003.0 Surface Sampling Operating Procedures

SURFACE SAMPLING - GENERAL GUIDELINES
REF: OP 019
R E V: 03
DATE:
26 April 1999
PAGE 1 of 9
1.0
GENERAL
GUIDELINES
1.1
Before sampling commences, the Client's Test Engineer must verbally confirm that separator
conditions are stable and suitable for sampling.
1.2
Chemical injection upstream of the separator must be stopped to avoid sample contamination
(delay between cessation of chemical injection and commencement of sampling must be of
sufficient length to ensure the separator has been purged). If flowing conditions dictate that
chemical injection must continue during sampling, injection rates, injection points and injected
chemicals must be recorded on the sample data sheets.
1.3
The well test service company's Shift Supervisor must be aware of the sampling operation before
sampling commences.
1.4
Sample datasheets must be completed with the correct data. The Client's Test Engineer should
confirm verbally that the correct information has been used.
1.5
Pressurised samples should be labelled as follows:- The box should have a plasticised label attached to the RHS handle.
- The bottle should have a plasticised label attached to the top protector.
- The green status tag should be removed.
- A completed sample datasheet should be placed inside the box in a poly self-seal bag.
- The correct hazard diamond labels should be stuck on the top of the box and on the sample
bottle.
1.6
Atmospheric samples should be labelled as follows:- The container should be marked up with sample details (sample no, sample nature, sample
point, well, test number, date/time, Client, installation) using a paint marker or similar indelible
pen.
- A completed self adhesive sample label should be stuck on the container, and if the container
has a handle, a plasticised label should be attached.
- Drums which are likely to be stored in the open should have sample and well number scratched
on.
- The correct hazard diamond labels should be stuck on the sample container.
The triplication of details is necessary as labels, paint, etc can all come off, rendering the sample
unidentifiable and useless.
1.7
When filling atmospheric containers with crude, leave a 10% space for expansion inside the
container. Allow the sample to de-gas for as long as possible before screwing the lid on, as agitation
during shipping causes evolution of gas which can rupture the container. Do not allow rainwater,
spray, etc to contaminate the sample while it is de-gassing.
1.8
Generally, atmospheric oil samples should be taken in metal containers and atmospheric water
samples into plastic or glass containers. Metal containers should be IATA approved. (UN number
on the can).
1.9
Do not use third party gauges for sampling as they may have been used for mercury displacement
sampling and may contaminate the sample (in the case of gas sampling the introduction of mercury
will damage the sample cylinder).
Warning: The controlled source document of this procedure is stored on Oilphase homepage
(http://www.aberdeen.oilphase.slb.com). Any paper version of this procedure is uncontrolled and
should be compared with the source document at time of use to ensure it is up-to-date.
PREPARED BY:
RS
VERIFIED BY:
DG
A P P R O V E D B Y : GD

