . .~~~t
. . . . . . . . . . . . . . . . . . . ". . ~~-l...! 4/23/2013
...~.-~~~"..~
:
.............~........ ,,,,., ....... ... ,,,,,..............{..... ...
0.1mg/ml
JDEMELAS
~''NA=f"""''w'"'"""'~v~W~WNh~-=w'""""'t
RMARTZ
4/24/2013
..............................~....1
..
4/24/2013 i
RMARTZ
'
''"~"M''"'1
4/24/2013 :
19
G~i
- .(j/1)111')
..
12
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"I)
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----------:-1'----~------------------------ ------cl---------~-------l--~-------------1----------+----------j--------l---
----------.--1----------------------
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------ -----+----------------~--------11 ----------------....

+----------------------------------
------------- ...
---
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----
-------------------~---------
--~-1--~--
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Gii7i
RA-226 NOTES
Printed: 4/19/2013 9:23AM
}!J E
~
Page 1 of 1
I
B E . R L . l .......
E::
SERVICES
#
1
Date
Dept
04/19/13 09:23
PREP
User
JBARNARD

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
13-04053
-~----~--~-~~------~----------~1
Analysis Code
Ra226
1
Notes
ALIQUOTED AND FILTERED THE DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- PH'D
SAMPLES- PRECIPITATED WITH BA AND PB CARRIERS AND AMMONIUM SULFATE- DECANTED
SAMPLES AND CENTRIFUGED- SUBMITTED RADIUM PRECIP TO SEPARATIONS
ii!ii73
Printed: 4/24/2013 6:55PM
Page 1 of 1
~E13ERLINE
~
SERVICES
Date
Dept
04/19/13 09:23
PREP
04/23/13 12:35
PREP
04/24/13 18:55
PREP
User
JBARNARD
LWALKER
LWALKER
Internal Work Order
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
13-04053
Notes
SAMPLES AND CENTRIFUGED- SUBMITTED_RADIUM PRECIP TO SEPARAI!ONS - - - - - - - ADDED EDTA TO PRECIP-VORTEX-LET SIT OVERNIGHT TO DIGEST.
FOLLOWED STEPS 12.1 TO 12.81N AP-006 REV 12 FOR RA 226 ANALYSIS (SYRINGE FILTERED
SAMPLES-PRECIP-FIL TERED-DRIED-OBTAIN FINAL WEIGHT) SUBMIT TO COUNT ROOM.
Printed: 4/25/2013 11:37 AM

Page 1 of 1
Eberline Analytical

R.~i:f9erft
R~iigent
..
~q:me
013376P
Ammonium Hydroxide
013575001
Ammonium Sulfate
012766014
Barium Carrier
1 mg/ml
012729007
Lead Carrier
166 mg/ml
013624P
Nitric Acid
013781S
EOTA
011383P
Acetic Acid
Reagent Grade
4/24/
013377001
Ammonium Sulfate
200 mg/ml
4/24/
Grade
i675
--r-------------1----------- - - - - - - - - - - - - - - t - - - - - - - - - - - f - - - - - - 1 - - - - - - - - - t - - - - - - - + - -
.
._:._,: ____
.:
..
.:
'
.. . .
RA-228 NOTES
&577
Printed: 4/19/2013 9:23AM
Page 1 of 1
}!;EBERLIN I::
~
SERVICES
#
1
Date
Dept
04/19/13 09:23
PREP
User
JBARNARD
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04053
Ra228
1
Notes
Cl
6i78
Printed: 4/29/2013 6:59PM
Page 1 of 1
j!J EBERL,INE
~
SERVICES
Date
Dept
User
Internal Work Order
601 Scarboro Rd.

Oak Ridge, TN 37830
Voice: 865.481.0683
Notes
I PREP
JBARNARD
I ALIQUOTED AND FILTERED THE DISSOLVED FRACTIONS- ADDED SPIKES AND TRACERS- PH'D
!1--+--~--------- I ---- c--:::-;----------~.-~~~:t~~-~~~RgE~~~~~~~G~~~~~~~~-;~ ~~~~~~~~~~~~~~~~~~A~~~~~TE- DECANTED
1
04/19/13 09:23
04/26/13 10:53icHEM
'-3!-64129/13 18 59
TSMITH
1-PRE_P____ - LWALKER
I
i
I
Placed filters from count room into labeled centrifuge tubes. Added EDTA to samples and swirled.
FOLTOWED STEPS 12.1 TO 12.7 IN A-P.:067"REV 17 (CHEMICAL CLEANUP FOR RA 228)
Printed: 5/1/2013 7:48AM
~
E E:1~1:::. .
~
Page 1 of 1
5!L,I.N.E:::
SERVICES
I
I

601 Scarboro Rd.
Oak Ridge, TN 37830
Voice: 865.481.0683
Internal Work Order
Analysis Code
Run Number
13-04053
Ra228
1
Date
Dept
04/19/13 09:23
PREP
JBARNARD
04/26/13 10:53
CHEM
TSMITH
Placed filters from count room into labeled centrifuge tubes. Added EDTA to samples and swirled.
04/29/13 18:59
PREP
LWALKER
FOLLOWED STEPS 12.1 TO 12.71N AP-007 REV 17 (CHEMICAL CLEANUP FOR RA 228)
05/01/13 07:48
CHEM
TSMITH
Followed steps 12.7 to 112.15 in AP-007 rev. 17 , ( Precipitated samples, hot bathed, centrifuged, and
discarded supernate. Dissolved precip, precipitated samples, hot bathed, centrifuged, and discardfed
supernate. Dissolved precip, precipitated and filtered samples, obtained final weights, covered with aluminum
foil and took to count room )
User
Notes
---
Eberline Analytical
Printed: 5/1/2013 9:10AM

Page 1 of 1
Analysis Code
Ra228

Reagent
ID
013376P
Reagent
Name
Reagent
Concentration
Ammonium Hydroxide
-~,~~~~~~~-~
Run
Recorded
Reagent Grade
~~-~~~~."~~~~-~~+~~~
200 mg/ml
~,~~~~~~~~~~!~~-~~
~~m7~~~~~
1 mg/ml
..........................+.,
166 mg/ml
JBARNARD
Reagent Grade
JBARNARD
: 4/19/2013!
TSMITH
4/26/2013
LWALKER~~~r4/29/2a13!
....
~-~~-~..........;
i 4/29/2013
i 4/29/2013
LWALKER
~~~Y... ~~_..J,,,. .,,~~ww~1
LWALKER
I
.....T4/2.9/7-'a131
t4J29/2a131
~~-~~
i 5/1/2013
... :.
.. . .. I
5/1/2013
...........,.
:~~~~~~~
~..........~.ts/1/2a131
~~+
18M
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SECTION VIII
ANALYTICAL DATA (ISOTOPIC URANIUM)
Eberline Services
Analysis Sheet
Printed: 412412013 5:31 AM

Page 1 of 3
13-04053
UUISO
Run 1
Analysis Code
Internal
Fraction
13-04053
Work Order
UUISO
1
Run
----t---o-4/05/13 15:58
4/9/2013
03
Lab Deadline
4/30/2013
04
DO
05
TRG
06
TRG
West Lake OU-1
Activity Units
pCi
1----A_I_iquotUn..
Matrix
07
WA
40
04/05/1315:58
r~~~~~oo~~oo
L________PZ-305-AI DIS
40
04/05/13 15:58
45
~ 04/05/13 00:00 '
1.0000E+OO
04/05/13 00:00
1.0000E+OO
c = 9 2_RG
DUP_D4
NAS NS-3050 Mod
Method
41
o4/o5!1-3oo:oo- --1-.ooo-oE+oo
- ------
41
04/05/13 00 00
0000~00
----------t-----+--------+
f-
----------
--------
Alpha Spectroscopy
Instrument Type
---+---+-------------
Radiometric Tracer
U-232
Radiometric Sol#
U-10a
1-- Tracer Act (dpmtg>
I _______,9.ooa
Carrier
.carrierConc(mg/ml)
---------l---------- --
~~=----=--
---r
1-----
45
------+-----
DUP o4 TOT
1.0000E+OO
DUP 03 TOT
DUP 03 DIS
TRG
TRG
08
r------1-.ooooE:OO
+--------~Z-30;~A;-TOT--- .. T
-+---
---------1
Report Level
1.0000E+OO
+--- 1.0000E+OO
04/09/13 00:00
02
Client I Engineering ManagementSupport,

Inc. -1
--
Sample
Aliquot
Sample
Date
04/09/13 00:00
-+--------
Login
CPM
01
Date Received
Project
Client
ID
Sample
Desc
----------
f------r----
'
i
1
_J I
'
-----+------------- -----------
':
i
---4---------~
_[------~-----
------+---
------
1
_____ _,_ _
I+----- --
1----
- ---------------
1--
==
I
C!~
;;,
l':l:)
~, ~
* SAF1 is used for Gross Alpha and all other radionuclides_ SAF2 is used for Gross Beta only.
**Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
Eberline Services
Analysis Sheet
Printed: 4/2412013 5:31 AM

Page 2 of 3
13-04053
UUISO
Run 1
Internal
Fraction
Sample
Desc
Tracer
Aliquot(g)
Tracer Total
ACT (dpm)
Radiometric
Tracer (pCi)
i Radiometric
I
I'
% Rec
::::I ---~ 1- ::::1
0.61
::
0.61
--~11.5
0.61 )46
'i
I - o.ool
I -
Grav Filter
Tare(g)
Grav Carrier
Added (ml)
Grav Filter
Net(g)
Grav Filter
Final (g)
Grav
%Rec
SAF
1*
Mean
%Rec
SAF
2*
t-__-r-----r
-r----{=
-+
----t--
0.61
: ~:: :- :::::~ ~ r-::

-~--
0.61
08
I TRG
09
TRG
, ---;
f------
---:
,
0.6006 I
11.5 I
II
0 . 6 0. r - = 6
11~~-t~-----_!
.... I
-----~
-:
'
l___
~~~-I
---
I
I
""1--
-----[-
1---..
+I
I
I
I
- ~
ji
---~I
--~
----=
.I
--T--+---
-~
I
I
I
--~
r--------r
i
i
'
-1-~
+------1-------
I
~--
--~------~--t--~-+------t---t--
---------+------+-
-+------
-j-----f---
f--~--~-!
;!;~
illii~
g!
* SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
I -_- -
t--~-------+~----t------+---1
---
-,
--------1
r-- -~--r
1-----+
-'-----------
__ j_
r----r---
--
-~
--u~
t----------ti
I
----
0.00 I
0.00 I
-r-------~---
I
i
l---~~----r----
Eberline Services
Analysis Sheet
Printed: 412412013 5:31 AM

Page 3 of3
13-04053
UUISO
Run 1
Internal
Fraction
I'
f-
04
--~
DUP
~-DO
~!_TRG
06
TRG
1--07
TRG
-~-
t'
I 04/19/13 08:50
JBARNARD
'--
I 04/19/13 08:50
I JBARNARD
' 04/19/13 08:50
--
. ---
----+--+-------
f--
By
t-----
~-
1 ______ -
~~-----L-~-~--
"
-+--------+
r---1
----~-t
r
.
'
---+----~-----
~-=------- !
---t~
~--------I
-11---------~--t
----+-
t--
-t
:
, -~- -
-1--==-=-
-~-~--
04/19/1308:50 I JBARNARD[--:_
------
------1
f~-1---~-_:;
-1
+-
-i -I
JBARNARD I
---
By
I ~RNARD I
04/19/13 08:50
Sep t1
Sept1
Date/Time
04/19/1308.:501 JBARNARD .
1-----+-
t-----+--
By
04/19/13 08:50 I JBARNARD
TRG 1
r----
Sep tO
Sep tO
Date/Time
Prep
:::::::: :::::-'-j:::~:::
--
OS
Prep
Date
By
L0~_1~::
03
Rough Prep
Rough Prep
Date
Sample
Desc
-+
--
--
~~
c:!!~
():)
(..11
SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
Actual mass exceeded the calibration curve range. Results should be qualified as appropriate.
(
I:
~
0::
Lab
U-234
LCS
Client
Identification
LCS
or-
.!04-
03
U-234
U-234
U-234
-----
PZ-305-AI TOT
U-234
09
U-234
c
Cll
E
Cll
Cl
cG
o,
c
w
u~
m
en
6.07E-02'
8.76E-02'
2.68E-01
c--
LCS
Flag
92.54
OK
MDA
Flag
RPD
Flag
Blank
Flag
OK
OK
OK
pCi/1
5.89E-01'
TRG
DUP 03 DIS
TRG
DUP 04 DIS
------+-- -+----------
_ _ _ i ____ ----
1---t
I
OK
1.44E-01:
2.78E-01
~-----
pC~
OK
8.86E-02j
j- - - -----+---------r--------+----+----f---
2.85E-01 i
pCi/1
7.45E-021
- --+------+------+-------+------+-
9.71E-01 I
pCi/1
-------+------+-DUP04 TOT
NA
-+-------:---------+-----+-----I----
1.92E-01 j
- - - - - - + - - - - - + - - - -------- :-
1.19E-011
1.84E-01:
1.14E-01 l
--- : - - - -- -t-----+-------+----+---+-----
DUP 03 TOT
1-----t-----------1------t- ---
Cll
Cll
-----------
--~----------------- ----
~--1:
~--t- -------
Cl
;:
6.85E-01.
pCi/1
1.62E-011
OK
1.21 E-01 ,
--+---- --!----------+
3.11E-01 i
1.38E-01i
-j-----
OK
8.92E-02!
---l---------1--------t
---+--
I
i
. _,_____ ------:------------i-----+---+-------+------l-------+-------1
'
I
I,
I
i
-+-------t-------t----r------+------+----+-------+--j
1
I
I
- - - - - - + - - - - - - - 1 - - - - t - - - - -- -+------+-----+---+----+-----+-----+----I
I
'
I
_L ____f---------t-----+------+----+-----+------1---~
1
cG
:E
--+-
TRG
-----r-; TRG
-------+------+~---
c.i
7.44E-02
1.96E-01
pCi/1
4.45E-01 i
-------------+--+-
:::s
8.13E+OOI
1.06E+OOi
LCS
%R
... -------
pCi/1
-----------------------+-----+-
t/)
pCi/1
LCS
Known
MDA
----
PZ-305-AI DIS
------- ---------------+-------- -+------ -----
Error Estimate;
---------------1-------+-------
Q.
Q.
Results
TRG
-------t---t---
08
-=t:
Activity
Units
pCi/1
PZ-305-AI TOT
U-234
BLANK
U-234
51~07
1:
I!
-----:---- ------------r--
~
Ill
I:
Sample
Desc
U-234
(f) I I 05
ct
'
0
-~
Work Order: 13-04053-UUIS0-1
Nuclide
Fraction
Printed: 4/25/2013 8:37AM

Page 1 of 3
Preliminary Data Report & Analytical Calculations
Eberline Services
II
.
-+--+
----+'
----l
-+----t--------r---+---+---+--1
--+
1----~---r--~----r---~----+
Eberline Services
Printed: 4/25/2013 8:37AM

Page 2 of 3
Sample
Desc
Sample
Date
LCS
04/09/13 oo:oo
MBL 1_____ 04/09/1:~0:00
----+-~
Sample
Aliquot
Radiometric
% Rec
L__~_oo~~i_ _2oo.1s!-~-i
1.00E+OO
116.761
Grav
% Rec
Mean
% Rec
o.oo
o._~~~~
0.00
~~~L-
Sep 11
Date/Time
SeptO
Date/Time
SAF
'
------- --L~---
---+~T~R-G ~-~4/0=~~;~~o~_oo_~~T-~~~~E+~-:= 107.731

---+---TR_G--11
~~~~~~~~~-:o_o___+-~-OOE~~~+-- 91.03
-+--+-~--t
~~-
c.i
--~----t-
~I 1----:::1
--+
en
--+
Cll
.,s:::
.,
Cl
::iiE
Cl
s:::
~I
Cll
.5
Cl
s:::
lil!ill
12~
<n
.... ~
~~--
04/05/13 00:00
I 1.00E+OOI
63.81
0.00
0.00
TRG 1
~-~~~;~~;~;~~---~---1.00E+~ol
107.43
o.oo
0.00
___ ,_
I
+-----+-
I
-------------------------I
i! -- ---------------------
I ---
--------~----r
------------------i
--
-------:-----
I
+-
-----~---------1
I
--------~-~
-+-----~------------------r----
____
J_
~-
_J_
i
t--
--~-----------------11--------1
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U-234
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U-234
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U-234
04
U-234
05
U-234
06
U-234
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LCS I
Halflife
(days)
DO I
:-~~~~
TRG
'
04/24/13 08:57
_"
04/24/13 08:57
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04/24/13 08:57
04/24/13 08:58
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04/24/13 11 :55
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---+-
170j5.30 ~~02 __
Alpha_o0ol4.47 E+OO
f.oo
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18.7
19.00 E-03
18.5
5.00 E-03
17.8
-----~ -------------~----_______j___1
A_Spec
jAipha_0181
170j2.21 E+01
1
A_Spec
i Alpha_024
170 12.58 E+01
A_Spec
7.00 E-03
15.3
17.1
17014.15 E+01
3.00 E-03
17.4
170 5.75 E+01
3.00 E-03
17.3
17011.33 E+01
4.00 E-03
19.5
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17.5
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Time
04/24/13 08:57
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Printed: 4/25/2013 8:37AM

Page 3 of 3
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Units
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U-238
Client
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LCS I
U-238
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U-238
U-238
pCi/1
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PZ-305-AI TOT
PZ-305-AI TOT
-
31
U-238
U-238
----------~------
PZ-305-AI DIS
pCi/1
6.45E-02
5.52E-01!
2.22E-01
.i
-----;-
5.87E-02:
LCS
%R
1
1
7.92E+oo( 103.83 /
pCi/1
pCi/1
7.93E-011
2.86E-01
8.18E-011
2.30E-01
9.50E-02!
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1.28E-01 i
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+- ]~-1-=
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Blank
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MDA
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3.62E-011
RPD
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pCi/1
pCi/1
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I
!
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1.31E-01 I
---- --------------
l_
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s.75E-02
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8.17E-021
--+
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pCi/1
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1.14E+ooi
MDA
!
I
i
I
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!
I
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I
DUP 03 TOT
U-238
8.23E+oo/
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1
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Printed: 4/25/2013 8:37AM

Page 1 of 3
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04/05/13 15:58
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U-238
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04/05/13 15:58
06
iI
U-238
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04/05/13 00:00
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04/05/13 00:00
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107.731
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75.00 i
1.00E+OO
+
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116.76[
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1
. ----+-----------+----+---
1.00E+OOi
04/05/13 15:58
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1.00E+OO
04/09/13 00:00
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Printed: 4/25/2013 8:37 AM

Page 2 of 3
+------------
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Date/Time
-r-1
02
U-238
MBL
04/24/13 08:57
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Alpha 013
170!5.83 E+02
04/24/13 08:57
A_Spec
Alpha_014~
170!6.66 E+OO
__ ,_____ -- _______J_____________
Eft
CPM
!2.00 E-03
-18.7
12.00 E-03
18.5
-f__
--+-- -
04
U-238
DO
04/24/13 08:57
A_Spec
en
05
U-238
TRG
04/24/13 08:57
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Alpha
:::J
:::J
06
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TRG
04/24/13 08:57
A_Spec
Aipha_025i
17015.78 E+01
!1.00 E-03
07
U-238
i TRG I
04/24/13 08:58
A_Spec
iAipha_027:
170[4.68 E+01
117.00 E-03
17.3
10.00 E+OO
19.5
DUP
04/24/13 08:57
--+---+
U-238 - -
..
U-238
LTRGiTRG
--------r-------
04/24/13 11:55
--- ---
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.5
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0
c.
c.
s:::
Cll
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Cll
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co
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17.8
17.00 E-03
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09
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Printed: 4/25/2013 8:37AM

Page 3 of 3
Eberline Services
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pCi/1
7.08E-02
6.74E-02
7.27E-02
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4.50E.02
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9.36E-02
1.45E-01
1.13E-01
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1.12E-01
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pCi/1
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Printed: 4/25/2013 8:38 AM

Page 1 of 3
Eberline Services
1--
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Printed: 4/25/2013 8:38AM

Page 2 of 3
1.00E+OO'
Mean
%Rec
Grav
%Rec
Radiometric
%Rec
Sample
Aliquot
100.18'
SAF
Septo
Sep t1
Date/Time
Date/Time
0.00
o.OOf
---------1------+-- -
1.00E+OO:
i-------+---------t---
::::j~~
-~~--~
f" -
:--~---T------~--
1.00E+OO!
107.73;
0.01
0.0~
1.00E+OOi
91.03;
o.ool
o.oo
63.81 i
0.001
--+-----------+
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-- --~--------- ------L_____
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107.431
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1
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1.00E+OOI
------1----
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0.00 I
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0.00 I
1.00E+oo:
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0.00 I
90.11 '
1.00E+OO i
----+ - - - - - - - - - + - - +
- ::::L ~::1--- ::1

0.00 I
116.76:
--+--.
-----1
---+---------------~
----1--------------1
Sample
Desc
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Date/Time
LCS
04/24/13 08:57
MBL
04/24/13 08:57
Halflife
(days)
I
.
Carroer
Detect
,
A_Spec
1Aipha_014
A_Spec
A_spec
----"
A_Spec
04/24113 08:57
TRG
04/24/13 08:57
Alph~~~2:____
'Alpha_024i
04/24113 08:58
04/24/13 08:58
,
1---+--------=-:== --==
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17016.83 E+OO
\1.00 E-03
17.1
Alpha_~t 1~~~~:00 _I .OO~;,l--".3 =

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2.00 E-03
110
04/24/13 08:57
] -- _
11:55
TRG
+----+
__04/24/13
_____
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1704.66 E+OO
04/24/13 08:57
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r
i
170:3:5~ ~~~1__to.o~=~~~-+----1~~----
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--+-~---~-~e~~ :Aiph~~o-~~:.
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Bkg
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Printed: 4/25/2013 8:38 AM

Page 3 of 3
Eberline Services
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Count Room Report

