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EI 1354-Industrial Instrumentation Lab

Expt: 01 MEASUREMENT OF FLOW IN PIPE USING ORIFICE PLATE


Aim:
To form a calibration chart for determining the water flow in the pipe using orifice plate.
Definition:
Orifice is a small opening of an cross section such as circular! triangular! rectangular!
rectangular etc.! and orifice plate is a circular plate! which has a circular sharp edged orifice at
its center through which a fluid is flowing. It is concentric with pipe. "enerall the orifice
diameter is #ept $.5 times the pipe diameter.
Prinip!e:
%hen a li&uid is flowing through an orifice plate! it increases the 'elocit of water and
thus the #inetic energ. The difference of head before the orifice plate and after orifice plate can
be calibrated to measure discharge.
De"ription:
The water is pumped to pass through orifice plate( the difference in head between
before and after the orifice is measured. The coefficient of discharge for the orifice plate can be
calculated using actual flow measurement. The calibration chart to determine the discharge for
different head difference can be formed.
App#r#t$" re%$ire&:
)top watch! measuring tape.
Form$!#e:
Theoretical discharge through the pipe!
gh
a a
a a
Q
th
*
*
*
*
1
* 1

=
%here!
+th - Theoretical discharge through pipe! m3,s
a1 - -rea of cross section of the pipe! m*
a$ - -rea of cross section of the orifice! m*
h - .ead difference between the inlet and outlet of the orifice! m of .*O
-ctual discharge through pipe!
+act / area of the tan# 0 water le'el raise in the tan#
/ lb.,t
%here!
1epartment of Instrumentation and 2ontrol Engineering 1
EI 1354-Industrial Instrumentation Lab
+act - actual discharge through pipe! m3,s
l - Length of the tan#! m ( b - breadth of the tan#! m
. - %ater le'el rise in the tan#! m! t - time ta#en for 1$cm raise of water
2o-efficient of discharge for orifice meter! cd / +act , +th
Proe&$re:
)witch on the pump 3 allow the water to flow through the pipe for flow measurement
using orifice meter test rig.
Open the #nobs for 4 - tube manometer to measure the head difference at orifice plate
in the pipe.
"raduall open the 'al'e and allow the ma5imum water flow in pipe.
6a#e the obser'ation for 'arious flow rates b graduall closing the 'al'e.
Re"$!t:
-ctual 1ischarge! +act / m3,sec
Theoretical 1ischarge. +th/ m3,sec
2o-efficient of 1ischarge! 2d /
O'"er(#tion
1iameter of the pipe! d1 / m
Orifice diameter! d$ / m
Length of the collecting tan#! l / m
7readth of the collecting tan#! b / m
T#'$!#tion:
Rot# meter M#nometer re#&in) *m+ Time t#,en for 10 ri"e of -#ter !e(e! in
o!!etor t#n,
. 1
*m+
. /
*m+
0 1 .12./ *m+
Gr#p.:
+act 's. +th
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Mo&e! #!$!#tion:
1. .ead difference at the orifice plate! h / m of .*O
*. Theoretical discharge! +th / a1 ao
)&uare root 8a1*-a$*9
3. -ctual discharge! +act / area of the tan# 0 water le'el raise in the tan#
/ lb.,t
- / d*,4
3. :rom graph!
+th / m3,s +act / m3,s
cd /+th , +act
T#'$!#r o!$mn:
For #!i'r#tion .#rt:
.ead difference at
orifice plate
h m34"T.eoreti#!
&i".#r)e
5t. m3,sDi".#r)e 5 1&6 5t. m3,s
Re"$!t:
Thus a calibration chart for determining the water flow in the pipe using Orifice
plate was formed.
7i(# 5$e"tion"
1) What are the diferent types of orifce?
Concentric orifce
Eccentric
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Segmental
Quadrant edge
2) Defne concentric orifce?
t has a circular hole in the middle and is installed in the pipe line !ith the
hole concentric to
the pipe" ts thic#ness depends upon pipe line si$e"
%) Defne eccentric?
t is installed in !ith the &ore tangential to the upper surface of the pipe' it
is used !here the
li(uid contains a relati)ely high * of dissol)ed gases"
+) Defne segmental?
ts hole diameter is ,-* of pipe diameter" t is installed !ith a cur)ed
section of the opening
Coincident !ith the lo!er surface of the pipe"
.) /ist the ad)antages of the orifce plate
0sed in !ide range of pipe si$es
0sed !ith pressure diferential de)ice"
1)aila&le in many materials
2) /ist the disad)antages of the orifce plate
3igh permanent pressure loss
4educes the use in slurry ser)ices
1ccuracy depends on the care during installation"
t has the s(uare root characteristics"
5) What is the diferent tapping of orifce?
6lange tape
7ipe tape
8enacontracta tape
Expt: 0/ C#!i'r#tion of Pre""$re G#$)e
Aim: To calibrate the gi'en pressure gauge using dead weight pressure gauge tester and
to draw the error cur'e and the periodic cur'e.
