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Abstract A mathematical model is constructed representing the non-executable equations to determine the mean flow stress (MFS) using both Sims and Ekelund approaches. The model considers the
redundant strain calculations. Solving the equations of the model develops a numerical solution and consequently the MFS is then calculated. The numerical values are taken from the rod mill logs, particularly when the interpass times are short, since the laboratory equipment cannot be used. The calculated MFS
values are then related to the inverse of the absolute rolling temperature to determine the non-recrystallization temperature (Tnr), the strain accumulation and the cyclic softening / dynamic recrystallizing
zones of the austenitic stainless steel.
At the finishing and prefinishing stages, the accumulated deformation and the deformation heating
affect temperature raising. However, at both stages, the coefficients of friction (m) decrease as the effect
of the rolling velocity becomes predominant. The MFS values calculated by Ekelund are always higher
than those calculated by Sims. The Tnr is detected as 1143 C. However, between 1143 and 1081 C, with
0.03 seconds interpass time, a stress accumulation zone is detected. At the high strain rate, 103 s-1, in the
temperature range 1063 and 1018 C, dynamic recrystallization is initiated. At higher strain rates (12001500 s-1), cyclic softening / dynamic recrystallizing is initiated. The finishing temperature is found to be
the most attributable to the grain size, whereas, the sub-grain structure is mainly due to multi-passes
deformation.
Rsum On construit un modle mathmatique reprsentant les quations non-excutables pour
dterminer la contrainte moyenne dcoulement (MFS) utilisant lapproche de Sims et celle dEkelund.
Le modle considre les calculs de dformation redondants. En rsolvant les quations du modle, on
dveloppe une solution numrique et, consquemment, la MFS est ensuite calcule. On utilise les
valeurs numriques des journaux dentres du laminoir, particulirement quand le temps entre les
passes est court, puisquon ne peut pas utiliser lquipement de laboratoire. Les valeurs calcules de
MFS sont ensuite relies linverse de la temprature absolue de laminage pour dterminer la
temprature de non-recristallisation (Tnr), laccumulation de dformation et les zones cycliques de
ramollissement/recristallisation dynamique de lacier inoxydable austnitique.
Aux tapes de finissage et de pr-finissage, la dformation accumule et la chaleur de dformation
ont pour effet dlever la temprature. Cependant, aux deux tapes, le coefficient de friction (m)
diminue mesure que leffet de vlocit de laminage devient prdominant. Les valeurs de MFS
calcules par Ekelund sont toujours plus leves que celles calcules par Sims. On dtecte Tnr 1143 C,
cependant, entre 1143 et 1081 C, avec 0.03 s dintervalle de passe, on dtecte une zone daccumulation
de contrainte. un taux lev de dformation, 103 s-1, dans la gamme de temprature entre 1063 et
1018 C, la recristallisation dynamique est initie. des taux de dformation encore plus levs (12001500 s-1), ladoucissement/recristallisation dynamique cyclique est initi. On trouve que la temprature
de finissage est attribuable principalement la taille de grain, alors que la structure du sous-grain est
principalement due la dformation par passes multiples.
488
INTRODUCTION
The mean flow stress (MFS) is usually used to detect the
events that take place during hot rolling [1]. These
microstructural events are like recrystallization, strain
accumulation and g-a phase transformation [2]. For
instance, three critical temperatures of steel rolling are recognized [3]. These are the temperatures below which the
recrystallization of austenite no longer takes place, Tnr, and
the start, Ar3, and finish, Ar1, of the austenite to (a +
Pearlite) transformation. Boratto et al. [3], were the first to
develop the procedure used to determine the Tnr, Ar3 and
Ar1 temperatures. These critical temperatures are located
on the inverse points of the curve relating the MFS to the
inverse of the absolute temperature [4]. Consequently, fractional softening and grain size can be expected [5].
Different mathematical modules and numerical models
have been developed to detect the MFS from the mill logs
[6,7]. Most of these models use Sims approach [8] to calculate the MFS.
