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b
t
E
2R
Constant Bend Radius
compression
tension
M M
t/2 y
Maximum bend-induced
tensile stress at surface, y=t/2
0
50
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Bend Radi us, mm
B
e
n
d
S
t
r
e
s
s
,
M
P
a
1 mm
0.7 mm
0.5 mm
0.3 mm
13
Corning Incorporated 2012
Reliability Design Diagram for Glass in Bending
hours
1050
900
750
600
450
300
150
seconds
700
600
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300
200
100
0
50
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Bend Radius, cm
B
e
n
d
S
t
r
e
s
s
,
M
P
a
0
200
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R
e
q
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t
h
,
M
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a
10 micron
25 micron
50 micron
75 micron
100 micron
125 micron
hours
seconds
125 proof
lifetime
thickness
E =70 GPa
14
Glaesemann and Gulati, Opt Engr (30) 6 1991
What is the strength of flexible glass sheets?
Corning Incorporated 2012
Measurement of Glass strength Ring-on-Ring
Ring-on-Ring test (ASTM C1499)
Maximum stress in region below inner ring on other side
Limitations: Thin glass (with deflection greater than half
thickness at failure) shows significant non-linear effects
15
Corning Incorporated 2012
Ring-on-Ring Testing and Large Deflections
16
Gulati et al., Overview of Strength Tests for LCD Substrates and Panels
Corning Incorporated 2012
Large Deflections during Ring-on-Ring Strength Test
Stress
(MPa)
Load (N)
17
Corning Incorporated 2012
Ball on Clamped Ring
0 200 400 600
0
500
1000
S
t
r
e
s
s
(
M
P
a
)
Load (N)
Stress under ball
Membrane Stress
o
mcmbunc
o
bcndng+ mcmbunc
18
Corning Incorporated 2012
Ball on Clamped Ring Contact Area
4 mm
19
Corning Incorporated 2012
0 100 200 300 400 500 600
-200
-100
0
100
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300
400
500
600
700
800
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1000
1100
1200
1300
1400
1500
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S
t
r
e
s
s
(
M
P
a
)
Load (N)
Measured Stress Under Ball
0.3mm
Maximum
Bend-Induced
Stress
20
Wrapping around
Ball
Membrane
Corning Incorporated 2012
Glass Surface Strength is Independent of Thickness
New test methods developed for flexible substrates
21
G.S. Glaesemann, et al., The Strength of Thin Fusion Drawn Glass Sheets, 11th ESG Conference 2012, Maastricht, The Netherlands
Strength, MPa
F
a
i
l
u
r
e
P
r
o
b
a
b
i
l
i
t
y
,
%
100 10000 1000
1.E-1
5.E-1
1
5
10
50
90
99
1.E-1
100 m
200 m
300 m
Strength (MPa)
F
a
i
l
u
r
e
P
r
o
b
a
b
i
l
i
t
y
(
%
)
21
Corning Incorporated 2012
Measurement of Glass strength 4 point bend
Four point bend strength (ASTM C158)
Maximum stress in region between loading points (opposite
surface)
Edges are often weaker than surface
Effecti vely tests only two bottom edges
22
Corning Incorporated 2012
Two Point Bend Concept
Upper Platen
Lower Platen
Glass Specimen
Upper Platen
Lower Platen
Glass Specimen
Bend a piece of glass between two platens
Elastic Beam Theory describes basic
behavior
Concept is not new (its been around for
decades)
Used extensively in the fiber industry
New concept: Use high speed video to
capture failure location
Upper Platen
Lower Platen
Glass Specimen
Failure Location
23
Corning Incorporated 2012
Two Point Bend Test Setup
Specimen goes here
Camera
Light Source
Mirror
Load Frame
Upper Platen
Lower Platen
Camera Rail
Screen
24
Corning Incorporated 2012
Strength, MPa
F
a
i
l
u
r
e
P
r
o
b
a
b
i
l
i
t
y
,
%
10 10000 100 1000
1. E-1
5. E-1
1
5
10
50
90
100
1. E-1
Edge Strength after Mechanical Score and Break of
100 m thick Glass
Score
side
Break
side
25
Surface failures as
suspensions
Corning Incorporated 2012
The Fracture Surface
26
Corning Incorporated 2012
Branching
Mirror Mist Hackle Branching Mirror Mist Hackle Branching
Mirror
Mist
Hackle
(points to origin)
Flaw
Origin
The Fracture Surface
27
Corning Incorporated 2012
Velocity Mist / Mist Hackle
Mist hackles occur beyond the mirror region and appear as a gray-matte
surface. These markings occur when the fracture approaches terminal velocity.
This feature is not present on low stressed breaks.
The shape of the hackle is indicative of the stress that was associated with the
break. The above sketches are the extremes - the shape of the mist region can
vary.
28
Corning Incorporated 2012
Origin
Bending Mist / Velocity Hackle
Bending Mist
Hackle
Secondary Wallner
Lines
29
Corning Incorporated 2012
540 MPa 320 MPa
Strength Determined from Mirror Radius
30
Corning Incorporated 2012
250 MPa 210 MPa
Return to
Mirror
Strength Determined from Mirror Radius
31
Corning Incorporated 2012
Glass Mechanical Reliability Key Principles
Every glass object has strength-limiting flaws
Machining, polishing
Glass chips scratching surface
Flaws potentially introduced at every handling step
Strength is not a pure, material property
Controlled by flaws
Determined by manufacturing and handling history
Statistical in nature
Strength is always a characterization of a flaw population
We never measure flawless glass
Strength is always measured after some damage has been done
Surface flaw due to contact
Edge flaw due to cutting
32
Corning Incorporated 2012
Strength Testing Flexible Glass
Match strength testing to the failure mode of interest
Failure mode 1
st
Strength testing 2
nd
Novel strength testing methods
Surface Strength Ball on Clamped Ring
Edge Strength Modified 2 point Bend
Fractography
Cause of failure
Foundational method for improving strength
33