App#r#t$" re%$ire&:
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E5perimental set up
1ead weights
;ressure gauge
Form$!# Re%$ire&:
1$$

=
e Actualvalu
alue Indicatedv e ActualValu
Error Percentage
T.eor8:
1ead weight piston gauge is used for the measurement of higher stead pressures and
for chec#ing elastic diaphragms or bourdon tpe of gauge. In the practical form! it is often used
as a standard of pressure measurement. In this tpe of instrument! the force produced on the
piston of #nown area is measured directl b the weight it will support.
Con"tr$tion #n& -or,in):
It consists of a 'er accuratel machined base and finished piston! which is inserted into
a close fitting clinder. The cross sectional area of both the piston and the clinder are #nown.
-t the top of the piston is pro'ided a platform on which the standard weight of #nown
accurac can be placed. -n oil reser'oir with the chec# 'al'e at its bottom is also pro'ided. -
displacement pump on its upward stro#e can suc# the oil from the reser'oir.
:or calibration purpose! first a #nown calculated weight is placed on the platform and
the fluid pressure is applied on the other end of the piston until enough force is de'eloped to
lift the piston weight combination and the piston floats freel within the clinder between the
limit stops. The error in the dead weight tester is less than $<.
In order to reduce the friction between the piston and the clinder! the piston is
generall rotated while a reading is being ta#en. =o oil must enter the gauge when testing the
o5gen pressure gauges! because the oil 'apor together with the o5gen will produce an
e5plosi'e mi5ture. :or pressures up to 3$$ psig! o5gen gauge ma be treated with water or
air. )pecifications> ?ange> 1 to @$ #g, cm* in steps of $.* #g,cm*.
Proe&$re:
Settin) $p:
;lace the tester on the rigid table in the instrument room. 1irect ras of the sun should
be a'oided. The instrument should not be near the furnace or in a hot area. 1ust is
'er harmful to the instrument.
2lean the instrument with the soft cloth! especiall the top region of the free piston.
1epartment of Instrumentation and 2ontrol Engineering 5
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2hec# the free mo'ement of the piston b mo'ing it up and down b hand. The feel of
dust in the piston should not be there. -lso chec# free rotation of the screw pump
handle and both the 'al'es.
a. Install Le'eling screws with loc# nuts and base pads.
i. Install weight carrier on the free piston
ii. Install the screw pump handle rods with #nobs
iii. Install wheel of the release 'al'e. 8If pac#ed separatel9
i'. Install Oil reser'oir on the reser'oir bloc#
;lace the spirit le'el on the weight carrier and adAusts b means of the le'eling screws
and loc# the le'eling screws b tightening loc# nuts on to the legs. If the tester is not
mo'ed! le'eling needs to be chec#ed onl periodicall.
Oper#tion:
;our a clean mineral oil to appro5imatel two third of the capacit of the reser'oir.
a. Open release 'al'e
b. Turn screw pump handle cloc#wise full to e5pel some air from the sstem! which
will bubble out in the oil cap. Turn the handle anti cloc#wise full to draw in oil to the
instrument.
c. ?epeat cloc#wise, anticloc#wise turning of the handle a number of times until no
7ubbles appear in the oil cup! finall draw in oil.
d. ?emo'e blan#ing plug from the union connector.
e. Open the gauge 'al'e
f. Turn the screw pump cloc#wise slowl. 4ntil oil slows at the union connector.
g. 1raw in oil full and close the release 'al'e.
Te"tin):
;lace the necessar weight on the weight carrier so that sum of the pressure 'al'es
of the carrier and weights loaded is e&ual to the first reading to be ta#en.
)lowl turn screw pump cloc#wise. This will build up pressure in the circuit! which
after a few turns will show on the pressure gauge.
?otate the weights with carrier b hand to reduce the effect of friction in the free
piston. 2ontinue it until the free piston rises up. The piston can rise a BCCmore
before the internal loc# stops further mo'ement.
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Tap the gauge b the finger to eliminate the friction.
;rogressi'el load weights in the desired step on the weight carrier and ta#e
reading at each point.
-fter the ma5imum reading has been ta#en! ta#e readings for decreasing pressure at
the same points as before.
T#'$!#tion:
).=o 1ead weight 8#g,cm*9 ;ressure gauge 8#g,cm9 < Error
Mo&e! C#!$!#tion:
1$$

=
e Actualvalu
alue Indicatedv e ActualValu
Error Percentage
Mo&e! Gr#p.:
Di#)r#m:
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EI 1354-Industrial Instrumentation Lab
NEEDLEVALVE
NEEDLE
VALVE
W
MEASURING
PISTONTO
HOLDWEIGHT
HANDOPERATED
PISTON
HANDLETOAPPLY
PRESSURE
Re"$!t:
Thus the gi'en pressure gauge using dead weight pressure gauge tester was calibrated
and graph for error and linearit cur'e were drawn.
7i(# 5$e"tion"
1) What is the function of a dead !eight tester?
