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Figure 1. In situ microfiltration device with needle, funnel, filter disks, and syringe with piston in equilibrium position.
priate solvent is connected to the syringe and immersed vertically into the suspension. Filtration begins as soon as the piston is released. If the sample volume is small, say 0.1-0.2 mL, as is typical of our IR analyses of liquids (2), the short time required by the filtration makes it convenient to draw the piston by hand, eliminating the spring. When the phase of interest is the solid, it may be convenient to dip the funnel near the bottom of the container or to keep stirring the mixture rather than allowing it to sediment the particulate. The filter disk with the solid is easily removed by substituting the syringe containing the solution with one filled with nitrogen or argon and giving a short stroke to the piston. Literature Cited
1. Rodriguez-Fern andez, E.; Vicente, M. A.; Manzano, J. L. J. Chem. Educ. 2008, 85, 1051. 2. Lunelli, B.; Comelli, F. Rev. Sci. Instrum. 1987, 58, 305307.
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Vol. 87 No. 4 April 2010 pubs.acs.org/jchemeduc r 2010 American Chemical Society and Division of Chemical Education, Inc. 10.1021/ed800147c Published on Web 03/09/2010