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Troubleshooting
Section B-Contents
Overview of Failure Indicators
Basic Strategy of Repair
:
'l'ypes of Failures
lIijector Errors
'I'ray Errors ................................................
Controller Errors ...........................................
Miscellaneous Errors
HP-IB/Controller Board Errors
Printed Error Messages
B.S
B-4
B-4
B.6
B-12
B.-22
B-24
B-27
B-27
8-1
~'.I7n;:'~}~.\,;
',f,.'ft,' '"
.":,
'!..(~~~~::",\
;,~'J:;t.~',,',I~'~
,":""
This section is intended to aid a trained service engineer in the troubleshooting process.
Included in this chapter is an overview of the failure indicators, a basic strategy of repair,
and a detailed action list for each type offailure.
WAHNING
B-2
~'
-'",
"
Red
Yelow
Green
Types of Failures
Throurhout this section, the following symbols identify the LEOs.
Injector
0
0
0
ControUer
Immn
1W.LL11J
Dol
Some error conditions can have more than one cause. The most frequent/simplest cause is
listed first, with other possibilities listed second or third. If possible, use the diagnostic
mode to isolate the problem to one of the causes and follow the steps for troubleshooting
that cause.
Eaoh action list contains several things for you to check. Go through each step in order,
and stop when you have found the failure. You may not necessarily complete ell the actions
in the list. After you have repaired the failure, retest by rpnning a normal sequence of
movement or using the diagnostics mode.
84
INJECTOR ERRORS
InJector Led
DllcrlpUon
Page
Red Steady On
Red 2 Rashes
Red 3 Rashes
Red 4 Rashes
Red 5 Rashes
Red 6 Rashes
Safety Error
Injector Syringe Error
Injector Turret Error
Injector Plunger Error
Incomplete Injection Error
Injector Memory Error
B-6
B-7
B-8
DllcrlpUon
Plge
B-12
B-13
B-15
B-17
B-19
B-21
B-21
Controller Led
D"crlpUon
Page
"8-22
B-22
B-9
B-11
B-11
TRAY ERRORS
Controller Led
Red Steady On
Red 2 Single Rashes*
Red 3 Single Flashes*
Red 4 Single Rashes*
Red 5 Single Aashes*
Red 6 Single Aashes*
. Red 7 Single Aashes*
CONTROLLER ERRORS
B-22
B-23
MISCELLANEOUS ERRORS
InJector Led
Controller L'd
DllcrlpUon
Page
Green On
Redan
None
B-24
B-25
B-26
* The HP.JB/controler board also uses Algie red 1IaIhn toCOIIVTUlIcIU error cordIons flllJld durilg Is powllr-up seIf-test. See
B-5
,"
';
Injector Errors
0
0
-IDmn
Safety Error
Injector door open.
Injector improperly mounted.
88
v.
a
~IIIIIll
Using the diagnostics mode, determine if the syringe carriage is moving properly. If it is,
suspect sensor failure; otherwise, check for obstructions Of motor failure.
2. With the syrinp carriage removed, ensure that the syringe motor/drive belt combination is moving freely. If not, remove the belt and check movement of both the idler
pulley and the motor. If either piece is not moving, replace it.
2.
Remove the motor and test it for opens and shorts. Replace motor if necessary.
8. Check for the presence of 18-V supplies at the iI\jector logic board. If they are not at
the proper voltage levels, proceed to diagnose the controller module and cables.
4. Although the LEDs indicate the motor windings are energized, they do not verifY that
the proper drive current is being supplied to the windings. Replace inJector logic board
and retest.
2. Check the syringe carriage for a magnet. Using a known good magnet, test to see if the
magnet in the carriage is installed properly (magnet faces should repel each other). If
the magnet is missing or installed improperly, replace the syringe carriage.
8. VerifY the syringe sensor is connected properly to the i~ector logic board. Retest the
sensor with the syringe carriage in the home position. If necessary, replace the syringe
carriage sensor (note that thls in one of a pair of sensors and both must be replaced).
Ire
1\'
0
O
IITIIID
Using the diagnostic modes, determine if injector turret is moving properly. If it is, suspect
sensor failure; otherwise, check for obstructions or motor failure.
Manually check to see if the injector turret is able to rotate freely through a full revolution. If it is not rotating freely, continue with next step.
2.
Open the uyector door and check the bottle stripper assembly. It should swinr freely in
and out. If not, remove the turret and check the arm for interference. Replace the bottle stripper assembly, spring or mounting sleeve if necessary.
2.
Check the connection of the turret motor to the injector logic board and retest
operation.
8. Check the irUector turret motor for shorts or opens. Replace motor if necessary.
4.
2.
Manually verify that the sensor is working, using the diagnostics mode. The green LED
should light when the sensor is tripped.
3. VerifY that the turret sensor is connected properly to the injector logic board. If necessary, replace the sensor (note that this is one of a pair of sensors and both must be
replaced).
.
8..8
~.
~mnlD
Using the diagnostic mode, determine if the plunger carrier is moving properly. If it is not,
suspect sensor failure; otherwise, check for obstructions or motor failure.
2. With a known good magnet (faces should repel), test the plunger carrier magnet. If it is
not good, replace the plunger carrier,
3. Check the ribbon cable connections at the sensor board and the iIijector loric board. If
connections are good, check the ribbon cable for open runs. Replace if necesBaIy.
4. Replace the plunger sensor board by replacing the syringe carriage and retest.
5. Replace the injector logic board and retest.
8-10
~llnnD
1. Remove the syringe from the injector end check it for stickiness and/or binding.
Replace if necessary.
2. Run the diagnostics mode for the plunger carrier. Replace plunger carrier and/or
syringe carriage if necessary.
8. Replace ixijector logic board end retest.
II.
a
a
L....-
IITITn
1. Verify that the injector processor (and the EPROM if present) is positioned properly
and seated in the PC board socket.
811
Tray Errors
_01
2. VerifY that the connection of the cable inside the tray is secure.
8. Check to see if the tray cable has opens or shorts.
2. Replace the tray board and then the controller board if necessary.
(_)01
2. Check the "deliver to" location for the vial and verifY that the location is empty and free
of obstructions.
S. Ensure that the tray is installed correctly on the mounting bracket.
4. Rerun the system to observe how the eITOr may have occurred.
VI~I
1. Remove the cover from the controller module and turn on the power. Make sure the
gripper is in the home position and the Z.LED is lit. Insert a bottle into the gripper and
check that the B--LED goes off. Remove the bottle and check that the BoLED goes on
again. If the BoLED is not lighting properly, continue.
2. Check the tray cable connection inside the bottom cover of the tray. Make sure the
connector is seated.
3. Remove the tray ann from the tray turret. Remove the tray arm covers and check the
gripper assembly. The lever should be holding a vial magnet and it should be aligned
.with the lower magnetic sensor on the sensor board. Press the gripper paddle. If the
vial magnet does not move away from the sensor, replace the gripper assembly.
4. Ensure that the connections on both the
properly.
6. Replace the ann sensor board and retest.
6. Replace the tray board and retest.
R~flex
Remove any obstructions that may have dislodged the vial from the gripper during tray
arm movement.
2,
Make sure sample vials meet HP specifications (see HP 7673 Operating Manual Appendix A, Consumables). If the vials are too tall, the vial in the gripper may be dislodged by
the ones in the traY.
3. Check the gripper jaws for smooth spring action movement. If either gripper jaw does
not close properly, replace gripper assembly.
<_) C11
Using diagnostic mode, determine if the tray arm is rotating properly. IT the arm moves
smoothly or if the theta motor fails to stop when the arm does, suspect sensor failure.
Otherwise, check for obstructions or motor failure.
rotation.
2. Slowly rotate the arm about its angular axis. It should move smoothly-do not force
the arm. The arm should move approximately 856 degrees from one stop to the other.
8. Remove the tray turret from the base. Check the theta-motor gear and the turret
gear for missing or broken teeth. Replace the motor assembly and/or turret assembly
as needed.
CAUTION
Improp.r mounting of turr.t ....mbly will damage the th.ta fllx elreutt. See
f1gur. ES for mbly In.tructlon.
Using the diagnostics mode, check the theta axis movement. Watch the T-LED on the
tray board. It should be lit for half of the rotation and ofT for the other half.
2. Check the theta-sensor connection at the termination board. Check the tray cable
connections at both ends.
3. Remove the tray turret from the base and replace the theta-sensor.. Before reassembling, test the operation of the theta-sensor by interrupting the sensor with a thin
object.
4.
B-16
<_)
01
Rod LED: 4
SJng~ Rash..
R motor inoperable.
Radial sensor inoperable.
Using diagnostic mode, determine if the tra,y arm is moving forward and backward properly.
If the ann moves smoothly or if the R~motor falls to stop when the arm does, suspect sensor
2. Remove the cover from the controller module and turn the power on. Hold the arm in
the middle and gently move the arm in its radial axis to the full back (home) position.
Do not force the arm to move. The R~LED should be lit.
8. Check arm rods and bushings for binding. Replace if necessary.
4. Open tray base and remove the large R~drive gear. Move the arm radially-the arm
should move smoothly and freely.
6. Check the R~motor pinion gear and the ann rack for missing or broken teeth. Check
that the pinion is free to turn in the turret. Replace as needed.
R Motor Inoperable
1. Remove the bottom cover from the tray and unplur the radial motor. Check the
resistance of the motor windings. Replace the motor if any windings are open or
shorted.
2. Check the radial motor gear for looseness. Replace the motor if necessary.
8. Check the tray cable for continuity and proper connections.
4. Replace tra,y board and retest.
2. Gently move the arm forward and check that the R-LED goes ofT.
8. Check the tray cable connections at both ends.
4.
Remove the arm assembly and verifY the presence and proper installation of the magnet
in the turret, Check the continuity of the sensor lines through the R-flex circuit. Check
the connection of the R-flex circuit to the theta-flex circuit on the turret.
5. With the arm removed, verify the continuity of the radial axis sensor's lines through the
theta-flex circuit and the tray cable. Replace the tray cable or the theta-flex cable if
necessary.
6. Replace arm sensor board and retest.
7. Replace the tray board and retest.
B-18
I,~:'!"r''''''.'!'
(_>
01
Using the diagnostic mode, determine if the gripper is moving up and down properly. If the
gripper moves smoothly or if the Z-motor fails to stop when the gripper does, suspect sensor
failure; otherwise, check for obstructions or motor failure.
Z Motor Inoperable
1. With the right half of the arm removed, run diagnostics. Watch the drive pulley on the
Z-motor for movement. The motion should be smooth until the gripper reaches the top
or the bottom of the stroke.
2. Check the connections for the Z-motor through the cables and reconnect or replace as
necessary.
S. Check the Z-motor pulley for looseness. Replace the arm core/motor assembly if
necessary,
4. Replace the tray board and retest.
8-19
Z Sensor Inoperable
1. Using diagnostic mode, run the Z-axis test and check for sensor operation. The Z.LED
should be on when the gripper is at the top of its movement.
2. Check the connections for the Zaxis sensor back through the flex circuits and tray
cable. Replace parts as needed.
3. Using a known good magnet, verify that the sensor is operating. Check the gripper
assembly for the presence of a magnet. Replace the gripper assembly if necessary.
4. Replace the tray board and retest.
8-20
<-J
01
<_)
01
1. Check the injector for proper installation on the mounting bracket. The right front foot
pin should be inserted into the hole in the bracket disk. The other three iIijector feet
should be in contact with the mounting bracket.
2. Check the tray for proper installation. The tray locks on the tray mounting bracket
should be inserted into the tray base.
3. Check the standoffs connecting the tray bracket to the injector bracket. The "A" positions are for HP 6890Aand HP 5700 GCs. The "B" positions are for the HP 5880AGC.
4. Make sure the sample vials meet HP specifications.
5. Make sure the needle support assembly has properly enpged the injector turret during
bottle pickup. If not, troubleshoot the injector for turret errors.
6. Run a sequence and watch the tray gripper as it attempts to retrieve a bottle from the
injector turret. The gripper should be aligned with the "neck" of the sample bottle. If
the gripper is misaligned with the bottle, troubleshoot the tray for the misaligned axis
(R, Z, or theta).
Controller Errors
5::::::::;=====1
((_))0
-)CJI
8-22
->)CI1
Red LED: 5
Doub~ Flashes
Confi~ration
Error
Option boards not installed in
the correct position.
Option board failure.
Miscellaneous Errors
Injector
Controller
Red
- On
Yellow - On
Green - On
Red
- Off
Green - On
B-24
Injector
Controller
Red
- On
Yellow - On
Green - On
Red
Green
On
Off
2. Unload the system by pulling out all the option boards plugged into the main power
supply board. If the + 18 V and/or -18 V works, plug in one option board at a time to
determine the defective board. Replace it.
8. If system is not responding with all the boards pulled out, replace the main power
supply board.
'P-'-',,'::, :'.'~ .,
InJector
Controller
Red
- Off
Yellow - Off
Green- - Off
Red
- Off
Green - Off
switch is on.
2. Check the line fuse located inside the line module of controller. Replace fuse if
necessary.
8. Check that the cables are connected.
+5~V
2. Unload the system by pulling out all the option boards plugged in the main power
supply board. If the + 5 V works, plug in one option board at a time to determine the
defective board. Replace it.
8. Replace the main board if necessary.
Error Message
2 flashes
3f1ashes
4 flashes
5 flashes
6 flashes
7 flashes
B-27
-, I,' ::"I"':'~
,:r'~'
c
Injector Module
Section C-Contents
Il\iector Operation
I1\Jector Replacement Parts
Injector Errors .............................................
Injector Diagnostics
Measuring Iniector Alignment
Printed Circuit Board Component Overlays
Iniector Pin Out Diagrams
C~2
C~6
C~14
C~15
C~18
C~21
C~28
Injector Operation
The HP 18593B Injector Module loads a syringe with a sample and injects the sample into
an HP gas chromatograph. The syringe and the sample vial are controlled by three key
assemblies: the syringe carriage, the plunger carrier, and the injector turret.
C-2
Turret Movement
The iJUector turret contains five positions for holding sample vials and wash/waste bottles
(figure C-5). The turret is mounted directly on the turret motor. The turret motor is a
four-phase stepper motor, with two common leads that are tied to + 12 V. A phase is energized by driving it low. The turret rotates. the vials and bottles into the it\iector tower to
allow access by the syringe.
When operating with a tray, the turret rotates to a specif1c position for the tray gripper
to pick up or deliver sample vials. The syringe carriage then engages the needle support
assembly into the turret to prevent any turret rotation during vial pickup or delivery. After
receiving the sample vial, the needle support is raised and the injector turret rotates to start
the iIijection sequence.
C-3
Turret Homing
The turret has a small magnet pressed into its lower, exterior surface. A magnetic sensor
mounted behind the turret senses this magnet to find the turret home position (figure C7).
During homing, the turret motor rotates the turret until the magnet is sensed. The turret
motor then rotates the turret a few steps in both directions to determine the center of the
magnet,
If the sampler system is operating without a tray and is using stand-alone control, a mag-.
netic bottle insert may be used to indicate the "last bottle" during a sequence. The turret
sensor also will home on this magnetic insert during its homing routines.
Safety Switches
There is a safety mechanism on the injector tower to protect the operator during injection.
When the plastic door covering the syringe assembly is opened, all motor movement in the
injector module is suspended. This is accomplished through a switch located inside the top
right corner of the door (flgure C6).
A second switch is used to determine if the injector is mounted correctly. The mounting
switch is located above the mounting sleeve and is closed by the mounting post when the
iI\jector is seated on the mounting bracket (figure C-B>'
Injector Electronics
All injector functions are controlled by a microprocessor on the iDJector main board
(figure C-g). All motors, sensors, and switches connect directly or indirectly to the iDJector
main board (figure Col). The iDJector draws its power supplies from the controller module
through the hijector cable. The cable is also used to transmit TTL and serial communication between the injector and the controller modules.
C4
InJector
Loalc Board
Controll.r
Modul.
Serial Out
Rlldy Out
Start Out
S.rlalln
Ready In
Start In
.Front Pan.1
>
fow.r SUDpn..
J1
MOlor.
Sol.nold
J&
J8
[~
J4 [
J7
- l ~ JB
~ Plung.r
J1
Syringe
Motor
Motor
J2
Plung.r
I.nlorl
Senior Board
Plunger
Solenoid
Syring. S.nlor
J3
Fan
Switch
Turret
MOlor
LEOI
....
J2 [ 1
J
Turr.t S.nlor
Mountlng IwUch
I
Door Switch
c-e
Elletronlal houllng
Start/ltop buttonl
..
s
'
.9
Fault LEDI
,o
Turret
B..e
e.G
','
Syringe Carrlag,
An,mbly
Screw
0515-052.