Dead !eight tester is used to cali&rate &ourdon gauges "t is used as a
measuring
de)ice and also as a cali&ration method"
2) What are the uses of Dead !eight 9ester?
t is used to measurement of higher steady pressures' and for chec#ing
the diaphragm
or &ourdon type of gauge"
Expt: 03 C#!i'r#tion of Temper#t$re *T.ermoo$p!e+
1epartment of Instrumentation and 2ontrol Engineering E
EI 1354-Industrial Instrumentation Lab
Aim:
To calibrate the thermocouple using thermometer and to stud the characteristics of
thermocouple
App#r#t$" Re%$ire&:
O= - O:: 2ontrol )et up
T.eor8:
The wor#ing principle of the thermocouple depends on the thermo electric effect. If
two dissimilar metals are Aoined together so as to form a closed circuit! there will be two
Aunctions where the meet each other. If one of these Aunctions is heated! then a current flows
in the circuit! which can be detected b a gal'anometer. The amount of current produces
depends on the difference in temperature between the two Aunctions and on the characteristics
of two metals. This was first obser'ed b see bec# in 1E*1 and is #nown as see bac# effect
To protect the thermocouples from harmful temperature! corrosi'e fluid! mechanical
damage to support the thermocouples or to permit entr into the pressuriFed sstem!
protecting tubes or wells are supplied. These tend to reduce the speed of response of the
thermocouple! so small mass thin wall or needle tpe installations are supplied where feasible.
1isposable tip thermocouples are supplied in furnace applications
Thermocouples are not limited to single point measurement. The can be connected in parallel
to pro'ide the a'erage temperature in a sstem. The can also be used to measure the
difference between the two temperatures. Two separate measuring instruments with proper
precautions can utiliFe a single thermocouple. 7ased on the possible combinations of metals!
there are large numbers of thermocouples a'ailable.
E/ 8T - T$9 G 8 T*- T$*9
%here
E/ thermo electric E6: in Holts
T - -bsolute temperature in hot Aunction
T$ - -bsolute temperature of cold Aunction
and are constants
C#!i'r#tion of T.ermoo$p!e:
- Thermocouple is calibrated b comparing its response with a standard thermometer
at the same temperature. The standard thermometer ma be another thermocouple a platinum
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resistance thermometer. )e'eral suitable calibration methods ha'e been de'eloped. -n optical
prometer is used to calibrate thermocouple for temperatures abo'e E$$2. In this case the
thermocouple is first placed in a furnace. The furnace is heated to a different temperature. The
response of the thermocouple is compared to the optical prometer reading.
Proe&$re:
To fin& t.e .#r#teri"ti" of T.ermoo$p!e:
2onnect the thermocouple sensor to the soc#ets in the #it mar#ed sensor
2onnect the heat source to the 5 pin soc#et pro'ided on the bac#side of the control
unit.
Insert the sensor and the thermometer through the top plate of the heat source bo5
)witch on -2 **$ H suppl to the control unit.
Jeep the miniature toggle switch in down position
-dAust the #nob of the controller to full cloc#wise direction! i.e :ull )cale -2
Holtage is applied to the heat source
?ecord the sensor output in milli 'olts along with the corresponding temperature
Tabulate the reading and plot the graph.
Temperature in 2 along 0 a5is and sensor output in milli'olts along K a5is is
drawn
To me#"$re t.e temper#t$re:
Jeep the miniature toggle switch in down position
6onitor the temperature in the digital panel meter and the temperature recorded b
the mercur thermometer.
Tabulate the readings and plot the graph.
T#'$!#r Co!$mn
).=o Indicated Halue 8L29 -ctual Halue
8L29
)ensor o,p
8mH9
< Error
1epartment of Instrumentation and 2ontrol Engineering 1$
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< Error / 8-ctual 'alue M Indicated Halue9 , -ctual Halue
Di#)r#m:
M E T A L A
M E T A L B
H O T
J U N C T I O N
C O L D
J U N C T I O N
T R A N S M I T T E R D I S P L A Y
M O T O R
H E A T E R
T H E R M O C O U P L E
Mo&e! )r#p.:
1epartment of Instrumentation and 2ontrol Engineering 11
EI 1354-Industrial Instrumentation Lab
Re"$!t:
Thus! the temperature of the hot Aunction was measured b using thermocouple and the
performance characteristics were drawn.
7i(# 5$e"tion"
19 %hat is Thermal 2oefficient of ?esistanceN
The change in resistance of a semiconductor per unit change in temperature o'er a
specific range of temperature.
*9 %hat is Thermal 2onducti'itN
The abilit of a material to conduct heat in the form of thermal energ.
39 %hat is a ThermistorN
- temperature-sensing element composed of sintered semiconductor material which
e5hibits a large change in resistance proportional to a small change in temperature.
thermistors usuall ha'e negati'e temperature coefficients.
49 %hat is a ThermocoupleN
The Aunction of two dissimilar metals which has a 'oltage output proportional to the
difference in temperature between the hot Aunction and the lead wires 8cold :unction)
.) Defne temperature?
9he temperature of a su&stance is a measure of hotness or coldness of
that su&stance"
2) Write some methods of measurement of temperature?