The most controlling factor separating conventional
rolling and dynamic recrystallization rolling is the length
of the interpass intervals and in particular whether this is
longer or shorter than 1 second [5]. Long interpass time
processes are those that involve reversing mills or when
early in the reduction process in the tandem mills. On the
other hand, in the rod finishing rolling, although the nominal pass strains are below the critical strain for dynamic
recrystallization (DRX), the interpass times are too short
for significant amounts of conventional static recrystallization (SRX) to occur [9]. As a result, the strain accumulates
from pass to pass until DRX is initiated. At the completion
of a pass involving DRX, the recrystallization that occurs
is no longer dynamic, rather it is metadynamic (MRX)
[10]. On the bases of previous works [11, 12], the MRX
process generates fine austenite grain sizes at high values
of Zener-Hollomon parameter which are at high strain rates
and relatively low temperature.
Physical simulation of rolling schedules by mean of
torsion tests has proved to be very powerful in the design
of rolling passes for reversing mills [3]. However, the high
strain rates associated with the finishing stages cannot
readily be achieved using laboratory equipment [13]. The
short interpass time processes are those that involve continuous mills, particularly when these are located at the finishing end of an operation, so that the stock is moving relatively quickly. Under these conditions, the strain rates can
be as high as 100-1000 s-1 (in the finishing stands of rod
mills) [14] and the associated deformation times are of the
order 1 ms.
Most of the previously published models were dealing
with hot flat rolling; however, there are few modeling
works on the rod hot rolling. The aim of the present work
is to construct a model for the evaluation of MFS from the
CANADIAN METALLURGICAL QUARTERLY
rod mill logs, particularly when the interpass times are too
short, to detect the non-recrystallization temperature, the
strain accumulation and softening zones of the austenitic
stainless steel.
In the present work, a previously constructed constitutive model for flat hot rolling [15] has been adapted and
validated to cope with rod hot rolling [16]. The results of
the adapted model are compared with those obtained from
mill logs. The adapted model has been developed by introducing further equations that help precise computation of
different parameters instead of treating them either as constant terms or neglecting their effects [16].
MODEL EQUATIONS
The mathematical model mainly depends on Simss
approach [8] and the developed Orowan method [15]. The
roll pressure can be calculated at the exit side by using
Simss approach
1
1
2
S+ p
h R2
-1 R
= 1 + ln + tan . j
k
h2 h2
4
h2
(1)
S- p
h R2
= 1 + ln +
k
4
h2 h2
1
1
tan -1 R 2 .q - tan -1 R 2 .j
h2
h2
(2)
fn =
h X
h2
tan 2
R
R 2
(3)
where
sf
1
1 h1 kexit
Z
X= ln
2 2 m h2
sb
1 - k
entry
(4)
489
where K=1 for the steel rolls, t should not be less than 700
C and v the roll velocity in m/s. and not more than 5.0.
and
R
R
tan -1
a
h2
h2
Z=2
(5)
( MFS) Ekelund =
P
W R Dh QEkelund
(12)
-1
QEkelund = 1 +
1.6 m
(6)
R Dh - 1.2 Dh
h1 + h2
(13)
(7)
( MFS) Sims =
3P
2 W R Dh QSims
(14)
then
where
Y = h2 + 2 R(1 - cos f n )
(8)
QSims =
W .Dh
(9)
h2
4(h1 - h2 )
(15)
R Y2 p
-1 h1 - h2
ln
p . tan
h2
h2 h1h2 4
e =
where P is the rolling force, W is the width and c is an elastic constant and is equal to
2pU
60
R
h1
(1 - e )
e
ln
1
1- e
(16)
where
c=
16 1 - n
(10)
pE
(11)
e=
h1 - h2
h1
(17)
490
MATERIAL
The rolled material is austenitic stainless steel billets to
produce 6.0 mm diameter wires. The steel chemical composition is presented in Table II.