,AONTVIEW
RIAR VIIW
.,:~.~.,!~~.,::~:""
'I,;",;
Plunger Clrrllr
Auembly
07&73110880
0787360820
Needle
Buppon
Auembly
0767380Q7li
Plunger
Sorlw
0787320li70
Mlgnel Preu.d
Inlo Back
SiniorBOlrd Conn'cUonl
Blak 01 Plunglr Carrier
Showing How 10 POllllon
Millor Clip Assembly
Sollnold Connector
Cln Go On Elth.r Way
c-a
White Samplelnllrl
07673-40226
Turret Magnet
Locatldon \
Bottom Edgl
r
c ..
...... 1;
T
a -
';.,
....
e!!=:a..
"""'IIJ:
:J.(
JD
e!
Ie"
-----...:.~~;;r
Turret A..embly
' f:
... ...
...,
07&13&0505
&
1.00'
c-s
K ...
Door Switch
81U'1.
07&73-15079 ........
0&2406112
Fan A...mbly
35900601120
.... ........
........
....... .
"...
~=-='-
BlckCovlr
,J!)'
07673-400711
~ Screw
0515-0810
Ribbon Clbl.
Cllpi
07173-40170
Syring. Motor
A...mbly
0787a.80580
071732015415
Scr.w
0151G-0637
Hom. S.nlors.t
(Includll Both S.nlorl)
07873105110
\Syring.
C.rrllg.
S.nlor
-L- Br.cket -~~~
-L- Br.cket
Wllb.r
21IlO-04011
1400-02110
Syring. Motor
Scr1 '"\=:::----Ifl.-~.
0I51G-OII10
Turr.t S.nlor
a:~!~~I1~
Hom. Senior
Scr.w
0824-0851
"'"
Turr.t
"'lliID';:O"......-s.nlor
Bonle Stripper
07673-81005
Sleeve Brlcklt
Spring
0767300185
07673-2067$
Berl.
051513D1
/'
Turret
Motor
Blck PlltlIB..I
Anembly
07873-808155
AI..mbly
07173-10810
Turrlt
Motor
Scriwi
0151111380
Fipre
..
InJlctor
Clble Aaaembly
<'
07873-80648
l1I
".
051a.QU24
\... J
Screw
0518-0883
or
07873-89025
Ground Clbll
07873-80838
tit;
80rlw
.~
L~
~jA
.1Y 'F"atP...I
.~
Door
0787....0215
Front Plnll
Baird AUlmbly
07&7310035
Screw
0381).2283
Injector Errors
An error condition is indicated if the red LED on the front panel is lit or flashing. Errors
can be caused by:
Motor failed.
Wiring damaged.
Refer to Section B, "Troubleshooting", to see a full list of error conditions and courses of
action. When the fault is corrected, clear the error by pressing the STOP button on the
injector. ~en restart the sequence.
C-14
Injector Diagnostics
The Injector Diagnostic Mode allows the service engineer to observe the operation of
injector motors and sensors during the troubleshooting process.
CAUTION
The diagnostic mod. overrides the door and mount safety switches. Be sure to
take the syringe out of the Injector before operating It In diagnostic mod. This
mode should only be u..d by a trained service technician.
Starting Ol,agnostlcs
1. Turn off the controller.
2. Simultaneously press the STOP and START buttons on the front of the injector. Keep
pressing;while you turn on the controller.
8. The Red LED should start flashing a double flash, indicating the first test in diagnostic
mode.
Telt
Red LED
Yellow LED
OrlinLED
Syringe Can1age
Two flashes
Turret
Three Rashes
Plunger
Four Rashes
.. "
i'f\~'T,'"
~I'.,
I':~;r
2. Press START to drive the syringe motor one step (2 phases energized).
8. Hold START down to run the syringe motor continuously. Wait about 10 seconds for a
response. Note the LEDs on the injector main board (figure C-ll). They should light in
the following sequence:
DSl
DS2
DS3
D84
ON
ON
OFF
OFF
OFF
ON
ON
ON
OFF
OFF
OFF
OFF
ON
ON
OFF
ON
Turret Test
1. Press START. The turret will go through its homing routine. The motor remains enarpzed for about 10 seconds. The green LED willllght when the turret sensor detects the
turret magnet.
2. Press START again. The turret will rotate and home on the next magnet. If there is
no magnetic bottle insert, the turret will find the original magnet again.
S. Move the turret manually to verifY the sensor trips when the magnet goes by.
4. Press STOP to advance to the plunger carrier test.
C18
Note the LEOs on the injector main board. DSB lights when the I?rocessor is sending a
signal to the plunger motor drive to enable the plunger motor.
DS5 is on except when the plunger motor is stalled. The plunger motor stalls briefly at
the top and bottom of the plunger carrier travel and during the setting of the sample
volume.
2. Manually move the plunger carrier up and down and verify that each sensor trips when
the magnet moves by.
3. Press STOP to return to the syringe carriage test.
C17
False Syringe
Turret Sleeve
Base Plug
These tools are part of the Alignment Tool Kit <HP part number 07673-60950).
Check the syringe carriage, the injector turret, and the turret motor for proper
installation.
Replace the syringe carriage and check alignment again. Repeat this process with
the injector turret and the injector back plate/base assembly if necessary.
C-18
C-19
Baae Plug
0767320820
FII.. Syrlngl
07873-20810
- - - - - - ""M=GlJIi-A'l
Injector BI..
Turrlt Sleevl
0787320800
Turrlt In.ert
07873-40160
T'"~.~_lll""ro---
...i .
..
~ ~
c-eo
a
0 840
I
J1
Il _____1
REV
B
I
J2
IL_____
JI
@!I CR3
oc:::J. R3
@!I CR2
0c:::J e R2
[ill
E!lCR1
0r:::=J. R1
a
0 830
07673-60010
0767360035
1:::9$:::1
~
I:::!!:::I
.....-
J1
'---
READY IN
FROM
CONTROllE
MODULE
TOU23
+
TURRETI~O+-_ _+-+
HOME
TOU32
+5V
J2
+12V
3
TURRET MOTOR
WINDING RESISTANCE
78 0 ..t115% EACH
1
2
II
II
J4
TO
SYRINGE
DRIVER
BLACK
RED/WHITE
RED
WHITE
GREEN
II
4
3
SYRINGE MOTOR
WINDING R8tBTANCE
0.340 j-10% EACH
J5
ON INJECTOR
MAIN BD
+18V
J1
J2
II
PLUNGER
STOP
SOLENOID
PLUNGER
STOP
PLUNGER
MOTOR (+)
TACH (+)
+12V
TACH
PLUNGER
HOME
++
17en
+12%
-25%
PLUNGER
MOTOR
un
+8%
-25%
,D
Controller Module
Section D-Contents
Controller Module Description
D-2
Common Configurations
D-5
Controller Module Block Diagrams
D-6
Control Signals
D-9
Fuses
D-9
Power Supply Usages ........................................ D10
Controller Replacement Parts
D-11
Printed Circuit Board-Component Overlays
D-12
Controller Main Board
D12
HP-IL Board ............................................ D-18
T'rL Board
014
HP 5880A Interface Board
D.15
Standard Controller Board .......................... ~
D-16
TraY Controller Board
D-17
RS-232 Board
D-18
Loop Board ............................... D-19
Bar Code Reader Board ................................... D-20
0-21
HPffi/Controller Board
HP5880A Mainfuune Board
D-22
HP 5880A Dlagnostic Mode
023
01
'''':I'\'''J:'l'~I':'''ll'''I~!''''~'1~I;W:~~~iM\!$Jl'Hnt~~!~~t'''7IIlW''~~~!!I
"I
I,.
Controller Slot
The following boards may be put into the CONTROLLER slot:
Standard Controller
(18594-60060)
(Rebuilt 18594-69060)
Coordinates the tray, the bar code reader, one or two injectors
for INET, stand-alone, "loop," or RS-282 control (see figure D-2).
HP 5880A Interface
(18594-60060)
Hp-m/Controller
(18594-60110)
(Rebuilt 18594-69110)
0-2
Communication Slot
The following boards may be put into the COMM slot:
HP-IL
(18594-60030)
TTL
(18594-60040)
RS-232 .
(18694-60080)
Loop
(18694-60090)
. Auxiliary Slot
The following boards may be put into the AUX slot:
TTL
(18594-60040)
0-3
Tray Slot
If there is a tray module, the tray board (1859460075 or rebuilt 18594~69075) must be in
the TRAY slot to control tray operation. Also, when a tray board is installed, you must have
the tray cable installed.
The main functions of the tray board are reading the status of the. three homing sensors and
the bottle sensor, driving the three stepper motors (Z, R, Theta) in the tray, and communieating with the controller board.
Common Configurations
~UUUUUu
Illij
il'
.-
..-,.
I
iii
~ltu
~UUUUUu
t:;
i!!
.am. ,.
til)
~gi
~I!!:
lID
III
!I! I
I
I
~uuuuuu
..-,.
II
t ij
I. ..... _11
~
~uuuuuu
100
I
I
Vol
II
:
....iMIlIli
.i)
~I~
it!:
I
.~
'2
.I
IlliJ
30
I
t
i
8
1
...G>
1
s:I
i8
~
...!
1:10I
I~:=~
.!)
0-5
,iL,..
0 --
:~
::::::II
Illi
8-
II
QI. IQ.L
I
I
If.Ii 1 i
- - .... - - - - - -
il I Itil
I
I
I
~-
Ifi ..
I
lill
JI
[]
II I
i
'- ......
--
IS
r-
,...
..
0
l .
08
I
I
I
I
I
E IIE'
1.--.
:~:l
:::: -::
11 H
:1:
I
iI
I
g
L~
I~
I
I
f
II
1
1
1
1
1
1
-1- - -
i I
I
'I
......
I-I-I--
-I
1.-- ..
u..
I
l-
--
- -- - - -
_/
[:;..
f-
.. --
I ..i
I
i
I I
u
,"'''I:J'l r:
,:,",,~.~:,
,J'~'.~'l(-~",~~~"~,~~,,,:,I
.'
"
':,'i:\r,~~':'t:""
0
1111.; IIiI I
&;
I;:
I
II
1
II
......
I--
.....I--
f---
10lio----1
1
1
1
1
1
1
1
1
,.-~-----------------
I
I
I
I
I
I
111
III 11 l!t ..
--
I
j I
I
I1
'I
.It
!I
(]I
I
I
I
I
I
I
I
I
14--
~--
II
I
t:
~
:::1:;
El
l
1
\\1::
I!
.
IlI
- ....
I
I
I
I
I
. IL
I
I
l'
;;::;::::::::.
~--
I
i
I II
il
07
0
I!I IIII i
.--- '"
DI
~
"-
if
Iif!
~
c
311
"0
c
II
I
I
I
I
I
I
f--------I
I
I
I
I
I
I
I
I
I
I
I
[]
I
I
Ii l1,1
I
I
I
E:'
.............. .........
'
II II: 11
j
!! -I
:{~~~~~~t:~~~~r~:
II
I
I
I) iilili
I
!I!
.L
....
r--r--r--r---
---------------- ~~---
!!
I--
"
..;.
:-
:f{i)r
.- ...
BIII
.II
~_
...
~--
.,::,,:.:,:':
:'1
I
! I!
I~
I
I
L~
.::;::"
.>
11
in! i i I
I
I
I
I
I II
I I I
I
II
II
ali
"'"
J!
III
I
I
I I
1.---
___________________
I;':'
I~
"
Control Signals
The control signals used between the controller and the injector are:
READY OUT
READY IN
START IN
START OUT
SERIALCOMM
All these signal lines are RS-232 compatible, and they are logically inverted. A logic high at
the injector is seen at the RS-232 line as -12 volts, and a logic low at the injector is seen at
the RS-282 line as + 12 volts.
Fuses
Fuses have been installed at several locations within the instrument for the protection of
major power circuits. They are designed to open as quickly as possible to prevent damage to
other components within the circuit. Occasionally, an opened fuse may have been caused by
a short one-time surge;' however, it is far more common that a component within the protected circuit has failed. When an open fuse is noticed, replace it. If the replacement blows,
suspect a component failure.
The following is a list of the fuses for the automatic sampler.
Reference Designator
Fuse Type
HPP/N
F1, F2
15A
2110-0054
Una Module
100 Une
3.0 A (NTO)
2110-0003
120 nne
2.5A (NTO)
2110-0083
220/240 nna
2A (TO)
2110-0303
POWER
SUPPLIES
.,
.,
+5V
+18V
WHERE
USED
+5V ~
+18V _
SYRINGE MOTOR
PLUNGER MOTOR
PLUNGER SOLENOID
..
+12V _
,
-18'1
~,
ALL m SIGNALS
ALL LED.
18V ..
12V ..
-23V _
~
RMOTOR
ZMOTOR
THETA MOTOR
TURRET MOTOR
THETA SENSOR
PLUNGER MOTOR CTLS RSENSOR
Z8ENSOR
SYRINGE MOTOR
PLUNGER MOTOR
PLUNGER MOTOR CONTROL
SERIAL COMMUNICATIONS
SYRINGE MOTOR CONTROL
BCRMOTOR
BCR SOLENOID
SERIAL COMMUNICATIONS
PLASTIO
OOVER
01Q40-40041
NAME
PLATE
1MG4-001OS
~"
OPTION BOARDS
SORew
1011il
0511
o'
-o.
@l-O_.J--... .
o'
@~
"o.
fI
a
=
Figure D-7. Controller main board (18594-80125).
0-12
~ ~
T2
ocmDO
oamo
T1
11
O[]IJO
oamo
O[]DO
o []DO
0C!!!J0
. O(][]O
O[]i]O
L.....1 O[][]O
OUiJO
OCiLJO
01
O[][]O.
ODO
I~
C1
0[]i]0
oCllJO
1
II
J1
U1
L.....-
10
II
14
,.
o[J!Jo
OCDJO
J2
K2
K1
R20-c::JC2 -e:::JC11
J1
J3
IB~~~~
BB B
U4
r+
B ~I
B
B
o
C4-c::::r
LJ
J3
B
E~
I--
U1
J1
-1
I--
d~:
-e::J- C.
CII
-e:J- CI
~R1B
--c::r R2 U2
I--
i
J2
-e:::r
-e:J-e:J-
C7
CB
CII
C10
OTP1
OTP2
OTP3
OTP4
OTPII
o Tl'1I
OTP7
OlPI
OTPII
OTP10
OTP11
OTP12
0-12
0+12
0+1
0+1
OGND
OOND
I---
<>
Ull
III
~itll~
~+.
U17
---l
J2
12
11
~::
BG~~
J3
'~D
1100
UK
UK
UK
~r
--<=>- CI
~III
IDO
IlIO
.8 ,B .B .B
B
E1
L.....l.
C1
C4--<=>-
CI--<=>-
U1
ce--<=>-
1.
CI--<=>J1
'iD"ii
,1"'"''
'':~~'II""r',' '~.":'1"
J2
111111111 It 11
0000000
1-0
C8
o
.B
: ,:0 ,8
o[l[Jo
o (liJO
,8
Figure-n14. Loop board (1859460090).
0-19
-i:
"J
J3
~ +Q
.
<>
cz
nu
011
011
01
7U
C4 +Cl
n
w
n l-
01. I
014
7U: : : _
80411
1111110 COMM.11)
1111110 COMM. 2)
r~=Cii:l
PABALCOMM.
, ~ ;J ~~~,:~ ,~
D
-11V
0 .
~:l.O'" . ~~ ~ ~:'
- ) TEST ole
FAULTWrrtl
J:.!IY
~U
niT
WID
NOlIlI
rv-J
+IV
.II
<>
Figure D-17. HP 5880A mainframe board (19321-80010).
On the HP 5880A end of the 19321-60010 mainframe board, the communication is done
over the standard MC5 (or MC2) bus. Communications between the HP 5880A control
board and the automatic sampler controller is encoded using + 12V and -12V.
The U44 code includes a system self-test program. The test covers the HP 5880A mainframe board, the cables, and the automatic sampler control board. For the purpose of this
test, the system is divided into 6 sections:
HP 6880A communications
TRAY communications
INJN1 communications
INJJII2 communications
PARALLEL communications
0-23
Each section is tested in sequence. If the test of the first section is successful, the test program proceeds with the second section, and so on. After the fifth section is tested success-
fully, the test LED (DS-1 on the control board) is turned ON for one second, and then the
complete test is repeated. If any of the sections fails the test, a corresponding light pattern
is displayed by the test LED and the failed section is tested again.
To get into the test mode, the followingprocedure needs to be followed.
1. Turn OFF power to both the HP 5880Aand the HP 7673A instruments.
2. Move the "NORMAL/ TEST" Jumper on the HP 5880A mainframe board to the
"TEST" position.
3. Set all switches of Sl on the HP 5880Ainterface board (HP part number 18594.60050)
toTSTMODE.
4. Verity that the cable (HP part number 19321-60510) is connected properly between the
controller and the HP 5880A.
5. Turn the HP 5880A power ON.
6. Check. the test LED on the mainframe board for one of the flashing patterns listed
under "symptom" in Table D2. Follow the corresponding "Action" instroctions to
troubleshoot the failure.