E;pansion 9hermometer"
6illed system 9hermometer"
Electrical 9hermometer"
7yrometer"
Expt: 09 Tor%$e Me#"$rement
Aim: To determine the tor&ue de'eloped in the circular shaft
App#r#t$" Re%$ire&:
1igital tor&ue indicator
?ectangular bo5
%eights
1epartment of Instrumentation and 2ontrol Engineering 1*
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Form$!#:
m N d f T
s
=
3
1D

%here
T- Tor&ue of the shaft =- m
:s-shear stress =,m*
d- 1iameter of the shaft 8m9

*
, m N
d l
w g
f
s

=
%here g - -cceleration due to gra'it 8I.Em,sec*9
d - 1iameter of the shaft 85.3@51$-*m9
l - Length of the shaft 8I.5E 5 1$-*m9
Proe&$re:
The rotor shaft arrangement is connected to the digital tor&ue indicator
-ppl a #nown weight of #ilogram to cantile'er beam.
The load is increased in steps and corresponding angle of twist and tor&ue are
calculated.
7 using the formula! tor&ue is calculated.
Indicated tor&ue and calculated tor&ue are tabulated and the errors are found.
the graphs are drawn between #+ %eight and tor&ue ':%eight and deflection
Mo&e! C#!$!#tion:
rved TorqueObse
ulated TorqueCalc
tionfactor Multilica
d l
w g
s
!incef
d
l
gw
d
s
f T
=

=
= =
*
1D
3
1D

T#'$!#r o!$mn:
S:No App!ie&
Wei).t
*;)+
Tor%$e
o'"er(e&
*;)2m+
An)!e of
T-i"t*<+
Tor%$e
*Nm+
M$!tip!i#tion
F#tor
Mo&e! Gr#p.:
1epartment of Instrumentation and 2ontrol Engineering 13
EI 1354-Industrial Instrumentation Lab
Re"$!t: Thus the tor&ue was de'eloped in the circular shaft.
7i(# 5$e"tion"
1) Defne tor(ue"
9or(ue is defned as the force !hich tends to change the linear motion
or rotation
of a &ody"
2) What is the other name for inline stationary tor(ue sensor?
4elati)e regular t!ist tor(ue sensor
%) What are the types of tor(ue transducer?
i) nline rotating tor(ue sensor ii) nline stationary tor(ue sensor
iii) <ptical tor(ue sensor i)) 7ro;imity tor(ue sensor
+" Write the relationship &et!een tor(ue and force"
9 = 6 " D
!here 9 >? 9or(ue ' 6 >? 6orce D >? 7erpendicular distance
&et!een the a;is of rotation of the line of action of the force
Expt: 0= 7i"o"it8 Me#"$rement
Aim:
To determine #inematic 'iscosit of gi'en sample at desired temperature. To put the
?elation between #inematic 'iscosit and temperature.
App#r#t$" re%$ire&:
?ed wood 'iscometer set up
Thermometer
Oil @5 ml
:las# 5$ 22
)top watch
T.eor8:
1epartment of Instrumentation and 2ontrol Engineering 14
EI 1354-Industrial Instrumentation Lab
Jinematic 'iscosit is ratio between absolute 'iscosit and densit of the fluid.
Hiscosit is the measure of flow abilit at the definite temperature. Two parallel plates
separated b an oil film of thic#ness as illustrate understand the concept. The lowest plate is
stationar where as the upper plate is mo'ing with 'elocit ' as it is being pushed b a force 8f9
is shown. 1ue to 'iscosit of oil adheres to both surfaces. The 'elocit of laer of fluid is in
contact with the lower plate is Fero at the 'elocit O'C. The conse&uence is linearl 'aring
'elocit profile whose slope is ',g.
The absolute 'iscosit of the oil can be represent mathematicall b
vig

=
le ocit"rofi sloeofvel
oil !hearstres sin
=
and the pneumatic 'iscosit is gi'en b
sec9 , 8
*
cm v = =

Form$!#: Jinematic 'iscosit


t
t v
1@*
D . * =
2entisto#es
%here t / time ta#en for oil to fill 5$ 22
De"ription:
The redwood 'iscometer consists of a clindrical co'er with the safe set the center of
its base can be closed b a ball 'al'e resting in hemispherical cabins forms on it. - manometer
holder is pro'ided for #eeping thermometer. The cup is placed in the bath! which can be heated
electricall. - stirrer is pro'ided to maintain uniform temperature.
Proe&$re:
Ensure the apparatus and the flas#s are maintained clean. 7efore starting! place the
5$22 measuring flas# under the set to permit the flow of steam of oil. %hen necessar insert
the two thermometers! one in the bath and the other in the oil. 2are should be ta#en to see that
the bulb of the thermometer doesnCt ta#e the metal surface. :ill the oil cup and heat the water
bath. )tirring is done to ensure uniform heat distribution when desired temperature is obtained.
- stopwatch is started simultaneousl so as to note down the time ta#en b the oil for 5$ 22
1epartment of Instrumentation and 2ontrol Engineering 15
EI 1354-Industrial Instrumentation Lab
:las#. The e5periment is repeated for 'arious temperatures. The readings are tabulated and the
#inematic 'iscosit is calculated. The re&uired graph is drawn and the characteristics are noted.