Client: Engineering Management Su
Printed: 4/24/2013 5:31 AM

Page 1 of 1
13-04053-UUIS0-1 (pCi/1) in WA
Tracer ID: U-1 Oa
A\~\./-'
Internal
Fjaction
1~/
Sample
Desc
~-
Client
ID
MBL
oupf
03,
04-rDO
05
TRG
06
TRG
I 04/09/13 00:00
--~-- Tracer
I
04/09/13 oo:ool1.oooo
-PZ-305-AIToT
04/0s/1315:58-, -1.0000
l04/05l1315~ 1 0000 I
PZ-305-AI TOT
1~-
PZ-305-AI DIS -
04/05/13 15:58
DUP 03 TOT
04/05/13 00:00
~--
--+--1='-
---u--
t--~~+------t---~-1
~~~
----+----+-1~~
I
f--------
I
!
!:lit'
Q~
UJi
t.n
0.6039
11.5798
o.oo
0.6012
0.00
11.4805 i
1---T--~-----.-
t- ------------
_,____
,
--
+-
-----------
1=-----+-----1
'
--------+
+--
---t---
SAF
2*
0.00
1.0000
'
0.00 I
0.00
SAF
1*
o.oo
c~115321 I_
Radiometric
% Rec
11.5454
~~~~~-~-~11.4901
=t
0.6046
---~--~~---~~~-------
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'
I
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Tracer (pCi)
1.0000
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11~6218
0.6086 I
+-~o.-6~~~--r-
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I
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ACT (dpm)
Aliquot (g)
1.0000
-----~s~LA-NK~-
---+----------
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LCS
o2
Sample
Date
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:
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Eberline Services
Page 1 of 1
Printed: 4/19/2013 8:50AM
Spike and Tracer Worksheet
JBARNARD
Isotope
Sol#
U-234
U-Sa
Activity
dpmlg
35.240
Solution
Date
4/19/2013
Approx
Addition
Volume
Used(g)
Volume
Used(g)
LCSD
.MSD
Volume
Used(g)
Volume
Used(g)
MS
Known
pCi
Error
Estimate
0.500
0.5121
S.13
0.293
0.500
0.5121
7.92
0.2S5
U-238
U-Sa
34.350
4/19/2013
Tracers
fraction
Activity
dpm/g
Volume
Used(g)
Approx
Addition
Sol#
~2
U-232
U-10a
19.096 4/19/2013
0.6086
0.6300
U-232
U-10a
19.096 4/19/2013
0.6064
0.6300
03
U-232
U-10a
19.096 4/19/2013
0.6046
0.6300
04
U-232
U-10a
19.096 4/19/2013
0.6039
0.6300
U-232
U-10a
19.096 4/19/2013
0.6017
0.6300
06
U-232
U-10a
19.096 4/19/2013
0.6012
0.6300
07
U-232
U-10a
19.096 4/19/2013
0.6005
0.6300
08
U-232
U-10a
19.096 4/19/2013
0.6006
0.6300
U-232
U-10a
19.096 4/19/2013
0.6016
0.6300
01
1--
05
[_ 09
l~:i; 6(i::::~j::::
::.:!::;:::...-i
'-1~~:~.t"';'
t-
I
1-----+-
0.000
~-_(JOOO
0.000
0.000
~::1 ::~i}
It
21
-~Or 6~J46
--~3 ~ ~:,o~:;::
-~~ 1 :1
~~ ( ;
Version 2.0 OS/99
Estimate
!":.:::
..
6:2; :l.
l:
~~~
MSD
Added
pCi
:;..: ;
~o., 6~?: :~~
WI
ooo(
o.ool
LCSD
I Error
Known
pCi
LCS
Tracer
--o 6~:~r-r~::;
-l::i, t:Dl):::::
G$
I
I
Error
Estimate
Balance Printer Tapes

Solution
Date
Isotope
Added
pCi
t=
t..::. E! 11:,
Matrix Spike
Error
Estimate
O.OOj
0.000
o.ool
o.ooo
Eberline Analytical
Printed: 4/19/2013 8:50AM

Page 1 of 1
Aliquot Worksheet
JBARNARD
Lab
Fraction
Type
LCS
MBL
DUP
DO
TRG
TRG
TRG
TRG
TRG
Client 10
01
02
03
04
05
06
07
08
09
LCS
BLANK
PZ-305-AI TOT
PZ-305-AI TOT
PZ-305-AI DIS
DUP 03 TOT
DUP 03 DIS
DUP04 TOT
DUP 04 DIS
Dilution Data
Muffle Data
Sample
I
Ratio
PostJPre
No'OfDils
Oil Factor
Aliquot Data
Ratio
_II':
--I
--
--
--
Aliquot
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
NetEquiv
MS Aliquot Data
Aliquot
H-3 Solids Only

---c---
Water Added
(ml)
NetEquiv
H3 Dist
Aliq
1.ooQo~;+oo
1.0000E-i-OQ
1.ooooE+op
1.0000E+OO
1.0000E+t:l6
1.ooooE+oo
1.0000E+()Q
1.0000E+OO
1.0000E+oO
I
I
--
--
--
1-=-I
--
I
----,-
+---------
--
I
~l
...l
Comments
Techo;aao
L____,,_,_
~J
oate
A frJ:?5"
Sample Description:
Spectrum File:
Batch Identification:
Sample Identification:
Sample Geometry:
Procedure Description:
SPIKE
\\OR-ALPHA1\Canberra\ApexAlpha\Root\Data\00000562
1304053A-UU
01
Shelf 2
u iso
Detector Name:
Chamber Serial Number:
Detector Serial Number:
Env. Background:
Reagent Blank:
Alpha_Ol3
13
System Bkgd 55195
<not performed>
Sample Size:
Sample Date/Time:
Acquisition Date/Time:
Acquisition Live Time:
Acquisition Real Time:
1.000E+000 +/- O.OOOE+OOO liter

8:04:50 AM
4/24/2013
4/24/2013
8:57:26 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Effective Efficiency:
Counting Efficiency:
Chern. Recovery Factor:
U232 UU-10A
0.609 mL
0.1872 +/- 0.0107
0.1869 +/- 0.0035 on 12/15/2012 11:26:45 AM
1.0018 +/- 0.0602
Control Certificate Name: Natu U-SA

Chern. Recov. of Control:
U-238
Peak Match Tolerance:
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.280
4.731
4.398
4.148
Net
Pk Area
1.012128 +/-
AREA
REPORT
Pk Area
Error %
367.79
530.49
35.00
582.66
0.077645
Ambient
Backgnd
2.21
0.51
0.00
0.34
10.26
8.51
33.60
8.12
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
20.6
34.0
5.7
22.6
Tracer Peak used for Effective Efficiency
NUCLIDE ANALYSIS RESULTS
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0. 996
0.993
0.999
0.991
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.22E+000
7.52E+000
6.12E-001
8.23E+000
+!+I+I+I-
5.84E-001
1.06E+000
2.17E-001
1.14E+000
'i/Js!IJ
MDA
(pCi/liter
1.13E- 001
7.44E-002
1. 05E-001
6.75E-002
+I+!+I+I-
1.27E-002
8.34E-003
1.18E-002
7.56E-003
0000056297.CNF
Live Time :10200.000 sec
Real Time :10200.000 sec
Start:
1:3547 .5(kev)
stop : 1024:6438.1(kev)
Acq. Start :wed Apr 24 08:57:26 2013
55
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:::s
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~~
Q:)
(J)
u:~
4500
ROI Type: 1
5000
Energy(kev)
5500
6000
ROI Type: 3
Channel Data Report
Page
4/24/2013
*******************************************************
*****
S P E C T R A L
DATA
R E P 0 R T
*****
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Channel Data Report

369:
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1
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i16U
Channel Data Report

801:
4/24/2013
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Sample Title:
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Page
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Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1304053A-UU
02
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_014
14
System Bkgd 55196
<not performed>
Sample Size:
Sample Date/Time:

4/24/2013
8:04:50 AM
4/24/2013
8:57:27 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.606 mL
0.2155 +/- 0.0116
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
1.1676 +/- 0.0666
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
1.19
1.53
0.34
0.34
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.280
4.734
4.384
4.170
421.81
4.47
4.66
6.66
9.56
109.71
94.59
78.18
5.7
2.9
2.9
2.9
-------------------------------------------------NUCLIDE ANALYSIS RESULTS

--------------------------------------------------
Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.996
0.994
1. 000
0.998
5302.50*
4761.50*
4385.50*
4184.40*
5.20E+000
5.51E-002
7.08E-002
8.17E-002
+I+!+I+!-
5.49E-001
6.07E-002
6.74E-002
6.45E-002
Jf/:>cf!?J
8.12E-002
8.76E-002
7.27E-002
5.87E-002
+!+I+I+!-
8.58E-003
9.26E-003
7.68E-003
6.20E-003
0000056298.CNF
start:
1: 3507. 9(kev)
stop : 1024:6512.2(kev)
Acq. start :wed Apr 24 08:57:27 2013
55
50
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35
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::::::1
8 30
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4000
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4500
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wmm j
5000
Energy(kev)
liB
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!!!!\!! 00
I!!
1\ m
!I
!!!
In
5500
6000
.....
2,
tJ;,,
ROI Type: 1
ROI Type: 3
!II
no
Ill
01\ !!!
6500
------
Channel Data Report
4/24/2013
Page
3:19:49 PM
*******************************************************
s P E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
02
Elapsed Live time:

Elapsed Real Time:
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Channel Data Report

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5156
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801:
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-305-AI TOT-DUP
1304053A-UU
03
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_018
18
System Bkgd 55197
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:04:50 AM
4/24/2013
8:57:56 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.605 mL
0.1332 +/- 0.0088
0.1776 +/- 0.0033 on 12/15/2012
0.7500 +/- 0.0516
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.259
4.707
4.328
4.130
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
259.98
22.15
1. 83
27.81
1:57:26 PM
12.18
42.57
152.56
38.09
Ambient
Backgnd
1. 02
0.85
0.17
1.19
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
7.0
3.1
3.1
3.9
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.987
0.979
0.977
0.980
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.18E+000
4.41E-001
4.50E-002
5.52E-001
+I+1+I+I-
6.73E-001
1.96E-001
6.89E-002
2.22E-001
MDA
(pCi/liter
1.26E-001
1.19E-001
1.03E-001
1.31E-001
+1+I+I+1-
1.63E-002
1.55E-002
1.33E-002
1.70E-002
JG
Jf/JS/13
61&8
0000056299.CNF
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1:3404.1(kev)
Stop : 1024:6604.2(kev)
Acq. Start :wed Apr 24 08:57:56 2013
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5111
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8112
\c.b\ ,...,
--l \l,..-4 \ /
Sample Description:
Spectrum File:
Sample Geometry:
PZ-305-AI TOT
1304053A-UU
04
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_022
22
System Bkgd 55198
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:04:50 AM
4/24/2013
8:57:57 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.604 mL
0.1162 +/- 0.0082
0.1531 +/- 0.0029 on 12/15/2012
0.7586 +/- 0.0556
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
1:57:26 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
2.55
1. 02
0.68
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.267
4.730
4.384
4.134
226.45
29.98
3.32
34.83
13.11
36.50
119.77
33.31
7.3
3.1
3.1
3.9

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.991
0.993
1. 000
0.982
5302.50*
4761.50*
4385.50*
4184.40*
5.18E+000
6.85E-001
9.36E-002
7.93E-001
+I+1+I+I-
7.18E-001
2.68E-001
1.13E-001
2.86E-001
~
tf/~113
1. 92E- 001
1.44E-001
1. 59E-001
9.50E-002
+I+1+I+I-
2.66E-002
2.00E-002
2.20E-002
1.32E-002
0000056300.CNF
start:
1: 3421.5 (kev)
Stop : 1024:6608.8(kev)
Acq. start :wed Apr 24 08:57:57 2013
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t:~
ROI Type: 1
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3:20:08 PM
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1116
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801:
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-305-AI DIS
1304053A-UU
05
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_024
24
System Bkgd 55199
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:04:50 AM
4/24/2013
8:57:58 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.602 mL
0.1541 +/- 0.0096
0.1710 +/- 0.0032 on 12/15/2012
0.9011 +/- 0.0587
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
Pk Area
Error %-
2:02:15 PM
REPORT
Ambient
Backgnd
Reagent
Backgnd
1. 70
1.19
0.17
0.51
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.259
4.708
4.370
4.123
299.30
25.81
6.83
34.49
11.37
39.61
76.08
33.66
9.8
3.6
3.1
3.6
-------------------------------------------------NUCLIDE ANALYSIS RESULTS

--------------------------------------------------
Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.986
0.980
0.998
0.974
5302.50*
4761.50*
4385.50*
4184.40*
5.16E+000 +1- 6.31E-001

4.45E-001 +I- 1.84E-001
1.45E-001 +/- 1.12E-001
5.92E-001 +I- 2.12E-001
lt4
'1/J-g/3
1.27E-001
1.14E-001
8.87E-002
9.00E-002
+!+1+I+I-
1.55E-002
1.39E-002
1.08E-002
1.10E-002
0000056301.CNF
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ROI Type: 1
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6500
Channel Data Report
4/24/2013
Page
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*******************************************************
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G121
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801:
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3:20:20 PM
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Sample Description:
Spectrum File:
Sample Geometry:
DUP 03 TOT
1304053A-UU
06
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_025
25
System Bkgd 55200
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:04:50 AM
4/24/2013
8:57:59 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.601 mL
0.1870 +/- 0.0107
0.1736 +/- 0.0032 on 12/15/2012
1. 0773 +/- 0.0649
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.279
4.739
4.425
4.170
Net
Pk Area
AREA
REPORT
Pk Area
Error %
362.83
41.49
2.66
57.83
1:57:27 PM
10.29
30.65
128.85
25.82
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.17
0.51
0.34
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
30.0
3.9
3.1
6.8

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.996
0.996
0.989
0.998
5302.50*
4761.50*
4385.50*
4184.40*
5.15E+000
5.89E-001
4.66E-002
8.18E-001
+I+I+I+I-
5.79E-001
1. 92E-001
6.03E-002
2.30E-001
AG
t.fj~/IJ
5.93E-002
7.45E-002
8.38E-002
5.90E-002
+I+I+I+!-
6.66E-003
8.37E-003
9.41E-003
6.63E-003
0000056302.CNF
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Channel Data Report

801:
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Sample Description:
Spectrum File:
Sample Geometry:
DUP 03 DIS
1304053A-UU
07
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_027
27
System Bkgd 55201
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:04:50 AM
4/24/2013
8:58:00 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.600 mL
0.1573 +/- 0.0097
0.1728 +/- 0.0032 on 12/15/2012
0.9103 +!- 0.0588
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
2:27:41 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
1.19
0.51
1. 36
1.19
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.283
4.730
4.355
4.152
304.81
57.49
4.64
46.81
11.25
25.98
105.44
29.07
26.2
4.3
4.8
6.4

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.997
0.993
0.993
0.992
5302.50*
4761.50*
4385.50*
4184.40*
5.15E+000
9.71E-001
9.66E-002
7.87E-001
+I+I+I+!-
6.24E-001
2.78E-001
1.03E-001
2.48E-001
l.llE-001
8.86E-002
1.43E-001
1.11E-001
+I+!+I+I-
1.35E-002
1.07E-002
1. 73E-002
1.34E-002
A4
tf/:>S/1)
li128
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i131
Channel Data Report

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&132
Sample Description:
Spectrum File:
Sample Geometry:
DUP 04 TOT
1304053A-UU
08
Shelf 2
U iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_029
29
System Bkgd 55202
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:04:50 AM
4/24/2013
8:58:01 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.601 mL
0.1241 +/- 0.0085
0.1945 +/- 0.0036 on 12/15/2012
0.6381 +/- 0.0453
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
2:30:02 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
0.34
0.68
0.68
0.00
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
5.262
4.681
4.364
4.130
240.66
13.32
4.32
17.00
12.64
55.28
102.62
48.92
5.4
4.7
3.1
4.7

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------U-232
U-234
U-235
U-238
0.989
0.955
0.997
0.979
5302.50*
4761.50*
4385.50*
4184.40*
5.15E+000
2.85E-001
1.14E-001
3.62E-001
+1+I+I+I-
6.91E-001
1.62E-001
1.18E-001
1.84E-001
1.02E-001 +/- 1.37E-002

1.21E-001 +I- 1.62E-002
1.49E-001 +I- 2.00E-002
1.28E-001 +I- 1. 71E-002
16
4/:>4t'!J
8133
0000056304.CNF
start:
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jj..IIJJJ,
(.,)
'*~"
ROI Type: 1
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6500
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4/24/2013
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Channel Data Report

801:
4/24/2013
Sample Title:
Page
3:20:48 !1M
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Sample Description:
Spectrum File:
Sample Geometry:
DUP 04 DIS
1304053A-UU
09
Shelf 2
u iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_003
3
System Bkgd 55191

<not performed>
Sample Size:
Sample Date/Time:
1.000E+000 +I- O.OOOE+OOO liter

8:04:50 AM
4/5/2013
4/24/2013 11:55:55 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
U232 UU-10A
0.602 mL
0.1876 +/0.0108
0.1746 +/- 0.0033 on 12/15/2012 11:26:47 AM
1.0743 +/- 0.0648
0.150 MeV
PEAK
Energy
(MeV)
Nuclide
U-232
U-234
U-235
U-238
5.286
4.745
4.369
4.173
T
Net
Pk Area
AREA
REPORT
Pk Area
Error %
364.30
21.98
4.49
22.66
Ambient
Backgnd
1. 70
1. 02
0.51
0.34
10.30
42.93
98.45
41.53
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
38.8
6.0
3.0
4.5
Nuclide
Id
Conf.
Energy
(keV)
U-232
U-234
U-235
U-238
0.998
0.998
0.998
0.999
5302.50*
4761.50*
4385.50*
4184.40*
Activity
(pCi/liter )
5.16E+000
3.11E-001
7.84E-002
3.19E-001
+I+I+I+I-
5.80E-001
1.38E-001
7.77E-002
1. 37E-001
~
J.f(J-~1r3
MDA
(pCi/liter
1. 04E- 001
8.92E-002
9.16E-002
6.74E-002
+!+1+I+I-
1.17E-002
l.OOE-002
1. 03E-002
7.57E-003
0000056305.CNF
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Channel Data Report
4/24/2013
Page
3:21:15 flM
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Channel Data Report

369:
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0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
1
0
5
6
4
14
20
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
1
1
1
0
0
0
0
0
1
1
1
0
0
0
1
0
0
1
3
1
1
2
5
10
13
16
3
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
3
0
0
0
0
0
0
0
0
0
1
0
0
0
1
0
0
1
1
5
4
2
10
11
16
3
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
2
3
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
2
0
4
2
6
5
15
16
0
0
1
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
1
1
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
1
1
1
2
2
1
0
6
6
6
11
10
0
0
0
1
0
0
0
0
0
0
0
1
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
1
4
4
5
16
8
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Gldl
Channel Data Report

801:
4/24/2013
0
Sample Title:
3:2l!.i
0
..
0
Page
0
09
809:
817:
825:
833:
841:
849:
857:
865:
873:
881:
889:
897:
905:
913:
921:
929:
937:
945:
953:
961:
969:
977:
985:
993:
1001:
1009:
1017:
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
51.42
Page 1 of 2
4/24/2013 5:32:06 AM
QA SUMMARY REPORT
Review Of QA Results - Pulser Check

Date
Time
: 4/24/2013
: 5:32:06 AM
CHAMBER
AIQ_ha 001
Alpha 002
Alpha 003
Alpha 004
AIQ_ha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha Oil
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha OJ 8
Alpha 019
AIQ_ha 020
Alpha 021
Alpha 022
AIQ_ha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
AIQ_ha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
21f
21f
21f
21f
21f
2If
2If
21f
21f
21f
21f
21f
2lf
2lf
21f
2If
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystiOODC
Alpha Analyst!OODC
Alpha Analyst!OODC
Alpha AnalystiOODC
Alpha Analyst!OODC
A!Qha Analyst!OODC
Alpha Analyst!OODC
Alpha Ana!Yst I OODC
A!Pha Analyst!OODC
Alpha Analyst!OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
DATE
4/24/2013 5:07:46 AM
4/24/2013 5:07:47 AM
4/24/2013 5:07:48 AM
4/24/2013 5:07:48 AM
4/24/2013 5:07:49 AM
4/24/2013 5:07:50 AM
4/24/2013 5:07:51 AM
4/24/2013 5:07:52 AM
4/24/2013 5:07:53 AM
4/24/2013 5:07:54 AM
4/24/2013 5:07:54 AM
4/24/2013 5:07:55 AM
4/24/2013 5:07:56 AM
4/24/2013 5:07:58 AM
4/24/2013 5:08:00 AM
4/20/2013 10:41:48AM
4/24/2013 5:08:02 AM
4/20/2013 10:41:52 AM
4/20/2013 I 0:41 :54 AM
4/24/2013 5:08:04 AM
4/24/2013 5:08:06 AM
4/24/2013 5:08:09 AM
Page 2 of 2
Review of QA Results - Pulser Check

4/24/2013 5:32:06 AM
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha Analyst I OODC
Alpha Analyst!OODC
Alpha Analyst!OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Passed
Passed
Not Done
Passed
Passed
Passed
APPROVED BY:
APPROVAL DATE:
C((t, 't/11
DATE
4/20/2013 10:42:02 AM
4/24/2013 5:08:11 AM
4/24/2013 5:08:14 AM
4/24/2013 5:08:17 AM
4/24/2013 5:08:19 AM
6/12/12
Library Listing Report
Page
12:17:04 PM
*************************************************************************
*****
L I B R A R Y L I S T I NG R E P 0 R T
*****
*************************************************************************
Nuclide Library Title:
Uranium
Nuclide Library Description:

Nuclide
Name
Half-Life
(Seconds)
U-232
U-234
U-235
U-238
2.174E+009
7.731E+012
2.221E+016
1.410E+017
Energy
(keV )
U-232,-234,-235,-238
Energy
uncert. (keV
0.000
0.000
0.000
0.000
5302.500*
4 761. 500*
4385.500*
4184.400*
Yield
(%)
99.8000
99.8000
80.9000
100.2300
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0.0000
0.0000
= key line
TOTALS:
Nuclides
Energy Lines
6.1 d 5
SECTION IX
ANALYTICAL DATA (ISOTOPIC THORIUM)
il
Eberline Services
Analysis Sheet
Printed: 4124/2013 5:31 AM

Page 1 of3
13-04053
ThiSO
Run 1
13-04053
Work Order
ThiSO
1
Analysis Code
Run
Date Rece;ved
4/9/2013
4/30/2013
Lab Deadline
Client I Engineering Management Support, Inc.

Project I
West Lake OU-1
Internal
Fraction
Sample
Desc
01
LCS
Login
CPM
Client
ID
~-. -------L~~-~
Sample
Date
Sample
Aliquot
04/09/13 00:00
BLANK
04/09/13 00:00
PZ-305-AI TOT
MBL- - - 1
03
I DUP
~--o~---t-- oo
05
I ~G
06
TRG
1-----
f1
-- ------
PZ-305-AI ToT
PZ-305-AI DIS
40
04/05/13 15:58
+-- -;o----1-a4/a~l1-~-5~8I
DUP 03 TOT
40
04/05/13 15:58
45
__________,_____ .______ _
T~G_-~-------- DUP 03 DIS
l-----~~- i
04/05/13 00:00
Activity Units
pCi
08
TRG I
DUP 04 TOT
41
04/05/13 00:00
I -------~
TRG
- ------~ ------
DUP 04 DIS
---~-----[---
Method I
NAS NS-3004 Mod

-
Instrument Type
Alpha Spectroscopy
Radiometric Tracer I
Th-229
Radiometric Sol# I
Th-18a
Tracer Act (dpm/g) I
Carrier
Carrier Cone (mg/ml)
22.467
. ---------
1.0000E+OO
-------~-----
----~----:
------+----t------- ------------------- ~---~--I

.
1.0000E+OO
l
~--!1
---~----
-----+--
---1-m;aoE-:ao
--1-------------------T-----~---=f------41
04/05/13 00:00
1.0000E+OO
~.-~--------- ----j+-------------..------------ --- ---------
---+------------- ---..
1.0000E+OO
1.0000E+OO
07
WA
1.0000E+OO
1.0000E+OO
Matrix I
04/05/13 00:00
1----09
Report Level
Aliquot Units
1.0000E+OO
I'
'
____j_
-----t~--t--------------~-------1
r-c----~---t
--+~------------'
--1
C:t'
....
~
J!li.:t
""-l
Eberline Services
Analysis Sheet
Internal
Fraction
Sample
Desc
Printed: 412412013 5:31 AM

Page 2 of 3
13-04053
ThiSO
Run 1
Tracer
Aliquot (g)
Tracer Total
ACT (dpm)
Radiometric
Tracer (pCi)
I Radiometric I Grav Carrier I

% Rec
I Added (ml)
Grav Filter
Final (g)
Grav Filter
Tare (g)
j__
1o:~J~ .
5~~ ... ~
1__ 01
Lcs
02
MBL
0.2341
DUP
0.2330 I
on1s1
04
e---06
TRG
1
07
08
I TRG
0.4740
5.2 I
5.2
o.oo[
0.00 I
0~2313
5.2
0.2328_- 5.2
--~-
~-
0.00 I
5.3
0.00
0.00
0.001
I
--
-------+------~----j-
---r--~1
----+---
+---~----+-----+--~-
ii
I
-----tj-T~
1I'-~---- ~
I
c---1----~-
Ii
II
'--1
III
-1~---i ----+-~-r--~----t
-1 -r ~--+
: :
!
+--
,I
I
II
,
II
--
l:
I
--+-
1-~-=11 --~---=11 - - - - - - -+-
--+-
+--
-----+-------J-.--.--~-1
. -~+- i-~
- -- , __
-----+-------+~-
u-~
~~-
(~)
!
!
---j-~---+------+----+---
~ll
1----~---~----~ -------f-~----~--J
______ L__________+-----!
1
f--
j_J
I
i
i
------r----
SAF
2*
----+--------1
1
I
SAF
1*
-1.
I
------~-'
f--
Mean
% Rec
I_
1~2324 ~-------~~ ---~~r--~-~R--
TRG i
Grav
% Rec
L_~.00 --t ------- ----+--~---~- I
Grav Filter
Net(g)
Eberline Services
Analysis Sheet
Printed: 412412013 5:31 AM

Page 3 of3
13-04053
ThiSO
Run 1
Internal
Fraction
Sample
Desc
Rough Prep
Date
I
I
Rough Prep
By
'
01
LCS
02
MBL
-------
_o~P
04
DO
TRG
L.
I
06
TRG
07
TRG
r-------
TRG
08
~------~ +-~-----
..
JBARNA~
04/19/13 08:4;;+
JBARNA~
04/19/13 08:49
JBARNARD
04/19/13 08:49
JBARNARD
04/19/13 08:49
JBARNARD
-----
Ii
' TRG
f-
L ___
----
---------
04/19/13 08:49 I JBARNARD
-------
I
~-- ~-1-r
I
1-------------
--- -- r -;
----------~--- -----~
----j---i
I
'
--~--~~
- - - - _j_
1-----------
-----
________L__I______~
r-----
JBARNARD
I :::::::: ::~~ -~:::~::: I - -
+~---------
09
Sep t1
By
Sep t1
Date/Time
---------
---
r--
I 04/19/13 08:49
--------
Sep tO
By
I
04119/13 08:49
i
1
Sep tO
Date/Time
Prep
By
-------~-~----------
1------
05
Prep
Date
I
I
------
--------
--- - - -
I
I
- ~-~--------~-+-~----- ---I
-~-JI
- - t----
iI
-~
r-----
-~
j---------
i
I
~-----
+-----I
I
----------- --
I
I
t- ---~----~-----~-
I
I
---~
----~---~~--
--~------
--
I
I
I
11&1!,
.....
t'lli.
SAF1 is used for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
Eberline Services
Printed: 4/25/2013 8:33AM

Page 1 of 3
Work Order: 13-04053-ThiS0-1
LCS
Known
LCS
%R
LCS
Flag
120.46
OK
RPD
Flag
MDA
Flag
Lab
Fraction
Nuclide
Sample
Desc
Client
Identification
Activity
Units
01
TH-228
LCS
LCS
pCi/1
6.21E+OO
9.18E-01
1.04E-01
02
TH-228
MBL
BLANK
pCi/1
3.59E-02
6.27E-02
1.12E-01
03
TH-228
DUP
PZ-305-AI TOT
pCi/1
2.14E-01
1.29E-01
1.36E-01
04
TH-228
DO
PZ-305-AI TOT
pCill
2.37E-01
1.33E-01
1.29E-01
OK
05
TH-228
TRG
PZ-305-AI DIS
pCi/1
1.33E-02
4.77E-02
1.08E-01
OK
06
TH-228
TRG
DUP 03 TOT
pCi/1
1.60E-01
1.01E-01
9.97E-02
OK
07
TH-228
TRG
DUP 03 DIS
pCi/1
3.19E-02
5.25E-02
9.19E-02
OK
08
TH-228
TRG
DUP 04 TOT
pCi/1
2.92E-01
1.38E-01
8.11E-02
OK
09
TH-228
TRG
DUP 04 DIS
pCi/1
-6.41E-03
3.80E-02
9.02E-02
OK
Results
Error Estimate
MDA
5.15E+OO
Blank
Flag
OK
--
OK
---
NA
OK
1----
~
0
.!/l
~
'ii
c:
q;
1------
rn
-'=
11----
~-
---
c.i
.5
~
0
c..
c..
:::1
...c
en
Cll
~I
E
en
IV
c
Cll
IV
:!:
en
c
;:
Cll
Cll
c
c
c,
w
t~ll
>hi ..
Ul
a~
---~----1----------
-1------
OK
Lab
Fraction
Nuclide
01
TH-228
~
Ill
1::
<
Mean
%Rec
Grav
%Rec
SAF
0.00
0.00
TH-228
04/09/13 00:00
1.00E+OO
108.92
0.00
0.00
03
TH-228
DUP
04/05/13 15:58
1.00E+OO
120.56
0.00
0.00
04
TH-228
DO
04/05/13 15:58
1.00E+OO
107.45
0.00
0.00
U)
05
TH-228
TRG
04/05/13 15:58
1.00E+OO
95.12
0.00
0.00
06
TH-228
TRG
04/05/13 00:00
1.00E+OO
118.78
0.00
0.00
07
TH-228
TRG
04/05/13 00:00
1.00E+OO
107.46
0.00
0.00
08
TH-228
TRG
04/05/13 00:00
1.00E+OO
102.94
0.00
0.00
TH-228
TRG
04/05/13 00:00
1.00E+OO
77.20
0.00
0.00
.!/I
Radiometric
%Rec
112.82
Sample
Aliquot
1.00E+OO
02
Sample
Date
04/09/13 00:00
a::
Sample
Desc
LCS
-"
MBL
----~--
1-
Q.
Q.
:I
...c
<f)
]I
Q)
Q)
Cl
I'll
I'll
:E
Cl
;:
Q)
Q)
a,
c
w
...en
~
t.n.....
~
Sep t1
Date/Time
~-
09
Sep to
Date/Time
1--------
~----------
c.i
..5
Printed: 4/25/2013 8:33AM

Page 2 of 3
Eberline Services

a::
8
.!/!
i;;
Lab
Fraction
Nuclide
Sample
Desc
Counting
Date/Time
01
TH-228
LCS
02
TH-228
03
Eff
Alpha_014
170 4.88 E+02
1.40 E-02
18.5
MBL
04/24/13 11:57
A_Spec
Alpha_018
170 2.62 E+OO
1.40 E-02
17.8
TH-228
DUP
04/24/13 11:57
A_Spec
Alpha_022
170 1.46 E+01
2.00 E-02
15.3
04
TH-228
DO
04/24/13 11:57
A_Spec
Alpha_024
170 1.61 E+01
1.70 E-02
17.1
en
05
TH-228
TRG
04/24/13 11 :57
A_Spec
Alpha_025
170.02 8.10 E-01
7.00 E-03
17.4
....
06
TH-228
TRG
04/24/13 11 :57
A_Spec
Alpha_027
170.02 1.21 E+01
1.10 E-02
07
TH-228
TRG
04/24/13 11:57
A_Spec
Alpha_029
170 2.47 E+OO
9.00 E-03
19.5
08
TH-228
TRG
04/24/13 11:57
A_Spec
Alpha_033
170 2.03 E+01
4.00 E-03
18.2
09
TH-228
TRG
A_Spec
Alpha_034
170 -3.40 E-01
2.00 E-03
..c:
Q.
Q.
::s
en
....
c
Cl
E
Cl
Cl
Cll
c
Cll
:E
Cl
c
;::
Cl
Cl
c
'51
c
r-.~
Bkg
CPM
A_Spec
uv
Counts
04/24/13 11:56
llli:it~
Count
Time
Carrier
.E
......
Halflife
(days)
Detect
--
~I
Printed: 4/25/2013 8:33AM

Page 3 of 3
Eberline Services
04/24/13 11:57
---
----
----
----
~-
17.3
18.6
Eberline Services
0::
LCS
Flag
98.67
OK
RPD
Flag
MDA
Flag
Sample
Desc
Client
Identification
Activity
Units
01
TH-230
LCS
LCS
pCi/1
5.40E+OO
8.20E-01
8.40E-02
TH-230
MBL
BLANK
pCi/1
1.42E-01
9.25E-02
7.74E-02
TH-230
DUP
PZ-305-AI TOT
pCi/1
4.72E-01
1.82E-01
9.47E-02
TH-230
DO
PZ-305-AI TOT
pCi/1
2.62E-01
1.35E-01
1.09E-01
OK
Error Estimate
Results
MDA
LCS
Known
LCS
%R
Nuclide
5.48E+OO
Blank
Flag
OK
---
02
~
Lab
Fraction
~-----
Printed: 4/25/2013 8:33AM

Page 1 of 3
- - - - - --
03
OK
NA
OK
OK
- - - - - t---
04
--
U)
05
TH-230
TRG
PZ-305-AI DIS
pCi/1
1.31E-01
9.80E-02
9.63E-02
OK
06
TRG
DUP 03 TOT
pCI/1
1.47E+OO
3.58E-01
8.52E-02
J:
TH-230
1-
OK
07
TH-230
TRG
DUP 03 DIS
pCi/1
8.03E-02
6.76E-02
7.16E-02
OK
08
TH-230
TRG
DUP 04 TOT
pCi/1
3.32E-01
1.46E-01
7.42E-02
OK
09
TH-230
TRG
DUP 04 DIS
pCi/1
4.93E-02
6.41E-02
8.86E-02
.!2
~
iV
t---
I
!
---
.5
~
0
c..
c..
:I
en
....
c
Cl)
~I
E
Cl)
Cl
Ill
Ill
:E
Cl
;:
Cl)
Cl)
a,
c
111.J
...
t.n
~
t.~
OK
Eberline Services
a:
or-
u
.!!!
Sample
Desc
Sample
Date
01
TH-230
LCS
04/09/13 00:00
1.00E+OO
112.82
0.00
0.00
02
TH-230
MBL
04/09/13 00:00
1.00E+OO
108.92
0.00
0.00
03
TH-230
DUP
04/05/13 15:58
1.00E+OO
120.56
0.00
0.00
04/05/13 15:58
1.00E+OO
107.45
0.00
0.00
"'s:::
C(
TH-230
-.c
1-
J
.E
~
0
c.
c.
::I
(/)
....r::
Cll
Cll
Cl
ns
ns
r::
:E
Cl
r::
;:
Cll
Cll
r::
c,
r::
w
u~
tl
SAF
TRG
04/05/13 15:58
1.00E+OO
95.12
0.00
0.00
06
TH-230
TRG
04/05/13 00:00
1.00E+OO
118.78
0.00
0.00
07
TH-230
TRG
04/05/13 00:00
1.00E+OO
107.46
0.00
0.00
08
TH-230
TRG
04/05/13 00:00
1.00E+OO
102.94
0.00
0.00
TH-230
__l TRG
-
SeptO
DaterTime
Sept1
DaterTime
1--
TH-230
-~----
....tlr,
DO
Sample
Aliquot
05
09
~I
--~
en
Mean
%Rec