Pass
shape
Effective
roll radius
(R)
mm
Exit bar
width
(W)
mm
h1
mm
h2
mm
Rolling
temp. (t)
C
R1
R2
R3
R4
R5
R6
R7
R8
R9
R10
I1
I2
I3
I4
F1
F2
F3
F4
F5
F6
F7
F8
PF1
PF2
PF3
PF4
PF5
PF6
PF7
PF8
PF9
PF10
Box
Box
Box
Box
Box
Box
Ov
O
Ov
O
Ov
O
Ov
O
Ov
O
Ov
O
Ov
O
Ov
O
Ov
O
Ov
O
Ov
O
Ov
O
Ov
O
286.05
282.20
291.65
295.05
231.35
226.75
241.00
237.60
245.65
242.80
201.85
199.30
205.15
202.75
207.15
204.60
158.65
156.20
159.40
156.95
159.60
157.85
102.00
100.95
84.70
84.05
85.15
84.65
85.80
85.10
86.15
85.65
171.0
140.0
141.8
112.0
111.2
86.0
76.2
67.3
60.3
53.2
47.2
41.5
39.4
32.6
30.6
25.2
25.7
19.8
21.7
16.7
17.8
14.6
15.6
12.4
12.7
10.6
10.4
8.9
8.9
7.4
7.3
6.1
162.3
171.0
118.5
141.8
90.1
111.2
70.2
76.2
67.3
60.3
53.2
47.2
41.5
39.4
32.6
30.6
25.2
25.7
19.8
21.7
16.7
17.8
14.6
15.6
12.4
12.7
10.6
10.4
8.9
8.9
7.4
7.3
120.0
140.0
88.0
112.0
69.0
86.0
58.0
67.3
43.0
53.2
33.5
41.5
25.0
32.6
20.0
25.2
15.0
19.8
12.0
16.7
11.0
14.6
9.4
12.4
8.0
10.6
6.8
8.9
5.5
7.4
4.6
6.1
1194
1178
1165
1156
1148
1143
1000
996
988
992
966
973
970
983
973
988
995
1018
1012
1034
1041
1056
1047
1063
1063
1064
1064
1067
1067
1072
1075
1081
Rotational
roll speed
(U)
rpm
8.8
11.1
14.3
17.4
29.2
37.9
15.4
19.4
25.7
31.8
51.4
62.5
81.1
100
129.3
160.8
268.3
340.8
395.4
476.8
523.9
616.6
1098.4
1348.1
1921.8
2271.2
2777.9
3282.9
4034.3
4767.8
5831.5
6891.7
Rolling
force
(P)
ton
166.6
139.9
189.0
132.7
128.8
93.1
116.5
77.2
115.6
67.1
78.1
46.9
69.6
40.1
51.9
32.3
38.1
21.8
27.1
14.6
18.4
11.1
11.5
6.8
8.0
4.6
6.4
3.6
6.0
3.6
4.9
3.1
C
0.03
Si
0.3
Mn
1.8
Ni
9.36
Cr
18.3
Mo
0.4
Cu
0.35
Al
.003
P
.020
S
.025
N
.079
491
NUMERICAL EVALUATION
287.51
284.21
294.47
297.64
234.16
228.90
247.66
244.37
249.93
252.33
205.60
208.09
210.00
210.86
213.31
215.33
163.75
162.69
165.05
163.06
165.99
166.09
105.17
104.75
87.39
88.03
88.13
89.65
89.54
91.18
90.73
93.36
0.682
0.689
0.695
0.700
0.704
0.706
0.786
0.788
0.793
0.791
0.807
0.803
0.805
0.796
0.803
0.793
0.789
0.775
0.778
0.765
0.761
0.752
0.758
0.749
0.749
0.748
0.748
0.746
0.746
0.743
0.742
0.739
0.387
0.333
0.325
0.319
0.303
0.335
0.226
0.194
0.316
0.171
0.314
0.169
0.285
0.183
0.247
0.163
0.254
0.194
0.222
0.178
0.189
0.143
0.227
0.179
0.228
0.155
0.214
0.134
0.200
0.133
0.180
0.121
0.41992
0.28642
0.21678
0.17528
0.09905
0.08444
0.14000
0.09542
0.11736
0.05142
0.05828
0.02579
0.03351
0.01751
0.01826
0.00966
0.00905
0.00544
0.00535
0.00357
0.00345
0.00221
0.00197
0.00127
0.00114
0.00065
0.00074
0.00039
0.00047
0.00027
0.00029
0.00017
0.26
0.33
0.44
0.54
0.71
0.90
0.39
0.48
0.66
0.81
1.09
1.30
1.74
2.12
2.80
3.44
4.46
5.57
6.60
7.83
8.75
10.19
11.73
14.24
17.04
19.98
24.76
29.09
36.23
42.47
52.58
61.78
0.349
0.231
0.343
0.273
0.308
0.297
0.221
0.143
0.517
0.145
0.534
0.148
0.585
0.219
0.564
0.224
0.599
0.299
0.578
0.300
0.482