-r
SYMPTOM
ACTION
ACTION
AmON
1. Replace HP 5880A mainframe board
(HP part number 19321-60010)
2. Replace HP 5880A ROM, RAM and processor boards.
Means defective communications between HP 5880A processor and the mainframe board.
SYMPTOM
ACTION
Means defective convnunlcatlon between HP 5880A processor and the mainframe board (bad data).
SYMPTOM
ACTION
Means defective convnunlcatlon In the tray path betWeen HP 5880A Interface board and the HP 5880A
mainframe board.
,'"r,.,
,.
,:,~
"v..
SYMPTOM
ACTION
Means defective communication In the Injector#! path between HP 5880A Interface board and the
HP 5880A mainframe board.
SYMPTOM
ACTION
Means defective communication In the InjectorN2 path between HP 5880A Interlace board and the
HP 5880A mainframe board.
SYMPTOM
ACTION
Means defective communication In the Injector's paraDel paths between HP 5880A Interface board and the
HP 5880A mainframe board.
0-28
E
Tray Module
;
Section E-Contents
Tray Operation .............................................. E-2
Vial Movement Sequence ...................................... E-5
Tray Replacement Parts
~
E-6
Theta-Flex Assembly Procedures
E-12
Tray Errors ................................................ E-18
Tray Diagnostics ............................................ E-14
Printed Circuit Board Component Overlays
E-15
'!'ray Pinout Diagrams
E-16
E-1
Tray Operation
The HP 18596B Tray Module includes four tray quadrants that hold sample vials and a
robotic manipulator that moves the sample vials to and from the injector module and the
bar code reader module.
There are three axes of movement for the tray module:
Tray Quadrants
The tray has four removable quadrants, each of which accommodates 25 sample vials.
Quadrants can be temperature controlled through the use of a circulating water bath. See
the HP 7678 Automatic Sampler Operating Manual for temperature and inlet pressure
specifications.
Tray Electronics
The tray module is controlled by the tray board located in the controller module. The signal
paths for the tray sensors and motors travel through the tray cable and two flex circuits.
The theta-flex circuit rotates within the tray turret. The R-flex circuit moves within the
arm in the R8Jds (figure E-l).
,-------1
r--------------------...//
TRAY ARM 1
-~~~~~
serne
ARM
SENSOR
SENSOR
BOARD
1
~
I1___ __ _ _ _ __ __l-t;;J--------J.~rr
RHOME
__ _
...J IENSOR
I
1
Z-MOTOR
J2
R.fLEX
-----------.
-----1 __
TRAYTUMET
I
I
1
--I
I
I
I
I
THETASENSOR
TRAY BASE
THETAMOTOR
I
RMOTOR
J1
I
(.-~~~~------------------ --~===-(
J4
TRAY CABLE
CONTROLLER
MODULE
E4
J:I;T'I;.'
,0'"
~',
,11,
Operation
The sequence starts when the START button on the front panel is pressed,
or via remote signal from an external controller such as INET.
Homing
Routine
The arm finds its home position for the Z-axis, the R-axis, and the thetaaxis.
Vial Check
If this is a start-up after a sequence interruption, the tray arm checks for
the presence of a sample vial in the gripper, the injector turret, and the bar
code reader (if installed). Ifa vial is found, it is returned to its proper position in the tray. The arm then returns to the home position to begin the
sequence.
Pickup
a Vial
The arm moves on the R-axis to the center row and then rotates on the
theta-axis to the proper angular position. It next moves on the R-axis to
align with the vial. The gripper moves down to the proper height and
rotates to grip the vial's neck. The arm makes small radial adjustments
during pickup to optimize alignment with the vial. The gripper moves up to
the Z-home position to confirm the presence of a vial.
Deliver the
Vial to the
Injector
The arm moves to the middle row on the R-axis then rotates on the thetaaxis to align radially with the iJijector. It moves on the R-axis to the turret
location then rotates on the theta-axis slightly to move the vial over the
sample position in the hUeetor turret. The gripper lowers the vial into the
turret, helped by the cone shape of the sample position. The gripper rotates
to disengage the vial, while the injector turret is stabilized by the needle
support assembly. The motions are then reversed to return the arm to the
home position.
Finish
E-8
QUldrlnt
Turret
Arm
Grlpplr
Gripper Ilwl
Slmpllvlll
TrIYBI..
E-6
ArmAllembly
1868660855
-,
CAUTION
bl elr,M
or elreu" wllltllr.
Do not pull on circuit.
Tee Mlnlfold
SNR 100361
Serl.
.0516-0886
(SII of.)
185n-.uJ016
Smooth Pulley
185118-401011
RFlex Circuli
18&118-80038
Senior BOlrd
1811111-110035
Arm Core/Motor
AllY
181596-110905
Screw
051&-0886
Screw
01115-08117
Screw
051501lU
CAl1TlON
Turret Anembly
1859860515
(Includ81 BUlhlngl)
Radial AlII Homing Magnll
Connector from Thltaoflel Anlmbly
Rod/Arm
1859&20500
<II.
CoRing
0510121&
Eg
,',I,",1~ {;'~j
T",
"".
~f
Screw 05150886
r.
J8
Sari.
0515-0888
Bottom Covlr
11511&.20745
Cotter Pin
1480-0858
Screw
0515-1823
Tbeta-Motor A..ambly
1859&-8OSQ5
CAUTION
Ulllnitanatlontooll
In IIrvlal klL
Sari.
OS15-0894
..-,
1lI111-aanlor
185M-B0830
-.dl
Drain
1859a-C0240
- ~
O-ring
01101-0583 ~
Tray Ball
18511s-&01575
Thrult Walher
14101229 "
EYIlet
03810014
185988087&
~~~~~~!~~~~~~~~~
T.ot-I~..,::o;;;..,
CAUTION
Orllntltlonor thlta-nel
Ixtrlmely Import.ntl
Tbilihouid only be.nembled
by tr.lnld service perlonnel.
(III Inembly D9url E-8.)
~. . ._
ThetlSlnlor
18598-80830
CAUTION'
Thltl.flll Cover
18598-40170
Thet.fI81 An.mbly
18&9&-80040
Turret
18&9880&1$
. ,,"r-: '
J1 Connector
2
Turn the tray base so that the
drain hole Is atthe front.
Thread the J2 connector through
the tray base.
Drain Hola
3
Place the square tab ofthe theta-
Tray Errors
If the red LED on the front panel of the controller is lit or flashing, an error condition is
indicated. Errors can be caused by:
The tray cable not plugged in when the tray board is installed.
Motor failure.
E-13
Tray Diagnostics
The Tray Diagnostics Mode allows the service engineer to observe the operation of tray
motors and sensors during the troubleshooting process.
Follow these steps to take the Tray Module through its Diagnostic tests.
Setup-The gripper moves to the home position (full up) and the Z-LED lights. The B
(Bottle Sensor) LED will also light. The B LED Is lit only when the pper I.
empty and the pper Is In the home position.
5. R-Cycle-The arm moves to the R-home position (full hack) and the R-LED lights.
The arm moves one full cycle (out and back) and the R-LED lights again at home.
6. Theta Cycle-The arm moves out to the center row and rotates counterclockwise to
the stop pin on the theta-axis, then reverses direction and rotates clockwise, again to
the stop pin. The T-LED lights for half of the revolution and is ofT for half the revolution. The arm then rotates back to the theta home position. The T-LED remains lit
throughout the other tests.
7. Z-Cycle-The arm moves forward on the R-axis beyond the edge of the tray. The gripper moves one full cycle (down and up). The Z-LED lights at the top (home position) of
the cycle.
The tray repeats this pattern until the controller is turned ofT. To keep the tray in the same
axis test, insert a vial into the gripper during the desired test. The tray continues to cycle
through the selected axis until the vial is removed or the power is turned ofT. Note that
the B-LED Is not lit while there Ie a vialln the gripper.
E-14
. - 18598B0075
o 0
J1
f
185116-80035
J4
C::'j
o 0
J4 ON REVERSE BIDE
Fllure E-9. Tray termination board (18596-60075) and
. arm sensor board (18596-60035).
E-16
CABLE
1,14
2,15
3
4
15
GND
+12V
RHOME
-& HOME
-& SENSE
8
7
ZC
8
1
10
11
. 12
13
18
17
18
11
20
21
22
23
24
25
1,2
3,4
15
7
1
11
13
115
17
11
21
23
25
8
Z03
201
RD1
R04
-&C
&2
&4
OND
ZHOME
BOTTLE
Z04
202
J3
J1
J4
10
12
14
18
18
20
22
24
RC
R01
Roa
-&01
&03
I
I
,
'I
IARM~ENSOR!O. 1~~
-R- -
FLEX
4
12
3~~
FLEX
J2
3 3
15
7
1
J1
J2::
4
8
88
15
10 10
15~;.;-e
2~~
4
8
--
10
1
7
SENSOR
r-~ - -
OPTICAL
3 t-...IILlI------IIILIIr.IJ.IJ.I.-----J
r--.--_.
-e
JII
12 a ~o.:-__-'l
12 a """"IIQ.III.I:I.-/'
- -J; 3
- -;-
11""'-+----.
I~:rr-"'"
' _ . _ . _ . _ . _2.
E18
i
,
..
r-I
'
I
I
I
I
I
I
I
I
I
1J1
DC
DD
DD
~:~
DID
DD
lID tal
DD
IlIID
25
28
r---------------II ~~
21
12
I1
12
DD
J2
TERM
BOARD
DD
I ~~
I~~I""
D a:D
I I ~~
D 1m I
1 l!ll!l
g 10 I IL. 10
DD
1
TERM
BOARD7
J4 1
TERM
BOARD5
J5
TERM
BOARD
]::
21
2 l!ll!l
--
~ [!][!l
1m 1m
D D
8I
[!][!l
8 [!] ~
[m
D D
l1:lil1:li
D D
2L
'"""------'
2 ~~
~ ~~
81
I [!]~
1
i I~r
~
I [!)
eo
FLEX
FLlX
J1
R
l!l
l!l [!] FLEX
[!][!l
1
,
10 II
1-------
1 eo
MOTOa! II
cONN'10
11"""1-__-----,
1 1 [!J[!]~~[!] II
1 2 1!ll!l1!ll!ll!l1 0
I
J2
a a a a a1
a a a aa2
J1
SENSOR
,BOARD
1 R I
J2
MOTOR
ARM
I CONNI
SENSOR
I
BOARD
&
SENSOR
CONN
&
II 10
I
J3
I~-.II(!)(!)
J1
J2
mm
DD
21
~~
![mDD
FLlX
1-------'
,--------_ ...
DD
II
I.-J......
~~ [!][!J
l!l~
I 2
D D
~ [!]
MOTOR
2 CONN
F
Bar Code Reader Module
The next revision of the Bar Code Reader Service Manual will be in this smaller format.
The current revision is available as HP part number 18587-90120.
F1
r.
~,J~ .', T ::
.: ;
G
Cable Diagrams
SectIon G-Contents
Remote Cables ............................................. G-2
HP 8896A <O3396-60550}
G~2
HP 8892A/8898A (18694-60500)
G-8
HP 5890A (18594-60570)
G-4
HP 5890A/8890A <l8594-60590}
G-5
HP 5700A SeriesJ8890A (18594-60600)
G-6
HP 5890Al18652A (18594-60610)
G-7
HP 5700A Seriesl18662A (18694-60620)
G-8
HP 5700A Series <l8594.6Q680} ............................. G-9
HP 5890Al85900AIB/C (85900-60820)
GlO
BCD Cables ..................................... G11
HP 8896A (08896-60560)
e-n
HP 8392A/3393A (1859460510) ............................ G12
General Purpose <l8594-60520}
G-18
Nelson (19164-60550)
G-14
HP 85900C (8590060850) ................................. G-15
Instrument Cables .................................. G16
Injector Cable (07678-60645)
G-16
Tray Cable (1859B-G07l5)
G17
HP 5880A Control Cable (198216051O)
G-18
G-1
-.
",,' ~
Remote Cables
HP 7873AEND
mr
111r~
PIN#
1
2
3
4
&
e"
a
g
10
11
12
HP 33Q8AEND
m!!=!O!lIO
13- - - - - -
SIGNAL NAME
START IN
GROUND
JMPRTOtM
JMPRTON3
READY OUT
JMPRTO#10
START OUT 1
GROUND
WIRE COLOR
ORANGE
BLACK
BLUE
BLUE
JMPRT018
BROWN
READY IN
WHITE
RED
BROWN
GREEN
BROWN
""----J
PIN #
SIGNAL NAME
1 START OUT 0
3 START IN
&
READY IN
g GROUND
13 START OUT 1
14 READYOUT
15 GROUND
WIRE COLOR
BLACK
GREEN
RED
BROWN
ORANGE
WHITE
DRAIN
HP 7873A END
HP 3392/93 END
12
'J1:"'~i=m..-J-l~---- --L~_
PINN
1
2
15
8
7
8
10
11
12
81GNALNAME
START IN 2
START IN 1
UNUSED
GROUND
READY OUT
JMPRTON10
8TARTOUT1
START OUT 0
WIRE COLOR
ORANGE
BLACK
BLUE
BLUE
RED
BROWN
GREEN
BROWN
JMPRTOft
BROWN
READY IN
WHITE
PINN
15
II
3
10
2
11
9
SIGNAL NAME
GROUND
STARTOUT1
GROUND/START IN0
READY IN
8TARTOUT2
START IN
READY OUT
WIRE COLOR
DRAiN
BLACK
BROWN
RED
ORANGE
GREEN
WHITE
HP 7&73A END
=
111'~
II
HP GaiDA END
11St4-1ll570
~2.1
~121111
2-
NOTE:
3
4
Ii
8
7
8
I
10.
11
12
81GNALNAME
START IN
GROUND
JMPRTOlll4
JMPRTON3
READY OUT 1
JMPR TONtO
START OUT 1
STARIOUTO
READY OUT1
JMPRTOlte
GROUND
READY IN
WIRE COLOR
ORANGE
BLACK
BLUE
BLUE
BROWN
GREEN
BROWN
BROWN
WHITE
PINN
1
2
3
4
Ii
I
7
I
10
11
12
81GNALNAME
STARliN
GROUND
JMPRTO*,
JMPRTON3
READY OUT 1
JMPRTONtO
START OUT 1
START OUT 0
READY OUT 1
JMPRTO'"
GROUND
READY IN
WIRE COLOR
GREEN
BROWN
BLUE
BLUE
WHITE
BROWN
ORANGE
BLACK
BROWN
PIN#,
1
2
3
4
5
I
7
II
10
11
12
SIONALNAME
START IN
GROUND
JMPRTO*,
JMPRTON3 .
READYOUT1
JMPRTON10
8TARTOUT1
START OUT 0
READY OUT 1
JMPRTOA4\
GROUND
READY IN
WiRE COLOR
ORANGE
BLACK
BLUE
BLUE
PIN#,
1
2
3
4
5
BROWN
GREEN
BROWN
II
10
11
12
BROWN
WHITE
SIGNAL NAME
START IN
GROUND
JMPRTON4
JMPRTO-..
READY OUT 1 .
JMPRTON10
BTART OUT 1
START OUT 0
READY OUT 1
JMPRTOfllB
GROUND
IlEADY IN
HP 7873A END
WIRE COLOR
BLUE
RED
BLUE
BLUE
WHITE
BROWN
ORANGE
BLACK
BROWN
HP IiSIlOA END
>
~,211"
-, --s
OO=mJ~.
2
HP 33110AEND
PIN#,
1
2
4
7
8iONALNAME
STARTOUl
ITARTIN1
GROUND
START IN 0
WIRE COLOR
BLUE
GREEN
RED
BROWN
PIN #
1
2
3
6
7
6
II
10
11
12
SIBNAL NAME
START IN 2
OROUND
UNUSED
GROUND
READYOUT1
READY OUT 0
START OUT 1
SlART OUT 0
READY OUT1
START OUT 0
GROUND
READY IN
WIRE COLOR
BROWN
ORANGE
BLACK
PIN#
A
E
E
E
DRAIN
RED
HP 7B73A END
'I:~HI,,"-===-J-'ts111l1UOlOO
-..-__..
SIGNAL NAME
READY OUT 1
READY OUT 0
START IN 0
START IN 1
WIRE COLOR
RED
BROWN
BROWN
GREEN
HP 57XXEND
...
--::.._iC'L--.....~....,~
-; - - -s
OO=I[g1]~.
2
HP USDA END
PIN
1
2
SIGNAL NAME
START OUT 0
STARTING
START OUT 1
START IN 1
WIRE COLOR
8HOWN
BLACK
GREEN
ORANGE
I"":.,,";''''''"
PINN
SIGNAL NAME
START IN
aROUND
JMPRTO#4
JMPRTON3
READY OUT1
JMPRTON10
START OUT 1
B!ABTOUIO
READY OUT 1
JMPRTOfMI
GROUND
READY IN
1
2
3
4
II
8
7
8
g
10
11
12
WIRE COLOR
ORANGE
BLACK
BLUE
BLUE
PINN
1
2
3
4
ri
6
7
I
g
10
11
12
BROWN
GREEN
BROWN
BROWN
WHITE
HP 7673AEND
.2
,,l1If
SIGNAL NAME
START IN
GROUND
JMPRTO#4
JMPRTON3
READY OUT 1
JMPRTON10
START OUT 1
START OUT 0
READYOUT1
JMPRTO_
GBOUND
READY IN
WIRE COLOR
BLUE
RED
BLUE
BLUE
WHITE
BROWN
ORANGE
BLACK
BROWN
HP SlgOA END
GW!J
_o....:.:;=;';':"'J-#
----,... - ---~--'221'"
,... _
NOTE:
Spade lug connection mUltba attached
to ground It the HP 7873A lor proper
operlllon.