REF: OP 019
R E V: 03
DATE:
26 April 1999
PAGE 2 of 9
1.10
Separator oil sampling point should be midstream on the oil line, upstream of the meters. The oil
level sight glass should be used only if there are no suitable sampling points on the oil line. The
sight glass must be purged and refilled several times and the check valve set in the "open" position.
Avoid emptying the sight glass while sampling (which allows the sample bottle to fill with gas).
1.11
Separator gas sampling point should be the highest available point on the separator gas outlet line,
upstream of the orifice meter. A sampling point on the underside of the gas outlet line should be
avoided however, as liquid carry over may if present be taken into the gas sample bottle.
1.12
Separator pressurised oil and gas sampling should be carried out at the same time where the
samples are to be used for recombination. This ensures that both samples are taken under the same
separator conditions and can be matched with each other.
2.0
LIQUID SURFACE SAMPLING using the Oilphase Conventional Bottle
2.1
Place sample bottle in stand (Item 9) using bottle collar (Item 7). Fit top oil manifold (item 5),
bottom manifold (item 4) and connect pump (Item 11) to the bottom manifold bleed valve V4.
Open CSB V3, CSB V1 and V4 and pressure up bottle to oil line pressure ie separator pressure. See
Figure 1.
2.2
Close V4 and disconnect pump.
2.3
Connect liner (item 3) between top manifold and sampling point valve V1.
2.4
Ensure all valves are closed.
2.5
Pressure up liner by opening valve V1.
2.6
Open V2 and purge liner by opening V3. Purge at least five liner volumes. Close V3.
2.7
Open CSB V2 and gently open CSB V1. Purge 2 to 3 liner volumes across piston in sample bottle
through 1/ 4" slimline autoclave elbow (Item 6) to CSB V1 port.
2.8
Close CSB V1. Remove 1/4" slimline autoclave elbow and plug CSB V1 port. Proceed to take
sample by gently opening V4 and allowing sample to displace the water/glycol mixture into the
measuring cylinder. Record time for commencing sampling. Observe sight glass level to avoid
drawing gas into the sample bottle.
2.9
Maintain separator pressure on bottom manifold gauge at all times and to avoid sample "flash".
Use V4 to control water/glycol displacement and bottle pressure.
2.10
After displacement of 600 cc of water/glycol V4 should be closed followed by CSB V2. check that
CSB V1 and V4 are closed, CSB V3 is open.
2.11
Open V4 and remove a further 60 cc of water/glycol to create a 10% gas cap for shipping.
CAUTION: Care should be taken not to allow the piston to bottom out as it will become
unbalanced.
2.12
Record the final pressure, the ambient temperature and the end time of sampling. Close CSB V3
and open V4 to bleed bottom manifold. Close V1, open V3 and bleed down liner pressure.
2.13
Disconnect the liner and both manifolds. Plug CSB V1, CSB V2 and CSB V3 ports. Check bottle for
leaks, label the bottle and box and complete a surface sample datasheet. When the sampling report
is printed, print an additional copy of the datasheets to accompany the sample.

REF: OP 019
R E V: 03
DATE:
26 April 1999
PAGE 3 of 9
Figure 1. Liquid Surface Sampling using the Conventional Sample Bottle (CSB)
Index
Item
Description
Reference
Qty
1
2
3
4
5
6
7
8
9
10
11
12
13
1/2" NPT (m) x 1/4" JIC (m) adapter

100K 1/4" JIC synflex liner (8 ft)
Oil manifold (bottom)
Oil manifold (top)
1/4" SL autoclave 90 purge nipple
Sample bottle collar
19 mm box spanner
Bottle stand
Test gauge (1,500 psig)
Enerpac hand pump
Measuring cylinder (1 Litre)
Conventional sample bottle (CSB)
QR0900
QR0899
QR0989
AR0886
AR0887
AR0892
QR0501
AT0157
QR0893
QR0904
QT0113
QT0143
PR0767
1
1
2
1
1
1
1
1
1
1
1
1
1

REF: OP 019
R E V: 03
DATE:
26 April 1999
PAGE 4 of 9
3.0
LIQUID SURFACE SAMPLING using the Oilphase Single-phase Sample Bottle
3.1
Check Sample Bottle Status Form (F-153) Under normal circumstances bottle will be shipped full of
50/50 glycol/water mix.
3.2
Place sample bottle in stand. See Figure 2.
Figure 2. Monophasic Liquid Surface Sampling using the Single-phase Sample Bottle (SSB)
Item
Description
Reference
Qty
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
1/2" NPT (m) x 1/4" SL Autoclave (m) adapter

1/4" NPT (m) x 1/4" SL Autoclave (m) adapter
Oil manifold (bottom)
Oil manifold (top)
1/4" SL autoclave 90 purge nipple
Sample bottle collar
19 mm box spanner
Bottle stand
Air operated glycol/water pump
Measuring cylinder (1 Litre)
Conventional sample bottle (CSB)
Single-phase sample bottle (SSB)
1/4" SL autoclave polyflex liner 8 ft
1/4" SL Autoclave (m) x 1/4" JIC (m) adapter
1/4" SL autoclave (m) x 1/4" JIC (m) adapter
OFN regulator c/w 1/4" JIC (m) adapter
OFN bottle spanner
QR0906
QR0526
QR0898
AR0888
AR0889
AR0892
QR0501
AT0157
QR0893
QR0902
N/A
QT0143
PR0767
PR0768
QR0897
QR0131
AR0901
QT0138
QT0174
1
1
1
1
1
1
2
2
2
1
1
1
1
1
3
4
1
1
1