Grav
%Rec
Nuclide
04
Radiometric
o/o Rec
Lab
Fraction
.g
Printed: 4/25/2013 8:33 AM

Page 2 of 3
04/05/13 00:00
--
- -
1.00E+OO
-----
---
0.00
77.20
-----
--
0.00
Eberline Services
Q:
Printed: 4/25/2013 8:33 AM

Page 3 of 3
Lab
Fraction
Nuclide
Sample
Desc
Counting
Date/Time
01
TH-230
LCS
02
TH-230
03
Halflife
(days)
Count
Time
Counts
Bkg
CPM
Eff
Detect
Carrier
04/24/13 11 :56
A_Spec
Alpha_014
170 4.24 E+02
7.00 E-03
18.5
MBL
04/24/13 11:57
A_Spec
Alpha_018
170 1.03 E+01
4.00 E-03
17.8
TH-230
DUP
04/24/13 11:57
A_Spec
Alpha_022
170 3.28 E+01
7.00 E-03
15.3
04
TH-230
DO
04/24/1311:57
A_Spec
Alpha_024
170 1.81 E+01
1.10 E-02
17.1
05
TH-230
TRG
04/24/13 11 :57
A_Spec
Alpha_025
170.02 8.15 E+OO
5.00 E-03
17.4
06
TH-230
TRG
04/24/13 11:57
A_Spec
Alpha_027
170.02 1.14 E+02
7.00 E-03
17.3
07
TH-230
TRG
04/24/13 11:57
A_Spec
Alpha_029
170 6.32 E+OO
4.00 E-03
19.5
08
TH-230
TRG
04/24/13 11:57
A_Spec
Alpha_033
170 2.35 E+01
3.00 E-03
18.2
09
TH-230
TRG
04/24/13 11 :57
A_Spec
Alpha_034
170 2.66 E+OO
2.00 E-03
18.6
~-------
'f"""
-
8
.!/l
;;;
c:::
'<1:
en
-.r:.
1-
-I
--
.E
~
0
Q.
Q.
..
:::l
en
~I
c
Cll
E
Cll
Cl
Cll
c
Cll
:E
Cl
c
.::
Cll
Cll
c
'0,
c
1:1!11
~
u~
!IJ1
-------
Eberline Services
~
c:
:::s
a::
or--
0
(.)
.~
~
<II
c:
<:(
LCS
Known
Nuclide
Sample
Desc
Client
Identification
Activity
Units
01
TH-232
LCS
LCS
pCi/1
5.82E+OO
8.70E-01
6.68E-02
02
TH-232
MBL
BLANK
pCI/1
2.05E-03
2.87E-02
8.20E-02
TH-232
DUP
PZ-305-AI TOT
pCi/1
1.51E-01
9.69E-02
7.53E-02
Results
Error Estimate
MDA
5.15E+OO
LCS
%R
LCS
Flag
112.94
OK
RPD
Flag
MDA
Flag
Blank
Flag
OK
OK
NA
OK
OK
-----
---~----
04
Lab
Fraction
03
Printed: 4/25/2013 8:33 AM

Page 1 of 3
DO
PZ-305-AI TOT
pCi/1
1.95E-01
1.11E-01
7.57E-02
OK
TRG
PZ-305-AI DIS
pCi/1
5.87E-02
6.42E-02
7.67E-02
OK
TRG
DUP 03 TOT
pCi/1
5.99E-02
6.39E-02
8.85E-02
OK
DUP 03 DIS
pCi/1
-6.46E-03
2.59E-02
6.65E-02
OK
DUP 04 TOT
pCi/1
2.82E-01
1.35E-01
8.46E-02
OK
DUP 04 DIS
pCi/1
5.23E-02
6.38E-02
7.72E-02
OK
TH-232
----------- ----------
en
05
.r;
06
-1-
TH-232
--
TH-232
---------------- - - - -
07
TH-232
TRG
- - - - - - - - - f--
08
TH-232
TRG
09
TH-232
TRG
------
c.i
.:
~
0
c.
c.
::I
en
~I
c
Ill
E
Ill
0'1
ns
c
ns
:E
0'1
;:
Ill
Ill
c;,
c
w
l:i~
flo.'
_L._
---
------
Eberline Services
tt
8
.!/1
~
c::
i;j
<(
Sample
Date
01
TH-232
LCS
04/09/13 00:00
1.00E+OO
112.82
0.00
0.00
02
TH-232
MBL
04/09/13 00:00
1.00E+OO
108.92
0.00
0.00
03
TH-232
DUP
04/05/13 15:58
1.00E+OO
120.56
0.00
0.00
04
TH-232
DO
04/05/13 15:58
1.00E+OO
107.45
0.00
0.00
en
05
TH-232
TRG
04/05/13 15:58
1.00E+OO
95.12
0.00
0.00
J:
06
TH-232
TRG
04/05/13 00:00
1.00E+OO
118.78
0.00
0.00
07
TH-232
TRG
04/05/13 00:00
1.00E+OO
107.46
0.00
0.00
08
TH-232
TRG
04/05/13 00:00
1.00E+OO
102.94
0.00
0.00
09
TH-232
TRG
04/05/13 00:00
1.00E+OO
77.20
0.00
0.00
1-
Q.
Q.
:I
f/)
c
Gl
E
Gl
Cl
CG
c
CG
:::E
Cl
c
c
Gl
Gl
.5
Cl
c
w
u~
lillj,hM
SAF
G~
Radiometric
%Rec
Mean
%Rec
Sample
Desc
Sample
Aliquot
Grav
%Rec
Nuclide
.5
c:
.S!
Lab
Fraction
Printed: 4/25/2013 8:33AM

Page 2 of 3
Sep tO
Date/Time
Sep 11
Date/Time
Eberline Services
1:
:=
a:
or-
.!/!
~
Ill
1:
oct
Halflife
(days)
Count
Time
Bkg
CPM
Nuclide
Sample
Desc
Counting
Date/Time
01
TH-232
LCS
04/24/13 11 :56
02
TH-232
MBL
04/24/13 11:57
A_Spec
Alpha_018
170 1.50 E-01
5.00 E-03
17.8
TH-232
DUP
04/24/13 11:57
A_Spec
Alpha_022
170 1.05 E+01
3.00 E-03
15.3
TH-232
DO
04/24/1311:57
A_Spec
Alpha_024
170 1.35 E+01
3.00 E-03
17.1
TH-232
TRG
04/24/13 11:57
A_Spec
Alpha_025
170.02 3.66 E+OO
2.00 E-03
17.4
Detect
Carrier
A_Spec
Alpha_014
Counts
170 4.57 E+02
3.00 E-03
Eft
18.5
i
r-------1----- ---
03
---
04
Lab
Fraction
r---~-----
.g
Printed: 4/25/2013 8:33AM

Page 3 of 3
-~-
--
en
-------
.J:
06
TH-232
TRG
04/24/13 11:57
A_Spec
Alpha_027
170.02 4.64 E+OO
8.00 E-03
17.3
07
TH-232
TRG
04/24/13 11 :57
A_Spec
Alpha_029
170 5.10 E-01
3.00 E-03
19.5
08
TH-232
TRG
04/24/13 11:57
A_Spec
Alpha_033
170 2.00 E+01
0.00 E+OO
18.2
09
TH-232
TRG
04/24/13 11:57
A_Spec
Alpha_034
170 2.83 E+OO
1.00 E-03
18.6
05
1-
--~--
1---
!---------
.E
t:
0
Q.
Q.
:I
rJ)
jl
u
....c
Cll
Cll
Cl
IU
IU
::E
Cl
;:
Cll
Cll
a,
c
w
1<131
l-'
Ul
(O
~-
Count Room Report

Internal
(I Fraction
\~
Sample
Desc
Client
ID
LCS -~-- LCS
03
DUP
ll(L o:;--1 D-o-t
\S L_-~:---~_l_!_~G-06
Tracer
Aliquot (g)
Tracer
ACT (dpm)
TRG
04/05/1315:58
1.0000
PZ-305-AITOT
; 04/05/1315:58
1.0000
1---CU315
PZ-305-AI DIS
DUP 03 TOT
--~-----r
~~-r----~-~---~-
04/05~~.:~-5~58
04/05/13 00:00
----------r----------t
i
~--r---tf----J
:
L~L-
1.0~00-
0~2286
__ - - -
~0000
0.2324
:i
---
Radiometric
% Rec
5.2011
0.00
'I . 0.00
o.oo I
5.1360
0.00
5.2213
0.00 !
SAF
2*
SAF
1*
l__ o.o~L
5.2595_____________
5.2348
1
10.6494
Ii
f-----r----~
,
__
0.2330
Radiometric
Tracer (pCi)
'
l : :__
--+1'
-----------r----~---+
-----~----------r--:----
----r=-- ---1- i ---~--- t-~---+--J-T---=

-+'I-------------------+--------+_
---i
+-,Ii
!'
U1
tn
PZ-305-AI TOT
-.
Sample
Aliquot
04/09/13 00:00
-----~---~---------------+------
11"-1.
Sample
Date
1.000~-~4740
021~- MB-L~BLAN-K--~-=-0;1o9/~oo:~~-- --1.ooo~~2-34-~r01 I"'(
Printed: 4/24/2013 5:31 AM

Page 1 of 1
13-04053-ThiS0-1 (pCi/1) in WA
Tracer ID: Th-18a
/\...- (~
--------~-
-r-------------+------------l---------___j
-~- ---------------+--+---
-I
t------~--1---~---~----------
i'
II
t------t---r-~
I
I
I
i --j------t----1-
Eberline Services
Page 1 of 1
Printed: 4/19/2013 8:49AM
JBARNARD
Th-228
Th-8b
Th-230
Th-1b
Th-232
Th-8b
Error
Estimate
Date
103.560
4/19/2013
5.151
0.1
--
23.525
4/19/2013
5.481
0.1
103.560
4/19/2013
5.151
0.1
---
Tracers
fraction
Activity
dpmlg

Solution
Date
Volume
Used(g)
Approx
Addition
Tracer
LCS
Isotope
Sol#
01
Th-229
Th-18a
22.467
4/19/2013
0.4740
0.2200
02
Th-229
Th-18a
22.467 4/19/2013
0.2341
0.2200
03
Th-229
Th-18a
22.467 4/19/2013
0.2330
0.2200
04
Th-229
Th-18a
22.467 4/19/2013
0.2315
0.2200
0.~
~J ~: 24::~: J.
474(:J
05
Th-229
Th-18a
22.467 4/19/2013
0.2286
0.2200
06
Th-229
Th-18a
22.467
4/19/2013
0.2324
0.2200
..-i~:;"
:.~ . -~ .!.
07
Th-229
Th-18a
22.467 4/19/2013
(!.2313
0.2200
. .e
tt
:~~~~;:::;t.
::::::;2 il
:?:~:.:!. :.: :
08
I Th-229
Th-18a
22.467
4/19/2013
0.2328
0.2200
09
Th-18a
22.467
4/19/2013
0.2373
0.2200
-C-J::
""'0
Th-229
ll
::::~
.::::::::
-~:~:; 2~57:5
--~--------~------+-------~---~--~--------~------~
I . ._,._.J
G!l
~...
en
Q)
Version 2.0 08/99
~~:!:I :::!167 ,,.J

0. I 1;::)~) :,
-[1:: :?~:::~::~::1
<HHl~) ~
Added
pCi
Matrix Spike
Eberline Analytical
Printed: 4/19/2013 8:49AM

Page 1 of 1
Aliquot Worksheet
JBARNARD
Lab
Fraction
Sample
Muffle Data
ClientiD
Type
Ratio
Post/Pre
LCS
BLANK
PZ-305-AI TOT
PZ-305-AI TOT
PZ-305-AI DIS
DUP 03 TOT
DUP 03 DIS
DUP04 TOT
DUP 04 DIS
LCS
MBL
DUP
DO
TRG
TRG
TRG
TRG
TRG
01
02
03
04
05
06
07
08
09
Dilution Data
Aliquot Data
MS Aliquot Data
H-3 Solids Only

Water Added
(ml)
'
NoofDiis
Oil Factor
Ratio
Net Equiv
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
r- 1.0000E+OO
1.0000E+OO
'
..
Aliquot
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
1.0000E+OO
Aliquot
NetEquiv
H3 Dist
Aliq
--
-~
-
--[--------
r-~--r-
'.
f--
...
--
'
.
--
.... ..
.
.
.
. ...
Commenm
f!)
~~oil
en
II-
Techo;c;ao
------
L _ ____
.....
I
~
_/
Date
4, W,.L :<
Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1304053A-TH
01
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_014
14
System Bkgd 55196
<not performed>
Sample Size:
Sample Date/Time:

4/24/2013
8:07:49 AM
4/24/2013 11:56:35 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.474 mL
0.2082 +/- 0.0125
0.1846 +/- 0.0034 on 12/15/2012 11:26:44 AM
1.1282 +/- 0.0711
Control Certificate Name: NatTh Th-8

TH-232
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.761
5.379
4. 871
4.634
3.960
Net
Pk Area
1.129355 +/-
AREA
REPORT
Pk Area
Error %
7.28
487.62
376.96
423.81
457.49
0.092575
87.08
8.90
10.13
9.54
9.17
Ambient
Backgnd
2.72
2.38
2.04
1.19
0.51
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
0.0
41.8
6.3
14.7
13.6

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.960
0.998
1. 000
0.993
0.993
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
9.50E-002
6.21E+000
4.82E+000
5.40E+000
5.82E+000
+I+I+I+!+1-
8.35E-002
9.18E-001
5.69E-001
8.20E-001
8.70E-001
MDA
(pCi/liter
1.12E-001
1.04E-001
9.96E-002
8.40E-002
6.68E-002
+!+I+I+I+!-
1.32E-002
1.23E-002
1.18E-002
9.92E-003
7.89E-003
AG
1/(~str-;
i162
0000056310.CNF
Start:
1:3507. 9(kev)
Stop : 1024:6512.2(kev)
Acq. Start :wed Apr 24 11:56:35 2013
60
55
50
45
40
35
V'l
-I-'
s:::::
::::s
8 30
25
20
15
10
5
0
II
0!!!!1
01\!1!\!D!
OO!i\1/:jl
010
OftD\!fp!lip:l!!!
4000
4500
(:;!;)
*'""'
en
(..,.)
ROI Type: 1
\'!UI~'
i!
11J1f!'j'l\!'10(''!1"ifl
5000
Energy(kev)
!!\!
I)!IPD[\IJOJJ\IJ
!llj
II
6000
5500
ROI Type: 3
010
OOI!!)OIJ!II!!l
6500
Channel Data Report
4/24/2013
Page
3:23:! WI
*******************************************************
s p E C T R A L DATA R E P 0 R T *****
*****
*******************************************************
Sample Title:
01
Elapsed Live time:

Elapsed Real Time:
10200
10200
1:
9:
17:
25:
33:
41:
49:
57:
65:
73:
81:
89:
97:
105:
113:
121:
129:
137:
145:
153:
161:
169:
177:
185:
193:
201:
209:
217:
225:
233:
241:
249:
257:
265:
273:
281:
289:
297:
305:
313:
321:
329:
337:
345:
353:
361:
10200
0
0
0
0
0
0
0
0
0
0
0
1
1
1
3
2
4
9
7
16
13
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
1
0
0
0
0
0
2
4
10200
0
0
0
0
0
0
0
0
0
0
0
0
0
0
2
4
5
9
11
13
17
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
2
4
0
0
0
1
0
1
0
2
0
0
0
1
0
0
0
1
1
5
9
7
15
12
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
1
0
3
2
2
1
0
0
0
0
0
0
1
0
0
0
0
0
0
0
1
1
5
6
11
11
12
10
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
1
0
0
1
1
0
4
2
0
0
0
0
0
0
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Channel Data Report

369:
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~ .U~:J
Channel Data Report

801:
4/24/2013
0
Sample Title:
3:23'''
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Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1304053A-TH
02
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_018
18
System Bkgd 55197
<not performed>
Sample Size:
Sample Date/Time:

8:07:49 AM
4/24/2013
4/24/2013 11:57:05 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.234 mL
0.1935 +/- 0.0159
0.1776 +/- 0.0033 on 12/15/2012
1.0892 +/- 0.0920
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.874
5.335
4.872
4.664
3.855
Net
Pk Area
AREA
REPORT
Pk Area
Error %
1.47
2.62
172.98
10.32
0.15
1:57:26 PM
240.74
173.91
14.95
63.32
1397.8
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
1. 53
2.38
1. 02
0.68
0.85
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
3.9
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.997
0.978
1. 000
1. 000
0.899
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
2.06E-002
3.59E-002
2.38E+000
1.42E-001
2.05E-003
+I+I+!+!+I-
4.98E-002
6.27E-002
3.84E-001
9.25E-002
2.87E-002
AG
q/;~1{3
MDA
(pCi/liter
9.98E-002
1.12E-001
8.67E-002
7.74E-002
8.20E-002
+!+!+I+I+!-
1. 61E-002
1. 81E-002
1.40E-002
1.25E-002
1.32E-002
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Channel Data Report

801:
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6171
Sample Description:
Spectrum File:
Sample Geometry:
PZ-305-AI TOT-DUP
1304053A-TH
03
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_022
22
System Bkgd 55198
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:07:49 AM
4/24/2013 11:57:06 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.233 mL
0.1846 +/- 0.0156
0.1531 +/- 0.0029 on 12/15/2012
1.2056 +/- 0.1043
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
6.000
5.349
4.870
4.627
3.975
Net
Pk Area
AREA
REPORT
Pk Area
Error %
0.45
14.60
164.30
32.81
10.49
1:57:26 PM
807.07
57.86
15.38
34.94
62.21
Ambient
Backgnd
2.55
3.40
1. 70
1.19
0.51
FWHM
(keV)
Reagent
Backgnd
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
6.2
3.1
6.6
3.1
3.1
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.889
0.987
1. 000
0.989
0.997
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
6.63E-003
2.14E-001
2.37E+000
4.72E-001
1.51E-001
+!+!+I+I+I-
5.36E-002
1.29E-001
3.92E-001
1.82E-001
9.69E-002
MDA
(pCi/liter
1.24E-001
1.36E-001
1. 06E- 001
9.47E-002
7.53E-002
+I+I+I+1+1-
2.05E-002
2.24E-002
1. 75E-002
1.57E-002
1.25E-002
llC
1/JSifJ
5171.
0000056312.CNF
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Acq. start :wed Apr 24 11:57:06 2013
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3:l.t
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Channel Data Report

801:
4/24/2013
0
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Page
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-305-AI TOT
1304053A-TH
04
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_024
24
System Bkgd 55199
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:07:49 AM
4/24/2013 11:57:07 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.231 mL
0.1838 +/- 0.0156
0.1710 +/- 0.0032 on 12/15/2012
1. 0745 +/- 0.0933
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.779
5.354
4.854
4.617
3.970
Net
Pk Area
AREA
REPORT
Pk Area
Error %
3.47
16.11
162.47
18.13
13.49
2:02:15 PM
129.55
53.71
15.46
48.73
54.53
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
1.53
2.89
1.53
1.87
0.51
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
4.7
13.9
4.7
6.2

Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.974
0.989
0.998
0.984
0.996
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
5.14E-002
2.37E-001
2.35E+000
2.62E-001
1.95E-001
+I+I+I+I+1-
MDA
(pCi/liter
6. 71E-002
1.33E-001
3.91E-001
1.35E-001
l.llE-001
ltG
'{jJSI/3
1. OSE-001
1.29E-001
1.03E-001
1. 09E-001
7.57E-002
+I+1+1+1+I-
1. 75E-002
2.14E-002
1. 71E-002
1.82E-002
1.26E-002
0000056315.CNF
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i186i
Channel Data Report

801:
Page
4/24/2013
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Sample Title:
04
ChannelJ------I-------I-------I-------J-------J-------1-------I-------J
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Sample Description:
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Sample Geometry:
PZ-305-AI DIS
1304053A-TH
05
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_025
25
System Bkgd 55200
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:07:49 AM
4/24/2013 11:57:08 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.229 mL
0.1651 +/- 0.0147
0.1736 +/- 0.0032 on 12/15/2012
0.9512 +/- 0.0866
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.802
5.332
4.873
4.620
4.040
Net
Pk Area
0.81
0.81
144.15
8.15
3.66
AREA
1:57:27 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
359.14
359.14
16.38
72.72
107.88
1.19
1.19
0.85
0.85
0.34
Reagent
Backgnd
FWHM
(keV)
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
3.5
3.1
3.1

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
0.988
0.976
1. 000
0.986
0.991
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
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4.06E-001
9.80E-002
6.42E-002
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1.08E-001
9.65E-002
9.63E-002
7.67E-002
+I+I+1+1+1-
1.90E-002
1.88E-002
1.69E-002
1.68E-002
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5182
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801:
4/24/2013
0
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Sample Description:
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Sample Geometry:
DUP 03 TOT
\\OR-ALPHAl\Canberra\ApexAlpha\Root\Data\00000563
1304053A-TH
06
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Detector Name:
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Alpha_027
27
System Bkgd 55201
<not performed>
Sample Size:
Sample Date/Time:
l.OOOE+OOO +/- O.OOOE+OOO liter

4/5/2013
8:07:49 AM
4/24/2013 11:57:09 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.232 mL
0.2052 +/- 0.0165
0.1728 +/- 0.0032 on 12/15/2012
1.1878 +I- 0.0982
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
2:27:41 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
5.780
5.384
4.864
4.639
3.983
0.81
12.13
182.15
113.81
4.64
359.14
61.14
14.56
18.48
105.45
1.19
1.87
0.85
1.19
1.36
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O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.2
6.4
10.0
4.1
3.2

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
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TH-228
TH-229
TH-230
TH-232
0.975
0.999
1. 000
0.994
0.999
5850.00*
5400.00*
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3.86E-002
1. OlE- 001
3.73E-001
3.58E-001
6.39E-002
A;G
lf/JS//J
8.74E-002
9.97E-002
7.77E-002
8.52E-002
8.85E-002
+!+I+!+!+!-
1.38E-002
1.57E-002
1.23E-002
1.34E-002
1.40E-002
0000056314.CNF
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4/24/2013
Page
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Channel Data Report

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Q1Si
Channel Data Report

801:
4/24/2013
0
Sample Title:
3:21tU
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619.1
Sample Description:
Spectrum File:
Sample Geometry:
DUP 03 DIS
1304053A-TH
07
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_029
29
System Bkgd 55202
<not performed>
Sample Size:
Sample Date/Time:

8:07:49 AM
4/5/2013
4/24/2013 11:57:10 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.231 mL
0.2090 +/- 0.0167
0.1945 +/0.0036 on 12/15/2012
1. 0746 +/- 0.0881
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
5.757
5.405
4.880
4.677
3.949
Net
Pk Area
1.15
2.47
184.66
6.32
-0.51
AREA
2:30:02 PM
REPORT
Pk Area
Error %
249.58
163.78
14.44
82.73
400.63
FWHM
(keV)
Ambient
Backgnd
Reagent
Backgnd
0.85
1.53
0.34
0.68
0.51
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.1
3.1
5.6
3.1
0.0
Nuclide
Id
Conf.
Energy
(keV)
TH-227
TH-228
TH-229
TH-230
TH-232
0.956
1. 000
1. 000
1. 000
0.988
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
Activity
(pCi/liter )
1. 50E-002
3.19E-002
2.35E+000
8.03E-002
-6.46E-003
+I+I+I+I+!-
3.75E-002
5.25E-002
3.68E-001
6.76E-002
2.59E-002
ltG
1/JS/f3
MDA
(pCi/liter
7.80E-002
9.19E-002
6.09E-002
7.16E-002
6.65E-002
+1+I+!+!+!-
1.22E-002
1.44E-002
9.54E-003
1.12E-002
1.04E-002
0000056313.CNF
Live Time :10200o000 sec
Real Time :10200o000 sec
start:
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stop : 1024:6597o5(kev)
Acq o start :wed Apr 24 11:57:10 2013
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6500
Channel Data Report
4/24/2013
3:28:3,
Page
"'
*******************************************************
*****
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Sample Title:
07
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tjj,i:::J4
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369:
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5195
Channel Data Report

801:
Page
4/24/2013
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Sample Title:
07
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~Apex-Alpha'"
Sample Description:
Spectrum File:
Sample Geometry:
DUP 04 TOT
1304053A-TH
08
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_033
04026479A
91132
System Bkgd 55203
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:07:49 AM
4/24/2013 11:57:25 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.233 mL
0.1878 +/- 0.0157
0.1825 +/- 0.0032 on 12/16/2012
1.0294 +/- 0.0879
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
TH-227
TH-228
TH-229
TH-230
TH-232
6.001
5.387
4.883
4.642
3.974
Net
Pk Area
AREA
REPORT
Pk Area
Error %
1.49
20.32
167.00
23.49
20.00
5:49:18 PM
190.02
44.32
15.21
40.95
44.91
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.51
0.68
0.00
0.51
0.00
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
3.0
3.0
7.9
4.5
5.9

Nuclide
Id
Con.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
0.887
0.999
0.999
0.995
0.997
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
2.16E-002
2.92E-001
2.37E+000
3.32E-001
2.82E-001
+I+I+I+I+I-
4.12E-002
1.38E-001
3.88E-001
1.46E-001
1.35E-001
7.61E-002
8.11E-002
8.50E-002
7.42E-002
8.46E-002
+I+I+1+1+1-
1.25E-002
1.33E-002
1.39E-002
1.21E-002
1.39E-002
JtG
tf(~5:/t)
ii197
0000056318.CNF
start:
1:3465.6(kev)
stop : 1024:6503.3(kev)
Acq. Start :wed Apr 24 11:57:25 2013
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.......
c::
:::3
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5000
Energy(kev)
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~ii!u:i,
U)
0:)
ROI Type: 1
ROI Type: 3
6500
Channel Data Report
4/24/2013
3:~''''
Page
*******************************************************
*****
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08
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S2ii6
Channel Data Report

801:
4/24/2013
0
Sample Title:
Page
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Sample Description:
Spectrum File:
Sample Geometry:
DUP 04 DIS
1304053A-TH
09
Shelf 2
Th iso
Detector Name:
Env. Background:
Reagent Blank:
Alpha_034
04026479B
91136
System Bkgd 55204
<not performed>
Sample Size:
Sample Date/Time:

4/5/2013
8:07:49 AM
4/24/2013 11:57:26 AM
170.0 minutes
170.0 minutes
Tracer Certificate:
Tracer Quantity:
Th229 TH-18A
0.237 mL
0.1433 +/- 0.0133
0.1856 +/- 0.0032 on 12/16/2012
0.7720 +/- 0.0731
0.175 MeV
PEAK
Energy
(MeV)
Nuclide
Net
Pk Area
AREA
5:49:43 PM
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
0.34
0.34
0.17
0.34
0.17
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
O.OOE+OOO
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
5.799
5.297
4.887
4.646
4.000
0.66
-0.34
129.83
2.66
2.83
305.43
592.90
17.21
128.85
120.53
3.0
0.0
4.7
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------TH-227
TH-228
TH-229
TH-230
TH-232
0.987
0.946
0.999
0.996
1. 000
5850.00*
5400.00*
4872.00*
4672.00*
3997.00*
1.25E-002 +I-6.41E-003 +I2.41E+000 +I4.93E-002 +I5.23E-002 +/-
3.84E-002
3.80E-002
4.41E-001
6.41E-002
6.38E-002
If(;.
tf(;sfrJ
9.09E-002 +I9.02E-002 +17.76E-002 +I8.86E-002 +I7.72E-002 +/-
1.66E-002
1.65E-002
1.42E-002
1.62E-002
1.41E-002
0000056317.CNF
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Acq. start :wed Apr 24 11:57:26 2013
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ROI Type: 1
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Channel Data Report
4/24/2013
Page
3:~11#.
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*****
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62&6
Page 1 of 2
4/24/2013 5:32:06 AM
ha
QA SUMMARY REPORT

Date
Time
: 4/24/2013
: 5:32:06 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha Oil
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2lf
2lf
21f
21f
2lf
21f
21f
21f
21f
2lf
2lf
2lf
2lf
2lf
21f
21f
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha AnalystlOODC
Alp_ha Analyst! OODC
Alpha AnalystiOODC
Alpha AnalystiOODC
Alpha AnalystlOODC
Alpha Analyst!OODC
Alpha AnalystiOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
DATE
4/24/2013 5:07:46 AM
4/24/2013 5:07:47 AM
4/24/2013 5:07:48 AM
4/24/2013 5:07:48 AM
4/24/2013 5:07:49 AM
4/24/2013 5:07:50 AM
4/24/2013 5:07:51 AM
4/24/2013 5:07:52 AM
4/24/2013 5:07:53 AM
4/24/2013 5:07:54 AM
4/24/2013 5:07:54 AM
4/24/2013 5:07:55 AM
4/24/2013 5:07:56 AM
4/24/2013 5:07:58 AM
4/24/2013 5:08:00 AM
4/20/2013 I 0:41 :48 AM
4/24/2013 5:08:02 AM
4/20/2013 I 0:41 :52 AM
4/20/2013 10:41:54 AM
4/24/2013 5:08:04 AM
4/24/2013 5:08:06 AM
4/24/2013 5:08:09 AM
Page 2 of 2
4/24/2013 5:32:06 AM
CHAMBER
Alpha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha Analyst 1OODC
Alpha Analyst! OODC
Alpha Analyst 1OODC
Alpha Analyst! OODC
Alpha Analystl OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Passed
Passed
Not Done
Passed
Passed
Passed
APPROVED BY:
APPROVAL DATE:
Cf(L. Y/tl
DATE
4/20/2013 10:42:02 AM
4/24/2013 5:08:11 AM
4/24/2013 5:08:14 AM
4/24/2013 5:08:17 AM
4/24/2013 5:08:19 AM
6/12/12
Page
12:16:29 PM
*************************************************************************
*****
LIBRARY LISTING REPORT
*****
*************************************************************************
Thorium
Nuclide
Name
Half-Life
(Seconds)
TH-227
TH-228
TH-229
TH-230
TH-232
6.873E+008
6.034E+007
2.487E+01l
2.379E+012
4.434E+017
Energy
(keV )
Th-227,-228,-229,-230,-232
Energy
Uncert. {keV
0.000
0.000
0.000
0.000
0.000
5850.000*
5400.000*
4872.000*
4672.000*
3997.000*
Yield
(%)
97.5000
99.9400
99.5200
99.8200
100.0000
Yield
Uncert. (Abs. +-)
0.0000
0.0000
0.0000
0.0000
0.0000
key line
TOTALS:
Nuclides
Energy Lines
ti2-GS
SECTION X
ANALYTICAL DATA (RADIUM-226)
Eberline Services
Analysis Sheet
Printed: 412512013 11:37 AM

Page 1 of3
13-04053
Ra226
Run 1
Run
Date Received I
Lab Deadline I
Sample
Aliquot
Client
ID
01
LCS
LCS
04/09/13 00:00
1.0000E+OO
02
MBL
BLANK
04/09/13 00:00
1.5000E+OO
4/9/2013
03
DUP
DUP 03 TOT
45
04/05/13 00:00
1.5000E+OO
4/30/2013
04
TRG
PZ-305-AI TOT
40
04/05/13 15:58
1.5000E+OO
05
TRG
PZ-305-AI DIS
40
04/05/13 15:58
1.5000E+OO.
West Lake OU-1
06
DO
DUP 03 TOT
45
04/05/13 00:00
1.5000E+OO

Project I
Sample
Date
Sample
Desc
Ra226
Analysis Code
Login
CPM
Internal
Fraction
13-04053
Work Order
Report Level
07
TRG
DUP 03 DIS
45
04/05/13 00:00
1.5000E+OO
Activity Units
pCi
08
TRG
DUP 04 TOT
41
04/05/13 00:00
1.5000E+OO
09
TRG
DUP 04 DIS
41
04/05/13 00:00
1.5000E+OO
Aliquot Units
Matrix
Method
Instrument Type
Radiometric Tracer
WA
EPA 903.0 Modified
Alpha Spectroscopy
Ba-133
Radiometric Sol#
Ba-6a
Tracer Act (dpm/g)
1010.144
Carrier
Carrier Cone (mg/ml)
11:1~11
......
~-1,
SAF1tiS: osed for Gross Alpha and all other radionuclides. SAF2 is used for Gross Beta only.
Actual mass exceeded the calibration curve range. Results should be qualified as appropriate .
Eberline Services
Analysis Sheet
Printed: 412512013 11:37 AM

Page 2 of3
13-04053
Ra226
Run 1
Internal
Fraction
Sample
Desc
01
LCS
0.9155
924.8
413.5
99.26
0.0225
0.0282
0.0057
02
MBL
0.9109
920.1
344.6
83.14
0.0225
0.0278
03
DUP
0.9079
917.1
354.8
85.88
0.0227
04
TRG
0.9032
912.4
349.1
84.94
05
TRG
0.9019
911.0
339.5
06
DO
0.9032
912.4
07
TRG
0.9035
08
TRG
09
TRG
Tracer
Aliquot(g)
Tracer Total
ACT(dpm)
Radiometric
Tracer (pCi)
Radiometric GravCa"ier
%Rec
Added(ml)
Grav Filter
Tare (g)
Grav Filter
Net(g)
SAF
1*
SAF
2*
99.26
2.04
1.00
0.0053
83.14
1.86
1.00
0.0293
0.0066
85.88
2.37
1.00
0.0228
0.0301
0.0073
84.94
2.58
1.00
82.73
0.0229
0.0287
0.0058
82.73
2.08
1.00
331.9
80.76
0.0230
0.0286
0.0056
80.76
2.00
1.00
912.7
403.6
98.17
0.0233
0.0305
0.0072
98.17
2.55
1.00
0.9027
911.9
378.2
92.08
0.0223
0.0298
0.0075
92.08
2.64
1.00
0.9057
914.9
365.3
88.64
0.0225
0.0288
0.0063
88.64
2.27
1.00
GravFilter
Final (g)
Grav
%Rec
Mean
%Rec
--
~)
M
-~~
1'\)
* SAE4<is used for Gross Alpha and all other radionuclides. SAF2 isrusedJor Gross Beta only.
Eberline Services
Analysis Sheet
Printed: 412512013 11:37 AM

Page 3 of3
13-04053
Ra226
Run 1
'ill
ll"li
Internal
Fraction
Sample
Desc
01
Rough Prep
Date
Rough Prep
By
Prep
Date
Prep
By
Sep to
Date/Time
Sep tO
By
LCS
04/19/13 08:4 7
JBARNARD
04/24/13 17:09
LWALKER
02
MBL
04119/13 08:47
JBARNARD
04/24/13 17:09
LWALKER
03
DUP
04119/13 08:4 7
JBARNARD
04/24/13 17:09
LWALKER
04
TRG
04/19/13 08:47
JBARNARD
04/24/13 17:09
LWALKER
05
TRG
04/19/13 08:47
JBARNARD
04/24/13 17:09
LWALKER
06
DO
04/19/13 08:47
JBARNARD
04/24/13 17:09
LWALKER
07
TRG
04/19/13 08:47
JBARNARD
04/24/13 17:09
LWALKER
08
TRG
04/19/13 08:4 7
JBARNARD
04/24/13 17:09
LWALKER
09
TRG
04/19/13 08:4 7
JBARNARD
04/24/13 17:09
LWALKER
SAF1is: used for Gross Alpha and all other radionuclidesi ,AF2 is used for Gross Beta only.
Sep t1
Date/Time
Sep t1
By
**Actual mass exceeded~tl)ercalibratiori curve range. Results should be qualified as appropriate.
Eberline Services
Lab
Fraction
Work Order: 13-04053-Ra226-1
Nuclide
Sample
Desc
Client
Identification
RA-226
LCS
LCS
Activity
Units
:::s
a::
02
RA-226
., ------------------
03
RA-226
~
.g
0
(J
.!!/
~
111
~II
MBL
BLANK
DUP
DUP 03 TOT
RA-226
TRG
---------
PZ-305-AI TOT
pCi/1
RA-226
TRG
PZ-305-AI DIS
O.OOE+OOi
4.94E-01:
pCi/1
1.13E+OOi
pCi/1
2.73E-01
RA-226
DUP 03 DIS
pCi/1
2.07E-01
~-t
07
08
RA-226
DUP 04 TOT
pCi/1
7.94E-01
prrlll I 09
RA-226
---
.
~
..
..
1.03E+01 102.04
----------------~-
RPD
Flag
MDA
Flag
OK
Blank
Flag
OK
OK
4.79E-02I
1.40E-01!
3.66E-01/
INV
1.58E-01/
I
,
-----t------------r--------
1.59E-01 \
1.12E-01)
pCi/1
7.33E-01:
2.59E-01 i
1.67E-01j
________ ..._
--------- ---
-~--'
~~
_____ ..j. __
~~~~~~-~---~~---~~--~-~--
~II
1::
q:
1.43E-01 j
2.29E-01 i
1
-----------~--------
06
DUP 03 TOT
-----------+I
O.OOE+OOj
-------------------- -
RA-226
--
LCS
Flag
------------ t--------------t---------+---------- --
------~--~--
05
~------- ---~--
LCS
%R
MDA
--- ~-t------ -- --------t--------------~--~---------
---
--------------
04
' Error Estimate
1.16E+OOj
r- -
pCi/1
-----
~c
'
Results
pCi/1
- --+------
1::
Printed:. 4/26/2013 9:07AM

