Escolar Documentos
Profissional Documentos
Cultura Documentos
& Design
Materials and Design 27 (2006) 566575
www.elsevier.com/locate/matdes
a,*
Department of Production Engineering, National Institute of Technology, Tiruchirappalli 620 015, Tamilnadu, India
Department of Mechanical Engineering, J.J. College of Engineering and Technology, Tiruchirappalli 620 009, Tamilnadu, India
c
Department of Metallurgical Engineering, National Institute of Technology, Tiruchirappalli 620 015, Tamilnadu, India
Received 16 June 2004; accepted 1 December 2004
Available online 3 February 2005
Abstract
Workability is concerned with the extent to which a material can be deformed in a specic metalworking process without the
initiation of cracks. The ductile fracture of components is the most common mode of cracks in any metalworking processes. Workability is the complex technological concept, depends upon the ductility of the material and the details of the process parameters. An
experimental research work was preformed for the understanding of the working behaviour of AlAl2O3 composite under various
stress state conditions, namely uniaxial, plane and triaxial stress states. Upsetting of AlAl2O3 powder metallurgy compacts with
various aspect ratios and initial preform densities were carried out and the working behaviour of the powder compacts at various
state conditions was computed. The curves plotted for dierent components such as axial strain vs. formability stress index, relative
density vs. axial strain, fracture strain vs. formability stress index and stress ratio parameters vs. axial strain were analyzed, using the
true strains induced during upsetting with the consideration of bulging eect.
2005 Elsevier Ltd. All rights reserved.
Keywords: Upsetting; Workability; Triaxial stress formability stress index; Powder metallurgy and relative density
1. Introduction
Powder metallurgy (P/M) is a highly developed method of manufacturing precision metal parts. Over the last
seven decades, the technology has matured from making
self-lubricating bearings for autos to complex carrier
gear set in automobile transmissions and high strength
powder-forged connecting rods in engines. P/M technology includes the basic steps: mixing of elemental powders, compaction and sintering or heating the shape in
a controlled atmosphere furnace to bond the particles
together metallurgically. After sintering the but prior
*
Corresponding author. Tel.: +91 431 250 1801; fax: 91 431 250
0133.
E-mail addresses: narayan@nitt.edu (R. Narayanasamy), trhashwek@yahoo.co.in (T. Ramesh), pandey@nitt.edu (K.S. Pandey).
0261-3069/$ - see front matter 2005 Elsevier Ltd. All rights reserved.
doi:10.1016/j.matdes.2004.12.005
567
and the corresponding level of deformation was experimentally observed. Petruska and Janicek [10] performed
a nite element test on cylindrical specimens with longitudinal surface notch under compression tests with various aspect ratio and frictional conditions for the
evaluation of the ability of various ductile fracture criteria to predict exactly the fracture initiation.
Narayansamy and Ponalagusamy [11] proposed a
mathematical theory of plasticity for compressible powder metallurgy materials. Yield stress values in the case
of simple upsetting compression tests were proposed.
Numerical integration was carried out for the computation of the yield stress. Further, they developed a theory
for the calculation of stresses using the plasticity equations. The plastic upsetting of a solid cylinder between
elastic platens was investigated by Lin [12] and the
spring back eect of the end surfaces of the billet and
the elastic deection of the dies were determined using
a thermo-elasticplastic coupling model. Distributing
of temperature and eective strain were also determined
through nite element approach. A theoretical and
experimental research work was carried out by Gouveia
et al. [13] for the prediction of ductile fracture conducting experiments on powder compacts with various geometrical shapes such as ring, cylindrical, tapered and
anged under several dierent loading conditions. Also,
the experimental work was veried with nite element
codes. Buijk [14] utilized the nite volume method to
study the behaviour of upset forging of cylinders using
rst and second order implementation of the nite volume method and predicted the die load for obtaining
the cylinder upsetting. Narayansamy et al. [15] proposed
a generalized yield criterion considering an-isotropic
parameters for porous sintered powder metallurgy metals and introduced a new ow rule with an-isotropic
parameters for porous metals. Further, they proposed
new generalized yield criteria with ve parameters constants for porous sintered powder metallurgy metals.