SIGNAL NAME
8TARTOUT1
8TARTIN
8TART OUT 0
OROUND
WIRE COLOR
GREEN
BLUE
BROWN
REO
',"\"
PINN
SIGNAL NAME
START IN 1
OROUND
1
2
3
5
READy OUT1
9
11
12
START OUT 1
START OUT 0
READY OUT1
DRAIN
READY IN
e
7
e
:
11'~
WIRE COLOR
GREEN
BROWN
BLUE
GRAY
VIOLET
ORANGE
BLACK
YELLOW
PIN N
B
A
E
E
RED
SIGNAL NAME
STARliN 1
READYOUT
GROUND
START IN 0
WIRE COLOR
ORANOE
RED
BROWN
BLACK
HP87XXEND
I 19t1=!O!2O
2 -
ts-- - - - - - - - - - _ ,
.".~.""".~
HP 7873A END
""".~----
---
,..
r \--CDl-_--liS=.tr~-.... r@
\
,----- I!::
~ =
...,
r@
HP 1ae152A END
PINN
SIGNAL NAME
C GROUND
B
START IN
WIRE COLOR
BROWN
ORANGE
c-a
.'":.'
HP 1673AEND
PINN
2
7
a
11
12
SIGNAL NAME
WIRE COLOR
GROUND/START IN BROWN
START OUT 1
ORANGE
START OUT 0
BLACK
GROUND
DRAIN
READY IN
RED
PINN
A
E
E
B
SIGNAL NAME
READY OUT
START OUT
START IN 0
START IN
WIRE COLOR
RED
BROWN
BLACK
ORANGE
II""
";".'
HP 7673 END
:: .
lB'~
i moo.tOI20
ts - - - -,
2 -
PINN
SIGNAL NAME
1
START IN
2
GROUND
3
JMPRTO#4
4
JMPRTO#3
5
READY OUT1
8
JMPR T0610
7
START OUT 1
8
START OUT 0
9
READY OUT 1
JMPRTOltl8
10
GROUND
11
READY IN
12
3
4
G
8
7
I
9
10
11
12
START IN
GROUND
JMPRTO#4
JMPRTO#3
READY OUT 1
JMPRTOH10
8TARTOUT1
BTABT OUT 0
READY OUT 1
JMPRTO_
GROUND
READY IN
.... _ - -\
,I
II
WIRE COLOR
ORANGE
BLACK
BLUE
BLUE
II
II
PINN
1
5
8
7
BROWN
GREEN
BROWN
SIGNAL NAME
GROUND
.lUITON I/O
paN
~
WIRE COLOR
BROWN/RED
GREEN/BLUE
ORANGE
WHITE/BLACK
BROWN
WHITE
HP 5890 END
WIRE COLOR
BLUE
RED
BLUE
BLUE
WHITE
BROWN
ORANGE
BLACK
BROWN
alOlOa
12
BCD Cables
"
~: ~j--
I:::T--- - - ..
....Q...
PINN
1
2
3
4
fi
8
BIGNALNAME
BCD fi
BCD 7
BCD II
BCD4
BCOO
BCD 3
BCD2
BCOt
GROUND
WIRE COLOR
GREEN
VIOLET
BLUE
YELLOW
BLACK
ORANGE
RED
BROWN
GRAY
HP 338SA END
HP 7873A END
PINN
1
2
3
4
8
II
7
8
I
0
( e
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zr'
(~
(
.'.'.'.'
.:
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SIGNAL NAME'
WIRE COLOR
BCD fi
BCD 7
BCD II
BCD4
BCDO
BCD 3
BCD2
BCOt
GROUND
GREEN
VIOLET
BLUE
YELLOW
BLACK
ORANGE
RED
BROWN
GRAY
HP 71173A END
HP 3392/3393A END
~~~j
16
PINN
5
7
II
4
1
a
2
SIGNAL NAME
BCOD
BC01
BC02
Bcoa
BCD4
BCD 5
BCD II
BCD 7
GROUND
12
1I5M-t0510
WIRE COLOR
BLACK
BROWN
REO
ORANGE
YELLOW
GREEN
BLUE
VIOLET
GRAY
qp----~~PINN
7
4
12
5
9
1D
3
11
1
SIGNAL NAME
8L1
al2
8U
ILl
8M1
8M2
SM4
8MB
GROUND
WIRE COLOR
BLACK
BROWN
RED
ORANGE
YELLOW
GREEN
BLUE
VIOLET
GRAY
HP lOl3AEND
:[{~j.- 1m
15
PINN
1
2
3
4
I
0
1
8
I
15
SIGNAL NAME
BCD I
BCDl
BCD 0
BCD4
BCD 0
BCD 3
BCD 2
BCD 1
GROUND
+5VDC
WIRE COLOR
GREEN
VIOLET
BLUE
YELLOW
BLACK
ORANGE
RED
BROWN
GRAY
WHITE
HP 7673A END
:[~j,
15
NELSON END
.-
11
I~
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.
PINN
&
8
7
I
4
1
3
2
SIGNAL NAME
BCD 0
BCD 1
BCD 2
BCD 3
BCD4
BCD II
BCD 8
BCD7
GROUND
WIRE COLOR
BLACK
BROWN
RED
ORANGE
YELLOW
GREEN
BLUE
VIOLET
GRAY
PINN
1
2
3
4
&
I
7
8
27
SIGNAL NAME
BCD 0
BCD 1
BCD 2
BCDs
BCD 4
BCDS
BCD I
BCD 7
GROUND
....,
'
WIRE COLOR
BLACK
BROWN
RED
ORANGE
YELLOW
GREEN
BLUE
VIOLET
GRAY
-:T'""T""" , ~,!0~~:'!~::'I';P'~"~
, "-'~,,"~,.;~,~:,~\
d~,,~'l""~~",,!,,":,'I-~,~r'
HP 7673 END
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15
ri!'
00
g~
0
1
2
3
4
15
8
7
.lJc
SIONALNAME
BCDli
BCD7
BCDS
BCD4
BCDO
BCD3
BCD2
BCD1
GROUND
NIC
WIRE COLOR
GREEN
VIOLET
BLUE
YELLOW
BLACK
ORANGE
RED
BROWN
GRAY
WHITE
~J
":?'
..
(,"~'(\~
HP 351100C END
Ie ~:>~~~~o~----
PIN#
';.
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0
00
:0
6
g
'---
PIN #
1
2
3
4
II
S
7
8
.lJc
SIONALNAME
GROUND
BCDO
BCD1
BCD2
BCD3
BCD7
BCDI5
BCDS
BCD4
N/C
WIRE COLOR
GRAY
BLACK
BROWN
RED
ORANGE
VIOLET
GREEN
BLUE
YELLOW
WHITE
.1,~,..:'-.':iB";~:~I",~.I:\;::'\""
'I
-.
"
Instrument Cables
21
20
CONTROLlER END
PIN/f SIGNAL NAME
1
2
II'
8
8
10
11
12
13
14
111
115
17
18
18
20
GROUND
+IIV SUPPLY
+18 VSUPPLY
+18 VSUPPLY
18VGROUND
18VGROUND
-18 VSUPPLY
-18 VSUPPLY
POP
POP
SERIAL COMM OUT
SERIAL COMM OUT
5VGROUND
START IN
II V GROUND
START OUT
II VGROUND
READY IN
IIVGROUND
READY OUT
IS
1
7
8
8
10
11
12
13
14
15
11
17
18
111
20
GROUND
+11 VSUPPLY
+11 V8UPPLY
+18VSUPPLY
11VGROUND
18VOROUND
-11 VSUPPLY
-11 V SUPPLY
POP
POP
SERIAL COMM OUT
SERIAL COMM OUT
ISVGROUND
START IN
ISVGROUND
START OUT
SVGROUNO
READY IN
eVGROUND
READY OUT
WIRE COLOR
BLACK
WHITE
BROWN
WHITE
RED
WHITE
ORANGE
WHITE
YELLOW
WHITE
GREEN
WHITE
BLUE
WHITE
VIOLET
WHITE
GRAY
WHITE
BLACK
BROWN
10
t-..cml
PINfi
1
2
3
4
15
7
8
1
10
11
12
13
14
15
18
17
18
11
20
21
22
23
24
215
SIGNAL NAME
GROUND
+12VSUPPLY
R-HOME
mETA-HOME
THETA-SENSE
Z-MOTOR COMMON
Z-MOTOR03
Z-MOTOR 01
R-MOTOR02
R-MOTOR04
mETA-MOTOR
mETA-MOTOR 02
mETA-MOTOR 04
GROUND
+12VSUPPLY
INTERLOCK
Z-HOME
BomE8ENSOR
Z-MOTOR04
ZMOTOR02
R-MOTOR COMMON
RoMOTOR 01
RMOTOR 03
THETAMOTOR 01
mETA-MOTOR 03
PlNfi
1
2
SIGNAL NAME
GROUND
GROUND
3
+12VSUPPLY
4
+12VSUPPLY
5
RHOME
a GROUND
7
THETAHOME
S
ZHOME
mETA-sENSE
10
BOTTLE SENSOR
11
Z-MOTOR COMMON
12 . I-MOTOR04
13
Z-MOTOR03
14
ZMOTOR 02
15
Z-MOTOR01
18
RMOTOR COMMON
17
RoMOTOR 02
R-MOTOR 01
18
11
RMOTOR 04
20
RMOTOR 03
21
mETA-MOTOR COMMON
22
mETA-MOTOR 01
23
THETA-MOTOR 02
24
mETAMOTOR 03
215
THETAMOTOR 04
..
HP 7673A END
:~~J""-"
Hi
PINN
1
2
3
4
5
Ii
7
8
II
10
11
12
13
14
11
SIGNAL NAME
GROUND
GROUND
TRAYXMIT
INJ 1 XMIT
SYS READY 2
INJ 1 RCV
INJ READY 1
INJ READY 2
GROUND
aROUND
GROUND
INJ2XMIT
SYS READY 1
INJ 2RCV
TRAYRCV
1::3
WIRE COLOR
BROWN
RED
ORANGE
YEllOW
GREEN
BLUE
VIOLET
GRAY
WHITE
BLACK
WHITE/BROWN
WHITE/RED
WHITE/ORANGE
WHITE/YELLOW
WH1TE/BLACK
C~]:
PINN
1
2
3
4
1
Ii
7
I
II
10
11
12
13
14
111
SIGNAL NAME
GROUND
GROUND
TRAYXMIT
INJ 1 XMIT
8Y8READY2
INJ1 RCV
INJ RUDY 1
INJ READY 2
GROUND
GROUND
GROUND
INJ 2XMIT
SYS READY 1
INJ 2 RCV
TRAYRCV
15
WIRE COLOR
BROWN
RED
ORANGE
YELLOW
GREEN
BLUE
VIOLET
GRAY
WHITE
BLACK
WHIMROWN
WHITElRED
WHITE/ORANGE
WHITE/YELLOW
WH1TE/BLACK
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Hewl.tt-P.ckard Ltd.
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Tell
(51Q) lI88-Ql111
TorontQ Are.
Hewl.tt-Paokard Oanad.
~d.77
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Ontario
8S1=<u',
L4V 1MB
tel: (4 ~ 818-l143O
.1..:
-83e44
Hewl.tt-P.okard (Oan.d.)
~d.
70 Qu..n.vlew Drlv.
OTTAWA, Ont.rlo
K2B 81(1
T.I: (1113) lI2O-&4l13
~td.
1 V.n An Rd Eut
HANGHAl
.1: 285550
Tel.x: 33571 OHPSB ON
C.bl.: 34111 Shangh.1
COLOMBIA
C... Clentl110aBlanoo y
gl. Sen C
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BOGOTA
T.1: 281-7368, 232~llS
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Hewl.tt-P.ck.rd A/B
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tel: 46 2"'1-8l14
.1. .: 3740Q hp elk
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~&ank.lllonl. 17
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A~ Berthelot
13 1I3 L MUU. Oedex
AlX-EN-PAOVENCE
t . l: 33-4a~Q-4102
.I.x: 41
OF
Quebec/Montr1Ar
Hewl.tt-Paokard (O.n.da)
Ltd.
17600 Tran.-oanad. Hwy
South 8erv1~
Hew1.tt-P.ok.rd I"ranee
~mln dee MouIIlQ
Ite Po.t.l. 1112
8;131 I!!CULLV Cedex
HQJ X8
Tel: (5~ IIQ7-4232
T.'-x:
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P 212 212
44~ NANTES Cedex
T.: (40) ~-22
Telex: 711
FRANC!!!
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Zone lndu.trl.lI. de
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Avenu. de. Trr~.
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T.I.x: 7
12F
Hewlett-P.tard France
L. "'erlpol.
3, Chemin du Plgeonnl... de
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3108 TOULOU8~ Oe<Mx
T.I: ~'~o-' 12
T.I.x:
183QI"
GERMAN FED!!!AAL
A!!!PUBLIC
Hewl.tt-Paokard tmbH
Vertrlebazentrum Itt.
Hewl.tt-p:r~[Mcr
GERMAN ...eDi!!RAL
REPUBLIC
Hewl.tt-P.ckard GmbH
GOh.tt..t~11e
~..eraohm tt.tr.... 7
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t . l: 4Q~731-7O-73-0
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Hewl.tt-Paok.rd GmbH
V.rtrl.b.zentrum A.tlngen
~~.fl."~~&1J~
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.Iexl 052411115 hpmoh
Hewl.tt-P.ck.rd GmbH
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fr~l.all. .
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GREAT SAITAIN
S Unlt.d KIngdom
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G.aoh.tt..t.lI.
Hewl.tt-P.okard A.I!!.
32\ Klfl.., Avenue
T.I: (~~~04-0
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GREECE
Hewl.tt-P.okard GmbH
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R5J7GA
371
Hell.moo
PM'o ~x 111628
1
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Tell 4'104Q
T.lex: 41441
GUAT!!!MALA
1PE8A ~Gfc.tem~l.
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Modem Electronlo
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SINGAPORe
Hawtett-P.okard Slng.pora
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1
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UNITED ARAB
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UNITED STATES
8~AH
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Hourlll~:
am - 6:00 pm
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UNITED KINGDOM
GREAT BRITAIN
ALABAMA
Ltd.
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Tal:
01181
Talax: ea~ ~~..MJM
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H-<IOl57 BASEL
Tal:
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081-881-::-13
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Aa
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fH-8G67 WlOg';N
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TAIWAN
Hewlett-Paokard T.lwan
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th Floor Hawlett-P.okarcl
~"dl~
Hawlett-Paokard Ltd.
~ar Houle
RI~ B~KNELL
~. R 121
al: ('1re~ "2"au
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gTOCKPORT
g~~I0500
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7~710 23<1-oGlll/3
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Cable:
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TRINIDAD. TOBAGO
Oomputer and control. Ltd.
W~ook
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Hewlett-P.okard Ltd.
lu.tomer Sart Cent.
.kd.le Ro
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~ 800tt
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Hawlett-P~kard
V~' . A.
3A
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Hewlett
Pablo ~~ 8.A.O.e.l.
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ARI~ONA
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Compd::-Yt
OAlJl"ORNlA
co. Ltd.
PatllOllll Avenue
64
33
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YUGOSLAVIA
HAWAII
Hewlett-P.okard Oompany
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YU-11
QRAe
T'l: (011) 3<12-&41
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ILUNOIS
Hewla,tt-Paokard Company
l5201 011Yl_ Drl~
ROLLINQ MEADOWS, IL
80008
Tal: (312~
Tal.1 81
-1088
INDIANA
Hawlatt-Paokard
11811 N. Marld~tr. .t
~ARM!L IN 4
al: (317) 844-.tOO
OOrnParlY
IOWA
Hawlatt-Paokard Company
~ft:'wataDrl~
S
MOINES, IA
Tal:
(616) 224-1436
'i1711~-Paokard
'1any
1 76 lnut~ ROt
~DOVER,
01 10
Ta: (817) 862-1l5OO
~leHIQAN
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38l5l5O Orohard HII
_
Dr.
NOVl, MI 4 =
Tal: (313)
200
~NES2TA
latt aokard Company
2026 W. LarPAnttr, Avanua
,T. PAULI MN
lt3
al: (812 144-1100
MISSOURI
Hewlatt-Paokard eomParlY
1001 E. 10t.t Tarraca
SUltalf
KANSA CITY, MO
r.131~
al: ( 18) 841-0.11
Hawlatt-Paokard ComParlY
~~~~~~~tD~
K.l!NTUCKY
Tal:
N. Hur8tbourna
Sulta 100
tOUISVlLLE. KY 40223
al: (602) 428-0100
NI!W JERSIY
=t-PaOkard company
120 C a n E d
~ARAM~S.