T#'$!#r o!$mn:
S:No Temper#t$re8L29 Time*Se+ 7i"o"it8*C"+
Mo&e! C#!$!#tion:
Form$!#:
t
t v
1@*
D . * =
1epartment of Instrumentation and 2ontrol Engineering 1D
EI 1354-Industrial Instrumentation Lab
T
1
T H E R M O C O U P L E
W A T E R
5 0 C C
B E A K E R
S T I R R E R
Mo&e! )r#p.:
Re"$!t:
Thus the gi'en #inematic 'iscosit of gi'en sample oil is determined and the graph
between 'iscosit and temperature is plotted
7i(# 5$e"tion"
1epartment of Instrumentation and 2ontrol Engineering 1@
EI 1354-Industrial Instrumentation Lab
1) Defne )iscosity"
t is the property of the @uid !hich gi)es the resistance to the @o!"
2) What are the units of density?
AgBm% or gmBlitre or gmBml
7ascal or 1CSD>2 or 1#gm>1 or poise
%) What are the diferent types of )iscometer?
Say &olt )iscometer
4ota meter type
Consistency meters"
+) E;plain the principle of say &olt )iscometer"
1s the )iscosity of the @uid )aries' the @o! rate and hence time ta#en to
drain the @uid
through the capillary tu&e )aries" 9he time indicates the )iscosity and is
denoted &y
say &olt num&er"
HI)2O)ITK
:luid propert! which influences the fluid motion to a great e5tent
7 #nowing the 'iscosit of a fluid! the fluid flow analsis can be carried out
:inds applications especiall in lubrication and combustion phenomena
2haracteristic of a fluid that has an important impact on siFing e&uipment and pipes
- measure of fluid resistance to flow when pressure is applied to it.
- measure of the fluidit of the li&uid or gas
Temperature dependent
Jnowledge of 'iscosit is necessar for the estimation of the re&uired temperatures for
storage! pumping and inAection.
Expt: > ECG An#!8?er
1epartment of Instrumentation and 2ontrol Engineering 1E
EI 1354-Industrial Instrumentation Lab
Aim:
To trace the E2" wa'eform and measure the 'arious time inter'al and amplitude of
E2" wa'eform to ma#e a diagnosis.
App#r#t$" Re%$ire&:
1. E2" setup bo5
*. 2ard Aell! cotton
3. 2?O
4. "raph
T.eor8:
The maAor tas# facing an e'aluator is that of presenting the reference signals to the
de'ice under test! and collecting annotation files from the de'ice. The details of this tas# will
'ar for each de'ice. - second tas# that of obtaining reference heart rate measurements should
be a much simpler Aob. Once all of this information has been gathered! the remaining wor#
re&uired -- that of comparing the de'icePs analsis against the QQgold standardPP -- can be
performed automaticall.
T#'$!#r o!$mn:
N#me of t.e -#(e Amp!it$&e D$r#tion
;
?
T
4
)T
Proe&$re:
2onnect the leads appropriatel
Trace the wa'eform
:ind the time inter'al of ;+!+?) comple5!)T inter'al 3 T inter'al
6easure the amplitude of ; wa'e!T %a'es inter'al !4 wa'e
Re"$!t:
Thus the E2" wa'e form and the 'arious time inter'als! amplitude of E2" wa'eform were
measured
Expt : 0@ U727i"i'!e "petrop.otometer
Aim:
To determine the percentage absorption and percentage transmission of solution based
on 7eerCs LambertCs law.
App#r#t$" Re%$ire&:
1epartment of Instrumentation and 2ontrol Engineering 1I
EI 1354-Industrial Instrumentation Lab
)pectrophotometer
%ater of 1$mm ;ath length
)olution
Prinip!e of oper#tion:
This spectrometer wor#s on the principle based on beer LambertCs law. %hen light falls
upon homogenous medium and the remainder is transmitted if the intensit of the incident light
is e5pressed b Io that of the absorbed light b Ia! that of the transmitted light b It ! and that
of the reflected light b Ir .
Then
Io / Ia G It G Ir
It is usuall eliminated b the uses of comparison cells! as it is mere 4 < onl.
Io / Ia G Ir
-s per LambertCs law! when monochromatic light passes through a transparent medium of
thic#ness I! It and # is constant for the wa'elength and the absorbing medium.
It / Ioe-#
%here Io is the intensit of the incident light falling upon an absorbing medium of thic#ness I!
It is the intensit of the transmitted light and # is the constant for the wa'elength and the
absorbing medium used.