Landre et al. [16] discussed the utilization of ductile
fracture criteria in conjunction with the nite element
method and predicted when and where the materials
are likely to fracture during cold forging and validated
their results with experimental data. Continuum damage
mechanics was used by Gupta et al. [17] for the ductile
prediction in axi-symmetric upsetting. A parametric
study was carried out to determine the eect of friction
and height to diameter ratio on the deformation level
which micro crack initiate at the die work interface, centre of the work piece and meridian surfaces.
In this paper, a complete investigation on the workability criteria of AlAl2O3 powder preform compacts
was prepared. Powder metallurgy compacts with various
aspect ratios and initial preform densities were discussed
for studying the behaviour of powder metallurgy compacts under various stress state conditions namely uniaxial, plane and triaxial state of stress. A new strain
568
equation is used including the eect of the bulging during cold upsetting. The curves are plotted for formability stress index and relative density against axial strain
and from which it is concluded that the aspect ratio
and initial preform density plays a major role in the
study of workability criteria.
Table 1
Sieve analysis of aluminium powder
2. Theoretical foundations
The mathematical expressions used and proposed for
the determination of various upsetting parameters of
upsetting for various stress state conditions are discussed below:
2.1. Uniaxial stress state condition
In the compression of a P/M part, under frictional
conditions, the average density is increased. Friction enhances densication and at the same time decreases the
height reduction at fracture. The state of stress in a
homogeneous compression process is as follows:
According to Abdel-Rahman and El-Sheikh [8]:
rz reff ; rr rh 0;
Sieve size
+150
+125
+106
+90
+75
+63
+53
+45
+38
38
3.60
3.60
2.50
0.71
8.30
9.20
16.70
15.80
3.62
35.71
Table 2
Characterization of AlAl2O3 powder compacts
Aspect
ratio
Height
(H0) (mm)
Diameter
(D0) (mm)
Initial preform
density (%)
Compressive
load (MN)
0.35
9.50
9.75
9.80
27.80
27.75
27.75
90
80
75
0.135
0.08
0.055
0.56
16.20
15.40
15.00
27.80
27.75
27.75
90
80
75
0.135
0.08
0.055
0.72
20.00
20.30
19.65
27.80
27.75
27.75
90
80
75
0.135
0.08
0.055
1.1
0.9
0.8
0.7
0.6
0.5
0.4
1.1
0.9
0.8
Axial Strain(z)
0.5
0.4
0.3
0.3
0.2
0.2
0.1
0.1
0
0
(a)
569
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.1
(b)
0.2
0.3
0.4
0.5
0.6
0.7
1.1
0.9
0.8
Aspect Ratio 0.56, Initial
Fractional Preform Density 0.9
0.7
Aspect Ratio 0.56, Initial
Fractional Preform Density 0.8
0.6
0.5
0.4
0.2
0.1
0
0
(c)
0.1
0.2
0.3
0.4
0.5
0.6
0.7
Fig. 2. (a) Axial strain (ez) vs. formability stress index b triaxial stress state condition. (b) Axial strain (ez) vs. formability stress index b triaxial
stress state condition (power law curve tting results). (c) Axial strain (ez) vs. formability stress index b triaxial stress state condition (parabolic
curve tting results).
570
As an evidence of experimental investigation implying the importance of the spherical component of the
stress state on fracture according to Vujovic and Shabaik [18] proposed a parameter called a formability
stress index b given by,
b 3rm =reff :
where A 2 R2 rh R2 rz 2rh , B 2 R2 rz
R2 rz 2rh , a = Poissons ratio and R = relative
density.
From the above Eq. (10), using the known values of
a, R and rz, the Hoop stress component (rh) can be
determined as follows:
rh 2a R2 =2 R2 2R2 arz :
11
The eective stress can be determined from the following relation as explained elsewhere [20].