Page 1 of 3
DUP 04 DIS
pCi/1
2.74E-01
(I)
'i"
~
..5
~
0
Q.
Q.
~~-~~--~~~-+-~ ~~~~--~ ~~.,. ~-
::s
(/)
....c::
c:
.!!
E
Cll
CD
ca
c::
ca
::E
CD
c::
;:;
Cll
Cll
c::
s,
c::
w
en
"~
~
~.~ill
----"!----
Cll
i---
Eberline Services
Nuclide
RA-226
Printed: 4/26/2013 9:07 AM

Page 2 of3
Work Order: 13-04053-Ra226-1
! Sample
Desc
LCS
Sample
Date
Sample
Aliquot
Radiometric
%Rec
Mean
%Rec
Grav
%Rec
99.26;
83.14
Septa
Datemme
SAF
0.00'
99.261
0.00!
83.14:
-----}--- -----+----
4/24/2013 17:09
- ---------+------- - ------+-----
0.001!
85.88
~---
84.94
0.001
------
82.73.
---------
0.001
--- -------t----
o.ool
-~-~r---
80.76
98.17
----+----1
92.08
O.OOi
85.88 i
---i----- - "- . .
84.94)
------~----
4/24/2013 17:09
82.731
4/24/2013 17:09
-- -----t------ -- ------r--
80.76j
98.~;;---
-~~j
88.64
----L-----~----i
'
4/24/201317:09
-tI
4/24/2013 17:09
88.64:
- ___ _j_
I
-r---
------+ ---- --
----+---------
---.! --- - . - --
---+
c:n
!"<,)
R-
(,.,1~
4/24/2013 17:09
-----;--- - 4/24/201317:09
92.08~
--+-- .... 1
4/24/2013 17:09
1--------
Sept1
Date/Time
Printed: 4/26/2013 9:07 AM

Page 3 of 3
Eberline Services
Work Order: 13-04053-Ra226-1
Sample
Desc
Counting
Date/Time
Halflife
(days)
LCS
04/25/13 14:47
Count
Time
Detect
A_Spec
:Aipha_033f
17013.52 E+02
-+---
04/25/13 14:47
A_Spec
Alpha_034f
04/25/13 14:47
A_Spec
Alpha_035f
Bkg
Counts
)2.00 E-03
17011.00 E+OO
!0.00 E+OO
110!1.85 E+01
j3.oo E-03
TRG
A_Spec
Aipha_o4o!_ _____
~~OI1.17 E~~----~~o E-03
DO
A_Spec
Alpha_041'
17013.31 E+01
04/25/13 14:47
A_Spec
Alpha_042i
TRG
04/25/13 14:47
A_Spec
Alpha_o~: --- ~~1;:;;~~~1_,_ -- ----+-------- --
TRG
04/25/13 14:47
A_Spec
Alpha_046
- -- ------ -----
170[8.32 E+OO
4.00 E-03
,1,00 E-03
170 i1.08 E+01
1.00 E-03
~
----
---.--1---
, ..
.E
Q.
Q.
::1
en
.....c
Cl)
E
Cl)
C'l
IG
c
IG
:E
C'l
c
;:
Cl)
Cl)
t:i!~
!">,)
lollol'll
t:n
. - - .. t ..
---. --- .. j_ _____ -----
1.10 E-02
--y
TRG
_j __ _
- --------
18.6
18.3
17.8
-~-----+----i- ..
---:-------------t--~-------
c
c;, I
c
Alpha_03~l---17~13.75 E+O;-n!~~~~ E-03

..
18.2
------+---------- .. ,... -
--~ --~----+------- --"'t ---~--------- -~-- ...
A_Spec
....c:
Eft
CPM
19
19.8
Count Room Report

Printed: 4/251201311:37 AM
Page 1 of 1
13-04053-Ra226-1 (pCi/1) in WA
Tracer ID: Ba-6a
.
Internal
Fraction
;;~
~
'J
Client
ID
Sample
Date
Sample
Aliquot
Tracer
Aliquot(g)
Tracer
ACT(dpm)
Radiometric
Tracer (pCi)
Radiometric
%Rec
SAF
1*
SAF
2*
i
01
LCS
LCS
04/09/13 00:00
1.0000
0.9155
924.7868
413.5000
99.26
2.04
1.00
02
MBL
BLANK
04/09/13 00:00
1.5000
0.9109
920.1402
344.6000
83.14
1.86
1.00
03
DUP
DUP 03 TOT
04/05/13 00:00
1.5000
0.9079
917.1097
354.8000
85.88
2.37
1.00
04
TRG
PZ-305-AI TOT
04/05/13 15:58
1.5000
0.9032
912.3621
349.1000
84.94
2.58
1.00
05
TRG
PZ-305-AI DIS
04/05/13 15:58
1.5000
0.9019
911.0489
339.5000
82.73
2.08
1.00
06
DO
DUP 03 TOT
04/05/13 00:00
1.5000
0.9032
912.3621
331.9000
80.76
2.00
1.00
07
TRG
DUP 03 DIS
04/05/13 00:00
1.5000
0.9035
912.6651
403.6000
98.17
2.55
1.00
08
TRG
DUP 04 TOT
04/05/13 00:00
1.5000
0.9027
911.8570
378.2000
92.08
2.64
1.00
09
TRG
DUP 04 DIS
04/05/13 00:00
1.5000
0.9057
914.8874
365.3000
88.64
2.27
1.00
if'\,J
Sample
Desc
Eberline Services
Page 1 of 1
Printed: 411912013 8:47AM
JBARNARD
Isotope
Sol#
Solution
Date
Ra-226
Ra-5b
411912013
Approx
Addition
0.500
LCS
MS
LCSD
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
LCS
Known
pCi
10.29
0.5181
MS
Error
Estimate
0.473
Tracers
fraction
Isotope
Sol#
01
Ba-133
Ba-6a
02
Ba-133
Ba-6a
Activity
dpmlg
Added
pCi
0.00
LCSD
Error
Estimate
0.000
Known
pCi
MSD
Error
Estimate
O.OOi
Added
pCi
0.000
0.00'1
Volume
Used(g)
1010.144 411912013
--1-
1010.144 411912013
0.9155
0.9109
Approx
Addition
LCS
Tracer
1.0000
1.0000
---
03
Ba-133
Ba-6a
1010.144 411912013
0.9079
1.0000
04
Ba-133
Ba-6a
1010.144 411912013
0.9032
1.0000
05
Ba-133
Ba-6a
1010.144 411912013
0.9019
13::
Ba-133
Ba-6a
1010.144 411912013
0.9032
1.0000
07
Ba-133
Ba-6a
1010.144 411912013
0.903~
1.0000
08
Ba-133
Ba-6a
1010.144 411912013
0.9027,
1.0000
09
Ba-133
Ba-6a
1010.144 411912013
0.9057
1.0000
0~ ~:ii29
1::; ~ :; ~
1.0000
06
(i~ ~5lf.;j_
91 ~:::::::;
~~1" ':~?7
;~j;: 9032
-.. ~;J:: 9fi 1. c;:
- c0 ~:;i e1 ~ )
_, (J 9 ~J ~: ~:~:
OJ
I'
-.. (J =::~c1 :~7

11
'""0
.t~
-J
I
I
-~---
It:~,
i'~)
t ....
,l
(0
Version 2.0 08199
----
:J
9121~57
::\
0.000
1--------+-1~+-1~I-------~---~--------+-L-=-

Solution
Date
Error
Estimate
Matrix Spike
::i
Eberline Analytical
Printed: 4/19/2013 8:48AM

Page 1 of 1
Aliquot Worksheet
JBARNARD
Lab
Fraction
01
02
03
04
05
06
07
08
09
..
Sample
ClientiD
LCS
BLANK
DUP 03 TOT
PZ-305-AI TOT
PZ-305-AI DIS
DUP 03 TOT
DUP 03 DIS
DUP04 TOT
DUP 04 DIS
Type
LCS
MBL
DUP
TRG
TRG
DO
TRG
TRG
TRG
Dilution Data
Muffle Data
r--
Ratio
Post/Pre
Aliquot Data
MS Aliquot Data
',,
'
Oil Factor
No of Oils
'
Ratio
>,
,
'
',
' :
.
.,
Aliquot
Net Equiv.
1.0000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO I
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
Aliquot
NetEquiv
H-3 Solids Only

Water Added
(ml)
H3 Oist
Aliq
1.0000E+.OO
~-
1.soooE:+oo
1..5000E+OO
1.5000E+OO
U5000E+OO
1.5000E+OO
1.5000E+OO.
1.5000E+.OO
1:5000E+OO
---
~-----------
------
J__
.,
...
,'
!----
'
------
',
-
',
~~-----
--
'
!---------''
~-Comments
Q;~
llw
t~)
Techoiciao
<;
3\. I
Date
4,l1_l.:!s---
Eberline Services - Oak Ridge

Version 1.0 9/1999
Printed: 4/24/2013 6:53 PM

Page 1 of 1
Gravimetric Worksheet
Gravimetric
Carrier
Analysis
Code
Work Order
Carrier Cone
(mg/ml)
Technician
Ra226
TRetec
LWALKER
Sample
Carrier Data
Type
Carrier Added
(ml)
Filter Data
Gravimetric
-~-
--~~------
Fraction
Client 10
01
02
--03
r----04
- - - - - - - c---------05
1-----06
----07
1------08
09
t------
t----
LCS
-BLANK
DUP
PZ-305-AI TOT
PZ-305-AI-----
DIS
DUP
03
TOT
----DUP 03 DIS---DUP 04 TOT
DUP 04 --DIS
LCS
MBL
----
DUP
TRG
--TRG
DO
TRG
TRG
TRG
--~---
---~-
Filter Tare
(g)
----
--
---
---~~------
0.02~
0.0233
0.0223
----------0.0225
---
--- - ------ --
--~----
Filter Net
(g)
0.0282
0.0278
0.0293
0.0301 I
0.0287
----------- r---0.0286
0.0305
0.0298
0.0288
------------
-- ------
------------- 1---
- - - - - 1---
--
t-------- - - r------------
---------- - -
--
----
----------------
~--------
---
-~-----~----~
0.0225
0.0225
0.0227
0.0228
--------0.0229
Filter Final
(g)
--~----~
-------
-------
----
----------
1-------------- r-------------1--
---------
- - - -----
- - 1--
------ 1-----
- ---
-+----~----1
- - - - !-------------
!!:!)
,...,
~:n
Technician:
'9:
"'"'
IVL-
Date:
_1_,4(3
0.0057
0.0053
0.0066
0.0073
0.0058
0.0056
0.0072
0.0075
0.0063
%
Recovery
Sample Description:
Spectrum File:
Sample Geometry:
SPIKE
1304053A-RA
01
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_033
04026479A
91132
System Bkgd 55203
<not performed>
Sample Size:
Generic Mult. Factor:
Sample Date/Time:

2.040E+000
Generic Div. Factor:
4/25/2013
5:09:11 PM
4/25/2013
2:47:23 PM
170.0 minutes
170.0 minutes

0.9926 +/0.1825 +/0.1811 +/-
0.0000
0.0032 on 12/16/2012
0.0032
Control Certificate Name: Ra226 Ra-5b

RA-226
0.500161 +/Peak Match Tolerance:
0.350 MeV
PEAK
Nuclide
Energy
(MeV)
Net
Pk Area
AREA
1.000E+000
5:49:18 PM
0.031852
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
-------------------------------------------------------------------------------RA-224
RA-226
5.534
4.666
485.81
351.66
8.91
10.46
1.19
0.34
O.OOE+OOO
O.OOE+OOO
6.1
3.9

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------RA-224
RA-226
0.970
0.982
5685.50*
4785.00*
1.50E+001 +/- 3.82E+002

1.05E+001 +/- 1.16E+000
2.03E-001 +/- 5.18E+000

1.43E-001 +/- 4.91E-003
&221
0000056415.CNF
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*"""2"4
Channel Data Report

801:
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10
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3
2
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2
0
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Sample Description:
Spectrum File:
Sample Geometry:
BLANK
1304053A-RA
02
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_034
04026479B
91136
System Bkgd 55204
<not performed>
Sample Size:
Sample Date/Time:

1.860E+000
4/25/2013
5:09:11 PM
4/25/2013
2:47:25 PM
170.0 minutes
170.0 minutes

0.8314 +/0.1856 +/0.1543 +/-
Energy
(MeV)
5:49:43 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/16/2012
0.0027
1.000E+000
Net
Pk Area
AREA
Pk Area
Error %-
REPORT
Ambient
Backgnd
Reagent
Backgnd
0.51
0.34
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
--------------------------------------------------------------------------------
RA-224
<not ID'd>
5.489
4.375
1.49
0.66
190.02
305.43
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------RA-224
0.951
5685.50*
3.28E-002 +/- 8.38E-001
1.15E-001 +/- 2.94E+000
0000056410.CNF
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ROI Type: 1
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/'!
I I
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5500
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I
6000
Channel Data Report
4/25/2013
5:41:17
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Channel Data Report

801:
4/25/2013
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DUP 03 TOT DUP

1304053A-RA
03
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Alpha_035
04026477A
58771
System Bkgd 55205
<not performed>
Sample Size:
Sample Date/Time:

2.370E+000
4/24/2013
5:09:11 PM
4/25/2013
2:47:20 PM
170.0 minutes
170.0 minutes

0.8588 +/0.1826 +/0.1568 +/-
Energy
(MeV)
5:49:42 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/16/2012
0.0027
1.000E+000
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
48.92
46.31
0.00
0.51
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------RA-224
RA-226
5.532
4.594
17.00
18.49
2.9
2.9

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
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RA-226
0.969
0.954
5685.50*
4785.00*
5.66E-001 +/- 1.32E+002

4.94E-001 +/- 2.29E-001
2.00E-001 +/- 4.67E+001

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Sample Description:
Spectrum File:
Sample Geometry:
PZ-305-AI TOT
1304053A-RA
04
Shelf 2
Ra
Detector Name:
Env. Background:
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Alpha_037
04026478A
91133
System Bkgd 55207
<not performed>
Sample Size:
Sample Date/Time:

2.580E+000
4/24/2013
5:09:11 PM
4/25/2013
2:47:22 PM
170.0 minutes
170.0 minutes

0.8494 +/0.1783 +/0.1514 +/-
Energy
(MeV)
RA-224
RA-226
3:28:25 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0033 on 1/26/2013
0.0028
1.000E+000
Net
Pk Area
5.524
4.557
AREA
REPORT
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37.49
42.50
32.26
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0.34
0.51
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FWHM
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O.OOE+OOO
O.OOE+OOO
4.4
4.4
Nuclide
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Conf.
Energy
(keV)
RA-224
RA-226
0.966
0.934
5685.50*
4785.00*
Activity
(pCi/liter )
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MDA
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1.58E-001 +/- 5.75E-003
&236
0000056408.CNF
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Channel Data Report

801:
4/25/2013
0
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5:41:43
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Sample Description:
Spectrum File:
Sample Geometry:
PZ-305-AI DIS
1304053A-RA
OS
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_040
06027396B
91135
System Bkgd 55210
<not performed>
Sample Size:
Sample Date/Time:

2.080E+000
4/24/2013
5:09:11 PM
2:47:35 PM
4/25/2013
170.0 minutes
170.0 minutes

0.8273 +/0.1900 +/0.1572 +/-
Energy
(MeV)
RA-224
RA-226
5:49:33 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0033 on 12/16/2012
0.0027
1.000E+000
Net
Pk Area
5.470
4.569
6.49
11.66
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
80.40
58.37
0.51
0.34
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
3.0
4.5

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.941
0.941
5685.50*
4785.00*
Activity
(pCi/liter )
1.89E-001 +/- 4.42E+001
2.73E-001 +/- 1.59E-001
MDA
(pCi/liter
1.53E-001 +/- 3.58E+001
1.12E-001 +/- 3.80E-003
6.2.ii1
0000056407.CNF
1:3459.0(kev)
start:
stop : 1024:6497. 3(kev)
Acq. Start :Thu Apr 25 14:47:35 2013
60+
[
55
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45
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35
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+-'
s:::
8 30
25
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10
5
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Gt
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~~~
I\~
3500
4000
4500
ROI Type: 1
5000
Energy(kev)
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4/25/2013
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Channel Data Report

801:
4/25/2013
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i2ii5
Sample Description:
Spectrum File:
Sample Geometry:
DUO 03 TOT
1304053A-RA
06
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_041
05026930A
91087
System Bkgd 55211
<not performed>
Sample Size:
Sample Date/Time:

2.000E+000
4/24/2013
5:09:11 PM
2:47:31 PM
4/25/2013
170.0 minutes
170.0 minutes

0.8076 +/0.1978 +/0.1598 +/-
Energy
(MeV)
RA-224
RA-226
5:49:31 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0034 on 12/16/2012
0.0028
1.000E+000
Net
Pk Area
5.562
4.590
6.15
33.13
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
(keV)
85.19
35.16
0.85
1. 87
O.OOE+OOO
O.OOE+OOO
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0.980
0.951
5685.50*
4785.00*
Activity
(pCi/liter )
1.70E-001 +/- 3.97E+001
7.33E-001 +/- 2.59E-001
MDA
(pCi/liter
1.65E-001 +/- 3.86E+001
1.67E-001 +/- 5.67E-003
0000056412.CNF
Start:
1:3452.7(kev)
stop : 1024:6506.6(kev)
Acq. start :Thu Apr 25 14:47:31 2013
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al!
M
,!:::~
%,.~
ROI Type: 1
4500
5000
Energy(kev)
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4/25/2013
5:42:01
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Channel Data Report

801:
4/25/2013
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Sample Title:
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DUP 03 DIS
1304053A-RA
07
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84185
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<not performed>
Sample Size:
Sample Date/Time:

2.550E+000
4/24/2013
5:09:11 PM
4/25/2013
2:47:33 PM
170.0 minutes
170.0 minutes

0.9817 +/0.1846 +/0.1812 +/-
Energy
(MeV)
RA-224
RA-226
5:49:29 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0032 on 12/16/2012
0.0032
1.000E+000
Net
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5.532
4.670
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REPORT
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Error %
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8.32
107.87
71.13
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Reagent
Backgnd
FWHM
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0.34
0.68
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Id
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Energy
(keV)
RA-224
RA-226
0.969
0.983
5685.50*
4785.00*
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2.07E-001 +/- 1.47E-001
MDA
(pCi/liter
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1.40E-001 +/- 4.78E-003
0000056413.CNF
1:3450.2(kev)
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Channel Data Report
4/25/2013
Page
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*******************************************************
*****
*******************************************************
Sample Title:
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Channel Data Report

801:
4/25/2013
0
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Sample Description:
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Sample Geometry:
DUP 04 TOT
1304053A-RA
08
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
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04026481B
84168
System Bkgd 55214
<not performed>
Sample Size:
Sample Date/Time:

2.640E+000
4/24/2013
5:09:11 PM
2:47:27 PM
4/25/2013
170.0 minutes
170.0 minutes

0.9208
0.1902
0.1751
Energy
(MeV)
RA-224
RA-226
0.0000
0.0033 on 12/16/2012
0.0031
5:49:26 PM
0.350 MeV
PEAK
Nuclide
+I+I+!-
1.000E+000
Net
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5.535
4.610
26.66
29.83
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
FWHM
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36.01
0.34
0.17
O.OOE+OOO
O.OOE+OOO
3.0
3.0

Nuclide
Id
Conf.
Energy
(keV)
RA-224
RA-226
0. 971
0.961
5685.50*
4785.00*
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MDA
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1.11E-001 +/- 3.79E-003
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Live Time 10200.000 sec
Real Time 10200.200 sec
start:
1 3447. 9(kev)
Stop : 1024 6485. 9(kev)
Acq. Start Thu Apr 25 14:47:27 2013
60
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VI
......
s::::
8 30
25
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5
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Ell
r,)
u~
~~.J
ROI Type: 1
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5000
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5500
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Channel Data Report
4/25/2013
5:42:20
Page
PM
*******************************************************
*****
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Sample Title:
08
Elapsed Live time:

Elapsed Real Time:
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Channel Data Report

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0
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0
Sample Description:
Spectrum File:
Sample Geometry:
DUP 04 DIS
1304053A-RA
09
Shelf 2
Ra
Detector Name:
Env. Background:
Reagent Blank:
Alpha_046
04026482B
58762
System Bkgd 55215
<not performed>
Sample Size:
Sample Date/Time:

2.270E+000
4/24/2013
5:09:11 PM
2:47:29 PM
4/25/2013
170.0 minutes
170.0 minutes
0.8864 +10.1789 +/0.1586 +/-

Energy
(MeV)
5:49:23 PM
0.350 MeV
PEAK
Nuclide
0.0000
0.0031 on 12/16/2012
0.0028
1.000E+000
Net
Pk Area
AREA
REPORT
Pk Area
Error %
Ambient
Backgnd
Reagent
Backgnd
66.70
60.10
0.17
0.17
O.OOE+OOO
O.OOE+OOO
FWHM
(keV)
-------------------------------------------------------------------------------RA-224
RA-226
5.535
4.615
8.83
10.83
4.5
3.0

Nuclide
Id
Conf.
Energy
(keV)
Activity
(pCi/liter )
MDA
(pCi/liter
-------------------------------------------------------------------------------RA-224
RA-226
0.970
0.963
5685.50*
4785.00*
2.78E-001 +/- 6.51E+001

2.74E-001 +/- 1.65E-001
1.32E-001 +/- 3.08E+001

1.06E-001 +/- 3.63E-003
0000056405.CNF
Live Time 10200.000 sec
Real Time 10200.000 sec
1 3453.7(kev)
start:
stop : 1024 6515 .4(kev)
Acq. start Thu Apr 25 14:47:29 2013
60+
[
55
50
45
40
35
V'l
.f-1
s:::::
::::s
8 30
25
20
15
10
5
0
3500
4000
4500
(;!!)
m
I'~)
ROI Type: 1
5000
Energy(kev)
5500
6000
'
6500
Channel Data Report
4/25/2013
5:42:29
Page
PM
*******************************************************
*****
*******************************************************
Sample Title:
09
Elapsed Live time:

Elapsed Real Time:
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!),10,:)
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Page 1 of 2
4/25/2013 5:37:47 AM
~~Apex-Aiphaj
QA SUMMARY REPORT

Date
Time
: 4/25/2013
: 5:37:47 AM
CHAMBER
Alpha 001
Alpha 002
Alpha 003
Alpha 004
Alpha 005
Alpha 006
Alpha 007
Alpha 008
Alpha 009
Alpha 010
Alpha 01 I
Alpha 012
Alpha 013
Alpha 014
Alpha 015
Alpha 016
Alpha 017
Alpha 018
Alpha 019
Alpha 020
Alpha 021
Alpha 022
Alpha 023
Alpha 024
Alpha 025
Alpha 026
Alpha 027
Alpha 028
Alpha 029
Alpha 030
Alpha 031
Alpha 032
Alpha 033
Alpha 034
Alpha 035
Alpha 036
Alpha 037
Alpha 038
Alpha 039
Alpha 040
Alpha 041
Alpha 042
DEVICE
2If
2If
2lf
2If
2If
2lf
2If
2If
2lf
2If
2If
2If
2lf
2lf
2lf
2lf
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
AIM730
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst 1OODC
Alpha AnalystiOODC
Alpha Analyst! OODC
Alpha Analyst! OODC
Alpha Analyst 1OODC
Alpha AnalystlOODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL '
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Not Done
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Not Done
Not Done
Passed
Passed
Not Done
Passed
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Not Done
Passed
Passed
Not Done
Passed
Not Done
Passed
Not Done
Not Done
Not Done
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
Passed
DATE
4/25/2013 5:23:02 AM
4/25/2013 5:23:03 AM
4/25/20 I 3 5:23:03 AM
4/25/2013 5:23:04 AM
4/25/2013 5:23:05 AM
4/25/2013 5:23:06 AM
4/25/2013 5:23:07 AM
4/25/2013 5:23:08 AM
4/25/2013 5:23:08 AM
4/25/2013 5:23:09 AM
4/25/2013 5:23:10 AM
4/25/2013 5:23:1 I AM
4/25/2013 5:23:12 AM
4/25/2013 5:23:13 AM
4/25/2013 5:23:15 AM
4/20/2013 I 0:41 :48 AM
4/25/2013 5:23:16 AM
4/20/2013 10:4 I :52 AM
4/20/2013 10:41 :54 AM
4/25/2013 5:23:18 AM
4/25/2013 5:23:20 AM
4/25/2013 5:23:21 AM
Page 2 of 2

4/25/2013 5:37:47 AM
CHAMBER
AIIJha 043
Alpha 044
Alpha 045
Alpha 046
Alpha 047
Alpha 048
DEVICE
Alpha AnalystJOODC
Alpha Analyst 1OODC
Alpha Analyst! OODC
Alpha Analyst! OODC
PARAMETER
ALL
ALL
ALL
ALL
ALL
ALL
FLAG
Passed
Passed
Not Done
Passed
Passed
Passed
APPROVED BY:
APPROVAL DATE:
~(/(/
DATE
4/20/2013 10:42:02 AM
4/25/2013 5:23:23 AM
4/25/2013 5:23:24 AM
4/25/2013 5:23:26 AM
4/25/2013 5:23:28 AM
6/12/12
Page
12:16:17 PM
*************************************************************************
*****
L I B R A R Y L I S T I N G R E P 0 R T
*****
*************************************************************************
Radium

Nuclide
Name
Half-Life
(Seconds)
P0-218
RN-222
RA-226
5.049E+010
5.049E+010
5.049E+010
Energy
(keV )
Ra-226, Po-218, Rn-222

Energy
Uncert. (keV
0.000
0.000
0.000
6003.000*
5490.000*
4?85.000*
* ::: key line

TOTALS:
Nuclides
Energy Lines
Yield
(%)
99.9800
99.9200
100.0000
Yield
Uncert . (Abs. +-)
0.0000
0.0000
0.0000
SECTION XI
ANALYTICAL DATA (RADIUM-228)
Eberline Services
Analysis Sheet
Printed: 51112013 9:10AM

Page 1 of3
13-04053
Ra228
Run 1
Analysis Code
02
MBL
BLANK
03
DUP
DUP 03 TOT
~: 04
TRG
PZ-305-AI TOT
1.5000E+OO
05
TRG
PZ-305-AI DIS
1.5000E+OO
06
DO
DUP 03 TOT
4/30/2013

West Lake OU-1
Sample
Aliquot
LCS
Date Received I
Project
Sample
Date
01
Login
CPM
Sample
Desc
Run
Lab Deadline
Client
ID
Internal
Fraction
Work Order
------
----t
LCS
04/09/13
04/09/13
~0:00
0~
1.0000E+OO
1.5000E+OO
Report Level
II
07
TRG
DUP 03 DIS
45
04/05/13 00:00
Activity Units
pCi
II
08
TRG
DUP 04 TOT
41
04/05/13 00:00
1.5000E+OO
09
TRG
DUP 04 DIS
41
04/05/13 00:00
1.5000E+OO
f---- ---
Aliquot Units 1
I
------
Matrix 1
WA
I
Method I
Instrument Type
EPA 904.0 Modified
Alpha/Beta GPC
---------
Radiometric Tracer I
Ba-133
Radiometric Sol#
Ba-6a
Tracer Act {dpm/g)
1010.144
1-
II_
--r-- -
---
--
--
---
---------
1~--
~-
Carrier
Carrier Cone (mg/ml) 1
Yttirum
34
II
~I
--+-
. 1---
I-
------\I
---
--~-------~~----.
1--
i
t----~t----
-----~
--+-
--------1
G,
1'\~
.,..l
G!l
Eberline Services
Analysis Sheet
Printed: 51112013 9:10AM

