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On: 30 January 2015, At: 22:01
Publisher: Taylor & Francis
Informa Ltd Registered in England and Wales Registered Number: 1072954
Registered office: Mortimer House, 37-41 Mortimer Street, London W1T 3JH, UK
To cite this article: Virgil A. Marple , Kenneth L. Rubow & Steven M. Behm (1991) A
Microorifice Uniform Deposit Impactor (MOUDI): Description, Calibration, and Use, Aerosol
Science and Technology, 14:4, 434-446, DOI: 10.1080/02786829108959504
To link to this article: http://dx.doi.org/10.1080/02786829108959504
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INTRODUCTION
435
FEATURES OF MOUDI
where
p, =particle density
C = slip correction
V , =average air velocity at the nozzle
exit = q / a ( ~ / 2 ) ~
D, = particle diameter
p = air viscosity
W = nozzle diameter
q =volumetric flow rate through the
nozzle
The Stokes number is a dimensionless parameter that can be used to predict whether
a particle will impact on an impaction plate
of a stage or will follow the air streamlines
out of the impaction region and remain airborne.
It is common practice to use d??? as a
dimensionless particle size and to define
as the value of v%
corresponding
to D,,,, which is the value of D, collected
with 50% efficiency. Thus
a,
Uniform Deposit
The uniform deposit feature of the MOUDI
was originally incorporated to facilitate the
elemental composition determination of the
deposits by X-ray fluorescence analysis
(Dzubay and Rickel, 1978). The uniform
deposit was achieved by using multiple nozzles at each stage and rotating the impaction
plate beneath the nozzles (Marple et al.,
1981). By placing the nozzles at specific
distances from the center of rotation, a uniform deposit was obtained upon the rotating
impaction plate.
Marple et al.
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IMPACTION PLATE
SUBSTRATE CLAMPING
RING
&POLE MAGNETS
NOZZLE PLATE
DOUBLE O-RING SEAL
.TEFLON
GASKET
STAGE BODY
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i
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are easily analyzed by a variety of techniques. However, these foils and filters are
very difficult to handle in the field because
they are thin and lightweight. Therefore, the
MOUDI has removable impaction plates
onto which the foil or filter substrates can be
attached before a run, placed in the MOUDI
for the run, and then removed after a run
and taken back to the laboratory for disassembly and removal of the substrates.
Transport covers with O-ring seals have been
designed for the impaction plates to keep the
substrates and deposits free of contamination
during transportation. Several sets of impaction plates can be used with one MOUDI
with pauses in MOUDI operation only long
enough to remove and replace the impaction
plates.
DESCRIPTION OF THE MOUDI
The MOUDI consists of two basic assemblies. One is the cascade impactor and the
other is the rotator. Figure 2 shows the
cascade impactor in the rotator. Gears on
Marple et al.
Nominal
cut-pointa (pm)
As calibrated
cut-pointa (pm)
Nozzle
diameter (cm)
Number of
nozzles
S/w
PIP:
Nozzle
Reynolds number
Inlet
1
2
3
4
5
6
7
8
9
10
'Based on flow rate of 30 L/min at standard atmospheric temperature and pressure.
b~ = jet-to-plate distance; W = nozzle diameter.
'P =>bsolGe pressure at stage exit with all upstream stages present; Po = pressure at MOUDI inlet
439
when sampling solid particles with an impactor. It is common practice to reduce particle bounce by coating the substrates with
an oil or light grease to form a sticky surface. If grease is used on MOUDI impaction
plates, it is possible to collect up to 3 mg of
solid particles on each stage without overloading the substrates.
The easiest method for applying oil to the
substrates is to spray the oil from an aerosol
can or small airbrush using a mask to protect the edges of the substrate. The mask is a
thin plastic sheet (overhead transparency
film) with either a 2.86- or 3.71-cm diameter hole for the 37- and 47-mm substrate,
respectively. The mask is placed over the
substrate such that the hole is concentric
with the center of the substrate. The oil,
such as No. 11025 silicon spray (ClingSurface Co., Inc., Angola, NY) is then
sprayed onto the substrate. After the oil has
been applied, it is necessary to bake the
substrates in an oven at 65C for 90 min.
The amount 'of silicone oil to be applied to
the substrates is dependent on the expected
amount of material to be collected. Coating
amounts of 0.25, 0.5, and 1.0 mg/cm2 (after
oven drying) have been used with dust mass
loadings of typically 0.2, 0.5, and 3.0 mg,
respectively.
AFTER-FILTER
The MOUDI uses a 37-mm diameter afterfilter. The choice of the filter material is
primarily dictated by the type of analysis
performed. For mass distribution deterrninations we use Gelman Teflo type R2PJ037
membrane filters or glass fiber filters.
It is also important that the filter material
have low pressure drop to minimize pump
size since the pressure drop through the
impactor and, therefore, the pump sue, will
be dictated by the after-filter and the smallest cut-size of the impactor. For example,
air at a flow rate of 30 L/min can be drawn
through the MOUDI with a 114-hp carbon
vane pump (model 0523-101G-G18DX, Gast
Marple et al.
DILUTION
AIR
ABSOLUTE
AEROSOL
GENERATOR
ELECTROSTATIC
CLASSIFIER
FILTER
NEUTRALIZER
MPACTOR
BALL\
VALVES
ELECTRICAL
AEROSOL
DETECTOR
441
Marple et al.
Aerodynamic
Particle Diameter, pm
Interstage Losses
Interstage losses within the MOUDI, as
shown in Figure 6, were determined using
monodisperse liquid and solid aerosols and
techniques similar to those used in the stage
collection efficiency calibration. A silicone
oil was applied to the impaction substrate
when solid particles were used. Loss determinations were measured by passing particles through the MOUDI and determining
where the particles were collected above the
stage at which the particles were expected to
be removed by normal impaction. Because
of the rather complicated flow between the
stages, particle losses are difficult to predict.
They are primarily caused by inertial deposition as the flow turns, exiting one stage and
443
Liquid Particles
I F - ' - - -
Solid Particles
Staae Number
-o
Q,
c.
L
40
10
+I
Stage
cut-points
Inlet
minutes). These data indicate a bimodal distribution with the lower and upper modes
consisting of diesel exhaust particles and
coal and rock dust, respectively.
SUMMARY
Marple et al.
445
ranged from sampling aerosols in the pristine atmospheres of the southwestern United
States to the industrial atmosphere in coal
mines.
This work was supported by the Department of Energy,
Contract No. DE-FG22-83PC61255, Electric Power Research Institute, Contract No. 10415, and the U.S. Department of Interior's Mineral Institutes program administrator by the Bureau of Mines through the Generic Mineral
Technology Center for Respirable Dust under allotment
grant no. G1135142.
REFERENCES
Dzubay, T. G., and Rickel, D. G. (1978). Electron
Microscopy and X-Ray Applications (P. A. Russell
and A. E. Hutchings, eds.). Ann Arbor Science, Ann
Arbor, Mich., pp. 3-20.
Marple et al.