12
rh 1 2a=2 arz
2R2 1r2eff
13
or
ln2D2b
D2c =3D20 ;
where DB is bulged diameter of the compacts, Dc is contact diameter of the compacts and D0 is the initial diameter of the compacts.
2.3. Triaxial stress state condition
According to Narayanasamy and Ponalagusamy [20],
the state of stress in a triaxial stress condition is given as
follows:
a A=B;
10
Since rh = rr
r2eff r2z 2r2h R2 rz rh r2h rz rh =2R2 1
reff
0:5
r2z 2r2h R2 r2h 2rz rh =2R2 1 :
14
3. Experimental details
Atomized aluminium powder was procured and analyzed for its purity and was found to be 99.7%. The
characterization of aluminium and alumina powder
was studied by determining the ow rate, apparent density, tap density and particle size distribution as shown
in Table 1. Fig. 1 shows the SEM photograph of an aluminium powder. A sieve analysis is made to determine
the particle size as stated in Table 1. The compacts were
Table 3
Curve tting results axial strain (ez) vs. formability stress index (b)
Axial strain (ez) vs. formability stress index (b)
Aspect ratio
Equation
R2 value
0.35
0.35
0.35
0.56
0.56
0.56
0.72
0.72
0.72
0.9
0.8
0.75
0.9
0.8
0.75
0.9
0.8
0.75
0.848
0.9444
0.9669
0.9784
0.972
0.7402
0.8638
0.9471
0.5812
571
0.95
0.95
0.9
0.85
0.85
0.8
0.75
0.75
0.7
0
(a)
0.8
0.9
0.2
0.4
0.6
0.8
0.7
0
1.2
0.2
0.4
(b)
0.6
0.8
1.2
0.95
0.9
0.85
Aspect Raqtio 0.72, Initial
Fractional Preform Density 0.80
0.8
0.75
0.7
0
(c)
0.2
0.4
0.6
0.8
1.2
Fig. 3. (a) Relative density (R) vs. axial strain (ez). (b) Relative density (R) vs. axial strain (ez) (parabolic curve tting). (c) Relative density (R) vs.
axial strain (ez) (power law curve tting results).
572
Table 4
Curve tting results Relative density (R) vs. axial strain (ez)
Relative density (R)
vs. axial strain (ez)
Aspect
ratio
Fractional
preform
density
Equation
R2 value
0.35
0.35
0.35
0.56
0.56
0.56
0.72
0.72
0.72
0.9
0.8
0.75
0.9
0.8
0.75
0.9
0.8
0.75
0.9219
0.9453
0.912
0.9432
0.954
0.9036
0.9045
0.9411
0.891
0.35
0.35
0.35
0.56
0.56
0.56
0.72
0.72
0.72
0.9
0.8
0.75
0.9
0.8
0.75
0.9
0.8
0.75
Polynomial equation
Y = 0.0812X2 + 0.1615X + 0.9008
Y = 0.1421X2 + 0.2758X + 0.8243
Y = 0.2609X2 + 0.4107X + 0.7581
Y = 0.08 19X2 + 0.1619X + 0.8909
Y = 0.1 141X2 + 0.251X + 0.8199
Y = 0.205X2 + 0.3277X + 0.7605
Y = 0.723X2 + 0.1551X + 0.8835
Y = 0.1222X2 + 0.2627X + 0.8127
Y = 0.213 1X2 + 0.3328X + 0.7563
0.9989
0.9985
0.9974
0.9982
0.9963
0.9994
0.9951
0.994
0.999
1.2
0.8
0.6
0.4
0.2
y = 2.0102x - 0.301
2
R = 0.8573
0
0.3
0.35
0.4
0.45
0.5
0.55
0.6
0.65
0.7
0.75
0.8
573
0.3
Aspect Ratio 0.35, Initial Preform
Density 90%
0.9
0.25
0.8
Aspect Ratio 0.56, Initial Preform
Density 90%
0.5
0.7
0.2
0.4
0.2
0.05
0.1
0
0.7
(a)
0.75
0.8
0.85
0.9
0.95
0.7
(b)
0.75
0.8
0.85
0.9
0.95
1
Aspect Ratio 0.35, Initial Preform
Density 90%
0.9
0.8
0.5
0.4
0.2
0.1
0
0.7
(c)
0.75
0.8
0.85
0.9
0.95
Fig. 5. (a) Stress ratio (rr/re) vs. relative density (R). (b) Stress ratio (rm/re) vs. relative density (R). (c) Stress ratio (rz/re) vs. relative density (R).