Page 2 of 3
13-04053
Ra228
Run 1
Radiometric I Grav Carrier
% Rec
Added {ml)
Internal
Fraction
Sample
Desc
01
LCS
0.9155
924.8
413.5
99.26
2.000
0.09651
0.1492
0.0527
77.50
76.931 1.00
02
MBL
0.9109
920.1
344.6
83.14
2.000
0.0966
0.1476
0.0510
75.00
62.36
1.00E
917.~
354.8
85.88
2.000
0.0966
0.1492
0.0526
77.35
66.43
~~~
912.4
349.1
84.94
2.000
0.0966
0.1490
0.0524
77.06
65.46
1.oo
339.5
82.73
2.000
0.0970
0.1501
0.0531
78.09
I
64.601 1.oo I -~
Tracer
Aliquot(g)
Tracer Total
ACT(dpm)
---
03
0~79
04
TRG
05
TRG .
0.9032 .
DO
06
~-911.0
0.9032 i
912.4
---- ----
07
I TRG
TRG
08
Radiometric
Tracer (pCi)
'
912.7
0.9035
0.9027 '
331.9
80.76
378.2
TRG
'
0.9057
914.9
365.3 _[
-----
Grav Filter
Final (g)
Grav Filter
Net(g)
0.09691
0.14841
Grav
%Rec
Mean
%Rec
SAF
1*
SAF
2*
1.00
2.000
0.0968
0.1472
1.oo
-.---
0.0515i
75.74
1.00
61.16
1.00
---
---
9~
403.6
911.9 .I
2.000
0.0504
74.12
72.76
1.00
1.00
-- ------
92.08
2.0001
88.64
2.000l---~~a9~-8
+-
09
Grav Filter
Tare(g)
0.14701
0.0951
0.0519
76.32
70.28
1.00
1.00
--~
0.1424
0.0506
74.41
65.96' 1.00 11.00
I
I
'
+--
I
I
I
---------
~---
I
--
I
---
I
I
-------
I
:
'
I
+--
-----
-----
I_
---t-=
I
I
I
--
I
II
I
'I
-1~------I
--
I
I
I
I
Q)
~~,)
'""'"~
II-'"'
-~---
Eberline Services
Analysis Sheet
Printed: 51112013 9:10AM

Page 3 of 3
13-04053
Ra228
Run 1
Internal
Fraction
Rough Prep
Date
Sample
Desc
Rough Prep
Prep
Date
By
Sep tO
Date/Time
Prep
By
Sep tO
By
Sep t1
Date/Time
Sep t1
05/01/13 05:14
TSMITH
01
I LCS
04/19/13 08:4 7
JBARNARD
04/24/13 17:09
LWALKER
By
--
02
I MBL
04/19/13 08:47
JBARNARD
04/24/13 17:09
LWALKER
05/01/13 05:14
TSMITH
03
1 DUP
04/19/13 08:4 7
JBARNARD
04/24/13 17:09
LWALKER
05/01/13 05:14
TSMITH
04
TRG
04/19/13 08:4 7
JBARNARD
04/24/13 17:09
LWALKER
05/01/13 05:14
TSMITH
05
TRG
04/19/13 08:4 7
JBARNARD
0412411317:09
UWALKER
05/01/13 05:14
TSMITH
04/19/13 08:4 7
JBARNARD
04/24/13 17:09
LWALKER I 05/01/13 05:14 I
TSMITH
04/19/13 08:4 7
JBARNARD
04/24/13 17:09 I LWALKER I 05/01/13 05:14 I
TSMITH
04/19/13 08:4 7
JBARNARD
04/24/13 17:09
04/19/13 08:47
JBARNARD
04/24/13 17:0~j___ LWALKER
II-
DO
06
07
TRG I
08
! TRG I
09
TRG I
L_
-t--
---
--=L=
-+I
I
I
r--
--
I L\Af)\LXER I 05/01/13 05:14

05/01/13~5:14 I
TSMITH
TSMITH
--+
1
r
1
----+-~--
I
,
--r-I ----t-----L
I
1--------+-
1---------t----+----------+-------+--------
(;,
r~~
""')
~"\,)
8
.!a
~
Cll
c:
C(
ca
0::
LCS
Flag
110.34
OK
RPD
Flag
MDA
Flag
Blank
Flag
Activity
Units
RA-228
LCS
LCS
pCi/1
9.95E+OO
1.12E+OO
1.52E+OO
RA-228
MBL
BLANK
pCUI
5.64E-01
5.90E-01
1.20E+OO
03
RA-228
DUP
DUP 03 TOT
pCi/1
1.21E+OO
6.06E-01
1.17E+OO
04
RA-228
TRG
PZ-305-AI TOT
pCUI
3.02E+OO
6.65E-01
1.10E+OO
OK
05
RA-228
TRG
PZ-305-AI DIS
pCi/1
7.22E-01
7.58E-01
1.54E+OO
OK
06
RA-228
DO
DUP 03 TOT
pCi/1
7.34E-01
7.69E-01
1.56E+OO
OK
07
RA-228
TRG
DUP 03 DIS
pCi/1
9.02E-01
6.82E-01
1.36E+OO
OK
08
RA-228
TRG
DUP 04 TOT
pCi/1
1.98E+OO
7.15E-01
1.31E+OO
OK
'
09
RA-228
TRG
DUP 04 DIS
pCi/1
5.30E-01
7.41E-01
1.53E+OO
OK
N
N
LCS
%R
Client
Identification
Results
Error Estimate
MDA
9.01E+OO
OK
r-----
02
co
{l
LCS
Known
Sample
Desc
01
a::
Work Order: 13-04053-Ra228-1
Nuclide
Lab
Fraction
Printed: 5/1/2013 2:56PM

Page 1 of 3
Eberline Services
OK
OK
NA
OK
--
I
c.i
..5
~
0
a.
a.
:I
...c
(/)
jl
Cll
Cll
Cl
nl
c
nl
:!!!
Cl
c
;:
Cll
Cll
.5
Cl
2,
M
'h~~
tll
c::::s
a::
or-
co
N
N
.!!!
ns
~
111
0:::
c:
oq
Work Order: 13-04053-Ra228-1
t:
0
c.
c.
::s
(/)
c
Gl
E
Gl
.!t
Cl
IG
IG
:E
Cl
;:
Gl
Gl
c
a,
c
w
t<n
II')
''~M
~
...
Sample
Aliquot
Radiometric
%Rec
Grav
%Rec
Mean
%Rec
SepW
Date/Time
Sep t1
Date/Time
Lab
Fraction
Nuclide
Sample
Desc
Sample
Date
01
RA-228
LCS
04/09/13 00:00
1.00E+OO
99.26
77.50
76.93
1.00
4124/2013 17:09
5/1/2013 5:14
02
RA-228
MBL
04/09/13 00:00
1.50E+OO
83.14
75.00
62.36
1.00
4/24/2013 17:09
5/1/2013 5:14
03
RA-228
DUP
04/05/13 00:00
1.50E+OO
85.88
77.35
66.43
1.00
4/24/2013 17:09
5/1/2013 5:14
04
RA-228
TRG
04/05/13 15:58
1.50E+OO
84.94
77.06
65.46
1.00
4/2412013 17:09
5/1/2013 5:14
05
RA-228
TRG
04/05/13 15:58
1.50E+OO
82.73
78.09
64.60
1.00
4/24/2013 17:09
5/1/2013 5:14
06
RA-228
DO
04/05/13 00:00
1.50E+OO
80.76
75.74
61.16
1.00
4/24/2013 17:09
5/1/2013 5:14
07
RA-228
TRG
04/05/13 00:00
1.50E+OO
98.17
74.12
72.76
1.00
4/24/2013 17:09
5/1/2013 5:14
08
RA-228
TRG
04/05/13 00:00
1.50E+OO
92.08
76.32
70.28
1.00
4124/2013 17:09
5/1/2013 5:14
09
RA-228
TRG
04/05/13 00:00
1.50E+OO
88.64
74.41
65.96
1.00
412412013 17:09
5/1/2013 5:14
SAF
-----
.E
Printed: 5/1/2013 2:56PM

Page 2 of3
Eberline Services
!
i
(
~I
-r-
co
.g
8
.!!!
N
N
0:::
ca
.5
~
0
c.
c.
::I
(/)
-~
.....
s::
Cll
E
Cll
Cl
CG
s::
CG
::liE
Cl
s::
'i:
Cll
Cll
s::
a,
s::
w
Q~
II'>,)
""~
u~
Work Order: 13-04053-Ra228-1
Lab
Fraction
Nuclide
Sample
Desc
Counting
Date/Time
01
RA-228
LCS
RA-228
03
Halflife
(days)
Count
Time
Counts
Bkg
CPM
Eft
Detect
Carrier
05/01/13 09:51
LB4110A
C1
120
671
1.4
0.4667
MBL
05/01/13 09:51
~LB4110A
C2
120
182 1.233333333
0.4578
RA-228
DUP
05/01/13 09:51
LB4~10A
C3
120
248
1.4
0.4699
04
RA-228
TRG
05/01/13 09:51
LB4110A
C4
120
340
1.2
0.4692
05
RA-228
TRG
05/01/13 12:01
LB4110A
C1
120
204
1.4
0.4667
06
RA-228
DO
05/01/13 12:01
LB4110A
C2
120
182 1.233333333
0.4578
07
RA-228
TRG
05/01/13 12:01
LB4110A
C3
120
219
1.4
0.4699
08
RA-228
TRG
05/01/13 12:01
LB4110A
C4
120
252
1.2
0.4692
09
RA-228
TRG
05/01/13 12:02
LB4110A
02
120
199 1.433333333
0.4682
02
s:::
Printed: 5/1/2013 2:56 PM

Page 3 of 3
Eberline Services
Count Room Report

Printed: 5/112013 9:10AM

Page 1 of 1
13-04053-Ra228-1 (pCi/1) in WA
Tracer 10: Ba-6a
Client
ID
Sample
Date
LCS
04/09/13 00:00
1.0000
1 MBL
BLANK
04/09/13 00:00
1.5000
0.91091
DUP
DUP 03 TOT
1__04/05/13 00:00
1.5000
0.9079 G7.1097-+-------+------+--
PZ-305-AI TOT
I 04/05/13 15:58
1.5000
0.91 )32 I
Internal
Fraction
Sample
Desc
01
LCS
--
Sample
Aliquot
Tracer
Aliquot(g)
0.9155
Tracer
ACT{dpm)
924.7868
02
920. 14_0_2-+-------+-
03
-----
04
TRG
05
TRG
06
DO
-+-----~
=+---+
-~---+----------t-
.---t-1
-~--1--~~--t
rI
-----+
i
1----r------+
I!;)
i'ot)
'J
Ol1
-+-
--+---------+---
Eberline Services
Page 1 of 1
Printed: 4/19/2013 8:47AM
JBARNARD
Activity
dpmlg
Isotope
Ra-228
Solution
Date
39.0191
--;;
Isotope
Sol#
01
Ba-133
Ba-6a
0.510
LCSO
MSD
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
Volume
Used(g)
0.5129
Activity
dpm/g
Known
pCi
Error
Estimate
0.460
,--
MS
Added
pCi
0.00
E"or
Estimate
0.000
lese-~
Known
pCi
Error
Estimate
00~---~000
MSD
Added
pCi
0.00
Error
Estimate
0.000

Solution
Date
Volume
Used(g)
1010.144 4/19/2013
0.9155
Approx
Addition
Tracer
LCS
1.0000
Ba-133
Ba-6a
1010.144 4/19/2013
0.9109
1.0000
Ba-6a
1010.144 4/19/2013
0.9079
1.0000
04
Ba-133
Ba-6a
1010.144 4/19/2013
0.9032
1.0000
05
Ba-133
Ba-6a
1010.144 4/19/2013
0.9019
1.0000
06
Ba-133
Ba-6a
1010.144 4/19/2013
0.9032
1.0000
07
Ba-133
Ba-6a
1010.144 4/19/2013
0.9035
1.0000
08
Ba-133
Ba-6a
1010.144 4/19/2013
0.9027
1.0000
09
Ba-133
Ba-6a
1010.144 4/19/2013
0.9057
1.0000
,--
LCS
9.01
Ba-133
03
4/19/2013
MS
Tracers
fraction
02
Approx
Addition
LCS
--
-----
Matrix Spike
I-..
---
I--
-
~n
,..,)
..J
;,J
Version 2.0 08/99
_L
,.
Eberline Analytical
Printed: 4/19/2013 8:48AM

Page 1 of 1
Aliquot Worksheet
JBARNARD
Lab
Fraction
01
02
03
04
05
06
07
08
09
ClientiD
LCS
BLANK
DUP 03 TOT
PZ-305-AI TOT
PZ-305-AI DIS
DUP 03 TOT
DUP 03 DIS
DUP04 TOT
DUP 04 DIS
Sample
Type
LCS
MBL
DUP
TRG
TRG
...
DO
TRG
TRG
TRG
Ratio
Post/Pre
Aliquot Data
Dilution Data
Muffle Data
Oil Factor.,.
No of Oils'
',
''
..
Ratio
Aliquot
1.0000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
Net Equiv
f.oOOOE+OQ
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
1.5000E+OO
H-3 Solids Only
MS Aliquot Data
Aliquot
water Added
(ml)
NetEquiv
H3 Dist
Aliq
+-I
_ L __ _ _ _ _ _ _
I
- --
..
'
r-------
-------------
..
..
Comments
t.i~
1'\)
....~
(:0
Technician:
---------
I
~
Dale:
Eberline Services- Oak Ridge

Version 1.0 9/1999
Work Order
TRetec
01
02
03
04
05
06
07
08
1--09
f---
- -----
~--
Analysis
Code
Gravimetric
Carrier
Carrier Cone
(mg/ml)
Technician
Ra228
Yttirum
34.0000
TSMITH
Sample
Carrier Data
Client ID
Type
Carrier Added
(ml)
LCS
BLANK
DUP
PZ-305-AI TOT
PZ-305-AI DIS
DUP 03 TOT
DUP 03 DIS
DUP 04 TOT
DUP 04 DIS
LCS
MBL
DUP
TRG
TRG
DO
TRG
TRG
TRG
Fraction
Printed: 5/1/2013 9:10AM

Page 1 of 1
Gravimetric Worksheet
--
r--
Filter Data
Filter Tare
(g)
2.0000
0.0965
2.0000
0.0966
2.0000
0.0966
0.0966
2.0000
2.0000
0.0970
2.0000
0.0969
2.0000
0.0968
0.0951
2.0000
1-------------2.0000
0.0918
Filter Net
(g)
0.1492
0.1476
0.1492
0.1490
0.1501
0.1484
0.1472
0.1470
0.1424
----~-----
+
-
- ---
'
----------
-----------------~----~-
-------j
-------
lt.O
--
t----
""')
....
J
77.50 .
75.00
77.35
77.06
78.09
75.74
74.12
76.32
74.41
0.0527
0.0510
0.0526
0.0524
0.0531
0.0515
0.0504
0.0519
0.0506
~--~------
Glt
%
Recovery
------- -------
---
-------------
Gravimetric
Filter Final
(g)
~//A
Technician: _ _ _ _ _ _ _ _ _ _ _ _ _ __
--------
Date:
--------------
_____!!_1 _I
I)
L ____________
Sheet1
fA)
,~:>
'U>
Detector ID Sample ID Alpha Beta Count Time Voltage

TOO
C1
1304053-01
50
671
120
1400 5/1/13 11:51
C2
1304053-02 17
1400 5/1/13 11:51
182
120
C3
1304053-03 29
1400 5/1/1311:51
248
120
C4
1304053-04 32
1400 5/1/13 11:51
340
120
l<r.1
f';,)
():)
ii:Ol1.)
Page 1
Sheet1
Detector ID Sample ID Alpha Beta Count Time Voltage

TOO
C1
1304053-05 15
204
120
1400 5/1/13 14:01
C2
1304053-06 14
182
120
1400 5/1/13 14:01
C3
1304053-07 21
219
120
1400 5/1/13 14:01
C4
1304053-08 13
252
120
1400 5/1/13 14:01
02
1304053-09 17
199
120
1400 5/1/13 14:02
C!~
,,,,,)
0)
....
Page 1
~~
Eberline Analytical
Printed: 5/1/2013 7:03AM

Page 1 of 1
GPC Detector Report

(ALL Backgrounds)
Detector
Alpha/Beta
Calibration Date
LB4110A- A1
Alpha
11/18/2007
LB4110A- A2
Alpha
11/18/2007
LB4110A- A3
----------LB4110A- A4
Count Date
Alpha ,_
11/18/2007
_____
---------------
LB4110A- C2
-1.92E+01
2.45E-01
1.97E+01
-9.90E-02
7.51E-02
2.49E-01
11/18/2007
5/1/2013
6.67E-02
-7.96E-02
7.27E-02
2.25E-01
-6.39E-02
5.33E-02
,_
-1.44E-01
7.91E-02
-1.53E-01
8.91E-02
3.31E-01
-1.80E-01
8.84E-02
3.57E-01
5/1/2013
l.OOE-01
11/18/2007
5/1/2013
1.33E-01
Alpha
11/18/2007
5/1/2013
1.17E-01
Alpha
11/18/2007
5/1/2013
5/1/2013
6.67E-02
-------- r--..------ r-------.. . . . ._. ___
11/18/2007
-------------11/18/2007
..
.........
--. --...
--
8.33E-02
5/1/2013
O.OOE+OO
-------------
_____
.......-1. 76E-01
---------------. ....-............---
-6.29E-02
1. 70E-01
3.02E-01
79E-01
__3._____
-----------1.01E-01
----:-~
,.
,_,_.,
6.89E-02
2.01E-01
__
I
I
I
Alpha
11/18/2007
5/1/2013
5.00E-02
-5.36E-02
8.42E-02
2.22E-01
LB4110A- D2
Alpha
11/18/2007
5/1/2013
8.33E-02
-7 .04E-02
6.03E-02
L64110A- D3
--. -----. ------
L64110A- 04
Alpha
11/18/2007
_5/1/2013
l.OOE-01
-4. 75E-02
7.20E-02
1.91E-01 I
1.92E-01
7.09E-02
1.99E-01
_.....- ........
--~
Alpha
---------. -----. ------ ............ .........- ..............-.---. - ---
11/18/2007
L64110R- A1
Alpha
11/24/2006
LB4110R- A2
Alpha
11/24/2006
L64110R- 61
LB4110R- B2
LB4110R- B3
Alpha
-----.
-.--...........-
1.67E-01
-- -5/1/2013
- - - - - ---
11/24/2006
........ .....------- ----------------
-5. 76E-02
Alpha
Alpha
-1.01!:-01
1.01E-01
3.03E-01
5/1/2013
l.OOE-01
-9.03E-02
7.74E-02
2.45E-01
1.17E-01
-7.38E-02
____
_____
7.68E-02
2.27E-01
-5.30E-02
7.18E-02
1.97E-01
2.20E-01
5/1/2013
11/24/2006
5/1/2013
LB4110R- B4
Alpha
11/24/2006
5/1/2013
LB4110R- C1
Alpha
11/24/2006
5/1/2013
LB4110R- C2
Alpha
11/24/2006
5/1/2013
.,
-9.60E-02
6.21E-02
5.00E-02
-6.951:-02
6.44E-02
1.98E-01
7.01E-02
2.06E-01
7 .44E-02
2.27E-01
7.23E-02
2.20E-01
8.48E-02
2.59E-01
..
..,
.... _
6.47E-02
l.OOE-01
-7.80E-02
1.67E-02
-7.54E-02
--r------ -----
Alpha
L64110R- 03
Alpha
......- ............-.........----'"
---"'"-----
L64110R- 04
Alpha
LB5100 - 1
Alpha
11/24/2006
11/24/2006
------. -.....- ....... _................-...11/24/2006
'---------- ----- --------

7/10/2006
5/1/2013
O.OOE+OO
5/1/2013
O.OOE+OO
----5/1/2013
. - . - ........ ....
O.OOE+OO
.... .......- .... --.
-------------....-- --.............-............. --.
______
10/26/2007
5.00E-02
LB4110R- D2
...
3.33E-02
p
Alpha
L64110RC3
11/24/2006
1.33E-01
5/1/2013
.... _.
...............- ...----...... _____....___. __ ____. ___ ..----... ---......- ...... - .......-- ----....
.......----. ------ ....- ..--------------. -. --..-----.
p
LB4110R- C4
Alpha
3.33E-02
11/24/2006
5/1/2013
--
p
Alpha
LB4110R- D1
O.OOE+OO
11/24/2006
5/1/2013
___
.,
1.83E-01
w .....______
-6.55E-02
_____5/1/2013
__ ______ __ -------. ___ . _,
---. ------- ---. --. --. ----. --.- - ......
-----11/24/2006
...
..--------
1.83E-01
5/1/2013
11/24/2006
------------ ---....-
5/1/2013
Alpha
-~----------
1.91E+01
LB4110A- D1
LB4110R- A3
:!ll
2.24E+01
2.63E-01
O.OOE+OO
-1.81E+01
2.24E-01
5/1/2013
1.85E+01
------------- ...------. -- ---------- - - - - - -----------------
------- ----- --------- -------"'------ --------- -. -------p

LB4110R- A4
Alpha
5.00E-02
11/24/2006
5/1/2013
'~)"')
2.94E-01
-1.85E+01
""
11/18/2007
Alpha
-L64110A- - - -C3
- ---L64110A- C4
Alpha
-2.18E+01
1.67E-02
Alpha
LB4110A- C1
5/1/2013
L64110A- 62
Alpha
1.50E-01
UCL
11/18/2007
Alpha
Alpha
8.33E-02
Mean
L64110A- 61
L64110A- 63
5/1/2013
5/1/2013
C-
LCL
------ 1--------..- 1--------..
3.33E-02
11/18/2007
- - - - ------
PFW
-----~---
5/1/2013
Alpha
L64110A- 64
Bkg CPM
----p
------
.... -------~--
--'"""""""-
-~------~--~
5.00E-02
-- ....... ---.
---.
-6.23E-02
---------- --------....--........
8.21E-02
2.27E-01
-9.90E-02
7.33E-02
2.46E-01
-7 .30E-02
7.27E-02
2.18E-01
-7.83E-02
7.24E-02
2.23E-01
- -""----""----....-...--. -- . ---------'"------....... . ---.......--
- ...-.........._
p
-8.93E-02
....................
________
-------- i - -...----..7.08E-02
2.06E-01
--
-6.96E-02
-1.56E-02
_
9.58E-02
7.74E-02
.......
..
..........
---------
2.24E-01
---~---~--
2.07E-01
rt ttr;;
Eberline Analytical
Printed: 5/1/2013 7:04AM

Page 1 of 1
GPC Detector Report

(ALL Backgrounds)
(__
Detector
Alpha/Beta
LB4110A- A1
Beta
LB4110A- A2
LB4110A- A3
--. --------
Calibration Date
Count Date
11/18/2007
5/1/2013
Beta
11/18/2007
5/1/2013
4.30E+00
Beta
11/18/2007
5/1/2013
1.37E+OO
- - - - - - - --------
. --------
LB4110A- A4
Beta
--------. -------- ----. --.....- ....- . --. --
11/18/2007
LB4110A- B1
Beta
11/18/2007
LB4110A- B2
Beta
11/18/2007
LB4110A- B3 _______Beta
---- , ________
Beta
---------.
LB4110A- B4
5/1/2013
--.
5.68E+01
-3.34E+01
3.01E+OO
3.94E+01
-1.05E+01
3.26E+OO
1.70E+01
-7.57E+OO
1.99E+OO
1.15E+01
5/1/2013
___ Beta
___________
LB4110A- C4
LB4110A- D1
Beta
11/18/2007
........--~------------ .....-.......
5/1/2013
-~
11/18/2007
11/18/2007
11/18/2007
11/18/2007
.............
---...
---~
1.40E+00
.... _...........
- ......... .....-.-
5/1/2013
1.20E+00.
5/1/2013
2.98E+00
---------...----..--
1.04E-01 ....... 1.36E+OO ...3:.~3~.::-~g_j

__________
"'"""-""""""-----------,_,,
.....
-7.62E+OO
1.97E+OO
-5.51E+OO
2.16E+OO
9.83E+OO~
3.80E-01
1.27E+OO
2.17E+OO
-----~----
p
p
p
1.43E+OO.
p
4.07E+OO
5/1/2013
---. --. ------------- ----. - -. -------p
5/1/2013
1.35E+00
5/1/2013
......
--
rrltJ
----- f--------- f - - - - - -....._
,_,.-~
LB4110A- C3
1.16E+01
----------......- ----------....-. ___...
___ _
4.69E-01
1.47E+OO
2.47E+00
.........
-1.77E+OO
-2.39E+OO
-6.84E-01
2.14E+00
2.59E+OO
6.06E+00
7.57E+00
1.57E+OO
3.82E+OO
1.22E+OO
4.47E+OO
7.73E+00
-4.54E-01
1.38E+OO
3.20E+OO
----------- --------
LB4110A- D4
Beta
LB4110R- A1
Beta
11/24/2006
5/1/2013
1.25E+00
-6.21E+01
3.78E+OO
6.96E+01
LB4110R- A2
LB4110R-..._,_
A3
Beta
Beta
5/1/2013
5/1/2013
1.12E+00
1.38E+00
-4.93E+01
,_. -4.57E+01
______
2.06E+OO
2.80E+OO
5.35E+01
---------
11/24/2006
11/24/2006
LB4110R- A4
Beta
11/24/2006
5/1/2013
1.25E+00
-4.56E+01
2.02E+OO
5.13E+O~_j
4.96E+01 i
LB4110R- B1
Beta
11/24/2006
5/1/2013
1.37E+00
-4.80E+01
2.05E+00
5.21E+01
LB4110R- B2
LB4110R- 63
LB4110R- B4
Beta
Beta
Beta
11/24/2006
11/24/2006
11/24/2006
5/1/2013
5/1/2013
5/1/2013
1.30E+OO
1.33E+00
............. .. . -----"""_ . __
1.28E+00
p
p
-4.79E+01
-4.77E+01
............
- ...... _____. __ __,.......
4.81E+01
LB4110R- Cl
Beta
11/24/2006
5/1/2013
1.42E+00
-4.78E+01
3.04E+OO
5.39E+01
LB4110R- C2
Beta
11/24/2006
5/1/2013
1.70E+OO
-4.78E+01
2.75E+OO
5.33E+01
- ......._...______. --.
_......1.32E+00
11/18/2007
------ --------- - - - - - - - - - - - - - - -
--------------- !-----....-------- ----------- ------
.......- ..............- ..........
- - - - - -r-------- - . - ...-
LB4110R- C3
Beta
11/24/2006
LB4110R- C4
Beta
_5/1/2013
_, __ - -
11/24/2006
5/1/2013
1.45E+00
LB4110R- D1
Beta
11/24/2006
5/1/2013
O.OOE+OO
LB4110R- D2
LB4110R- D3
----------. -----......... .......
LB4110R- 04
.....
LB5100 - 1
(...~
2.68E+00
1.23E+OO
-5.14E+01
1.82E+OO
5/1/2013
-. --.....- ........ . ,...
2.55E+00
11/18/2007
...
3.63E+01
5/1/2013
Beta
Beta
3.12E+02
2.54E+OO
5/1/2013
LB4110A- C2
LB4110A- D3
7.63E+OO
-3.12E+01
11/18/2007
UCL
-2.96E+02
2.22E+00
- 11/18/2007 ...-- ....-........-5/1/2013
..................--........-........_..._. ------.................-.......,_. .............-.....................
.......... .........__________
Mean
..............--. --- --......
--r----..--...
5/1/2013
LB4110A- D2
. --
LCL
-----------. ----. -- ......._____......_,___ ----......------"""-----. - .-......
0)
7.53E+00
11/18/2007
____
Gll~
--------------~
Beta
Beta
Beta
------p
8.77E+00
LB4110A- C1
PFW
----
1.15E+00
1.40E+OO
-----~---
I'\)
Bkg CPM
Beta
Beta
. ___................
Beta
....
Beta
11/24/2006
.....
.... ........
~----
..
__
_.
5.34E+01
-4.83E+01
2.56E+OO
--. ..._______. __. ___ ---------- ------. -----. _,
,_,
-5.45E+01
2.99E+OO
6.05E+01
-4.52E+01
5.80E+OO
5.68E+01
-4.87E+01
1.96E+OO
O.OOE+OO
p
-5.20E+01 ____
O.OOE+OO
5.77E+OO
5/1/2013
,_.
.... _, ___,...............--. ---......- ..-... --.......... ... ....--. ---- .....-...- ...-...--. - ......-----. -----....... _..
p
-4.84E+01
2.33E+00
O.OOE+OO
5/1/2013
-------- ----- -----
-3.19E-01
F
1.58E+OO
10/26/2007
4.52E+00
5/1/2013
11/24/2006
..........-----""""'"-"'"---. --...--... -..
11/24/2006
7/10/2006
........
,.,
2.08E+OO
5.21E+01
2.71E+00 ----....
__,........_._,...
------------------- 5.31E+01
1.95E+OO
5.20E+01
________
--
--
---
_______
5.27E+01
..
6.36E+01
--
. -----... ...........____............
5.31E+01
3.48E+OO
Eberline Analytical
Detector
Count Date
Eff
PFW
LCL
Mean
UCL
-0.0194
0.2146
0.4485
Alpha
11/18/2007
5/1/2013
0.2415
LB4110A- A2
Alpha
11/18/2007
5/1/2013
0.2072
-0.0568
0.1724
0.4016
LB4110A- A3
Alpha
11/18/2007
5/1/2013
0.2070
-0.0804
0.1612
0.4028
0.2206
-0.0588
0.1802
0.4192
5/1/2013
0.2209
0.1943
0.2247
0.2550
Alpha
11/18/2007
5/1/2013
LB4110A- B1
Alpha
11/18/2007
LB4110A- B2
Alpha
11/18/2007
5/1/2013
0.2106
0.1930
0.2218
0.2507
LB4110A- B3
Alpha
11/18/2007
5/1/2013
0.2422
0.1291
0.2326
0.3361
0.2333
0.2091
0.2367
0.2644
--
LB4110A- B4
Alpha
LB4110A- C1
Alpha
11/18/2007
5/1/2013
0.2219
0.1973
0.2208
0.2444
LB4110A- C2
Alpha
11/18/2007
5/1/2013
0.2250
0.1966
0.2252
0.2539
11/18/2007
5/1/2013
LB4110A- C3
Alpha
11/18/2007
5/1/2013
0.2511
0.2228
0.2494
0.2760
LB4110A- C4
Alpha
11/18/2007
5/1/2013
0.2203
0.1965
0.2258
0.2551
LB4110A- D1
Alpha
11/18/2007
5/1/2013
0.2186
0.2037
0.2335
0.2632
LB4110A- D2
Alpha
11/18/2007
5/1/2013
0.2464
0.2279
0.2585
0.2891
LB4110A- D3
Alpha
11/18/2007
5/1/2013
0.2506
0.2315
0.2639
0.2964
LB4110A- D4
Alpha
11/18/2007
5/1/2013
0.1781
0.1652
0.1999
0.2347
LB4110R- A1
Alpha
11/24/2006
5/1/2013
0.2375
0.2030
0.2389
0.2748
0.1899
0.2207
0.2515
LB4110R- A2
Alpha
11/24/2006
5/1/2013
0.1992
LB4110R- A3
Alpha
11/24/2006
5/1/2013
0.2237
0.1963
0.2249
0.2535
LB4110R- A4
Alpha
11/24/2006
5/1/2013
0.2367
0.2159
0.2457
0.2755
0.2208
0.1877
0.2261
0.2645
Alpha
11/24/2006
5/1/2013
LB4110R- B2
Alpha
11/24/2006
5/1/2013
0.2106
0.1801
0.2176
0.2551
LB4110R- B3
Alpha
11/24/2006
5/1/2013
0.2508
0.2067
0.2440
0.2814
LB4110R- B4
Alpha
11/24/2006
5/1/2013
0.2199
0.1938
0.2320
0.2703
LB4110R- C1
Alpha
11/24/2006
5/1/2013
0.2088
0.1861
0.2153
0.2445
LB4110R- C2
Alpha
11/24/2006
5/1/2013
0.2221
0.1963
0.2249
0.2534
LB4110R- C3
Alpha
ll/24/2006
5/1/2013
0.2328
0.2064
0.2398
0.2732
5/1/2013
0.2091
0.1860
0.2230
0.2600
0.0418
0.2081
0.3744
0.0483
0.2366
0.4250
0.0475
0.2325
LB4110R- C4
~-~"
Calibration Date
LB4110A- A1
LB4110R- B1
ctm~
Alpha/Beta
LB4110A- A4
I"")
(II;}
Printed: 5/1/2013 7:04AM

Page 1 of 1
GPC Detector Report

(ALL Efficiencies)
Alpha
11/24/2006
<:_.
)/1/f'")
'
'
'
LB4110R- D1
Alpha
11/24/2006
5/1/2013
0.0000
LB4110R- D2
Alpha
11/24/2006
5/1/2013
0.0000
LB4110R- D3
Alpha
11/24/2006
5/1/2013
0.0000
LB4110R- D4
Alpha
11/24/2006
5/1/2013
0.0000
0.0365
0.4174
r-------0.1873
0.3382
LB5100 - 1
Alpha
10/26/2007
0.3368
0.3332
0.3455
7/10/2006
---
0.3578
Eberline Analytical
Detector
())
(.111
Count Date
Eff
PFW
LCL
Mean
UCL
0.2027
0.5628
0.9229
Beta
11/18/2007
5/1/2013
0.5493
LB4110A- A2
Beta
11/18/2007
5/1/2013
0.4782
0.1535
0.4632
0.7729
LB4110A- A3
Beta
11/18/2007
5/1/2013
0.4722
0.0807
0.4570
0.8332
LB4110A- A4
Beta
11/18/2007
5/1/2013
0.5272
0.1331
0.4876
0.8421
0.5152
0.4638
0.5307
0.5976
Beta
11/18/2007
5/1/2013
LB4110A- B2
Beta
11/18/2007
5/1/2013
0.5115
0.4638
0.5277
0.5915
LB4110A- B3
Beta
11/18/2007
5/1/2013
0.5406
0.3186
0.7455
LB4110A- B4
LB4110A- C1
Beta
Beta
11/18/2007
11/18/2007
5/1/2013
5/1/2013
0.5413
0.5067
0.4922
0.4501
0.5321
0.5547
0.5027
LB4110A- C2
Beta
11/18/2007
5/1/2013
0.4958
0.4278
0.5012
0.5745
LB4110A- C3
Beta
11/18/2007
5/1/2013
0.5978
0.5275
0.5901
0.6527
0.4567
LB4110A- C4
Beta
11/18/2007
5/1/2013
0.5216
LB4110A- 01
Beta
11/18/2007
5/1/2013
0.5159
0.4800
0.5251
0.5544
0.5935
0.6288
LB4110A- 02
Beta
11/18/2007
5/1/2013
0.5454
0.4907
0.5890
0.6872
0.5998
0.5367
0.6156
0.6945
0.3866
0.4736
0.5607
0.4812
0.4207
0.5680
Beta
11/18/2007
5/1/2013
LB4110A- 04
Beta
11/18/2007
5/1/2013
0.4347
LB4110R- A1
LB4110R- A2
Beta
Beta
11/24/2006
11/24/2006
5/1/2013
5/1/2013
0.5573
0.4846
0.5089
0.6547
0.5971
LB4110R- A3
Beta
11/24/2006
5/1/2013
0.5294
0.4579
0.5398
0.6217
LB4110R- A4
Beta
11/24/2006
5/1/2013
0.5943
0.5098
0.5917
0.6736
LB4110R- B1
LB4110R- B2
Beta
Beta
11/24/2006
11/24/2006
5/1/2013
5/1/2013
0.5298
0.5083
p
p
0.4534
0.4311
0.5428
0.5203
0.6323
0.6095
LB4110R- B3
Beta
11/24/2006
5/1/2013
0.6115
0.5014
0.5913
0.6811
LB4110R- B4
Beta
11/24/2006
5/1/2013
0.5243
0.4624
0.5501
0.6379
0.4591
0.4244
0.5034
0.5825
Beta
11/24/2006
5/1/2013
rtr'')
0.6172
0.5553
LB4110R- C1
1\)
Calibration Date
LB4110A- A1
LB4110A- 03
'
Alpha/Beta
LB4110A- B1
~)
Printed: 5/1/2013 7:04AM

Page 1 of 1
GPC Detector Report

(ALL Efficiencies)
LB4110R- C2
LB4110R- C3
Beta
Beta
11/24/2006
11/24/2006
5/1/2013
5/1/2013
0.5094
0.5542
0.4503
0.4813
0.5293
0.5714
0.6084
0.6615
LB4110R- C4
Beta
11/24/2006
5/1/2013
0.4903
0.4326
0.5267
0.6208
LB4110R- 01
Beta
11/24/2006
5/1/2013
0.0000
0.0989
0.4976
0.8963
LB4110R- 02
Beta
11/24/2006
5/1/2013
0.0000
0.1119
0.5591
1.0064
LB4110R- 03
LB4110R- 04
Beta
Beta
11/24/2006
11/24/2006
5/1/2013
5/1/2013
0.0000
F
F
0.5431
0.4470
0.9775
0.0000
0.1086
0.0859
LB5100 - 1
Beta
7/10/2006
10/26/2007
0.4428
0.4555
0.4731
0.4906
0.8082
SECTION XII
BARIUM-133 ANALYTICAL TRACER DATA
C-
VAX/VMS Peak Search Report Generated 25-APR-2013 10:19:52.00

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
25-APR-2013 00:00:00
1304053-01
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
30.86
35.02
52.36
58.27
62.01
65.81
81.30
92.91
112.04
115.99
160.89
185.93
190.94
238.92
248.94
277.03
303.00
306.90
333.72
338.62
353.14
356.47
383.83
387.14
391.15
415.09
418.36
421.22
437.21
469.56
511.59
604.22
654.64
912.20
2066
502
47
29
293
117
892
48
209
27
52
30
15
19
20
45
169
29
79
35
10
525
149
234
43
39
27
15
108
10
8
6
7
6
65
47
109
30
88
85
126
89
56
67
65
53
45
37
14
52
22
29
12
12
10
11
17
7
2
8
9
10
12
11
12
3
1
1
2
2
0
4
4
4
0
0
2
2
0
1
1
1
1
0
2
2
1
1
2
2
2
2
2
3
3
3
0
0
0
0
0
0
'-lft,,f>IJ
DKAlOO>: [GAMMA. SCUSR.ARCHIVE] SMP_l30405301 GEl BAFIL 19094l.CN

PEAK Vl6.9 PEAKEFF V2.2
SPIKE
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.44
1.68
1.95
2.09
1.87
2.11
1. 95
1.29
1.72
1. 81
2.20
1. 72
1. 73
1.77
1. 78
1.22
1. 73
2.00
1.84
1.84
2.04
1. 67
2.05
1. 78
2.07
2.29
2.30
2.30
1. 84
1.31
2.45
2.39
2.68
1. 52
31.09
35.25
52.59
58.50
62.24
66.04
81.53
93.14
112.26
116.22
161.12
186.16
191.16
239.13
249.16
277.24
303.22
307.11
333.93
338.83
353.35
356.68
384.04
387.35
391.36
415.29
418.57
421.43
437.42
469.76
511.79
604.42
654.83
912.37
Left
Pw
27
27
49
57
57
57
76
90
108
108
157
182
182
236
236
273
300
300
329
329
351
351
380
380
380
411
411
411
433
466
509
601
652
909
14
14
8
13
13
13
11
7
12
12
7
13
13
17
17
8
12
12
15
15
11
11
16
16
16
16
16
16
10
6
7
6
6
6
25-APR-2013 10:04:35
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.28 0.0%
4096
10.00000
Cts/Sec %Err
2.30E+00
5.58E-01
5.22E-02
3.17E-02
3.26E-01
1. 31E-01
9.91E-01
5.28E-02
2.32E-01
2.99E-02
5.79E-02
3.38E-02
1.65E-02
2.12E-02
2.21E-02
4.96E-02
1.88E-01
3.27E-02
8.78E-02
3.91E-02
1. 07E- 02
5.83E-01
1.65E-01
2.60E-Ol
4.76E-02
4.30E-02
3.03E-02
1.69E-02
1.20E-01
1.07E-02
9.22E-03
6.67E-03
7.50E-03
6.19E-03
2.2
5.1
41.1
27.7
7.8
17.4
4.1
36.0
8.7
57.2
29.3
38.0
75.9
48.2
40.4
31.8
8.4
42.6
14.0
24.1
52.8
4.5
8.9
7.2
29.6
22.7
36.0
55.2
11.4
64.9
74.6
61.2
47.4
54.6
Fit
1. 70E+Ol
6.12E+00
3.70E+00
3.42E+00
2.09E+00
9.22E+00
1.90E+00
2.35E+01
9.75E+00
2.15E+00
i287
Summary of Nuclide Activity

Sample ID : 1304053-01
Acquisition date
Total number of lines in spectrum

Number of unidentified lines
Number of lines tentatively identified by NID
Nuclide Type
Nuclide
BA-133
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
4.135E+02
Total Activity
:
---------
4.135E+02
Wtd Mean
Decay Corr
pCi/filter
4.135E+02
2-Sigma
Decay Corr
2-Sigma Error %Error Flags
18.82
0.778E+02
---------
4.135E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
AM-241
432.20Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.949E+02
1. 00
2.981E+00
Total Activity
Grand Total Activity :
Flags: "K"
"E"
14.71%
FISSION
Hlife
10.50Y
Nuclide Type
34
29
5
Page :
2
25-APR-2013 10:04:35
---------
Wtd Mean
Decay Corr
pCi/filter
3.949E+02
2.981E+00
---------
3.979E+02
3.979E+02
8.114E+02
8.114E+02
= Key line not found

= Manually edited
Decay Corr
2-Sigma
0.649E+02
16.43
1.657E+00
55.58
"M"
"A"
= Manually accepted
= Nuclide specific abn. limit
6288
Nuclide Line Activity Report

Sample ID : 1304053-01
Acquisition date
Page :
3
25-APR-2013 10:04:35
Nuclide Type: FISSION

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for
Uncorrected Decay Corr 2-Sigma

%Eff
pCi/filter pCi/filter %Error
1.963E+01 4.135E+02
4.135E+02 18.82
4.915E+00 5.805E+02
5.806E+02 33.73
6.963E+00 3.773E+02
3.773E+02 17.62
3 Valid Peaks
Status
OK
OK
OK
4.135E+02+/- 7.783E+01 ( 18.82%)
Nuclide Type: NATURAL

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
Flag:
11
* 11
Keyline
1 Valid Peaks
35.90*
Final Mean for

%Eff
5.865E+01 3.949E+02
3.949E+02 16.43
8.010E+01
1 Valid Peaks
3.949E+02+/- 6.490E+01 ( 16.43%)
2.981E+00
Status
OK
2.981E+00
55.58
OK
2.981E+00+/- 1.657E+00 ( 55.58%)
Combined Activity-MDA Report

Sample ID : 1304053-01
Acquisition date
Page :
4
25-APR-2013 10:04:35
---- Identified Nuclides
Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filter)
Act error
4.135E+02
3.949E+02
2.981E+00
7.783E+01
6.490E+01
1.657E+00
MDA
(pCi/filter)
1.752E+01
5.454E+01
4.219E+00
MDA error
Act/MDA
2.876E+00
1.748E+00
9.899E-02
23.607
7.240
0.706
MDA error
Act/MDA
6.747E+00
2.679E+01
3.632E-03
7.148E-02
7.724E+00
0.303
-0.085
0.000
2.714
0.405
Non-Identified Nuclides
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/filter)Ided
6.551E+00
-1.759E+01
O.OOOE+OO
1.032E+01
2.570E+01
Act error
1.282E+01
1.507E+02
O.OOOE+OO
1.821E+00
4.166E+01
MDA
(pCi/filter)
2.161E+01
2.071E+02
1.933E-01
3.804E+00
6.344E+01
ii29i
~
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30405302 GEl BAFIL 190943.CN

BLANK
25-APR-2013 00:00:00
1304053-02
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
30.84
35.04
53.43
62.03
66.11
81.26
91.97
111.98
116.28
160.58
276.66
303.20
308.40
334.56
356.37
378.49
384.06
387.14
391.63
415.98
437.29
468.56
511.97
1803
428
59
259
137
743
64
205
39
28
67
127
35
76
529
7
138
236
60
13
116
21
29
60
48
111
81
68
90
70
56
66
63
29
52
26
50
19
9
11
6
4
35
5
9
0
2
2
0
4
4
0
0
3
3
0
0
0
0
0
0
0
2
2
2
0
0
0
0
l(f'LJ7 (-::>
Acquisition date :
Sample Qu~ntity
Sample Geometry
DetectorGeometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.34
1.68
2.19
1.94
1.97
1.95
1.43
1. 60
2.00
1. 28
1. 21
1. 55
1.51
1.83
1.92
1. 43
2.06
1. 74
2.07
1. 22
1. 84
2.15
3.46
31.08
35.27
53.66
62.26
66.34
81.49
92.20
112.21
116.50
160.81
276.87
303.42
308.61
334.77
356.58
378.70
384.27
387.35
391.83
416.18
437.49
468.76
512.17
Left
Pw
27
27
50
58
58
78
88
107
107
157
274
299
307
330
353
375
381
381
381
412
432
466
508
12
12
8
16
16
9
8
13
13
7
7
8
6
8
9
5
20
20
20
6
11
6
9
'
25-APR-2013 10:29:05
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.27 0.0%
4096
10.00000
Cts/Sec %Err
2.00E+00
4.75E-Ol
6.57E-02
2.88E-01
1.52E-01
8.26E-01
7.15E-02
2.27E-01
4.28E-02
3.09E-02
7.40E-02
1.41E-01
3.84E-02
8.44E-02
5.88E-01
7.92E-03
1.53E-01
2.62E-01
6.63E-02
1.45E-02
1.28E-01
2.33E-02
3.22E-02
2.4
5.6
33.4
8.2
14.5
4.3
25.7
8.8
38.0
51.0
18.3
13.3
31.1
19.8
4.6
72.8
9.2
7.3
15.8
75.8
10.1
31.4
18.6
Fit
6.97E+00
2.25E+00
1.33E+00
5.64E+00
&2.91

Sample ID : 1304053-02
Acquisition date

23
19
4
Page :
2
25-APR-2013 10:29:05
17.39%
Nuclide Type : FISSION

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.446E+02
Total Activity
3.446E+02
Wtd Mean .
Decay Corft
pCi/filter
3.446E+02
Decay Corr
2-Sigma
19.00
0.655E+02
3.446E+02
Nuclide Type : NATURAL

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.489E+02
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
3.489E+02
3.489E+02
3.489E+02
6.935E+02
6.935E+02
Keyline not found

Manually edited
"M"
"A"
2-Sigma
Decay Corr
17.23
0.601E+02
= Manually accepted
6292

Sample ID : 1304053-02
Acquisition date
Page :
3
25-APR-2013 10:29:05

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.446E+02 19.00
1.963E+01 3.446E+02
4.915E+00 4.353E+02
4.353E+02 39.48
6.963E+00 3.804E+02
3.804E+02 17.73
3 Valid Peaks
Status
OK
OK
OK
3.446E+02+/- 6.546E+01 ( 19.00%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
5.865E+01 3.489E+02
3.489E+02 17.23
1 Valid Peaks
Status
OK
3.489E+02+/- 6.011E+01 ( 17.23%)

Sample ID : 1304053-02
Acquisition date
4
Page :
25-APR-2013 10:29:05

Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.446E+02
3.489E+02
6.546E+01
6.011E+01
MDA
(pCi/filter)
1.773E+01
4.990E+01
MDA error
Act/MDA
2.910E+00
1.599E+00
19.443
6.991
MDA error
Act/MDA
7.335E+00
2.592E+01
3.632E-03
6.574E-02
6.889E+00
1.489E-01
0.451
0.547
0.000
2.295
0.596
1.673
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
1.059E+01
1.096E+02
O.OOOE+OO
8.028E+00
3.372E+01
1.062E+01
Act error
1.388E+01
1.229E+02
O.OOOE+OO
1.692E+00
3.437E+01
3.230E+00
MDA
(pCi/filter)
2.349E+01
2.004E+02
1.933E-01
3.499E+00
5.659E+01
6.347E+00
- - - - -
sf~\\?
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE].SMP_l30405303 GEl BAFIL 190945.CN

DUP 03 TOT
25-APR-2013 00:00:00
1304053-03
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
30.82
35.02
51.86
61.93
65.69
81.18
111.37
160.38
182.62
185.93
276.91
303.06
307.71
334.06
338.71
356.37
376.88
384.02
387.12
391.69
414.95
418.62
422.83
437.34
468.83
511.65
802.95
1922
467
55
240
98
765
138
36
14
44
47
143
22
68
27
545
19
120
200
43
35
36
12
92
9
28
8
66
47
99
78
81
107
129
73
18
27
36
17
17
23
12
29
16
13
10
4
4
7
8
19
11
20
0
2
2
0
2
2
0
0
0
1
1
0
2
2
5
5
0
0
2
2
2
1
1
1
0
0
0
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.42
1. 51
2.67
1.73
1. 74
1. 85
1. 71
1. 66
1. 72
1.72
1.40
1.63
2.01
1. 99
2.01
1.98
2.64
1.62
1. 91
1.86
1.89
1. 90
1. 90
1. 77
1. 36
2.69
1. 77
31.05
35.25
52.09
62.16
65.92
81.41
111.59
160.60
182.84
186.16
277.13
303.28
307.92
334.27
338.93
356.58
377.08
384.23
387.33
391.90
415.16
418.83
423.03
437.54
469.03
511.85
803.12
Left
Pw
27
27
49
58
58
78
108
156
181
181
272
299
299
331
331
352
374
382
382
382
410
410
410
433
465
506
800
13
13
8
12
12
7
8
10
9
9
9
20
20
11
11
11
7
14
14
14
18
18
18
10
6
13
6
25-APR-2013 10:46:13
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.26 0.0%
4096
10.00000
Cts/Sec %Err
2.14E+00
5.18E-01
6.16E-02
2.67E-01
1.09E-Ol
8.50E-01
1.53E-01
3.95E-02
1.50E-02
4.88E-02
5.22E-02
1.59E-Ol
2.43E-02
7.53E-02
3.05E-02
6.06E-01
2.08E-02
1.34E-01
2.22E-01
4.77E-02
3.85E-02
3.97E-02
1.33E-02
1.02E-01
1.04E-02
3.07E-02
8.89E-03
2.3
5.3
33.6
8.5
18.9
4.3
16.6
47.9
46.4
24.2
27.2
9.2
38.6
16.2
31.6
4.7
42.3
10.5
9.1
20.6
21.4
21.9
48.1
13.9
63.9
38.2
35.4
Fit
1.38E+Ol
4.37E+00
2.33E+00
1.45E+00
2.44E+00
5.05E+00
l.lOE+OO

Sample ID : 1304053-03
Acquisition date

27
23
4
Page :
2
25-APR-2013 10:46:13
14.81%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.548E+02
Total Activity
---------
3.548E+02
Wtd Mean
Decay Corr
pCi/filter
3.548E+02
2-Sigma
Decay Corr
18.92
0.671E+02
---------
3.548E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.235E+02
Total Activity
Flags: "K"
"E"
---------
Wtd Mean
Decay Corr
pCi/filter
3.235E+02
---------
3.235E+02
3.235E+02
6.783E+02
6.784E+02
= Key line not found

= Manually edited
2-Sigma
Decay Corr
17.81
0.576E+02
"M"
"A"
= Manually accepted

Sample ID : 1304053-03
Acquisition date
Page :
3
25-APR-2013 10:46:13

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.963E+01 3.548E+02
3.548E+02 18.92
4.915E+00 4.908E+02
4.908E+02 34.53
6.963E+00 3.919E+02
3.919E+02 17.84
3 Valid Peaks
Status
OK
OK
OK
3.548E+02+/- 6.712E+01 ( 18.92%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
5.865E+01 3.235E+02
3.235E+02 17.81
1 Valid Peaks
Status
OK
3.235E+02+/- 5.763E+01 ( 17.81%)
Keyline
i297

Sample ID : 1304053-03
Acquisition date
Page :
4
25-APR-2013 10:46:13
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.548E+02
3.235E+02
Act error
6.712E+01
5.763E+01
MDA
(pCi/filter)
2.130E+01
6.177E+01
MDA error
Act/MDA
3.497E+00
1.979E+00
16.658
5.237
MDA error
Act/MDA
6.871E+00
2.917E+01
3.632E-03
6.458E-02
7.686E+00
1.496E-01
0.204
-0.137
0.000
2.229
0.083
1.175
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
4.498E+00
-3.099E+01
O.OOOE+OO
7.661E+00
5.237E+00
7.489E+00
Act error
1.235E+01
1.457E+02
O.OOOE+OO
1.663E+00
3.920E+01
3.512E+00
MDA
(pCi/filter)
2.201E+01
2.255E+02
1.933E-01
3.437E+00
6.313E+01
6.375E+00
&298
~~~?
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30405304 GEl BAFIL 190948.CN