0.230
0.513
0.267
0.506
0.201
0.524
0.181
0.562
0.215
0.544
0.215
0.097
0.083
0.081
0.080
0.075
0.084
0.055
0.047
0.078
0.041
0.078
0.040
0.070
0.044
0.060
0.039
0.062
0.047
0.054
0.043
0.046
0.034
0.055
0.043
0.056
0.037
0.052
0.032
0.048
0.031
0.043
0.028
0.446
0.81
0.314
0.83
0.424
1.52
0.353
1.55
0.383
3.02
0.381
3.48
0.276
1.58
0.191
1.58
0.595
3.87
0.186
2.93
0.612
7.97
0.188
5.95
0.655
14.75
0.263
12.37
0.624
26.29
0.263
22.80
0.661
55.45
0.346
52.44
0.632
91.15
0.343
79.63
0.528 122.69
0.264 100.85
0.569 225.96
0.310 202.20
0.562 389.06
0.238 304.99
0.576 616.40
0.213 464.29
0.610 1008.49
0.246 791.07
0.587 1588.54
0.243 1262.44
Neutral
angle
(jn).
rad
0.125 124.5
0.117 143.9
0.112 91.7
0.112 115.8
0.108 71.7
0.116 89.1
0.088 59.9
0.079 68.8
0.106 45.8
0.071 54.5
0.105 35.8
0.070 42.5
0.096 27.0
0.074 33.7
0.087 21.6
0.066 26.1
0.088 16.3
0.076 20.7
0.079 13.0
0.070 17.5
0.071 11.8
0.059 15.2
0.082 10.1
0.071 12.9
0.083
8.6
0.064 11.0
0.078
7.3
0.056
9.2
0.073
5.9
0.055
7.6
0.067
5.0
0.050
6.3
8.23
10.21
12.58
11.67
14.79
13.17
24.72
22.90
19.75
27.03
20.64
29.64
22.22
27.47
23.06
30.48
25.33
28.23
23.12
23.63
22.28
25.42
22.07
23.82
22.87
26.74
22.56
28.12
24.58
32.00
25.71
34.91
0.438
0.443
0.443
0.442
0.436
0.428
0.528
0.525
0.519
0.509
0.506
0.490
0.467
0.440
0.407
0.363
0.303
0.261
0.264
0.253
0.250
0.242
0.247
0.239
0.239
0.238
0.238
0.237
0.237
0.234
0.233
0.230
8.08
9.73
12.25
11.21
14.35
12.83
22.25
20.52
18.60
24.26
19.68
26.82
22.00
25.85
24.17
30.34
30.57
31.59
29.49
26.85
28.06
28.42
27.90
26.85
29.11
29.13
29.22
30.60
32.81
35.92
34.62
39.79
492
1200
0.1
1100
0.01
1000
0.001
900
35
0.0001
0
10
15
20
25
30
Stand number
Fig. 1. Interpass time and rolling temperature at different stands
0.5
10
0.4
0.3
10
0.2
0.1
0.1
10
15
Figure 3 shows a presentation of the rolling force at different mill stands. The presentation is a comparison between
the measured values at the mill logs and the prediction from
an adapted model [20] constructed for rod hot rolling calculations. The predicted values are always lower than those
measured. However, the difference in value is much higher
at the roughing stage than at the intermediate and finishing
rolling stages. However, the two curves have the same trend,
where the trend of the rolling force decreases continuously
from one stand to the other as the cross-sectional area of the
rolled stock decreases. The difference in rolling force
between the measured and predicted values occurs because
it is difficult to represent and measure the actual amount of
reduction in cross-sectional area in rod rolling processes
where the actual amount of reduction is much more than that
theoretically measured at each stand [22]. This difficulty
leads to a deficiency in modeling the rod rolling processes.