REF: OP 019
R E V: 03
DATE:
26 April 1999
PAGE 5 of 9
3.3
Fit upper Item 5 and lower item 4 manifolds. Note Sample bottle valves are operated using 19 mm
box spanner. (Item 8).
3.4
Connect glycol/water pump to the lower manifold bleed valve V4. Flush manifold with glycol/
water prior to tightening connection to bottle.
3.5
Open V4, SSB V3, SSB V1 and pressure up lower manifold and below bottle piston to wellhead
pressure.
3.6
Close V4 and remove pump.
3.7
Connect liner (Item 15) between upper manifold and sampling point V1.
3.8
Ensure all valves are closed (except for SSB V3).
3.9
Pressure up liner by opening valve on sampling point V1.
3.10
Purge line through bleed valve V3, then open SSB V2 and purge across sample bottle piston by
opening SSB V1.
3.11
Close SSB V1. Note: If oil is extremely viscous glycol/water pressure below piston may have to be
reduced in order to allow flow across the top of the piston.
3.12
Proceed to take sample by gently opening lower bleed valve and allowing sample to displace water
into measuring cylinder.
3.13
Maintain wellhead pressure on gauge at all times to avoid sample "flash" using V4 to control
pressure and water flow.
3.14
A 600 cc sample should be taken then V4 should be closed, followed by SSB V2.
3.15
Bleed off line between upper manifold and sample point, disconnect liner.
3.16
Connect regulated oxygen free nitrogen (OFN) supply to valve CSB V1.
3.17
Connect glycol/water pump to valve CSB V3.
3.18
Connect OFN liner (Item 15) between CSB V2 and SSB V4 (port marked N).
3.19
Purge OFN line by opening valves CSB V1, CSB V2, SSB V4 and loosening liner connection at SSB
V4. Tighten liner connection to SSB V4.
3.20
Regulate OFN supply to 200 psig and fill booster bottle slowly by opening valve CSB V3 and
glycol/water pump bleed valve.
3.21
Increase OFN pressure to maximum bottle pressure (max pressure of full cylinder is 2,000 - 3,000
psig).
3.22
Close CSB V1. Bleed OFN and rig down liner.
3.23
Ensure valve SSB V4 is open, boost OFN pressure using glycol/water pump to sample pressure.
3.24
Using glycol/water pump regulator set at least 500 psi above sample pressure, slowly open valve
V4 and remove a further 60 cc of glycol/water in order to create a nitrogen gas cap for shipping.
3.25
Close all sample bottle valves, bleed off pressure in manifolds prior to removing. Plug all valves.

REF: OP 019
R E V: 03
DATE:
26 April 1999
PAGE 6 of 9
3.26
Label the sample bottle and box, and complete a sample datasheet. A copy of the datasheet must
accompany the bottle.
4.0
GAS SAMPLING
4.1
Check bottle has been evacuated to less than 1.0 mbar or less than 10 mmHg.
4.2
Connect gas manifold (Item 4) to top valve on bottle, GSB V1 with suitable test gauge (separator
pressure >33%, <75% of full scale.)
4.3
Connect liner (Item 3) to V1 on separator gas sampling point and to V2 on gas manifold. See Figure
3.
Figure 3
Item
Description
Reference
Qty
1
2
3
4
5
6
7
8
9
10
11

Gas sampling manifold
Secondary gas sampling manifold
1/4" NPT (m) x Gerzat adapter
1/4" JIC (m) x Gerzat adapter
Gerzat PTFE bush
20 litre Luxfer gas sample bottle
20 litre Gerzat gas sample bottle
QR0900
QR0899
QR0898
AR0890
AR0891
QR0904
AR0706
AR0894
QT0705
1
1
2
1
1
1
1
1
1
1
1