PZ-305-AI TOT
25-APR-2013 00:00:00
1304053-04
FILTER
GEl
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
30.81
35.02
52.44
61.80
65.89
81.20
84.25
92.80
111.90
143.95
160.12
186.73
192.65
276.75
292.62
295.66
303.20
307.56
331.79
337.82
356.24
384.27
387.18
391.55
414.95
418.43
422.84
437.28
468.17
473.15
507.94
511.20
918.38
1872
406
59
255
102
753
22
24
200
17
30
22
30
67
9
9
164
32
24
34
528
129
180
30
52
26
12
93
29
8
5
19
9
56
57
115
73
71
53
53
97
93
68
60
58
47
8
10
10
12
15
11
22
15
7
3
3
7
5
3
6
5
5
0
2
0
3
3
0
2
2
6
6
0
0
0
0
0
0
1
1
1
4
4
1
1
0
5
5
5
2
2
2
0
6
6
3
3
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.47
1. 58
2.04
1.73
1.74
1.63
1. 52
1. 08
1. 66
2.75
2.44
2.02
2.88
1. 80
1. 81
1.81
1. 75
2.22
1. 67
1. 84
1.95
2.51
1. 82
1. 92
2.08
2.09
2.09
1. 96
2.24
3.11
2.15
2.36
2.11
31.04
35.26
52.67
62.03
66.12
81.43
84.48
93.03
112.13
144.17
160.34
186.95
192.87
276.97
292.84
295.87
303.41
307.77
332.00
338.03
356.45
384.47
387.39
391.76
415.15
418.64
423.05
437.49
468.37
473.35
508.14
511.40
918.56
Left
Pw
27
27
49
57
57
78
78
89
107
141
156
184
190
271
271
271
300
300
328
328
351
380
380
380
411
411
411
433
462
462
506
506
916
13
13
9
13
13
9
9
8
8
7
8
6
6
28
28
28
27
27
14
14
9
17
17
17
16
16
16
9
16
16
10
10
6
25-APR-2013 11:01:41
l.OOOOOE+OO filter
0
BAFIL
0 00:15:00.26 0.0%
4096
10.00000
Cts/Sec %Err
2.08E+00
4.51E-01
6.60E-02
2.83E-01
1.13E-01
8.37E-01
2.46E-02
2.70E-02
2.22E-01
1. 89E-02
3.29E-02
2.46E-02
3.35E-02
7.49E-02
9.70E-03
9.63E-03
1.83E-01
3.55E-02
2.68E-02
3.75E-02
5.86E-01
1.44E-01
2.00E-01
3.35E-02
5.75E-02
2.85E-02
1.29E-02
1.03E-01
3.25E-02
8.45E-03
6.01E-03
2.15E-02
1. OOE-02
2.3
5.8
34.8
8.1
16.7
3.9
96.5
72.9
10.9
84.0
48.9
58.5
40.5
14.0
63.7
68.2
8.1
38.2
32.4
28.7
4.6
13.7
8.6
23.6
16.2
29.4
46.5
11.5
23.7
90.4
45.3
31.1
33.3
Fit
1. 87E+Ol
3.81E+00
2.09E+Ol
1.81E+00
3.72E+00
9.95E+00
4.28E+00
1.49E+00
1.16E+00
1.31E+00

Sample ID : 1304053-04
Acquisition date

33
29
4
Page :
2
25-APR-2013 11:01:41
12.12%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.491E+02
Total Activity
---------
3.491E+02
Wtd Mean
Decay Corr
pCi/filter
3.491E+02
2-Sigma
Decay Corr
0.649E+02
18.58
---------
3.491E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.437E+02
Total Activity
Flags: "K"
"E"
=
=
---------
Wtd Mean
Decay Corr
pCi/filter
3.437E+02
---------
3.437E+02
3.437E+02
6.928E+02
6.928E+02
Keyline not found

Manually edited
2-Sigma
Decay Corr
17.06
0.586E+02
"M"
"A"
=
=
Manually accepted
Nuclide specific abn. limit

Sample ID : 1304053-04
Acquisition date
Page :
3
25-APR-2013 11:01:41

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.963E+01 3.491E+02
3.491E+02 18.58
4.915E+00 5.646E+02
5.647E+02 33.39
6.963E+00 3.793E+02
3.793E+02 17.68
3 Valid Peaks
Status
OK
OK
OK
3.491E+02+/- 6.486E+01 ( 18.58%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
* 11
Keyline

%Eff
5.865E+01 3.437E+02
3.437E+02 17.06
1 Valid Peaks
Status
OK
3.437E+02+/- 5.863E+01 ( 17.06%)

Sample ID : 1304053-04
Acquisition date
4
Page :
25-APR-2013 11:01:41
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.491E+02
3.437E+02
Act error
6.486E+01
5.863E+01
MDA
(pCi/filter)
1.688E+01
6.129E+01
MDA error
Act/MDA
2.771E+00
1.964E+00
20.684
5.608
MDA error
Act/MDA
5.960E+00
2.514E+01
3.632E-03
6.898E-02
6.861E+00
1.624E-01
-0.453
0.026
0.000
2.550
0.161
1.548
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-8.641E+00
5.126E+00
O.OOOE+OO
9.358E+00
9.062E+00
1.071E+01
Act error
1.229E+01
1.370E+02
O.OOOE+OO
1.761E+00
3.856E+01
3.695E+00
MDA
(pCi/filter)
1.909E+01
1.944E+02
1.933E-01
3.670E+00
5.635E+01
6.921E+00
C--

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
25-APR-2013 00:00:00
1304053-05
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
2
2
0
1
1
0
0
0
0
0
1
1
4
4
4
1
1
0
1
1
1
1
2
2
0
0
0
30.62
34.82
52.47
61.61
65.67
80.81
111.11
160.06
185.91
195.65
269.85
276.53
302.73
307.36
312.25
333.53
337.86
355.99
376.85
383.87
386.84
390.87
414.46
418.34
437.09
467.65
510.91
1659
432
45
200
96
708
141
27
27
21
14
31
92
30
15
77
21
429
16
92
199
40
41
18
88
19
22
78
63
127
73
71
118
192
55
45
44
20
15
20
17
10
5
5
28
18
16
10
10
19
23
17
8
5
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
'-{('"L.(l,,
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_130405305 GE3 BAFIL 190942.CN

PZ-305-AI DIS
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1.42
1. 59
1. 78
1. 51
1. 52
1. 31
1. 43
1. 28
1.29
2.73
1.77
1.78
1.64
2.40
2.41
1. 83
1.83
1.54
1.86
1. 87
1. 71
1.88
2.08
2.09
1.44
1. 27
3.55
30.94
35.14
52.79
61.93
65.99
81.13
111.42
160.37
186.22
195.96
270.16
276.84
303.04
307.67
312.56
333.83
338.17
356.30
377.15
384.17
387.14
391.17
414.76
418.64
437.39
467.95
511.21
Left
Pw
26
26
49
57
57
77
107
158
183
193
267
267
299
299
299
328
328
352
374
374
374
374
409
409
434
464
508
16
16
8
12
12
7
9
6
6
7
18
18
19
19
19
17
17
8
22
22
22
22
13
13
8
7
9
25-APR-2013 10:11:25
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.68 0.4%
4096
10.00000
Cts/Sec %Err
1.84E+00
4.80E-01
5.00E-02
2.22E-01
1.06E-01
7.87E-01
1. 57E- 01
2.98E-02
3.00E-02
2.33E-02
1.52E-02
3.50E-02
1.02E-01
3.30E-02
1.62E-02
8.53E-02
2.33E-02
4.76E-01
1.79E-02
1.02E-01
2.21E-01
4.46E-02
4.50E-02
1.95E-02
9.79E-02
2.07E-02
2.39E-02
2.5
5.8
46.0
9.7
17.0
4.5
19.7
48.0
43.7
56.8
53.5
26.5
13.1
35.4
62.6
12.2
31.7
5.3
42.6
13.5
7.9
29.1
23.3
48.4
13.5
35.0
28.0
Fit
6.38E+00
1.93E+00
1.63E+00
3.04E+00
1.64E+00
2.75E+00
4.45E+00