07662
al: ( 1) 2
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MASSACHUSeTT~
LOUISIANA
Hawlatt-Pa~ard ~pany
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3701
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.t
BALTIM RE~..ie&227
Tal: (301~
Talex: 71
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Hawlatt-Paok&r'9 Company
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(314) 344-6100
Hawlatt-Paokard ComWy
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SCA A AY NJ 06854
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era.. ~ attica P
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144l5O
al: ( 18) 223-0860
Hawlatt-Paokard Company
rm~e~Blvd.
RPO L,
13011
Tal: (316) 461-1820
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3 ~IW~ Park Wa~t
W
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~NY 1187
Tall (6ltl)
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or.
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al: (1101) 34ll-a370
1
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tt ackard ComparlY
Hewlatt-Paokard Company
44 Vantao- Way
SUlta 180
~AS~E~ 37226
al: (81)
127t
OHO
TEXAS
Hewlatt-Paokard Company
1~ Harwlq{rl~
~ ~ON,
7038
al: ( 13) 778-&400
ie~sF~%J
27420
a: (1 ) M,H800
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1
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~Road
, OH 44138
1)
2~7300
Hawlatt-Paokard ~
0010 S~~o Pika
~18 ~6342
all (613)
OKLAHOMA
Haw\att-Paokard ComParlY
ee66 South L_I.
SUltll06
TlA. A ~. 74138
Tall (gl ) 461-8700
OR!GON
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111 ata rl~
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371132
: (8 ) eee.:.747
Hawlatt-Packard ~cy
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all
(214) 23\-810t
Hawlatt-Paokard Company
1~ ~ral P.rkwalo' 80.
ONIO, TX 76232
all (612) 484-8338
urAH
Hawlatt-Paokard Com8any
~~OO~h
AL
C
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Tall
(601) 874-1700
14 118
VIRGINIA
Haw"tt-P~okard
4306 Cox
cad
Company
~NAU.N
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al: (804) 7~b-
WASHINGTON
Hewlatt..paokrd Company
166115 8.!. 3 th St~t
,e~, WA 88OOl1
at: ( ) ll43-o4OOo4
Wl8T VlRQINIA
Hawlatt..packard Company
mJ3t~~r
. .t WV 25304
L S ON
Tall (304) 826--0482
W180ON~IN
Fli;' HEWLETT
a:~ PACKARD
r"3
HBWLETT
~PACKARD
Manual Part No.
07073-10111
PrIm.d In USA
Printing History
The information contained in this document may be revised without notice.
Heratellerbeschelnlgung
Hiermit wird 6esc:heingt, daB das GerAt/System HP 7673 in Ubereinstimmung
mit den Bestimmungen von Postverfilnung 1046/84 funkentstOrt ist.
Chapter 1. Setting Up
1-2
14
1-7
1-13
1-17
1-24
1-28
Chapter 3. Operation
Preparing Sample Vials ...........................
Using the Injector Fan
Controlling Sample Vial Temperatures
Preparing the Solvent and Waste Bottles.. .
......
Selecting and Installing Syringes ...................
Preparing the Inlet ..............................
Adapting for Cool On-column Injection . . . . . . . . . . . . . .
Setting the Run Parameters. . . . . . . . . . . . . . . . . . . . . . .
Checklist
Running the Samples
Using 1\vo Injectors. . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
nay Control Commands
3-2
3-8
3-10
3-16
3-28
3-34
336
3-37
3-46
3-47
3-50
3-54
PIIIII,r Olrrler
0&0
Plualler butto.
allde
Syrllll' 01111I
Syrall'
For more information on selecting and installing a syringe, see page 3~28.
2-7
HP 3396A Integrator
1. Set the run time to 0.1 minutes by pressing
4.
Turn to page 2~ 12, column two for instructions on setting the run
parameters.
TIU.1 STOP
PUP SEQ
ALS INFOIUlATION
INET SAMPLEI CONTIOL [Y./N];
717 SA SAMPLER;
LOOP ADDU!!;
FRONT INJECTOll
INJ /BOTTLE
2-8
a
a ->
Y.
'CAUTION
Inspecting Syringes
Before installing the syringe.
1. Roll the syringe on the edle of a clean flat surface. If the tip of the needle
seems to follow a circular motion, bend it aliJhtly ncar where it connects to
the syringe barrel and check it apin.
Check for a rough needle. The needle may contain closely spaced
concentric ridges that act_like a miniature me and abrade pieces of the
septum into the inlet. The ridges are easy to see under lOX magnification.
If there are ridges. polish the needle by pulling it through a folded piece of
fine emory paper between you rmger and thumb until the ridges are gone.
Be careful not to modify the special blunt tip of the syringe.
~.
Check for a sticky plunger. Slide the plunger of the syringe up and down a
few times. It should move smoothly-without sticking or binding.
3-28
Installing Syring
After completing this task. check your work with the instructions on page 3-32.
There are three functioning parts to keep in mind.
1.
The syringe is held onto a plastic syringe carrier by metal spring clips.
The needle is supported by a set of plastic jaws at the end of a spring
loaded rod.
The plunger carrier moves the syringe plunger up and down. The carrier
holds the plunger with a "thumb screw.
Open the injector door.
2. Slide the gray loop of the plunger carrier up as faras it will go.
3. Find the black and white plastic needle support jaws.
4. With your fingernail, lift and turn the tab of the upper, white plastic jaw 80
that it swings toward you.
Syrl.g. ollpaltt.clltd
to ayrl.g. CirrI_g.
"
3-30
S.
Position the syringe in front of the metal syringe clips. The top of the
syringe barrel should fit into the guide.
Move the tip of the needle into the notch of the black plastic needle
support Jaw. Uft and close the white plastic jaw around the needle.
8. Loosen the plunger screw about S turns, Slide the gray loop of the plunger
carrier down SO that the plunger button fits into th~ hole of the plunger
carrier. TIghten the plunger screw.
Plaager carrier
Plaager button
C!> Gild.
I
)--,-...,....---,---,---1
Syrlagl ell,.
Syrngl
7}------__..
N_II lappon IIWI
3-31
.........''N
Checking Your Work
Move the gray loop of the plunger carrier up and down. If the syringe
plunger does not move along with the carrier, return to step 8. Be sure the
plunger carrier screw is tight.
Be sure the jaws of the needle support are closed around the needle. Push
up on the bottom of the needle support jaws (compressing the spring). If
the jaws of the needle support do not slide up and down the needle freely,
return to step 4. Also check for flaws on the needle as described in
"Inspecting Syringes" on page 3-29.
Check the alignment of the syringe needle with the cone shaped lead on
the septum nut to ensure an average septum life of 200 injections. Follow
these instructions.
1. Pull down the syringe carriage until the needle tip is near the top of
the inlet's septum retainer nut. Use the plastic tab on the syringe
carriage. Figure 3-24 shows a syringe needle over the septum retainer
nut of a packed inlet.
I~
1If.
Plulglr .crlw
The needle should be centered exactly over the hole in the septum
retainer nut. Use a small light to see that the needle will hit the septum without rubbing on the nut.
3-32
ti
ExpIoded~
,
I
~.
"
oo
'(
0l
1',
~'
[tZZZZ77ZZZZ711~
Il~~ .
'~
1
/ !
3 standoffs (18597-20710)
(Drawn fLt seas )
I
1 tray bl'acket (18597-00135-1)
r-::
r.!
,-
~~
g..
>-
...
~:
-c
i
r
d. Push the mounting supports you installed in step 1 so they are flush
against the left side panel
;.
e.
Line up the hole on the far side of the bracket Qabeled 5890) with the
threaded hole of the rear mounting support. Screw one pan head screw
into the mounting support with a No.2 Point Pozidriv.
f.
Line up the hole on the near side of the bracket Oabeled 5890) with the
threaded hole of the front mounting support. Screw one flat head screw
into the mounting support with a No.2 Point Pozidriv.
[,
~'.
b. H the top of the standoff's do not line up with the holes labeled with the
letter A, check the location of the standoffs against figure 2 on page 5.
~C',
c.
Using a No.2 Point Pozidriv, screw in the three pan head screws
through the holes labeled A and into the standoffs.
i.\
g. Tighten the four screws that attach the mounting supports to the side
of the flow panel.
1:.~_.,
f'
~.
r
~~:::
f,
r-
r:
~'
i~
.".
'."~ .'
o-:
a.
;~
Screw the three standoffs (hexagonal posts) into the injector mounting
bracket. Use the holes identified in figure 2. Hyou do not use the
correct holes, the tray will not be able to deliver sample vials to the
;:$
.j~..:~.
.~..
injector.
'.
The three screws that attach the tray bracket to the standoffs on the
injector bracket must go through the holes labeled A on the tray
bracket.
~-:.;
..~
j
-~
To mount the tray on the bracket and connect the cable to the controller,
see chapter 1 of the operating manual "Setting Up."
~I
, -I
.,~
-::.~
'~
""
.:.;
':1
~~
--;~
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--;,
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;:..-.
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a.
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Using a No.2 Point Pozidriv, attach the two bracket supports to the
flow panel on the left-hand side of the GC. Do not tighten the screws
until the end of step 3.
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Pull out the yellow worksheet from the center of this guide, Organize the
hardware and tools for each step. Full-scale drawings of the screws help
identify which ones you need for each step. If any of the hardware is
missing, contact your HP representative.
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Before you install the tray bracket, you must do the following:
Install the split top cover for the HP 5890 SERIES II Gas
Chromatograph (Kit No. 07673-61 (65) (only if installing onto an
HP 5890AGas Chromatograph).
Install the left side panel (Part No. 05890-61480) for the HP 5890
SERIES II Gas Chromatograph (only if not already installed). You can
also install the bracket on the support rails.
Ii
I
After you have completed the installation, place this link manual in the
binder of your operating manual for the HP 7673 Automatic Sampler
(Part No. 07673-60995) after the tab for appendix C "Link. Manuals."
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Link
Manual
~PACKARD
Printed fn U.S.A.
October 1989
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.ctZ77777777ZZZ}tD
3 standoffs (18597-2071.0)
(Drawn fIJ scale )
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((
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J:-
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2 ~ standoffs (18597-20755)
( Inwn U scale )
b)-
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4 pal head screws (0515-0915)
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1lis wor1<sheet is for Ilsta1ilg the ITlOlIlti1g bracket for the HP 18593B In;ector
ModLie and the HP 18596B Tray MCKUe to CI1 HP 5880A Gas ChrornatDgaJtl.
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Referring to the figure below, connect the HP 5880A control cable to the
rear of the HP 5880A and the rear of the controller. This control cable is
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the only controlling cable needed, whether one or two injectors are
installed.
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Operation
This section contains operating information for the automatic sampler,
including:
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wID a Tray
{
19321~111
...
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20
21
,
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When using the HP 5880A, do not use sample inserts in the turret.
d. Directly above the selected slot, install the plastic board guide (notched
end a'WRy from you) inthe roof of the card cage.
When the tray is installed, all sample vials are loaded into the tray, and the
sample position in the injector turret is left empty. WIthout a tray you can
only ron one sample at a time by placing it in the turret's sample position.
e.
Install the lower board guide, J2 connector, and ribbon cable assembly.
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---';~
c~
':;~
-',",
.-~~
Attach the lower board guide to the card cage with the pan-head screws.
'.,
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,~
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List the parameters stored in the auto sequence table for the front injector
from terminal 11 by pressing
EJ~rn
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tile uameplale
-~-.~
-~
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INJECTOR 1:
o. MODE (O=NORMAL. I=ON COLUMN) = 0
1. PRE-INJECTION SAMPLE WASHES = 2
2. VISCOSITY = 0
3. SAMPLE PUMPS = 6
4. SAMPLE VOLUME = 1
5. POST-INJECTIOff SOLVENT A WASHES .. 2
6. POST-INJECTION SOLVENT B WASHES = 2
7. INJECTIONS PER BOTTLE 1
8. FIRST BOTTLE = 1
9. LAST BOTTLE = 1
- "'J
RMU'ODd lUlu
IIwer IM1I gIHts
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22
w_
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h.
j.
Replace the blank key caps from the terminal keyboard with the AUTO
SEQ keycaps in this kit.
19
~"
,
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:;....
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~.
a. Select a slot in the card cage for the sampler board. You can use slots
9,10,11, or 12. Ifan HP767ln2A board is installed, it must be
e,~
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removed
b.
;-;...
~.
Remove the boards between the selected slot and the back of the GC.
As each board is removed, record its location so that it can be placed in
c.
~.
(wg) CD c::::J CD
rn
~-
~
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rn
For example, to set the sample volume parameter for the front injector to 2,
press these keys on terminalll
'-'"
nlue of ]
[ paramettr
Q)
RHIne
You can change a parameter in the auto sequence table for either injector
from the same terminal. Indicate the number of the injector, the number of
the parameter, and the value of the parameter by pressing
8
-:
11110
[iII#]1 wg I
[~....l
c::::J
[.=rl
rn
Injector #1 is the front injector and injector 112 the rear injector.
If you do not enter an injector number, the edit affects the auto sequence
table associated with the terminal you are using. Terminal #1 controls the
front injector (Il) and terminal 12 controls the rear injector (#2).
i.
The [mj II may be 3; "3" indicates that you want simultaneous injections
(i.e., front and rear injectors inject at the same time).
@
For more information on simultaneous injection see "SYNC Mode" on
page 28.
...
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..."
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18
23
~~
Description of Parameters
O. INJECTION MODE: Specifies whether the injector is in the normal or
on-column injection mode. The on-column injection mode is used with cool
on-column inlets. For the on-column injection mode, the injector changes
the injection speed to 500 milliseconds and lowers the tip of the syringe
needle an additional 19 mm (814 inch) to the column.
b.
Remove the ROM board (part number 19300-60155) from slot 2 of the
HP 5880A card cage.
e.
Set to "0" for normal injection mode. Use this setting with packed and
capillary inlets.
-i
Replace the group 4 EPROMs Oabeled G4L and G4R) with the EPROMs
in this kit according to the follOwing table and illustration. The table
shows which EPROMs are in each accessory and whether they go into
the left or right position.
Accessory Number
HP 19321A
HP 19321B
HP 19321C
Left (G4W
19300-80070
19300-80090
193DO-80110
..;.::
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Right (G4ID
19321-80080
19321-80100
19321-80120
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Replace
...
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'i.so
L'-
24
17
~-
~-
0"
~;--"--
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This section explains how to upgrade the EPROMs on the ROM board and
how to install the sampler board to the GC.
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CAUTION
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CAUTION
WARf\;ING
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CAUTION
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16
25
3 ~.'r.~
9. LAST BOTTLE: Specifies the tray or injector turret position of the last
sample vial. Tray values range from 1 to 100. Injector turret value is l.
This parameter may be a BASIC variable.
An empty bottle position between the FIRST BOTrLE and the LAST
BOTTLE parameters will be interpreted as an error, and the sequence will
abort.
.'
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Double-check. the following:
Be sure. the new septum nutts) and dummy septum nutfs) are installed
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properly.
Be sure the three screws that attach the tray bracket to the standoffs
.,.:.~
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-1
(ST",") [~:,o)
bracket.
rn.
[ST",")(~ )8
.c;
o Be sure the flat head screw for attaching the tray bracket is in the
correct position. See page 14-
rn.
All
see chapter 1,
.~
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After you have completed the installation, place this Link Manual in the
binder of your Operating Manual for the HP 7673 Automatic Sampler
(part number 07678-60995) after the tab for appendix C "Link. Manuals."
c.,
You can override the parameters in the auto sequence table for FIRST
BOTTLE and LAST BOTTLE. The following example starts a sequence for
sample vials in tray positions 6 through 26 using the injector associated
with the terminal you use.
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26
15
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b.
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d.
Line up the hole on the rear of the bracket Oabeled 5880) with the
threaded hole of the tray bracket support. Screw one pan-head screw
into the mounting support with a ne. 2 point Pozidriv.
e.
lfthe top of the standoff's do not line up with the holes labeled with the
letter B, check the location of the standoffs against the figure on
page 12.
c.
!""..
t.r.
Place the tray bracket on the mounting supports and the standoffs
installed in steps 1 and 2. The top of the standoffs should fit into the
holes labeled with the letter B on the tray bracket.
Line up the hole on the front of the bracket (labeled 5880) with the
threaded hole of the tray bracket support. Screw one flathead screw
into the mounting support with a no. 2 point Pozidriv.
Stopping a Sequence
To slop ron, press ( STOP
)( We? I
rn.
This command can be used at any time. The run in progress is completed,
and no further injections are made. The command must be entered on the
same terminal or channel that you started the sequence.
Single Sample
With a tray installed, you can interrupt a sequence and run a single sample
from the turret of an injector by the following procedure.