REF: OP 019
R E V: 03
DATE:
26 April 1999
PAGE 7 of 9
4.4
Check V1 and GSB V1 are closed . Open V2 and V3. Open V1 and purge at least five liner volumes
of gas through the gas manifold.
4.5
Close V3. The gas manifold gauge should now read separator pressure.
4.6
Crack open bottle valve GSB V1, avoiding pressure drop on gauge. Record time for commencing
sampling.
4.7
Set GSB V1 so gas is bleeding as slowly as possible into bottle (this can be heard through bottle
wall).
4.8
Sampling time for 20 litre cylinder should be 20-30 mins - periodically check bottle is filling by
cycling GSB V1 again avoiding pressure drops on gauge.
4.9
When bottle is full close valves V2 and GSB V1.
4.10
Reduce gas manifold pressure by carefully opening and closing valve V3. (Drop pressure by
minimum registerable on test gauge).
4.11
Open cylinder GSB V1 and confirm gas manifold gauge pressure rises to original sampling
pressure. (This confirms cylinder is full of gas and did not plug during sampling).
4.12
Open V2 to restore separator pressure to bottle.
4.13
Close GSB V1. Record the final pressure, ambient temperature and the time for the completion of
sampling.
4.14
Close V1, open V3 and bleed down liner and gas manifold pressure.
4.15
Disconnect the liner and gas manifold. Plug GSB V1 and GSB V2 and attach red FULL tags to GSB
V1 and GSB V2 valve bodies.
4.16
Check bottle for leaks, label the bottle and box (refer to step 1.4) and complete a surface sample
datasheet. When the sampling report is printed, print an additional copy of the datasheet to
accompany the sample.
4.17
It is not advisable to install a test gauge on bottle valve GSB V2 to monitor pressure, as condensate
which forms in the bottle during sampling will be lost when the gauge is removed, thus changing
the sample composition.
4.18
If multiple gas samples are to be collected simultaneously connect second liner (Item 3) from
manifold valve V3 to secondary manifold valve (Item 5) valve V4 and continue from Step 4.3.
5.0
PRODUCED WATER SAMPLING (For general chemical analysis, not for dissolved organics)
5.1
Use new, clean glass or polyethylene bottles, one litre is preferable. The caps should have a plastic
not paper or foil liners.
5.2
Collect the sample using a small tube or hose inserted into the bottle to the bottom. Let the water
overflow the bottle for a half bottle volume. The idea of the tube is to minimise aeration. Once the
bottle is full, dump a little (50 ml) out to allow for expansion.
5.3
If possible, measure and record the pH and temperature of the sample.
5.4
Seal the bottle, check for leaks, label the bottle (refer to step 1.6) and complete a Surface Sampling
Datasheet.

REF: OP 019
R E V: 03
DATE:
26 April 1999
PAGE 8 of 9
5.5
Collect a second sample of the same water in a new bottle using the technique described above.
Add 5 ml of 10% HNO 3 (nitric acid) to the bottle. NOTE: HCl can be used but the added Cl can
confuse analysis. This will prevent iron and calcium from precipitating as the samples cool and
oxidise. The second sample is not critical, but very useful when it comes time to look at corrosion.
5.6
It is recommended to repeat this process several times during the well test. This is the only way to
know if all the drilling fluids have been flushed out of the system
6.0
PRODUCED WATER SAMPLING (for dissolved organics)
6.12
Use clean glass bottles, not polyethylene.
6.2
Fill through a tube as above but do not overflow.
6.3
Seal the bottle with a cap using telfon liner. Check for leaks, label the bottle. Refer to Step 1.6 and
complete a Surface Sampling Datasheet.
7.0
ATMOSPHERIC OIL SAMPLING
7.1
When dead oil sampling is to be undertaken, ensure that the separator or sample flowline is
suitably earthed.
7.2
Only rated pressure equipment is to be used for this task. Ensure that all valves, adapters and
hoses are suitable for the pressure, temperature and service involved
7.3
Only metal IATA approved cans are to be used. They can be identified by the UN logo marked in
white near the can or drum base.
7.4
The earthing cable with clips MUST be fitted between the sampling hose end outlet and the sample
can and also from the IATA can to the separator earth point . These earthing cables MUST be fitted
prior to and during sampling.
7.5
Personnel must ensure that metal buckets/drip trays are used for the collection and gathering of
hydrocarbon samples or waste.
7.6
This earthing connection to the bucket/drip tray must be directly to the bucket/drip tray body and
not the bucket handle, it is not acceptable to consider the bucket/drip tray sufficiently earthed by
way of its physical contact with the separator skid or the rigs decks.
7.7
All operational personnel must ensure that no plastic containers, buckets, sampling cylinders, drip
trays and associated vessels that may be used, or have the potential to be used for the collection or
storage of hydrocarbons, are present in the well test area, workshop or laboratory.
7.8
The only exception to this will be during the taking of a sample of hydrocarbon for the measurement of liquid specific gravity or a BS&W. In this case the sample may be collected in the supplied
glass measuring cylinders that will now replace the previous used plastic versions.
7.9
If the client requires a dead oil sample to be taken from the separator oil line or the surge tank, then
an earthing cable must be fitted between the valve at which the sample will be emitted, or the fitted
flying lead on the separator, and the sample container ensuring that a metal to metal contact exists
between the earthing cable clip and sample container.
7.10
If it is necessary to purge hydrocarbons from any valve or sampling point to atmosphere via a
metal bucket or drip tray, the following procedure must be followed.