Sample ID : 1304053-05
Acquisition date

27
23
4
Page :
2
25-APR-2013 10:11:25
14.81%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.395E+02
Total Activity
---------
3.395E+02
Wtd Mean
Decay Corr
pCi/filter
3.395E+02
2-Sigma
Decay Corr
18.22
0.618E+02
---------
3.395E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
5.957E+02
Total Activity
Flags: "K"
"E"
=
=
---------
Wtd Mean
Decay Corr
pCi/filter
5.957E+02
---------
5.957E+02
5.957E+02
9.352E+02
9.352E+02
Keyline not found

Manually edited
2-Sigma
Decay Corr
20.54
1.224E+02
"M''
"A"
Manually accepted

Sample ID : 1304053-05
Acquisition date
Page :
3
25-APR-2013 10:11:25

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.395E+02
3.395E+02 18.22
6.222E+00 2.486E+02
2.486E+02 33.30
5.860E+00 3.661E+02
3.661E+02 17.26
3 Valid Peaks
Status
OK
OK
OK
3.395E+02+/- 6.185E+01 ( 18.22%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"
Keyline

%Eff
2.648E+01 5.957E+02
5.957E+02 20.54
1 Valid Peaks
Status
OK
5.957E+02+/- 1.224E+02 ( 20.54%)

Sample ID : 1304053-05
Acquisition date
4
Page :
25-APR-2013 10:11:25
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.395E+02
5.957E+02
Act error
6.185E+01
1.224E+02
MDA
(pCi/filter)
2.096E+01
1.242E+02
MDA error
Act/MDA
3.206E+00
6.671E+00
16.197
4.796
MDA error
Act/MDA
1.145E+00
1.662E+01
3.957E-02
3.698E-02
4.700E+00
9.150E-01
-0.314
0.046
0.653
1.215
0.077
1.648
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
-3.149E+00
9.307E+00
1.817E+00
3.160E+00
4.502E+00
3.067E+01
Act error
6.101E+00
1.158E+02
1.383E+00
1.362E+00
3.589E+01
9.718E+00
MDA
(pCi/filter)
1.003E+01
2.016E+02
2.782E+00
2.600E+00
5.814E+01
1.861E+01
-if~\~)
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKAlOO: [GAMMA.SCUSR.ARCHIVE]SMP_l30405306 GE3 BAFIL 190944.CN

PEAK V16.9 PEAKEFF V2.2
DUP 03 TOT
25-APR-2013 00:00:00
1304053-06
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
30.58
34.94
52.88
61.68
65.54
70.80
80.81
91.73
111. 73
153.76
276.75
302.65
333.67
337.25
356.02
383.70
386.87
391.26
414.53
417.87
437.13
469.41
508.35
511.29
1760
456
33
250
87
19
692
16
162
23
43
128
71
23
432
73
147
38
37
14
92
12
9
11
3
3
0
1
1
1
0
0
0
0
0
0
3
3
0
6
6
0
1
1
0
0
7
7
Bkgnd
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
70 1.45
81 1. 55
90 1. 85
76 .1. 51
73 1.52
71 1.52
136 1.30
105 1. 76
109 1. 27
65 2.04
22 1. 89
23 1.45
19 2.21
20 2.22
12 1.69
30 2.30
21 1. 35
21 1. 93
13 1. 89
14 1. 90
15 1.47
9 1.85
0 3.45
0 2.38
30.89
35.26
53.20
62.00
65.86
71.12
81.13
92.05
112.04
154.07
277.06
302.96
333.98
337.55
356.32
384.00
387.17
391.56
414.83
418.17
437.43
469.71
508.64
511.59
25-APR-2013 10:29:34
l.OOOOOE+OO filter
0
BAFIL
0 00:15:03.82 0.4%
4096
10.00000
Left
Pw
Cts/Sec %Err
27
27
50
57
57
57
77
90
109
150
275
299
329
329
354
381
381
390
406
406
432
465
507
507
14
14
6
20
20
20
8
7
6
8
7
7
15
15
7
9
9
6
20
20
10
7
9
9
1.96E+00 2.5
5.07E-01 5.6
3.64E-02 49.1
2.77E-01 8.5
9.70E-02 18.8
2.06E-02 74.7
7.69E-01 4.8
1.78E-02108.6
1.80E-01 12.9
2.58E-02 63.3
4.76E-02 23.5
1. 42E- 01 10.8
7.84E-02 16.6
2.54E-02 51.8
4.80E-01 5.0
8.16E-02 23.2
1.63E-01 9.7
4.24E-02 25.9
4.16E-02 21.7
1. 55E-02 62.9
1. 02E-01 13.1
1.38E-02 48.5
9.55E-03 20.2
1.27E-02 41.8
Fit
1.21E+Ol
2.65E+00
1.92E+00
7.21E+00
2.20E+00
9.34E-01
i3i7

Sample ID : 1304053-06
Acquisition date

24
20
4
Page :
2
25-APR-2013 10:29:34
16.67%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 3.319E+02
Total Activity
Nuclide Type
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.447E+02
Total Activity
=
=
2-Sigma
Decay Corr
18.48
0.613E+02
---------
3.319E+02
NATURAL
Nuclide
Hlife
TH-234 4.47E+09Y
Flags: "K"
"E"
---------
3.319E+02
Wtd Mean
Decay Corr
pCi/filter
3.319E+02
---------
Wtd Mean
Decay Corr
pCi/filter
7.447E+02
---------
7.447E+02
7.447E+02
1.077E+03
1.077E+03
Keyline not found

Manually edited
"M"
"A"
=
=
Decay Corr
2-Sigma
1.366E+02
18.34
Manually accepted

Sample ID : 1304053-06
Acquisition date
Page :
3
25-APR-2013 10:29:34

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.319E+02
3.319E+02 18.48
3.463E+02 29.87
6.222E+00 3.463E+02
5.860E+00 3.693E+02
3.693E+02 16.91
3 Valid Peaks
Status
OK
OK
OK
3.319E+02+/- 6.135E+01 ( 18.48%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
* 11
Keyline

%Eff
2.648E+01 7.447E+02
7.447E+02 18.34
1 Valid Peaks
Status
OK
7.447E+02+/- 1.366E+02 ( 18.34%)

Sample ID : 1304053-06
Acquisition date
4
Page :
25-APR-2013 10:29:34
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
3.319E+02
7.447E+02
Act error
6.135E+01
1.366E+02
MDA
(pCi/filter)
1.757E+01
1.325E+02
MDA error
Act/MDA
2.687E+00
7.114E+00
18.893
5.622
MDA error
Act/MDA
1.124E+00
1.544E+01
4.650E-02
3.769E-02
4.402E+00
9.833E-01
0.053
-0.008
0.981
0.811
-0.300
1.797
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
5.166E-01
-1.417E+00
3.206E+00
2.150E+00
-1.633E+01
3.594E+01
Act error
5.569E+00
1.328E+02
1.594E+00
1.392E+00
4.095E+01
1.133E+01
MDA
(pCi/ filter)
9.839E+00
1.873E+02
3.270E+00
2.650E+00
5.446E+01
2.000E+01
G31i
~t%'"'
...t\
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130405307 GE3 BAFIL 190946.CN

DUP 03 DIS
25-APR-2013 00:00:00
1304053-07
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30.59
34.86
52.21
58.82
61.65
65.63
80.79
91.84
111.64
116.16
161.61
207.53
276.55
302.72
306.77
333.42
338.13
355.88
364.33
383.67
386.84
391.37
414.53
417.87
421.87
436.91
467.88
472.07
510.92
2144
526
105
29
259
159
842
44
243
73
59
19
49
141
26
85
32
490
15
99
188
47
31
34
11
131
31
12
23
86
98
113
31
67
84
178
69
74
84
97
60
34
20
30
28
13
18
11
35
68
15
12
12
12
.7
1
3
0
3
3
0
1
1
1
0
0
6
6
0
0
0
2
2
0
0
0
0
1
1
0
1
1
1
0
2
2
0
AcquisitiG:>n date
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 39
1. 55
2.23
1.50
1.51
1.52
1.32
1. 36
1. 66
2.31
3.80
0.98
1. 64
1.43
1.99
1. 36
1. 43
1.50
1.85
1.87
1.86
1.92
1.89
1. 90
1. 90
1.61
2.13
2.13
2.49
30.91
35.17
52.53
59.14
61.97
65.95
81.11
92.15
111.96
116.48
161.93
207.84
276.86
303.02
307.07
333.73
338.44
356.18
364.64
383.97
387.15
391.67
414.83
418.17
422.17
437.21
468.18
472.37
511.22
Left
Pw
26
26
49
58
58
58
77
89
98
98
157
205
274
298
298
330
337
351
362
381
381
390
411
411
411
432
463
463
507
17
17
8
12
12
12
8
6
23
23
11
7
8
13
13
7
5
10
6
10
10
6
15
15
15
10
13
13
9
25-APR-2013 10:46:52
1.00000E+00 filter
0
BAFIL
0.4%
0 00:15:03.23
4096
10.00000
Cts/Sec %Err
2.38E+00
5.84E-01
1.16E-01
3.22E-02
2.87E-01
1.76E-01
9.36E-01
4.92E-02
2.70E-01
8.06E-02
6.56E-02
2.11E-02
5.40E-02
1. 57E-01
2.84E-02
9.44E-02
3.55E-02
5.45E-01
1. 70E-02
1.10E-01
2.09E-01
5.17E-02
3.41E-02
3.82E-02
1. 21E- 02
1.45E-01
3.41E-02
1.33E-02
2.56E-02
2.2
5.2
20.2
34.0
8.4
12.0
4.4
33.2
8.4
26.9
34.7
71.3
25.3
9.3
42.6
15.0
25.0
4.8
42.2
15.7
10.6
21.3
26.5
26.4
66.3
9.6
19.6
42.8
20.9
Fit
8.85E+00
8.56E+00
1. 97E+00
4.39E+00
1.54E+01
2.55E+00
8.79E-01

Sample ID : 1304053-07
Acquisition date

29
24
5
Page :
2
25-APR-2013 10:46:52
17.24%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 4.036E+02
Total Activity
4.036E+02
Wtd Mean
Decay Corr
pCi/filter
4.036E+02
2-Sigma
Decay Corr
0.730E+02
18.10
4.036E+02

Nuclide
Hlife
TH-234 4.47E+09Y
AM-241
432.20Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.716E+02
1. 00
8.380E+00
Total Activity
Flags: "K"
"E"
=
=
Wtd Mean
Decay Corr
pCi/filter
7.716E+02
8.380E+00
7.800E+02
7.800E+02
1.184E+03
1.184E+03
Keyline not found

Manually edited
"M"
"A"
=
=
2-Sigma
Decay Corr
1.395E+02
18.08
68.29
5.723E+00
Manually accepted
i312

Sample ID : 1304053-07
Acquisition date
Page :
3
25-APR-2013 10:46:52

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 4.036E+02
4.036E+02 18.10
6.222E+00 3.833E+02
3.833E+02 27.79
5.860E+00 4.189E+02
4.189E+02 16.67
3 Valid Peaks
Status
OK
OK
OK
4.036E+02+/- 7.304E+01 ( 18 .10%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

AM-241
59.54
Flag:
11
* 11
Keyline
1 Valid Peaks =
35.90*
Final Mean for

%Eff
2.648E+01 7.716E+02
7.716E+02 18.08
2.893E+01
1 Valid Peaks
7.716E+02+/- 1.395E+02 ( 18.08%)
8.380E+00
Status
OK
8.380E+00
68.29
OK
8.380E+00+/- 5.723E+00 ( 68.29%)

Sample ID : 1304053-07
Acquisition date
4
Page :
25-APR-2013 10:46:52
Identified Nuclides
Nuclide
BA-133
TH-234
AM-241
Activity
(pCi/filter)
Act error
4.036E+02
7.716E+02
8.380E+00
7.304E+01
1.395E+02
5.723E+00
MDA
(pCi/filter)
2.200E+01
1.402E+02
1.355E+01
MDA error
Act/MDA
3.364E+00
7.530E+00
6.663E-01
18.349
5.504
0.618
MDA error
Act/MDA
1.253E+00
1.558E+01
4.253E-02
3.991E-02
4.492E+00
0.494
-0.190
0.784
1. 229
-0.587
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
Key-Line
Activity K.L.
(pCi/filter)Ided
5.414E+00
-3.591E+01
2.343E+00
3.450E+00
-3.264E+01
Act error
6.176E+00
1.391E+02
1.475E+00
1.495E+00
4.402E+01
MDA
(pCi/filter)
1.097E+01
1.889E+02
2.990E+00
2.806E+00
5.557E+01
\cJ,;S'\v)
""\
Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
Pk It
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
1
1
1
0
0
2
2
1
1
0
1
1
0
0
0
0
1
1
0
1
1
1
4
4
4
0
0
0
0
0
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130405308 GE3 BAFIL 190949.CN

DUP 04 TOT
25-APR-2013 00:00:00
1304053-08
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
Energy
Area
Bkgnd
FWHM Channel
Left
Pw
27.81
30.65
34.76
46.44
52.18
61.61
65.73
80.76
83.74
92.78
111.72
115.54
160.53
277.27
302.94
307.12
333.71
337.86
355.98
383.61
386.87
391.53
415.50
421.90
425.97
436.81
455.84
468.17
511.08
1097.73
40
1904
411
34
63
245
144
789
26
24
208
56
26
36
129
28
93
29
465
130
216
38
41
21
10
82
10
17
19
6
104
81
55
80
100
86
79
56
46
108
61
57
76
44
16
20
16
14
10
8
7
6
9
6
5
5
4
12
3
0
1. 43
28.13
1. 38
30.97
1. 45
35.08
1.84
46.76
2.47
52.49
1. 66
61.92
1. 67
66.05
1. 54
81.08
1. 55
84.06
2.14
93.09
1. 59 112.04
1. 60 115.85
1. 55 160.85
1.48 277.58
1.41 303.25
1. 81 307.42
1.83 334.01
1. 83 338.17
1. 66 356.29
1.87 383.91
1.87 387.17
1.88 391.83
2.52 415.80
2.53 422.20
2.53 426.27
1.55 437.11
1.41 456.14
1. 94 468.47
2.97 511.37
1. 33 1098.00
26
26
26
43
49
57
57
77
77
91
109
109
157
273
300
306
328
328
351
380
380
380
410
410
410
432
451
463
508
1094
14
14
14
7
7
16
16
10
10
7
11
11
8
10
6
5
15
15
10
16
16
16
21
21
21
8
8
8
8
7
25-APR-2013 11:02:42
1.00000E+00 filter
0
BAFIL
0 00:15:03.56 0. 4%
4096
10.00000
Cts/Sec %Err
4.46E-02
2.12E+00
4.57E-01
3.77E-02
7.01E-02
2.72E-01
1.59E-01
8.77E-01
2.93E-02
2.64E-02
2.31E-01
6.23E-02
2.89E-02
4.01E-02
1.43E-01
3.10E-02
1.03E-01
3.18E-02
5.17E-01
1.44E-01
2.40E-01
4.17E-02
4.51E-02
2.33E-02
1.07E-02
9.12E-02
1.11E-02
1.87E-02
2.10E-02
6.67E-03
37.8
2.4
5.9
47.3
29.1
8.6
12.7
3.8
67.7
75.0
9.0
27.4
61.8
38.4
10.1
30.3
11.8
30.8
4.8
10.2
8.2
22.0
24.5
41.0
68.1
11.9
46.9
43.2
29.0
40.8
Fit
5.60E+00
1.70E+00
1.06E+01
9.25E-01
1.27E+00
8.16E+00
4.56E+00

Sample ID : 1304053-08
Acquisition date

30
26
4
Page :
2
25-APR-2013 11:02:42
13.33%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.782E+02
Total Activity
---------
3.782E+02
Wtd Mean
Decay Corr
pCi/filter
3.782E+02
Decay Corr
2-Sigma
0.664E+02
17.56
---------
3.782E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
7.313E+02
Total Activity
Flags: "K"
"E"
=
=
---------
Wtd Mean
Decay Corr
pCi/filter
7.313E+02
---------
7.313E+02
7.313E+02
1.109E+03
1.110E+03
Keyline not found

Manually edited
Decay Corr
2-Sigma
1.347E+02
18.42
"M"
"A"
=
=
Manually accepted

Sample ID : 1304053-08
Acquisition date
Page :
3
25-APR-2013 11:02:42

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
1.899E+01 3.782E+02
3.782E+02 17.56
6.222E+00 3.485E+02
3.486E+02 28.90
5.860E+00 3.971E+02
3.972E+02 16.69
3 Valid Peaks
Status
OK
OK
OK
3.782E+02+/- 6.642E+01 ( 17.56%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag:
11
* 11
Keyline

%Eff
2.648E+01 7.313E+02
7.313E+02 18.42
1 Valid Peaks
Status
OK
7.313E+02+/- 1.347E+02 ( 18.42%)

Sample ID : 1304053-08
Acquisition date
Page :
4
25-APR-2013 11:02:42
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.782E+02
7.313E+02
6.642E+01
1.347E+02
MDA
(pCi/filter)
1.973E+01
1.309E+02
MDA error
Act/MDA
3.017E+00
7.028E+00
19.174
5.589
MDA error
Act/MDA
1.269E+00
1.553E+01
4.624E-02
3.878E-02
4.106E+00
9.796E-01
0.722
0.384
0.719
1.220
-0.164
1.811
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
8.020E+00
7.227E+01
2.337E+00
3.326E+00
-8.335E+00
3.608E+01
Act error
5.956E+00
1.223E+02
1.650E+00
1.445E+00
3.710E+01
1.042E+01
MDA
(pCi/filter)
1.111E+01
1.884E+02
3.251E+00
2.727E+00
5.079E+01
1.992E+01
&318
~shl
\V
~

Configuration
Analyses by
Client ID
Deposition Date
Sample Date
Sample ID
Sample type
Detector name
Elapsed live time:
Start channel
Sensitivity
Critical level
DKA100: [GAMMA.SCUSR.ARCHIVE]SMP_130405309 - GE3 BAFIL 190951.CN

DUP 04 DIS
25-APR-2013 00:00:00
1304053-09
FILTER
GE3
0 00:15:00.00
25
3.00000
No
Pk It
Energy
Area
Bkgnd
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
30.61
34.81
52.36
61.64
65.57
80.80
92.74
101.10
111.61
116.35
213.44
276.44
288.20
302.73
307.27
311.33
315.01
333.62
338.04
355.96
364.22
383.71
386.91
391.06
411.34
414.68
418.06
422.53
437.00
468.10
511.21
1794
404
82
274
106
762
76
38
218
71
13
67
10
151
35
12
11
76
13
434
11
112
187
44
7
43
25
10
99
15
18
86
67
158
77
84
112
125
77
74
79
49
26
20
18
12
7
4
17
14
11
11
9
9
9
0
1
2
3
11
16
5
1
1
0
3
3
0
0
0
5
5
0
0
0
4
4
4
4
2
2
3
3
2
2
2
2
2
2
2
0
0
0
Acquisition date :
Sample Quantity
Sample Geometry
Detector Geometry:
Elapsed real time:
End channel
Gaussian
FWHM Channel
1. 37
1. 45
2.21
1. 82
1.83
1. 30
2.04
2.77
1.60
2.34
1.11
2.10
2.71
1. 50
2.40
2.41
1. 97
1. 95
2.02
1.49
2.24
2.06
1. 86
2.06
2.08
2.08
2.09
1.90
1. 52
1.79
2.99
30.93
35.13
52.68
61.95
65.89
81.12
93.06
101.42
111.93
116.66
213.75
276.75
288.51
303.03
307.58
311.63
315.32
333.93
338.35
356.27
364.53
384.02
387.21
391.36
411. 64
414.98
418.36
422.83
437.30
468.40
511.50
Left
Pw
26
26
48
58
58
77
88
99
108
108
210
273
286
298
298
298
298
328
328
352
352
380
380
380
410
410
410
410
432
464
508
14
14
10
11
11
8
11
6
16
16
7
8
7
20
20
20
20
16
16
16
16
15
15
15
18
18
18
18
8
8
9
25-APR-2013 11:18:31
1.00000E+00 filter
0
BAFIL
0 00:15:03.64 0.4%
4096
10.00000
Cts/Sec %Err
1.99E+00
4.49E-01
9.10E-02
3.04E-01
1.18E-01
8.47E-01
8.49E-02
4.25E-02
2.42E-01
7.83E-02
1.46E-02
7.47E-02
1.10E-02
1.68E-01
3.92E-02
1.31E-02
1.19E-02
8.46E-02
1.49E-02
4.82E-01
1.25E-02
1.25E-01
2.07E-01
4.88E-02
7.87E-03
4.73E-02
2.80E-02
1.12E-02
1.11E-01
1.67E-02
2.04E-02
2.5
5.9
30.7
7.7
18.2
4.3
30.5
39.6
8.9
26.9
93.4
17.9
86.2
9.0
31.4
79.2
66.7
13.8
60.5
4.9
63.8
11.1
9.1
25.7
42.4
17.5
33.3
51.0
11.5
52.9
33.6
Fit
5.45E+00
2.90E+00
1.69E+00
2.10E+00
3.82E+00
5.45E-01
5.32E+00
2.49E+00

Sample ID : 1304053-09
Acquisition date

31
27
4
Page :
2
25-APR-2013 11:18:31
12.90%

Nuclide
BA-133
Hlife
10.50Y
Wtd Mean
Uncorrected
Decay pCi/filter
1. 00
3.653E+02
Total Activity
---------
3.653E+02
Wtd Mean
Decay Corr
pCi/filter
3.653E+02
2-Sigma
Decay Corr
18.04
0.659E+02
---------
3.653E+02

Nuclide
Hlife
TH-234 4.47E+09Y
Wtd Mean
Uncorrected
Decay pCi/filter
1.00 8.173E+02
Total Activity
Flags: "K"
"E"
=
=
---------
Wtd Mean
Decay Corr
pCi/filter
8.173E+02
---------
8.173E+02
8.173E+02
1.183E+03
1.183E+03
Keyline not found

Manually edited
2-Sigma
Decay Corr
16.80
1.373E+02
"M"
"A"
=
=
Manually accepted

Sample ID : 1304053-09
Acquisition date
Page :
3
25-APR-2013 11:18:31

Nuclide
BA-133
Energy
81.00
302.84
356.01
%Abn
33.00*
17.80
60.00
Final Mean for

%Eff
3.653E+02 18.04
1.899E+01 3.653E+02
27.36
4.100E+02
6.222E+00 4.099E+02
16.77
3.707E+02
5.860E+00 3.706E+02
3 Valid Peaks
Status
OK
OK
OK
3.653E+02+/- 6.591E+01 ( 18.04%)

Nuclide
TH-234
Energy
63.29
%Abn
3.80*
Final Mean for

Flag: "*"

%Eff
2.648E+01 8.173E+02
8.173E+02 16.80
1 Valid Peaks
Status
OK
8.173E+02+/- 1.373E+02 ( 16.80%)
Keyline
6321
-------------------------------------------

Sample ID : 1304053-09
Acquisition date
4
Page :
11:18:31
25-APR-2013
Identified Nuclides
Nuclide
BA-133
TH-234
Activity
(pCi/filter)
Act error
3.653E+02
8.173E+02
6.591E+01
1.373E+02
MDA
(pCi/filter)
1.840E+01
1.298E+02
MDA error
Act/MDA
2.814E+00
6.970E+00
19.852
6.298
MDA error
Act/MDA
1.153E+00
1.413E+01
3.869E-02
3.827E-02
3.838E+00
9.871E-01
0.145
0.156
0.373
1.124
-0.269
1. 863
Nuclide
C0-57
CD-109
PA-231
PA-234
NP-237
AM-241
Key-Line
Activity K.L.
(pCi/filter)Ided
1. 464E+.00
2.671E+01
1.016E+00
3.024E+00
-1.277E+01
3.741E+01
Act error
6.070E+00
1.161E+02
1.417E+00
1.441E+00
3.542E+01
1.046E+01
MDA
(pCi/filter)
1.009E+01
1.714E+02
2.720E+00
2.691E+00
4.748E+01
2.008E+01

Engineering Management Support, Inc.: West Lake OU-1

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ENGINEERING MANAGEMENT SUPPORT, INC.

West Lake OU-1

EBERLINE ANALYTICAL/OAK RIDGE LABORATORY

Chain of Custody & pH Check Sheet

Analytical Results Summary

Quality Control Sample Results Summary

Laboratory Technician's Notes

Analytical Data (Isotopic Uranium)

Analytical Data (Isotopic Thorium)

Analytical Data (Radium-226)

Analytical Data (Radium-228)

Barium-133 Analytical Tracer Data

Last Page Number

STANDARD OPERATING PROCEDURE

Eberline Services - Oak Ridge laboratory

Eberline Services Work Order # _ _ _

Technical/Clerical Corrections, Signatures Needed, Problems, Etc

Date pa ckage approved by:

Chain of Custody Record

Sampler (Print Name):

Relinquished by: (Signature)

Po~ !A.N.Jfl. ~d.

Heceived by: (::lignature)

Sample Custodian Remarks (Completed By Laboratory):

Total # Containers Received?

'r::f d:'~ ).J R 'r-l/

'-1/L(!'S 15;}.-j._J ~~IJ!.d)5

601 Scalboto Road

COC Seals Present?

... ..., ,...,

Chain of Custody Record

Sampler (Print Name):

Relinquished b'}J (Signature)

Received by: (Signature)

)(J lXJ '/j

RE ~o ADR 0 9' 2013

-\1 X l,xj 1J >\:) )j

rc;{ .iJ:1~ ~'A r ~V

Received by: ( ii!JI'!8IUI'&)

Sample Custodian Remarks (Completed By laboratOf)'):

Total # Containers Received?

COC Seals Present?

Fxns 04, 06 & 08 are TOTAL

Location (circle one)

Printed: 4/9/2013 2:24PM

Oak Ridge Laboratory

Fxns 04, 06 & 08 are TOTAL

Location (circle one}

"" " "

":'I ~t ~~1) ... -

ofu T-(vl Lf/22/13

Printed: 4/9/2013 2:24PM

Oak Ridge Laboratory

Fxns 04, 06 & 08 are TOTAL

Printed: 4/9/20t3 2:24PM '-"'

Oak Ridge Laboratory

Fxns 04, 06 & 08 are TOTAL

Printed: 4/9/2013 2:24 PM

Printed: 4/9/2013 2:03 PM

Internal Work Order

(Volumes, pH, & CPM)

PZ-305-AI TOT I'

Volume1LI '''. ;.:.;,c CJIIM,:c''''

Radionucllde of lnteresd :- 23 ~U J