1.
Note the sample vial number currently running and interrupt the
sequence by pressing
iI:-:". ~
!J-:
(STOP I(We?
~~
~-
2.
rn.
Change any run parameters using the EDIT SEQ keys explained on
page x,
3.
4.
FIaIbeatIICI'IW
(STAAT)( We? )8
5.
rn.
Reset the run parameters for the sequence you interrupted, including
the FIRST BO'ITLE, and restart the sequence.
14
27
1."il
-..0:;
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,;~
~~
SYNC Mode
-.,~
-~~
Using a no. 2 point Pozidriv, remove the two screws that hold on the
panel on the left-hand side of the GC. Remove the side panel
"
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b.
For these types of applications. the SYNC feature must be turned "ON" by
pressing
.jj
Position the new side panel (part number 19300-01260) and attach it
with two short standoffs (part number 18597-20745). Tighten them
with a 318-in. crescent wrench.
.~
-~4
c. Using a no. 2 point Pozidriv, attach the tray bracket support with two
pan-head screws.
When using an oven temperature program, enter the parameters for each
injector from its own terminal. Also set the SYNC feature to "ON" on both
terminals.
If the injector bracket is installed over the A and C inlets, use the rear
set of holes.
'1
.~.-~
If the injector bracket is installed over the B and D inlets, use the
front set of holes.
-
-~
~~~
Start the synchronous sequences from the terminal associated with the
greater number of runs by pressing
(START) GO ('Wa' )
rn.
Rear IIoIes
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DIIIctor
aaaanel2
28
Detector
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13
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CAUTION
a. Screw the three standoffs (part number 18597-20710) into the injector
mounting bracket. Use the holes identified in the illustration. lfyou do
not use the correct holes, the tray will not be able to deliver sample
vials to the injector.
"l
~,
~~
If you start the sequence from the termlnal associated with the
smaller number of runs, the excess runs will not be performed.
The following illustration shows splitting a sample and using two columns
and two detectors to analyze it. The signal from each detector goes to a
different terminal The terminals must be synchronized so that they start
at the same time.
Onl
CU11e11
DItecttr
I
CU11De12
['
Deteder
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CAUTION
(~
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For more information regarding the use of SYNC, consult the ttHP 5880A
Instrument Manual."
~.
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12
29
=.
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..~~
-c".=;
~
0:.-;
c~
l!
This example illustrates how to do a sequence of runs using the tray and the
front injector.
The following terminal display shows editing five parameters of the auto
sequence table. These parameters tell the GC that:
b.
~o--~}
.~
..';1
...~
. 1.. i
Screw each mounting post clockwise into the threaded holes of the
bracket. Tighten the posts with a flathead screwdriver.
;~'"
If you are installing the tray bracket, continue on the next page.
-.
<~
\~
If you are not installing the tray bracket, turn to page 15.
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20
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30
='~
INJECTOR 1:
O. MODE CD-NORMAL. 1=ON COLUMN} = 0
1. PRE-INJECTION SAMPLE WASHES = 2
2. VISCOSITY = 0
3. SAMPLE PUMPS = 4
4. SAMPLE VOLUME m 1
5. POST-INJECTION SOLVENT A WASHES = 2
6. POST-INJECTION SOLVENT B WASHES = 2
7. INJECTIONS PER BOTTLE = 3
8. FIRST BOTTLE = 20
9. lAST BOTTLE = 25
~~
.~;~
11
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~-
Load the six sample bottles into the tray positions 20 through 25. The
instrument wiD make 18 runs (three runs for each of the six vials).
a. Attach new septum nuts (part number 19243-605(0) on the packed and
on-eolumn inlets that are being used with the automatic sampler. Do
not place septum nuts on the inlets that are not being used.
H the GC has a eapi11sry inlet, route the gas lines on the inlet nut
over the mounting bracket. Push the inlet nut down and turn it clock.wise. Tighten it with the inlet wrench.
it
The gas lines must not interfere with the feet of the injector. Small
white circles on the bracket show where the injector feet touch the
brackeL H necessary, gently bend the gas lines so they do not cross the
white circles.
it>
".
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b.
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;
,.
c.
Place the plastic alignment toolls), honeycomb side up, over the inlet(s)
of your GC. Move the bracket until both alignment tools fit flush on
the bracket. Hyoo cannot make them fit flush by moving the bracket,
you may have to adjust the position of the inlets.
'\
~I
00.
Tighten the four screws that hold down the brack.etwith a no. 2 point
Pozidriv. Remove and save the alignment tools for future adjustments.
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10
31
b.
OterI
DeItc10r
---,:;j
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4
~I
The injector mounting bracket enables you to mount two injectors over
nonadjacent inlets-either A and C positions or B and D positions. Decide which positions you need.
C~m111
-,j1
Line up the top of the standoffs with the slots on the bracket. Screw the
pan-head screws into the threaded holes of the standoffs. Do not
tighten the screws until step 5.
-::~
5i
.~
-~
When installing the bracket over the A and C positions, use only three
screws.
Detector
posltlu BauD
This requires the SYNC mode to be turned OFF on both terminals. Press-
li!IlMiil (~)
Gl*l
rn
i
-~
i.
.,
""~
on both terminals.
.il
~~:~
The sequence for the front injector requires the same ron parameters as in
the first example, except each vial is ron only once (one injection per vial).
From the terminal controlling the front injector, edit INJECTIONS PER
BOTl'LE to "1."
;1
.~;:.-'-~
Enter the necessary changes to the rear injector on the terminal for
channel 2. The sample vials for the rear injector are in tray positions 5
through 15.
- -
.... ............
.
~-
,r' .
f~
;~-~
-~#
- --~
32
.:~
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c~
The following illustration shows the editing commands and the auto
sequence tables for both injectors.
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If
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8
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INJECTOR 1:
00 MODE (O=NORMAL. l=ON COLUMN) = 0
1. PRE-INJECTION SAMPLE WASHES = 2
2. VISCOSITY = 0
3. SAMPLE PUMPS = 4
4. SAMPLE VOLUME = 1
5. POST-INJECTION SOLVENT A WASHES
6. POST-INJECTION SOLVENT B WASHES =
70 INJECTIONS PER BOTTLE = 1
80 FIRST BOTTLE = 20
9. lAST BOTTLE = 25
INJECTOR 2:
O. MODE (O=NORMAL. l=ON COLUMN) = 0
1. PRE-INJECTION SAMPLE WASHES'" 2
2. VISCOSITY = 0
3. SAMPlE PUMPS 4
40 SAMPLE VOLUME = 1
5. POST-INJECTION SOLVENT A WASHES = 2
6. POST-INJECTION SOLVENT B WASHES 2
70 INJECTIONS PER BOTTLE = 1
80 FI RST BOTTLE '" 5
IL..-- 9. LAST BOTTLE'" 15
----'
33
Load the seventeen sample bottles into the tray positions 5 through 15 and
20 through 25. The instrument will make 17 runs (one run for each vial).
b.
. . B
~-
'i
;~
- .~~~
r-J"l
Start the sequence for the front injector from the terminal controlling the
front injector by pressing
(OT_I( ~:n
rn
>f-
-;/
Start the sequence for the front injector from the terminal controlling the
front injector by pressing the same keys.
~~
.?
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~~
;1
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1
_-_ci,
"
Save any standoffs you do not use for future adjustments or different
configurations.
34
-: .--",..1
~~
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~~
a.
f~
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~.
Remove the screws that hold down the inlets with a no. 2 point
Pozidriv.
!
~.'
Error Messages
Depending on circumstances, the HP 5880A may print an error message on
its terminal to indicate a fault condition or certain occurrences in
communications. The following is a list of these messages and a brief
definition of their meaning:
..*
~.
~.
ERROR
*..
The START or STOP button on injector 2 (or 1) bas been pushed. but
no channe12 (or 1) has been configured in the instrument (no
integrator/plotter 2 or 1).
J'- .
~~-
~'
~
,~'
17
1'-
t.
A START 1 (or 3) AUTO SEQ command has been attempted either with
no injector on channel 1, or with the power controller turned off.
The auto sequence calls for a bottle (Jf) in the tray. but there is none in
the requested position.
35
-(1
9':
,~
.**
ERROR
**.
.~
**.
**.
'~
Install the right cover (part number 19324-00(70) with two pan-head
screws.
FAILURE
~,
b. It the GC has a capillary inlet lightfs), remove the light and attach it to
the new lamp holder (part number 19321..()()()B(). Disconnect wires and
route them through the tie wraps where necessary,
_:i!l
ERROR TRAY
':t!
"_-
--<:-.-"
'
.
.
c. Attach the lamp holder and the left cover (part number 19321-0(010)
with two pan-head screws.
:;.-.
-:.-~~
..
i
.~
The tray arm is attempting to move a bottle from the injector back to a
tray position that currently contains a bottle.
.:
.1.
.- ~~
'II
I
I~
,'"
~ 11I1111111111111I11I11111I11I111I11111111111I
36
1111111111
a. 11I11
5
WARNING
~.'
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CAUTION
~
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=
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~~
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~:.
1. Remove the ExIsting Top Cover, Side Panel, and Septum Nuts.
a
7<.-_
~.
!<c.
Using a no. 2 point Pozidriv, remove the top cover and left side panel of
theGC.
c. For capillary inlets, loosen the inlet nut with the inlet wrench. Turn the
nut counterclockwise until it is off the threads and lift it out of the way.
CAUTION
Tum off the gas flows before you remove the Inlet nut to &voId
damaging the pecklng In the Inlet liner. Avoid contaminating the
Inlet while" I, uncovered. The braze joints that hold the ga9
nnes to the Inlet are fragne.
~:
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-~
2
Installing the Brackets
'"
'~
Pull out the yellow.worksheet from the. center of this link manual. Use this
worksheet to organize the hardware and tools for each step. Full-scale
drawings of the screws help identify which ones you need for each step. If
you do not use the worksheet for this complex task, you may not be able to
complete the instaIlation successfuIly.
~.: ".~-"
-~I
':d
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Step by step
~ ~.
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...;1,........
2 ........... c.r
--
-....-
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i
...........
1 ........ 0= . . . . . .
r-w
1........ . . . . - . - . .
5;c
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Optien IIIIlber
1932tA
193218
19321C
Support" featanl
ALS,loop, DlA.
V<rNe Driver, sec,
ald DC!
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Old EPROMI
1818-3119
1818-3120
1818-3121
1818-3122
19335-8001 0
19335-80015
NewEPROMs
19300-80070
19300-80080
19300-8000O
19300-801 00
19300-80110
19300-80120
Sample diagrams for connecting the cables for the automatic sampler to
an HP 5880A GC. Turn to page 20.
General operating instructions for using the automatic sampler with the
HP 5880A GC. Turn to page 21.
Common error messages. Turn to page 35.
@
~,
~~-_~r-._~?~i~~~~it~!:#:&0l1i$&~*)
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. HEWLETT-PACKARD .~
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Unk
Manual
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\
~HEWLETT
~PACKARD
PrInted In U.S.A.
April 1990
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7
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Exploded diagcrn
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til~""l2ii}e
3 standoffs (18597-20520)
00
1/4-i'1. ru ckiver
i1etwrench
~.
~
No.2 Pm Pozkiriv
2 aIigi. nent tools (18597-40030)
~:
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F,
c,
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a. Hold the bracket with the bend on the left side and slide it onto the cylinders that you attached to the side wall in step 1. Allow the bracket to
rest on top of the standoffs.
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a.
Route the gas lines on the inlet nut over the mounting bracket. For
most configurations, the gas lines should be routed over the front or
rear of the bracket.
The gas lines must not interfere with the feet of the injector. Small
white circles on the bracket show where the injector feet touch the
bracket. H necessary, gently bend the gas lines so they do not cross the
white circles.
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b.
Push the inlet nut down and turn it clockwise. Tighten it with the inlet
wrench.
F)
b.
Line up the top of the standoffs with the hole and slot on the bracket.
Screw the pan head SCI'eVr'S into the threaded holes of the standoffs. Do
not tighten the screws until step 5.
t1
Figure 7. Route the gas lines over the bracket and reattach the inlet
nut.
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._~
Place the plastic alignment toolfs), honeycombed side up, over the inletts) of your GC. Move the bracket until both alignment tools fit flush
on the bracket. Hyou cannot make them fit flush by moving the
bracket, you may have to adjust the position of the inlets.
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For a splitlsplitless inlet, route the gas lines over the bracket. If you do
not, you cannot replace the inlet liner without removing the bracket.
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b. Tighten the two screws that hold down the bracket with a No.2 point
Pozidriv. Remove and save the bracket alignment tools for future
adjustments.
CAUTION
'
Turn off the gas flows before you remove the inlet nut or you
may damage the packing In the inlet liner. Avoid contaminating
the Inlet while It Is uncovered.
a.
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Loosen the inlet nut with the inlet wrench. Turn the nut counterclockwise until it is off the threads and lift it out of the way. The braze joints
that hold the gas lines to the inlet are fragile.
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Figure 8.
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base assembly
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Figure 4. Detach the inlet nut and lift it out of the way.
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Screw one standoff onto the bottom of the mounting bracket to act as a
support leg. The hole has a silver-colored pem (small threaded washer)
on the top, right-hand side of the bracket. Tighten the standoff with a
1/4-in. nut driver.
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d. Screw two of the standoffs (small hexagonal posts) into the threaded
holes located near the inlets. Tighten them with a 1I4-in. nut driver.
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replaced the cooling tower with the septum nut base assembly.
If gas lines are routed over the bracket, be sure the lines are not near
the white circles.
Self-tapping screws.
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If you are installing a tray, install the tray bracket before mounting the
injector.
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a. Remove the port pan by inserting a finger into the U-shaped cut on the
panel and pulling up.
b.
c.
Using a 1/4-in. nut driver and the two self-tapping screws, attach the
two small cylinders onto the left side wall of the chromatograph.
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!NET and REMOTE cable connections are located under the right top panel
of the HP 5890. Other connections, such as the RS-232-C connector, are
found on the back.
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Remote connector
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FilUre 10. Signal cable connections.
13
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Pull out the yellow worksheet from the center of this link manual. Organize
the hardware and tools for each step. Full-scale drawings of the screws help
identify which ones you need for each step. ITany of the hardware is
missing, contact your HP representative.
A Simple INET Loop
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Sample diagrams for connecting the cables for the automatic sampler to
the lIP 5890 Gas Chromatographs (GCs).
Before installing the injector mounting bracket on an. HP 5890A, you must
first install the split top cover for the HP 5890 SERIES IT Gas
Chromatograph.
t~
WARNING
Allow the inlets and oven to cool before InstaJllng the injector
mounting bracket. The metal surfaces of the GC are very hot
and could bum your skin. If you have a split/splitless
Injection port, you could damage the column.
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After you have completed the installation, place this link manual in the
binder of your operating manual for the HP 7673 Automatic Sampler
(Part No. 07673-60995) after the tab for appendix C "Link Manuals."
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Figure 12. Cable connections for a dual injector system using INET.
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October 1989
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Item
1
Description
Part No.
QTY
ControllerlHP-IB Board
HP-IB Cable
M3 Screws
T#6 Washers
Bezel, Blank
Bezel. Blank
18594-60110
8120-4654
0515-0912
2190-0065
18594-00115
18594-00116
1
1
6
6
2
2
Item
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Description
Part No.
QTY
RS-232-e Board
Controller EPROM
Controller Board
RS-232-e Manual
18594-60080
18594-8NNNN
18594-60060
18594-90300
1
1*
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1
Included in HP 18599R kit only. NNNN indicates the last four digits of the
part number for most recent EPROM.
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Description
Part No.
Loop Board
Controller EPROM
Loop .y" Cable
Controller Board
18594-60090
18594-8NNNN
18594-60650
18594-60060
Included in 18599L kit only. NNNN indicates the last four digits of the
part number for most recent EPROM .
Item
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1
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1
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Description
Part No.
QTY
18594-60075
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Set the HP-IB address switches on the rear panel as shown in the following
illustration. The address should be unique for each instnunent.
Board
.
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In the illustration the example switches on the right are set to address 8.
This is the usual address for the first automatic sampler connected to a
ChemStation. For an additional automatic sampler, choose any unused
address.
an
Select
address from 1 to 29
Must be different Ihan aD other
Instrument HP-IB addresses.
Address
SwItches
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This section includes information for configuring the board with either a
ChemStation or Lab Automation System, for connecting the cables, and for
interpreting the turn-on behavior of the controller when the HB-IB board
is installed.
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CD
The following illustration shows the location of the address switches on the
controllerlHP-IB board. Configure the board for either a ChemStation or a
Lab Automation System with the fonowing instructions. Be sure to
properly ground yourself to eliminate any static discharge problems.
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Iddms IWIcIIn
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2
3
4
7
8
9
10
11
12
13
14
15
16
17
1.
1.