574
ial stress state condition. It is observed that for the selected range of aspect ratios and initial preform densities, the initiation of the fracture of the compacts has
been observed at a very high strain value for the cases
of the compacts having lower aspect ratios and higher
initial preform densities. Two dierent curve-tting
techniques, namely parabolic and power law expressions, were used and the respective equations determined and the correlation coecient (R) are shown in
Table 4. From Table 4, it is observed that the constant
values decrease with decreasing initial fractional preform density.
Fig. 3(b) shows the parabolic curve tting results
for the plots between the relative density and the axial
strain. The parabolic equation has been found to be
the best curve tting for the compacts having medium
value of aspect ratios and medium initial preform
densities.
Fig. 3(c) shows the power law curve tting results
for the plot between the relative density and the axial
strain. In addition to the parabolic curve tting result,
the power law expression has also been tried and this
shows the best tting results for the compacts having
medium aspect ratios and with the medium initial preform densities. Among both the curve tting results,
the parabolic curve tting expression shows a very
good correlation coecient (minimum of 0.997 and
maximum of 0.998).
Fig. 4 has been drawn between the fracture strain
and the formability stress index for the upsetting of
AlAl2O3 powder compacts for the various aspect
ratios and three dierent initial preform densities under triaxial stress state condition. It is observed that
the fracture strain of the compacts is purely depends
on the aspect ratio and initial preform density. From
this gure, it is noted that for the compacts with higher aspect ratios and higher initial preform densities,
the initiation of crack appeared at a very high fracture
strain. For the case of compacts with lower aspect
ratios and lower initial preform densities, the initiation
of crack readily appeared at a low fracture strain.
Further, it is observed that for the case of compacts
with lower aspect ratios and with very high initial
preform densities a very high fracture strain is
obtained. A straight line tting is used for the plot
between the fracture strain and the formability stress
index and the slope of the straight line is found to
be 2.0335.
Figs. 5(a)(c) have been plotted between the various
stress ratios, namely (rr/re), (rm/re) and (rz/re) and
the relative density (R) for the upsetting of AlAl2O3
powder compacts with various aspect ratios and three
dierent initial preform densities under triaxial stress
state condition. It is observed that a very high stress ratio is obtained for the case of the compacts made with
the lower value of the aspect ratios and very high initial
5. Conclusion
The stress formability index increases with increase in
initial preform fractional density and lower the aspect
ratios.
Parabolic curve tting shows the better results for the
plot between the axial strain and the stress formability index.
Among the curve ttings, the parabolic type one
shows a very good correlation coecient (minimum
of 0.997 and maximum of 0.998) for the plot between
the relative density and the axial strain.
For the compacts with higher value of the aspect ratio
and with higher initial preform density, the initiation
of crack appeared at a very high fracture strain
For the case of the compacts with lower value of
the aspect ratio and with very high initial preform
density, a very high stress ratio parameter is
obtained.
References
[1] Kuhn HA, Downey CL. Deformation characteristics and plasticity theory of sintered powder materials. Int J Powder Metall
1971;7(1):1525.
[2] Green RJ. A plasticity theory for porous solids. Int J Mech Sci
1972;14:21524.
[3] Shima S, Oyane M. Plasticity theory for porous metals. Int J
Mech Sci 1976;18:28591.
[4] Gurson AL. Continuum theory of ductile rupture by void
nucleation and growth: Part I Yield criteria and ow rules for
porous ductile media. J Eng Mater Technol Trans ASME
1977:19.
575