It / Io 1$-$.4343JR / Io1$-JR
%here # / # , *.3$*D! and - is usuall termed -bsorption 2oefficient. "enerall described as
the reciprocal of the thic#ness re&uired to reduce the light to 1,1$ of its intensit. The ratio of
It , Io is the fraction of the incident light transmitted b the thic#ness I of the medium and
termed as transmittance. -bsorbance of the medium 8 called the optical densit 9 is gi'en b
- / Log 8Io , It 9
T.eor8:
The mainl comprises of light source of monochromator! ;hotodiode! processing electronics
and read out. Light from the tungsten filament halogen lamp is focused on to the entrance slit
b condensating optics. The light from the slit is collimated 'arious wa'elength are scanned b
rotating the grating mountings. The monochromatic light isolated b e5it slit! passes through
blan# standard 8or9 sample 8held in a cu'ette9 and the transmitted light falls on the photo diode.
1epartment of Instrumentation and 2ontrol Engineering *$
EI 1354-Industrial Instrumentation Lab
The output signal from the photo diode is amplified processed read to percentage transmit 8<9
absorbance 8-bs9 and concentration as selected.
Proe&$re:
C#!i'r#tion:
Thus the O= - O:: switch to O= position
Jeep the < T! 2oncentration selector switch to < T position. -dAust nm
control to read the wa'elength at which the test is desired to be carried out at
the cursor in the nm window.
)lide open the lid of the sample compartment. Turn the filter sliding control to
get the appropriate filter for the wa'elength at which the test is desired to be
carried out into the optical path for below 3I5nm filter position for abo'e 3I5
nm and below D$ nm.
Turn the coarse and fine controls at their ma5imum and adAust $< control to get
$.$ displas on the read out with filter position in 1.
;ull the cu'ette position control out to perpendicular position.
-dAust coarse 1$$<T control to read appro5imatel 1$$ on the read out.
-dAust fine 1$$< T control to read precisel 1$$ on the read out.
;ush the cu'ette position 2ontrol I= to 1 position.
;ull the cu'ette position control O4T to * position. ;erform the operation of @
3 E to set precisel 1$$ on the read out.
;ush the cu'ette position control In to 1 position and chec# for $.$$ on the read
out.
Mo&e! Gr#p.:
1epartment of Instrumentation and 2ontrol Engineering *1
EI 1354-Industrial Instrumentation Lab
T#'$!#tion:
).=o 2oncentration 8=9 -bsorbance 8<9
Re"$!t:
Thus the concentration of the gi'en test solution was determined.
Expt: 0A p0 meter "t#n&#r&i?#tion #n& me#"$rement of p0 (#!$e" of
"o!$tion"
Aim:
To prepare 7uffer and standardiFation of p. meter
To measure the p. 'alues of the solutions
App#r#t$" re%$ire&:
p. meter with glass electrode
)tandard calomel electrode
7uffer solution of #nown p. 4 and I
1epartment of Instrumentation and 2ontrol Engineering **
EI 1354-Industrial Instrumentation Lab
1$$ml bea#er
6icro burette
.2l! =aO. )olution
Titration flas#
;ipette
T.eor8:
-ll p. meters ha'e pro'isions for standardiFation the glass electrode in the buffer
solution of #nown p.. This is necessar because different electrodes ha'e different asmmetr
potentials. Once the adAustments has been made! so that meter registers the #nown p. of the
buffer solution! the instrument gi'es the p. of the other solution without an calculation
6easurement of p. is also emploed to monitor the course of acid base titrations. The
p. 'alues of the solution at different stages of acid base neutraliFation are determined and are
plotted against the 'olumes of the acid al#ali added. On adding a base to the acid! the p. rises
slowl in the initial stages.
+
=
#
#
1
log
then it changes rapidl at the end point. Then it flattens out. The end point of the titrations can
be detected where the p. ranges more rapidl. .owe'er the shape of the infle5ion point 8i.e.
where the p. ranges abruptl9 an smmetr of the cur'e on its two sides! depends on the
ionisabilit of the acid and the acidit of the base.
Proe&$re:
St#n&#r&i?#tion of t.e in"tr$ment:
)witch on the instrument! wait for 1$ -15 mts! so that it gets warmed up.
;repare the buffer solution ha'ing p. / 4 and p. / I. These can also be
prepared in the laborator. $.$5 6 solution potassium hdrogen thalate gates a
buffer solution of p. 4.$$E at *5S2! $.$16 solution of bora5 gi'es a buffer
solution of p. I.1E at *5S2.
%ash the calomel and glass electrode with distilled water.
Ta#e the buffer solution 8p. / 49 in a clean glass and a polthene bea#er. Lower
the electrodes so that the are immersed in the solution to a depth of about one
inch.
1epartment of Instrumentation and 2ontrol Engineering *3
EI 1354-Industrial Instrumentation Lab
6easure the temperature of the solution b a thermometer and set temperature
compensate control to this 'alue.
)et the selector switch to @ p. e5actl b a set Fero control.
;ut bac# the selector to Fero control. %ash the electrodes with distilled water
and standardiFe the p. meter b using the buffer solution of p. /I.
)ame procedures described abo'e are followed e5cept now the selector switch
is put to a p. range of @ - 14.
Proe&$re for p0 metri titr#tion":
)tandardiFe the p. meter as described abo'e
2lean the electrodes b distilled water and wipe them with tissue paper or filter
paper.