20
21
22
23
24
25
2&
27
28
29
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0oo
00001
80010
00111
10100
00101
00110
00111
01000
01001
11010
01011
01100
01101
01110
01111
1eooo
10001
10010
10011
10100
10101
10110
10111
11000
11001
11010
11011
11100
11101
12
Remove the plastic cap from the connector on the back of the
ControllerlHP-IB board. Save it for later use.
.~
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For Use With an HP 3350 Lab Automation System (A series only)
When configuring for use with a Lab Automation System, you must
configure the HP-ill and RS-232-C boards.
This configuration requires an lIP 35900B Dual Channel Interface. The
model designation is on the Serial Number plate on the rear panel.
.~
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Connecting Cables
1. Plug the tray cable into the connector of the tray board in the left-hand
slot on the back panel of the controller.
2. Secure the plug to the connector with a small flathead screwdriver.
Jmper
2.
If any of the following are true, the controller board is not compatible with
the tray board. Contact you HP representative to order the necessary part.
;!~~
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Set the HP-IB address switches on the rear of the HP-ill board to
address 8 as shown in the following illustration.
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Install the RS-232-C Interface board in the COMM slot and the HP-ffi
board. in the CONTROLLER slot. Leave the plastic cap on the HP-ffi
connector.
14
11
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tTray Board
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For information on mounting and operating the tray, see the automatic
sampler operating manual. For A modules, see part number" 07673-60990.
For B modules, see part number 07673-60995.
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Connecting Cables
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The tray board you received with this accessory must be able to
communicate with the controller board. There are a few cases where the
controller board must be modified.
Locate the board in the slot labeled C?~~R. If any of the following
are true, turn back to page 6 and continue installing the tray board.
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DualCbameI
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Turn-on Behavior
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For instructions, turn to the page for the board you are adding.
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The red fault light also flashes to indicate problems with the tray board. If
the tray board is installed but the ~ is not attached, the red light turns
on and remains on. This prevents seeing any of the diagnostic flashes from
the controllerffiP-m board.
16
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Tray Board
~,
18594-60075
"
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ControDer Slot
Connectors
RS-232-C Board
TRAY
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CONTROlLER
COnroIerIHP-IB Board
18594-60110
1-
COMM
RS-232-e Board
18594-60080
LoopBoa-d
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18594-60090
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588CA ComTuicatioos
Board 18594-60050
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18594-903(0).
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For initial operation information, see section 2 of the "HP 7673 Automatic
Sampler with RS-232-C Serial Interface Manual" (part number
1.
CONTROLLER
Bald rate set tI !I6GO
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IHET Board
18594-60030
co .- , .
mBoard
18594-60040
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AUX
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IF NNN is less than 120, remove the board in the CONTROLLER slot
and lay it on a flat surface.
e.
d. Turn back to page 6, remove any board or blank bezel from the
COMM slot, and install the RS-232-C board in the COMM slot.
3. Remove the board in the CONTROLLER slot. Install the controller
board (18594-60060) provided in the kit in the CONTROLLER slot.
B
SlIt
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Tum back to page 6, remove any board or blank. bezel from the COMM
slot, and install the RS-232-C board in the COMM slot.
18
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3. Configure the Board(s)
For instructions, turn to the page for the option board you are adding.
For the tray board, turn to page 10.
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Loop Board
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a. Determine in which slot the option board belongs from the table on
page 8. If there is a board or blank bezel (i.e., metal plate or cover) in
the slot, remove it.
b. Line up the tab and plug(s) on the bottom edge of the board with the
slot and eonnectorfs) on the base or the controller. Press the board
gently into place.
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d. Using a No. 1 Point Pozidriv, attach the boards bezel to the back of the
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d. To be sure the front bezeltab is seated, wiggle the bezel back. and forth
with the tip of your fingers while pressing down on the board.
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IF NNN is less than 120, remove the board in the CONTROLLER slot
and lay it on a flat surface.
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Turn back to page 6 and install the board in the controller to complete
the following:
5.
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Screws
HP 185948
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Screws
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Connecting Cables
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This task is completed the same way for either an A module or a B module.
See the illustrations on the page 5.
:.-"
a. Remove the controller top cover by removing two screws located on the
1. Connect the 15-pin connector to the loop board in the controller and
~,
rear edge of the plastic top cover with a No. 1 Point Pozidriv.
l2.
it
Plug the two plugs of the Y end of the cable into J 4 and J5 on the HP
18653B SlECM box. These connectors are keyed to define their proper
locations.
2.
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a. Remove the five screws of the top plate with a No.2 Point Pozidriv.
b.
a. Remove the four screws at the corners of the top plate with a No.' 2
Point Pozidriv.
b.
Loosen the four screws that hold the boards and bezels to the metal top
plate with a No.1 Point Pozidriv.
c.
GC
Remove the top plate by lifting the front edge and sliding it toward the
front of the controller.
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Operation
The Loop Board provides communication between the Lab Automation
System (HP 3350A and lIP 3357A) and the HP 7673 Automatic Sampler.
Communication is limited to passing the next bottle number to the
automatic sampler. All other parameters need to be entered via the control
switches on the front panel of the HP 185938 Injector Module. For more
information on the control switches, see chapter 4, "Standalone Control" in
the operating manual (part number 07673-60995).
Valid bottle numbers with the tray installed are 01-00 (where 00 is
interpreted as 100). Valid bottle numbers when the tray is NOT installed
are 01-03. Once a valid bottle number is sent to the automatic sampler, the
sampler will begin its pre-run sequence. When an injection occurs, a start
signal is sent from the automatic sampler to the SlECM which starts the
AID and the gas chromatograph.
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~~
Installing a Board
.'"
-~
.~-
Pull out the yellow worksheet from the center of this link manual Find the
content list for the accessory you ordered. Check the hardware you
received against the list of hardware on the yellow worksheet. If any of the
hardware is missing, contact your lIP representative.
,;1
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You need a No. 1 Point Pozidriv and a No. 2 Point Posidriv to complete
these instructions.
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Once the data system detennines that a run has finished and the next one
should be started, it sends the next bottle number to the automatic sampler
indicating that a new run is being initiated.
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This link. manual describes how to install and configure the printed-circuit
board associated with the option you ordered into either an HP 18594A or
HP 18594B Controller Module.
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Turn off the power of the controller and disconnect the power cord.
CAUTION
After you have completed the installation, place this link manual in the
binder of your operating manual for the HP 7673 Automatic Sampler
(part number 07673-60995) after the tab for appendix C "Link Manuals."
Copyright 1989 by Hewlett-Packard Company
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November 1989
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1/4-.1. rM ctiver
3 standoffs (18597-20520)
( Drawn flj scale )
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net wrench
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2 aqrnerttools (18597-40030)
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Place the plastic alignment toolfs), honeycombed side up, over the
inletfs) of your GC. Move the bracket until both alignment tools fit
flush on the bracket. If you cannot make them fit flush by moving the
bracket, you may have to adjust the position of the inlets.
b.
Tighten the two screws that hold down the bracket with a no. 2 point
Pozidriv screwdriver. Remove and save the bracket alignment tools for
future adjustments.
a. Route the gas lines on the inlet nut over the mounting bracket. For
most configurations, the gas lines should be routed over the front or
f<
~.
The gas lines must not interfere with the mounting of the injector. If
necessary, gently bend the gas lines.
I:
b. Push the inlet nut down and turn it clockwise. Tighten it with the inlet
~ :;.;
wrench.
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Figure'7. Route the z:as lines over the bracket and reattach the inlet
nut.
10
11
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Hold the bracket with the bend on the left side and slide it onto the
cylinders that yon attached to the side wall in step 1. Allow the bracket
to rest on top of the standoffs.
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This section reviews the steps for installing the upgrade injector bracket
and shows an exploded View. For detailed instructions, refer to the link.
manual "Installing and Operating the Injector and Tray on HP 5880A GCs"
(part number 07673-90235). Some of the parts are packaged with the
upgrade bracket and the rest with the HP 5880A injector/tray mounting
hardware (part number 18597-6(675).
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The exploded view on the next page shows the bracket being installed over
positions B and D.
2.
Replace the pan head screws that hold the inlets to the GC top cover
with the appropriate standoffs (small hexagonal posts}.
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For a position without an inlet, attach the piece ofsheet metal and
two large standoffs.
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Line up the top of the standoffs with the hole and slot on the bracket.
Screw the pan head screws into the threaded holes of the standoff's. Do
not tighten the screws until step 5.
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For a split/splitless inlet, route the gas lines over the bracket. H you do
not, you cannot replace the inlet liner without removing the bracket.
CAUTION
Tum off the gas flows before you remove the inlet riut or you
may damage the packing in the Inlet nner. Avoid contaminating
the inlet while it Is uncovered.
a,
Loosen the inlet nut with the inlet wrench. Turn the nut
counterclockwise until it is off the threads and lift it out of the way.
The braze joints that hold the gas lines to the inlet are fragile.
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Figure 4. Detach the inlet nut and lift it out
or the way.
13
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e. Screw one standoff onto the bottom of the mounting bracket to act as a
support leg. The hole has a silver-colored pem (small threaded washer)
on the top, right-hand side of the bracket. Tighten the standoff with a'
114-in. nut driver.
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This section reviews the steps for installing the upgrade injector bracket
and shows an exploded view. For detailed instructions, refer to the link
manual "In.sta.lling and Connecting the Injector and Tray on HP 5710/30190
GCs" (part number 07673-9(225).
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For a capillary inlet, use the largest standoffs to support the tray
and the smallest standoffs to support the injector bracket.
14
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d. Screw two of the standoffs (small hexagonal posts) into the threaded
holes located near the inlets. Tighten them with a 1I4-in. nut driver.
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If gas lines are routed over the bracket, be sure the lines are placed
according to figure 7 on page 10.
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If installing on an lIP 5890A GC, you must first install the HP 5890
SERIES II split top cover .. You.must also remove the existing injector
bracket and supports.
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Remove the port pan of the split top cover by inserting a finger into tha
U-shaped cut on the panel and pulling up.
b.
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Self-tapping screws.
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e. Using a 1/4-in. nut driver and the two self-tapping screws. attach the
two small cylinders onto the left side wall of the chromatograph.
If the GC has an on-column inlet, be sure you have the correct inlet
top-either the cooling tower or the septum nut base assembly with the
needle guide top.
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The next step is to install the tray bracket. Refer to "Installing the Tray
Bracket on 5890 GCs" (part number 07673-90205).
16
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Pull out the yellow worksheet from the center of this link manual. Organize
the hardware and tools for each step. Full-scale drawings of the screws help
identify which ones you need for each step. If any of the hardware is
missing, contact your HP representative.
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bracket.
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Tlis worksheet isfor instaIi1g the rnot..rFfilg bfackets forthe HP 185938 Ir1ector
Mo<lie cr1d the HP 185968 Tray Me>roe to an HP 5710/3CV90 Gas Chromatogaph.
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a. Place the plastic alignment tool, honeycombed side up, over the inlet of
your GC. Move the bracket until the alignment tool fits flush on the
bracket. If you cannot make it fit flush by moving the bracket, yon may
have to adjust the position of the inlet.
b. Tighten the four screws that hold down the bracket with a no. 2 point
Pozidriv. Remove and save the bracket alignment tool for future
adjustments.
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a. Screw each mounting post clockwise into the threaded holes of the
bracket. Tighten the posts with a flathead screwdriver.
If you are installing the tray bracket, continue on the next page.
If you are not installing the tray bracket, turn to page 12.
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Screw the three standoffs (hexagonal posts) into the injector mounting
bracket. Use the holes identified in the illustration. If you do not use
the correct holes, the tray will not be able to deliver sample vials to the
injector.
a.
b.
~-
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Hold the bracket with the bend on the left side. Allow the bracket to
rest on top of the threaded washers or standoffs.
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Line up the top of the threaded washers or standoffs with the holes on
the bracket. Screw the pan head screws (English thread) into the
threaded holes of the standoffs.
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Using a no. 2 point Pozidriv, screw in the three pan head screws (metric
thread) through the holes labeled A and into the standoffs..
Line up the hole on the far side of the tray bracket Oabe1ed 5700) with
the threaded hole of the rear standoff'. Screw one pan head screw
(English thread) into the mounting support with a no. 2 point Pozidriv.
For an inlet in the A position attach any standoffs to the rear set of .
threaded washers.
d.
Line up the hole on the near side of the tray bracket Oabeled 57(0) with
the threaded hole of the front standoff'. Screw one flat head screw
(English thread) into the mounting support with a no. 2 point Pozidriv.
Ii'
b.
c.
..
If the top of the standoffs do not line up with the holes labeled with the
letter A, check the location of the standoffs against the figure on
page 10.
For a capillary inlet use the two largest standoffs (part number
18597-20650) to support the tray and the two smallest standoffs (part
number 18597-20660) to support the injector bracket.
;;.:
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For a packed inlet use the two medium-sized standoffs (part number
18597-20640) to support the tray, but do not use any standoffs to
support the injector bracket. The injector can be used with a packed
port in the B position, but not with one in the A position.
a. Place the tray bracket on the five standoffs installed in steps 3 and 7.
-c,
For an inlet in the B position attach any standoffs to the front set of
threaded washers.
a. Attach the necessary standoffs to the threaded washers on the top cover
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a. There are two holes on the right-hand side ofthe top cover for an
on-column capillary inlet. Cover one or both holes with the plastic
plugs.
b.
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Replace the existing septum nut with the one supplied in this kit.
D The three screws that attach the tray bracket to the standoffs on the
injector bracket must go through the holes labeled A on the tray
bracket.
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D The flat head screw for attaching the tray bracket is in the correct
position. See page 11.
For detailed information on mounting and connecting the injector and tray,
see chapter 1, "Setting Up", in your operating manual
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PllIgs
After you have completed the installation, place this link manual in the
binder of your operating manual for the HP 7673 Automatic Sampler
(part number 07673-60995) after the tab for appendix C "Link Manuals."
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To replace the top cover, you may have to remove hardware that is attached
to the existing top cover (e.g., the inlet control module).
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a.
Using a no. 2 point Pozidriv, remove the 5 screws that hold on the top
cover of the GC.
b.
ft.
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d. Using a no. 2 point Pozidriv, attach the top cover with 5 screws (English
[~~,
thread).
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03392 60800
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Your special hardware kit contains all of the hardware you need to install
the new top cover, the injector bracket, and the tray bracket for the
automatic sampler, except for the brackets. Find the injector bracket in the
controller box and the tray bracket in the tray box.
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4
Pull out the yellow worksheet from the center of this link manual. Organize
the hardware and tools for each step. Full-scale drawings of the screws help
identify which ones you need for each step. If any of the hardware is
missing, contact your HP representative.
1894-50&00
step by step
WIthout a chart recorder, connect a cable between the controller and the
GC.
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With an AID converter, connect the three instruments with the appropriate
cable or cables. The following illustrations show two example.
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Sample diagrams for connecting the cables for the automatic sampler to
an HP 5710/30190 GC.
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1 a594 -60820
To change the position of the injector, you must change the position of the
mounting bracket,
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WARNING
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35900-60800
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AEIIlOTE
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35900-M620
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Copyright 1989 by Hewlett-Packard Company
All Rights Reserved
15
HEWLETT- PACKARD
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December 1989
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Place the plastic alignment toolfs), honeycombed side up, over the inletfs) of your~. Move the bracket until both alignment tools fit flush
on thebrackeL If you cannot make them fit flush by moving the
bracket, you may have to adjust the position of the inlets.
~-
b. Tighten the two screws that hold down the bracket with a No.2 point
Pozidriv. Remove and save the bracket alignment tools for future
adjustments.
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a. Screw the mounting post clockwise into the threaded hole of the
bracket. Tighten the post with a flathead screwdriver.
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The A and B injector modules need different parts when mounting over a
coolon-column inlet.
The A module needs the cooling tower or needle guide top to be inplace.
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10
11
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4. Attach the Inlet Nut
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The gas lines must not interfere with the feet of the injector. Small
white prcles on the bracket showwhere the injector feet touch the
bracket. If necessary, gently bend the gas lines so they do not cross the
white circles.
This section reviews the steps for installing the injector bracket and shows
J~
a. Route the gas lines on the inlet nut over the mounting bracket. For
most configurations, the gas lines should be routed over the front or
rear of the bracket.
b.
Push the inlet nut down and turn it clockwise. Tighten it with the inlet
wrench.
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inlets.
For a packed inlet, replace the pan head screws with the small
standoffs.
For a capillary inlet, replace the pan head screws with the large
standoffs.
For a position without an inlet, attach the piece of sheet metal and
two large standoffs.
Figure 7. Route the gas lines over the bracket and reattach the inlet
nut.
12
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a. Hold the bracket with the bend on the left side and slide it onto the cylinders that you attached to the side wall in step 1. Allow the bracket to
rest on top of the standoff's.
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the GC.
Line up the top of the standoff's with the hole and slot on the bracket.
Screw the pan head screws into the threaded holes of the standoff's. Do
not tighten the screws until step 5.
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Figure 10.
00
an HP 5880A GC.
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Figure 6.
