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INFORME TCNICO
De:
Mauricio Cruz
Divisin Tcnica
A:
Fecha:
19 de enero de 2015
Ref.:
Mantenimiento de un Titulador
Estimada Licenciada
Por intermedio del presente informe, ponemos en su conocimiento lo siguiente acerca del equipo.
Equipo:
Marca:
Modelo:
Serie:
Desmontaje
Limpieza
Ajustes
Ajustes de mtodo
Calibracin
Prueba de funcionamiento
Nmero de lote:
HC380818
Nmero de producto:
1.88055
Contenido de agua:
Incertidumbre:
Fabricante:
MERCK
Solvente:
Cloroformo, N-Hexano
Reactivo:
Maquinaria y Materia Prima para la Industria * Reactivos * Material de Laboratorio * Instrumentos de Ingeniera
Datos obtenidos:
n PESO g
% de Contenido de Agua
1 1.0299
0.002%
2 1.0502
0.002%
3 1.0234
0.002%
4 1.0862
0.002%
5 1.0465
0.002%
0.002 %
0.00 %
srel.
0.00 %
Estado actual: Actualmente el equipo se encuentra funcionando normalmente estando todos sus
parmetros dentro de lo descrito por el fabricante para este modelo de equipo.
Sin otro particular me despido con saludos cordiales.
Atentamente,
Mauricio Cruz
DIVISIN TCNICA
CORIMEX LTDA.
OFICINA CENTRAL
Calle Montevideo 130
Telf.: 2440330 (Piloto)
Fax: (591-2) 2440230
jcluque@corimex.com
Certified reference materiel for coulometric water determination acc. to Karl Fischer.
Method of analysis
For certification the water content was determined acc. to ISO 760 with the Karl Fischer method by
means of a coulometer using a cell with diaphragm.
Water content:
0.0020 % H2O
Measurement uncertainty:
Equivalent to the expanded measurement uncertainty with coverage factor k = 2 for 95% coverage
probability.
Traceability
This reference material is directly traceable to standard reference material SRM 2890 from NIST,
National Institute of Standards and Technology, Gaithersburg, USA.
Application
Water standard oil (15-30 ppm) is intended for use as a reference material for checking the accuracy of
Karl Fischer equipment acc. to ISO 9001. It can also be used to check measuring results.
Instructions for correct use
1. Open ampoule at the marked point of break.
2. Rinse a glass or plastic syringe 1-2 times with about 1 ml of standard solution.
3. Draw up entire ampoule content in the rinsed syringe.
4. Weigh the filled syringe before injection.
5. Inject about 1-2 ml of standard solution into titration cell and start titration.
6. Determine exact standard solution weight by reweighing the syringe after injection.
7. Repeat determination. The content of one ampoule is sufficient for 3-4 determinations.
Important: Open the ampoule only directly prior to starting of measurement. Solvent in the opened
ampoule can absorb moisture and distort results.
Date of release:
2013/01/17
2016/01/31