One of the targets of the present work is to evaluate the
mean flow stress (MFS) for each pass by both Sims and
Ekelund approaches. The MFS is presented against the reciprocal of the absolute value of the rolling temperature in
Figure 4. This presentation reflects clearly the behaviour of
the austenitic stainless steel during deformation under the
specified conditions. The MFS values calculated by Ekelund
are always higher than those calculated by Sims. This is
because Ekelund considered the value of the friction coefficient and Sims did not pay attention to it.
200
100
20
25
30
35
Coefficient offriction
0.6
On the other hand, the coefficient of friction (m) decreases throughout the roughing stands and begins to rise sharply
at stand 7 due to the loss of some of the rolling temperature
and velocity as a side effect of the lopper existence.
Afterwards, m decreases again where the effect of the rolling
velocity becomes predominant over the effect of rolling temperature (Equation 11) [18].
Coeficient of friction
175
Rolling temperature, C
Rolling temperature, C
Interpass time
150
125
100
75
50
25
0
0
Stand number
Fig. 2. Coefficient of friction and rolling velocity at the different mill
stands
CANADIAN METALLURGICAL QUARTERLY
10
15
20
25
Pass number
Fig. 3. Presentation of rolling force at different mill stands for both mill
log and predicted data
45
40
35
30
25
20
15
10
5
0
0.65
(2)
1081 C
493
(4)
1018 C
Sims
Ekelund
(3)
1063 C
(5)
966 C
(1)
1148 C
0.675
0.7
0.725
0.75
0.775
0.8
0.825
0.85
1000/T, K-1
Fig. 6. Microstructure of a 25 mm diameter rod 100 (rolling temperature 988 C with 22.8 s-1 strain rate)
494
Both microstructures presented in Figures 5 and 6 confirm what was detected in Figure 4 ensuring that the finishing temperature is the most attributable to the grain size;
whereas, the sub-grain structure is mainly due to multi-passes deformation. All that was reported regarding the
microstructure emphasizeses that the detection of
microstructure events during hot deformation by the MFS
temperature relationship is a reliable method.
CONCLUSIONS
1. At the finishing and prefinishing stages, the accumulated deformation and the deformation heating affect temperature rising.
2. The coefficients of friction (m) decrease throughout the
roughing stands and begin to rise sharply at the intermediate process. Afterwards, m decreases again as the effect of
the rolling speed becomes predominant.
3. The MFS values calculated by Ekelund are always
higher than those calculated by Sims.
4. The Tnr is detected as 1143 C.
5. Between 1143 and 1081 C with 0.03 second interpass
time, there would not be a chance for stress annihilation but
rather stress accumulation.
6. At a high strain rate, 103 s-1, in the temperature range
1063 and 1018 C, dynamic recrystallization of the austenite grains is initiated.
Sa
fn
h1
h2
W
c
R
R
Kexit
Kentry
sf
sb
Y
v
U
ov
o
t
x
xr
xt
x.
P
Z
Qdef
MFS
t
T
Tnr
m
DRX
SRX
MRX
S+
Meaning
mean flow stress
rolling temperature
absolute rolling temperature
non-recrystallization temperature
coefficients of friction
dynamic recrystallization
static recrystallization
metadynamic recrystallization
normal roll pressure at the exit side
Units
1.
2.
3.
4.
5.
Kg/mm
C
K
C
Kg/mm2
Kg/mm2
rad.
rad.
MM2
MM2
MM2
MM2
MM2
Kg/mm2
Kg/mm2
Kg/mm2
Kg/mm2
MM2
mm/sec
Rpm
sec
sec-1
ton
erg
REFERENCES
NOMENCLATURE
Symbol
6.
7.
8.
9.
10. R.A. Petkovic, M.J. Luton and J.J. Jonas, Recovery and
Recrystallization of Polycrystalline Copper after Hot
Working, Acta Metall., 1979, vol. 27, pp. 1633-1648.
495
13. T.M. Maccagno, J.J. Jonas and P.D. Hodgson, Spread Sheet
Modeling of Grain Size Evaluation during Rod Rolling,
ISIJ International, 1996, vol. 36(6), pp. 720-728.