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4
Installing on HP 5710/30/90 GCs
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For a split/splitless inlet, route the gas lines over the bracket. lfyou do
not, you cannot replace the inlet liner without removing the bracket.
I.
This section reviews the steps for installing the injector bracket and shows
an exploded view. For detailed instructions, refer to the link manual
"Installing and Connecting the Injector and Tray on lIP 5710130190 GCs"
(part number 07678-90225).
You can mount only one injector on an lIP 5710130190. To mount the
injector over the front inlet a.e., in the A position), install the bracket over
the rear set of threaded holes. To mount the injector over the rear inlet
(i.e., in the B position), install the bracket over the front set of threaded
holes.
~>c. '1"
lH
.....
CAUTION
'~i
,d
Tum off the gas flows before you remove the Inlet nut or you
may damage the packing In the inlet liner. Avoid contaminating
the Inlet while it Is uncovered.
:~
Loosen the inlet nut with the inlet wrench. Turn the nut counterclockwise until it is off the threads and lift it out of the 'Nay. The braze joints
that hold the gas lines to the inlet are fragile.
'~
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Replace the GC top cover and attach the plugs and septum nut.
1!
4.
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Figure 4. Detach the inlet nut and lift it out of the way.
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14
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e. Screw one standoff onto the bottom of the mounting bracket to act as a
support leg. The hole has a silver-eolored pem (small threaded washer)
on the top, right-hand side of the bracket. Tighten the standoffwith a
1/4-in. nut driver.
~-
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AiIIllMlJt tool
MeDDtiII post
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If lIP 5890 SERIES n cool on-column inlets are installed in both the
front and rear positions of the GC, do not install this standoff. Without this
standoff, the stability of an injector in the rear position may be affected.
15
'~'-::-~
',~~
d. Screw two of the standoffs (small hexagonal posts) into the threaded
holes located near the inlets. Tighten them with a 1/4-in. nut driver.
-~~
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The following diagram illustrates how to attach the adapter cable required
to connnect an HP 18593B Injector Module to an HP 18594A Controller
Module.
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Remove the port pan by inserting a finger into the U-shaped cut on the
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c.
Using a 1/4-in. nut driver and the two self-tapping screws, attach the
two small cylinders onto the left side waD of the chromatograph.
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If the GC bas an on-column inlet, be sure that you have the correct inlet
top: either the cooling tower or the septwn nut base assembly, with or
without the needle guide top.
o
o
o
Self-tapping screws.
Pan head screws.
If you are installing a tray, install the tray bracket before mounting the
injector. Instructions for installing the tray bracket are packaged with the
f'
tray.
I;
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17
2
Installing on HP 5890 GCs
Pull out the yellow worksheet from the center of this link manual. Organize
the hardware and tools for each step. Full-scale drawings of the screws help
identify which ones you need for each step. If any of the hardware is
missing, contact your HP representative.
Step by step
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To install the hybrid bracket, remove the existing bracket and bracket
supports.
For an lIP 5890A or SERIES II Ge, you can mount both injectors at
the same time. Turn to page 3.
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Hyour automatic sampler includes a tray. you must install the new tray
bracket onto the existing tray bracket supports (often called side rails).
Directions for installation are packaged with the new tray bracket.
"
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For an HP 5880A Ge. you can mount both injectors over inlets in positions A and C or B and D. Turn to page 12.
For an HP 5710/30/90 Ge. you can mount only one injector at a time.
Turn to page 14.
Toattach the adapter cable required to connnect an HP 18593B Injector Module to an HP 18594A Controller Module, turn to page 16.
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HEWLETT
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ManuaJ Part No.
1859790140
Printed In U.S.A.
December 1989
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1 rigt side of top cover (05890-00402)
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Using a No.2 Point Pozidriv, a flat washer, and the largest pan head
screw, attach the cylindrical lid shaft to the right-hand section of the
new top cover.
Place the cupped end of the lid shaft over the knob on the left-hand side
of the GC.
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b.
Push the hole on the right-hand side of the top cover over the knob on
the right-handside of the GC.
c.
Using a 1/4-in. nut driver, a flat washer, and a self-tapping screw, secure
the top cover to the right-hand side of the GC. H the GC has a
grounding wire, attach it to the threaded post with the lock washer and
nut that you removed in step 1.
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b.
Open the oven door and place the front panel bezel (or grill) on the top
front edge of the GC.
Using a 1J4-in. nut driver, remove the screws and washers that make up
the hinge of the top cover. If the GC has a grounding wire, disconnect
it by removing the nut and lock washer with a 9/32-in. nut driver.
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b.
Start each of the three pan head screws from below with your fingers.
Tighten each screw with a No.2 Point Pozidriv,
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Remove the top cover by pushing one of the metal tabs over the knob
with your thumb.
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Figure 3.
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Remove the injection port pan from the top cover by pushing in the
sides and lifting up. The next two paragraphs describe one method.
Using the thumbs of both hands, push to the left and lift the left-hand
side oftha port pan. The left-hand side should pop out of the top cover.
Close the oven door and lower the right-hand side of the top rover.
b.
Place the front edge of the port pan on the front bezel. Push the back
edge with the U-shaped notch down until the port pan snaps into place"
Next, pull up on the right-hand side with your fingers. The right-hand
side should pop out of the top cover. Lift the port pan off the top cover.
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Checking Your Work
Be sure that all the screws are tight.
o Be sure the edge of the top cover is flush with the front grill.
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If it is not
Pull out the yellow worksheet from the center of this link manual. Organize
the hardware and tools for each step. Full-scale drawings of the screws help
identify which ones you need for each step. If any of the hardware is missing, contact your HP representative.
2 _ .... _
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Next, install the left side panel of the HP 5890 SERIES II Gas
Chromatograph. The instructions are packaged with the left side panel.
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You must upgrade the top cover of an lIP 5890A Gas Chromatograph (GC)
with the split top cover of the HP 5890 SERIES II GC before installing the
mounting bracket for the HP 18593B Injector Module. The SERIES II
design enables you to open and close the top cover while the injector
mounting bracket is installed.
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WAR.NING
You
After you have completed the installation, place this manual in the binder of
your operating manual for the HP 7673 Automatic Sampler
(Part No. 07673-60995) after the tab for appendix C "Link Manuals."
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HEWLETT-PACKARD
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HEWLETT
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October 1989
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a.
Place the new left side panel on the GC and slide it forward. Be sure
the front edge is seated. Be sure the gas lines are not in the way.
b.
Using a No.2 Point Pozidriv, screw the two pan head screws into the
side of the GC.
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Be sure the front edge of the left side panel is seated into the GC.
Be sure aD screws are tight.
Next, install the split top cover for the HP 5890 SERIES II Gas
Chromatograph. The instructions are packaged with the split top cover.
If the split top cover is already installed, install the injector mounting
bracket. The instructions are with the mounting hardware that is packaged
with the controller.
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tie,
After you have completed the installation, place this link manual in the
binder of your operating manual for the HP 7673 Automatic Sampler
(Part No. 07673-6(995) after the tab for appendix C "Link Manuals."
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Using a No.2 Point Pozidriv, remove the two pan head screws that hold
the existing left side panel onto the left side of the GC.
b.
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Figure 2. Removing the old left side panel.
1
Before You Start
You must upgrade the left side panel of the HP 5890A Gas Chromatograph
(00 before installing the mounting bracket for the HP 1859GB Tray
Module.
Figure 1 lists the hardware and tools that you need to complete the installation. If any of the hardware is missing, contact your HP representative.
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~PACKARD
185i7-90170
PrInted In U.S.A.
October 1989
The following sample vials and caps should not be used with a tray.
~_I
100
500
500
500
i.f'.' .':.
12
cIBar
5080-8779
f.:
~~-
~-
~- ~
~.
~
t~
c&r'witKUcaps
5180-4197
ctEa' 'til caps &beD: 5061-3350
amber wIhcU caps
5061-3369
lInber wQh caps &bat 5061-3348
_
_
with ilserts
withot.t ilserts
~ withot.t ilsefts
nicn:lIIiaI inserts (A)
IirnIBd YOI. ilserts (B)
5181-1269
5181-3375
5181-3376
5181-1270
5181-33n
100
clear
9301-09n
clear
9301-0978
5181-1259
100
100
cIecI'
9301-1128
100
9301-1131
9301-1130
L
~
A-12
100
100
100
100
akrT*un metaJ
blue metal
IJ'88I1 metal
red metal
5181-1210
5181-1215
5181-1216
5181-1217
A-13
HP Recommended Supplies
4-mI soh'ent orwash tQIJe wih screw cap
144
c&I'
9301-0723
j
~
Diffusk)n caps
12
07673-40180
$epa ~ 4-ml1xdes
144
Selecting and ordering the correct consumables like sample vials, syringes, and
septa are an important part of operating the lIP 7673 Automatic Sampler. By
using Hewlett-Packard rerommended supplies, you can help maintain the
reliability of the automatic sampler. For more information, see the current
issue of the Chroma/Qgrophy Usen Couz/og.
9301-1031
The following example illustrates the organization of the information.
s-aJ lIescriptioI
_~
...._
Or dIM
~q:wlIhcaps~
.itnetlt.......,
500
anmer willcaps & box
500
anDlrwithott caps
PIrt .......
A-14
':
A-11
SyrInges
Inlet Uners
You must use the correct inlet liner or insert with the automatic sampler. If
you do not, you may introduce peak area discrimination prOOlems into the
analysis.
WIth split or spIitI.ess inlets, you may try these liners:
4-mm, borosilicate glass liner with glass wool plug (part number
9301-0713
9301-0725
9301-0892
19251-60540)
4-mm sitantred, borosilicate glass liner with single taper and S1la n ized, glass
wool plug (part number 5062-3587)
.
4-mm sitanired, borosilicate glass liner with a double taper' (part number
5181-3315)
on-caum iEts
1
6
1
1
1
5181-1267
5181-3360
5181-1273
5181-3321
5181-1265
4-mm S1lantm1, borosilicate glass liner with single taper (part number
5181-3316)
The single taper liners with or without the glass wool plug are possille choices
for many environmental analyses. The single taper liner without the glass wool
plug is usoaDy better when the anaIytes tend to degrade in the inlet.
~
HlpI.n.B........
5181-3319
The flow inverter liner (part number 18740-60840) and the quartz splitless liner
(part number 18740-80220) are not reoomm.ended for use with the automatic
sampler.
Practically every sample rontains nomoIati1e material that accumulates and
partially pryolyzes in the liner. Period.ally. the liner must be replaced or
A-10
A-15
Inlet septa
Inlet septa
Inlet septa should last at least 200 injections before there is any sign of
leakage. The following factors impact the life expecta.ncy of septa.
~lIIII
25
LiIer
red, sokI
24
Cool ~ cI
lIIeI
gray, sold
5080-8896
InIettemperature.
red, said
se,tI.
25
25
'i
Change septa at the end of the day's work. It takes several hours for the gas
flow to sweep out any contaminants introduced to the inlet and for the flow
rate to equi1iJrate.
Select the proper septa diameter for your GC from the following diagram.
Type ci lnIet
Gas ctvornatogra.gt
9301-1263
e-Dbt
5181-1260
5181-1261
~rnn
HP5890
11-nvn
5-mm
HP 5880A
11-mm
5-mm
HP 5700 series
9.5-rrm
Septa are made from materials that give off volatiles especiaJly in heated inlets.
H not swept away in a septum purge design, these volatiles may interfere with
the analysis. The following list of inlet septa may help you select the correct
type.
I
R
CAUTION
,.5-...
red lew bleed septa are DOt l'eCO'MH'aded fer use witIltile HP
7673Autoautic S8D1p1er. TIte smaller septa teIKI to . . . IMI'e rreq.w
replacement
The
25
5181-1263
~
A-16
A-9
The following diagram illustrates the shapes of the two fixed needles.
Inlet Uners
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5181-3315
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Injection volumes vary with the sample volume parameter set on the
controlling device, the size of the syringe, and whether the injector is set up for
nanoIiter injection (lIP 18599N Nanoliter Adapter).
F;;
8an1*l voome
settilg
1
2
~
r
SniloeSize
Halder IlIiectk!1I
5pJ
10u.J
0.2
0.1
as
2.0
4.0
1.0
1.5
2.5
5.0
2.0
1.0
2.0
3.0
4.0
1
1
The following table mts the aWllwmate injection volumes available with the
automatic sampler.
Standard kpetioo
5u.J
10u.J
0.5
1.0
1.0
2.0
1.5
3.0
19251-60540
25
5080-8732
~e
I
stalldlld
1 _ to 1/4-il. metal
1 adap: to1/B-it metal
25 ~ ilIet inIlr
19359-20550
18745-80010
18709-80030
5080-8732
19245-20580
I
R--bIsert
A-a
A-17
C...--:J
Syringes
18587A Blr' Cooe Reader labels
NlJrDlred
1 to 1,(XXl
1,001 to 2,000
2,001 kJ3,000
3,001 kJ 4,000
4,001 to 5,000
5,001 to 6,000
6,001 to 7,000
7,00110 8,000
8,001 to 9,000
label appicatoc
5958-9450
5958-9441
5958-9442
5958-9443
5958-9444
5958-9445
5958-9446
5958-9447
FIXedand removable needle syringes are available to use with the automatic
sampler.
23/26 gaugetapered needle used with on-column mlets, TIm syringe can
be used as a general JKlIpose syringe with all inlets.
The syringe needle must have a flat tip. Do not use sharp-tipped needles (e.g.,
point style 2). When used with the automatic sampler, these needles tear the
inlet septum causing leaks. Also, sharp-tipped needles wipe off on the septum
as they exit resulting in a large solvent tail on the chromatogram..
5958-9448
18587-60560
cawed vials
IIf"NlIImf1
TestviaJ
vials
sw,tip
18587-00120
18587-D0130
RIIU,
18587-60540
------JH,
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, ,: n
A-18
A-7
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Miscellaneous
4-ml bottles are placed in the injector turret to bold solvents used for washing
the syringe between samples and to hold the solvent and sample rinses. During
a solvent wash. the syringe needle cannot reach the last 2.5 ml in the bottle.
For more information, see "Filling and Placing the Bottles" on page 3-17.
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Vial racks
5
5
You can use diffusion caps or septa on these bottles to reduce evaporation and
diffusion of your solvents and waste. HP reoommends diffusion caps over septa
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For many common solvents, the rate of diffusion out of the bottle is less
with a diffusion cap than with a septum that has been punctured with a
standard syringe needle.
.----==
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18596-40015
11-1TIll ~ I*Jg
1000
9301-0990
ser.cap
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12
871D-0979
5181-1213
~..
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4-al1IInII1I'waslllIatUt
A-6
,/
A-19
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e......
GIllie TIf
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A......,
e
I
Dbt: se,b.
I-Sprag
R-Iaert
Once the vial septum is punctured by the ~ needle, the sample may
interact with the septum material and affect the a.naI)'sis. There are three types
of septum used in vial caps. Each has a different resistance to interaction with
solvents.
'* 5880A
MolI'Iting post
1
19245-20670
19245-80520
19245-60760
Red: Made from silicone rubber coated with Thfloo- on both sides. A high
quality, low extractable silicone rubber intended fOr' applications requiring
resistance to high extremes of heat. Somewhat resistant to solvents after
puncture. Slightly poorer resealing characteristics when application calls
for multiple injections from the same vial
1~~
07673-61035
Redlorange: Made from natural robber and coated with Thfloo- on the
sample side. A general purpose rubber formulation .intended primarily for
aqueous liquid fill products with a pH range 4-0-7.5. Least resistant to
solvents after puncture.
CAUTION
,11
.~
Black septa made fI'MI Vitae are BOtrecoII1DleDded Cor use with the UP
18593A ud B IDjec:ter Modules. UsiDc VitoB. may cause syringeerror.
The following diagram illustrates the recommended and minimum diameter for
vial septa.
NalOOlef adaPer
1
HP 18599N
i.5I (0.221 iL) rtCOII.eHed
U5 (0.113"')
Basic ~ KI
6
144
144
1000
5
144
07673-60840
1Q-p.l2:Vl61aA*ed syrilges
4-mI soMIlfIu;h baties wIh caps
dffuslon caps
2-m sam;:E vials wih cri11l caps
viaf racks
11-rrm 5eJD
.il'."
AI fiIIeaIots II 1Il1n.cm
';
H you are loading vials directly into the injector turret. you can use 2-ml
sample vials with screw caps. Do not use screw cap vials with the tray.
Use amber glass vials for light-sensitive samples.
A-20
A-5
~
~
The following diagram illustrates most of the aitical dimensions for the sample
vials and microria1 inserts. These dimensions do not make up a complete set of
specifications- Some of the dimensions are too difficnh to measure without
special instruments.
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A-4
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Selecting Consumables
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1
Introduction
This is an integral part cl the lIP 7673 Automatic Sampler Operating Manual
(part number 07673-60995). It is designed to be updated on a regnIar basis and
kq)t in the manual's binder after the chapter tab for appendix A,
"Cons:mnahles...
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Syringes.
Inlet septa.
Inlet liners,
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