REF: OP 019
R E V: 03
DATE:
26 April 1999
PAGE 9 of 9
7.11
Place an empty metal bucket/drip tray on the separator skid or rig deck immediately below the
point of hydrocarbon release and connect the earthing flying lead directly to the bucket body so
that the bucket is grounded to the pipe or vessel containing the hydrocarbons.
7.12
Slowly open the valve to release the hydrocarbons in a controlled manner so as to reduce as far as
practicable the potential to create fluid friction and any resultant static.
NOTE: Any static that is produced will dissipate to earth via the earthing cable from the
metal bucket/drip tray to the rig structure, this prevents a potential difference between the
hydrocarbon source and receptor and the resultant chance of a static charge being released.
7.13
Always use an empty bucket/drip tray before commencing operations of this nature and once the
operation is complete or if the bucket becomes half full, empty the bucket before continuing the
operation.
NOTE: It is critical that the inventory of hydrocarbons contained in open buckets or drip
trays is kept to a minimum in the well test area, this would be crucial in the event of a fire.
7.14
Once the operation is complete close the sampling/purging valve and then remove the
earthing cable from the container and remove it from the area to the waste oil drum. Empty
the contents from the waste container to the drum and then replace the drum cap.
7.15
If replacing the bucket/drip tray to the site of hydrocarbon discharge the earthing cable must
be reconnected before leaving the area.
7.16
Never hang a bucket from any point on the well test equipment by its handle, all buckets or
drip trays must be in physical contact with the equipments skid or rigs deck and an earthing
lead connected.
7.17
Leave at least a 10 - 20% space for expansion inside the container. Allow the sample to de-gas for
as long as possible before screwing on the lid as agitation during shipping causes evolution of gas
which could cause the vessel to rupture. Do not allow rainwater, spray, etc to contaminate the
sample while it is de-gassing.
7.18
The sample should be labelled as per Section 1.6 of this procedure.
WORKSHOP SERVICE OF CSB

REF: OP 091
R E V: 03
DATE: 28 June 2000
PAGE 1 of 4
DO NOT PROCEED with service until it has been established that the CSB has at least 6 months of valid
certification left.
When using this procedure, all personnel must wear the appropriate PPE:- safety glasses,
safety boots, coveralls, etc. Protective gloves should be worn when handling all
chemicals.
BEFORE CONTINUING with the process of emptying and cleaning a bottle, confirm that the bottle does
not contain a sample still required by the Client. Do not proceed unless written confirmation exists to
proceed.
WARNING: The contents of the sample bottle may contain poisonous and/or flammable gas. The
contents should be tested for the presence of hydrogen sulphide using a suitable meter and the
appropriate steps taken to reduce exposure to the Operator.
1.0
EMPTYING CONVENTIONAL SAMPLE BOTTLE (CSB)
1.1
1.2
1.3
1.4
1.5
1.6
1.7
Ensure all valves on sample bottle and single valve end are closed.
Remove all valve plugs. Beware of any pressure trapped behind plugs.
Connect bleed pipe to valve port V2 and put other end into waste container.
Slowly open V2 to allow sample to escape into waste container.
Once sample has stopped close V2, leaving bleed pipe connected to V2.
Connect nitrogen hose to V3 and use nitrogen regulator to apply 100 psi.
Open V3 and push sample piston to top of bottle, slowly opening V2 draining the remaining
sample into the container.
Once sample cylinder empty close V3 and V2, bleed off and disconnect nitrogen hose from V3.
Disconnect bleed pipe from V2 and connect to V3.
Connect nitrogen hose to V2.
Using nitrogen regulator apply 100 psi. Open V2.
Slowly open V3 allowing sample piston to move to bottom of sample cylinder pushing water/
glycol out into waste container.
Close V2 and bleed off and disconnect nitrogen hose.
Open V2 ad V3 slowly draining remaining nitrogen above sample piston.
Disconnect bleed pipe and open all valves fully, ensure there is no pressure left inside sample
cylinder.
Slacken off cylinder grub screw and remove single valve end.
Remove piston and agitation ring from sample cylinder carefully.
Remove o-rings, GT seals, back up rings and slipstrip from sample piston and single valve end.
BUR and slipstrip can be re-used if necessary.
1.8
1.9
1.10
1.11
1.12
1.13
1.14
1.15
1.16
1.17
1.18
Refer to DR 766
N O T E : ALL CSB COMPONENTS SHOULD BE KEPT TOGETHER DURING CLEANING AND