Ta#e *5 ml of .2l solution in a 1$$ ml bea#er and immerse the electrodes
)et up the burette containing standard =aO. solution
6easure the temperature of the solution and set the temperature
compensate to this 'alue.
;ut the selector to the e5pected p. range. This reading shown on the scale
of the meter is the p. 'alue of the un#nown solution.
-dd =aO. generall from the burette $.5 ml at a time. =ote the corresponding
'alue from the meter. =ear the end point and 'er small of =aO. as
possible because the change in p. will be 'er much appreciable because
when the acid is neutraliFed! further addition of such small amount as $.$1
ml rises the p. to about I to 1$.
;ut the selector to the Fero position after p. measurement and before remo'ing
the electrodes from solution! lea'e the selector in the Fero position when not
in use.
;lot the graph between p. and 'olume of =aO. re&uired for the complete
neutraliFation of .2l
1epartment of Instrumentation and 2ontrol Engineering *4
EI 1354-Industrial Instrumentation Lab
Re"$!t:
Thus the buffer is preferred and p. 'alue of the solution is measured.
Expt: 0B Le(e! Me#"$rement $"in) Differenti#! Pre""$re Tr#n"mitter
Aim:
To measure the le'el using differential pressure transmitter
App#r#t$" Re%$ire&:
E5perimental set up 1;T
-mmeter 8$- *$ m-9
T.eor8:
Le'el measurement trainer is an e5clusi'e unit for measuring the le'el b using
differential pressure transmitter 81;T9 i.e. the le'el of the tan# is measured b determining the
1epartment of Instrumentation and 2ontrol Engineering *5
EI 1354-Industrial Instrumentation Lab
pressure at the bottom of the tan#. ;ressure at the bottom of the tan# depends on three
parameters namel! fluid! fluid densit! acceleration due to gra'it. %here ; - pressure at the
bottom
. - height of the fluid from the sensor
T - densit of the fluidC
g - acceleration due to gra'it
;ressure at the bottom of the tan# is the function of height. .ence from the pressure at the
bottom the le'el can be calculated.
To measure the different in pressure! 1;T is used as the name indicates it gi'es the
current output depending upon the difference in pressure. 7asicall 1;T is compound of
mechanical arrangements li#e diaphragm or bellow to determine the differential pressure. The
mechanical position are then con'erted to electrical &uantit thereb output is proportional to
the differential pressure. In smart 1;Ts micro controller is used for accurate and reliable
measurements
Wor,in):
The water is pumped from the reser'oir to the process tan#. The le'el of the water in
the process tan# has its own pressure at the bottom. The high end of 1;T is connected to the
bottom of the tan# and the lower end is #ept open to the atmosphere. .ence the 1;T output
depends on the absolute pressure at the bottom of the tan#. The 1;T is calibrated in such a
wa that for the le'el of Fero mm the 1;T output is 4m- 2urrent and for le'el of 5$$mm! The
1;T output is *$m- 2urrent. The 1;T output can be measured b connecting ammeter in
series 3 U displa shows. The le'el of process tan# is directl in mm.
Proe&$re:
Ensure the a'ailabilit of water is reser'oir tan#
Initiall .H* is full closed and .H1 is full opened. 2onnect the multimeter across
the 1;T output
)witch On the power and set the speed of pup! b adAusting the control #nob
8Hariable )peed9
%hen the water has reached sufficient height switch Off the pump
=ote the 'alue of current and le'el in displa
?educe the le'el b adAusting the hand 'al'e 8.H*9
?epeat step 5 and D and tabulate the result
;lot le'el Hs current output
1epartment of Instrumentation and 2ontrol Engineering *D
EI 1354-Industrial Instrumentation Lab
2alculate instrument Error
T#'$!#r Co!$mn:
).=o -ctual le'el
8mm9
82urrent9
)ensor
Output8m-9
Indicated
Le'el 8mm9
< Error
Mo&e! Gr#p.:
1epartment of Instrumentation and 2ontrol Engineering *@
EI 1354-Industrial Instrumentation Lab
Re"$!t:
Thus the le'el of the tan# was measured using 1ifferential pressure transmitter.
7i(# 5$e"tion"
1epartment of Instrumentation and 2ontrol Engineering *E
EI 1354-Industrial Instrumentation Lab
1) What is 4ota meter?
t is an e;ample of )aria&le area @o! meter" When @uid enters lopped
mo)es from the
&ottom to top" Distance is proportional to the @o! rate"
2) /ist the direct le)el measuring methods"
6loat type le)el indicator
Displacer type detector
Sight glass type"
%)) /ist the indirect le)el measuring methods"
3ydrostatic measurement
1ir purge system
Eoiler drum system"
+) What are the ad)antages of sight glass le)el instrument?
Direct reading is possi&le"
Special designs are a)aila&le"
Flass less de)ices is a)aila&le in numerous material for corrosion
resistance"
.) What are the ad)antages of displacer le)el instrument?
3igh accuracy
4elia&le to clean li(uids
Dounted internally or e;ternally
1dapta&le to li(uid interface measurement"
1epartment of Instrumentation and 2ontrol Engineering *I
EI 1354-Industrial Instrumentation Lab
Expt:10 Me#"$rement of p$!"e r#te4re"pir#tion r#te:
Aim:
To measure the pulse rate of a human bod
App#r#t$" Re%$ire&:
-utomatic wrist blood pressure monitor #it
T.eor8:
The rate at which our heart beats. Kour pulse is usuall called our heart rate! which is
the number of times our heart beats each minute 8bpm9. .owe'er! the rhthm and strength of
the heartbeat can also be noted! as well as whether the blood 'essel feels hard or soft. 2hanges
in our heart rate or rhthm! a wea# pulse! or a hard blood 'essel ma be caused b heart
disease or another problem.-s our heart pumps blood through our bod! ou can feel a
pulsing in some of the blood 'essels close to the s#inPs surface! such as our wrist! nec#! or
upper arm. 2ounting our pulse rate is a simple wa to find out how fast our heart is beating.
Reor&e& '!oo& pre""$re 1 "8"to!i 4 Di#"to!i
Norm#! '!oo& pre""$re 1 1/04A0 mm0)
Aepte& norm#! #&$!t r#n)e:
C#te)or8 S8"to!i Di#"to!i Reommen&e& f!o- $p
=ormal V1*$ VE$ ?echec# in * rs
.igh normal 1*$-13I E$-EI ?echec# in 1 r
)tage 1 14$-15I I$-II 2onfirm with in * wee#s
)tage * 1D$-1@I 1$$-1$I ?efer for additional care
)tage 3 W1E$ W11$ ?efer for additional care
immediatel
T#'$!#r o!$mn:
A)e C#te)or8 S8"to!i
pre""$re
Di#"to!i
pre""$re
P$!"e r#te Con&ition
Proe&$re:
;lace the wrist cuff on the left wrist with our thumb pointing up
.old the bottom part of the cuff and wrap it around the wrist pulling
Ta#e the readinga9sstolic b9 diastolic pressure of different patient are tabulated
Tabulate the pulse rate of the patient
1epartment of Instrumentation and 2ontrol Engineering 3$
EI 1354-Industrial Instrumentation Lab
Re"$!t:
Thus the pulse rate and respirator rate was measured
Expt: 1/ Con&$ti(it8 Te"t
Aim:
To measure the conducti'it of the test solution.
App#r#t$" Re%$ire&:
2onducti'it bridge
Test )olutions
1epartment of Instrumentation and 2ontrol Engineering 31
EI 1354-Industrial Instrumentation Lab
;ower )uppl
Prinip!e:
In conductometric titration! the changes in e&ui'alent conductance of an electrolte b
the addition of another electrolte 8titrant9 are measure. The addition of =aO. to .2l acid
causes the change in the e&ui'alent conductance of the acid.
-cid solution is pipetted out into a bea#er of =aO. solution of #nown strength
is added from the burette. The changes in the conductance of acid after each addition of 1ml of
=aO. is measured.
The 'alues of conductance corresponding to the 'arious increment of the titrant are
plotted against the 'olume of the titrant. The plot consists of two lines! which interest at a
particular point! #nown as the e&ui'alent point.
:rom the 'alue! the amount of acid present in the gi'en solution is calculated.
;rocedure>
The conducti'it meter is warmed up to 1$ mts. The gi'en .2l acid solution is made
up to 1$$ml in the standard measuring flas#. *$ml of the made up acid solution is pipetted out
into the clean bea#er and 1$$ml of distilled water is also added to enable. The conducti'it cell
to immerse well in the cell. The solution in the bea#er b a magnetic stirrer or glass rod.
The burette is filled with standard sodium hdro5ide solution b following usual
precautions and incorporated into the bea#er containing the .2L acid.
The conducti'it cell in the bea#er containing the acid. The initial conductance of the
acid is noted. =aO. solution from the burette is added at the rate of 1 ml at a time! stirred for
3$ sec and conductance is measured. The 'alues of conductance are getting decreased after
each addition of titrant. -fter reaching the e&ui'alent point! the conductance 'alue gets
increased. =ear the e&ui'alent point! =aO. solution is added at the rate of $.1 ml at a time!
stirred for 3$ sec and the 'olume of the solution added and the corresponding conductance
'alues are noted. -dditional =aO. solution is continued until the e&ui'alent point is crossed b
at least 1 ml. - graph is drawn b ta#ing conductance in ordinate K a5is and the 'olume of the
burette solution is obcissa 80 a5is. - smooth cur'e is drawn b lin#ing the points. The point of
intersection of that is noted and plotted to the 'olume scale which is the end point of the
titration. :rom this 'alue the amount of the sodium hdro5ide present in the gi'en solution is
calculated.
T#'$!#tion:
1epartment of Instrumentation and 2ontrol Engineering 3*
EI 1354-Industrial Instrumentation Lab
).=o -mount of =aO. 8ml9 2onducti'it of )olution
8Xmho 5 1$49
Mo&e! )r#p.:
Re"$!t:
Thus the conducti'it of the test solution was measured.
1epartment of Instrumentation and 2ontrol Engineering 33

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