ASSEMBLY PROCEDURES. ENSURE ALL COMPONENTS ARE SUITABLY ENGRAVED/
ETCHED WITH SERIAL NUMBER OF BOTTLE.
P R E P A R E D B Y:
DMW
VERIFIED BY:
DG

REF: OP 091
R E V: 03
DATE: 28 June 2000
PAGE 2 of 4
2.0
CLEANING AND REDRESS OF CONVENTIONAL SAMPLE BOTTLE (CSB)
2.1
Clean all parts thoroughly using either a designated solvent cleaning system or in the absence of
such a system use a suitable solvent such as Safety Kleen washing out the residue with a pH 7
detergent such as Decon Neutracon. Ensure that all local environmental and health regulations
are followed when disposing of waste and handling solvents and chemicals.
Dry all components thoroughly, ensure all moisture is removed from the sample areas.
Note and update sample bottle history Form (Form 058) with any changes of serial numbers on
component parts. CHECK ALL PARTS OF THE BOTTLE ARE PRESSURE RATE THE SAME ie
10K, 13K or 15K. DO NOT MIX RATINGS.
Dry all components thoroughly. Ensure all moisture is removed from sample areas.
Inspect all components for wear or damage.
Note and update Sample Bottle History (Form 058) with any changes of serial numbers on
component parts. CHECK THAT ALL PARTS OF BOTTLE ARE PRESSURE RATED THE SAME IE
10K, 13K OR 15K. DO NOT MIX RATINGS.
Inspect and reassemble bottle with new seals. Molykote silicone grease should be used to coat
elastomers. Do not apply excessively.
2.2
2.3
2.4
2.5
2.6
2.7
3.0
INSPECTION OF CSB BEFORE REDRESS
3.1
Sample cylinder
- Cylinder bore including o-ring seal face - free of scratches.
- Internal thread - no damage or galling.
- Autoclave threads - no damage or galling.
- Autoclave seat - no scratches, etc.
Piston
- GT seal groove - no scratches.
- Outside diameter - no high spots.
Agitation Ring
- No scratches or high spots.
Single Valve Block
- o-ring grooves - no scratches.
- Thread - no damage or galling.
Autoclave Valves - To Check Valve Packing Torque
- Remove valve handle.
- Slacken off packing grub screws.
- Using torque wrench (35 - 40 ft/lbs) check torque on packing nut is correct.
- Tighten grub screws.
- Replace valve handle.
3.2
3.3
3.4
3.5

REF: OP 091
4.0
R E V: 03
DATE: 28 June 2000
PAGE 3 of 4
ROUTINE PRESSURE TEST FOR CSB
SAFETY NOTE
All pressure testing to take place in pressure test bay ensuring the pump is situated outside the test
bay. On no account should any unauthorised personnel enter the test bay when high pressure is
applied to the assembly. Use only fully rated and traceable pressure fittings and hoses. Do not overtighten high pressure metal to metal sealed fittings and connections.
Inspect all pressure equipment and fittings prior to carrying out testing.
All pressure tests should be recorded on a calibrated chart recorder (six month re-calibration interval)
4.1
4.2
4.3
4.4
4.5
4.6
4.7
4.8
4.9
4.10
4.11
4.12
4.13
4.14
4.15
4.16
4.17
4.18
4.19
4.20
4.21
4.22
4.23
4.24
4.25
4.26
4.27
4.28
4.29
4.30
4.31
4.32
4.33
4.34
Close V3 and open V1 and V2 connect nitrogen line to V3 and regulate nitrogen to a maximum of
100 psi.
Open V3 slowly pushing the piston and agitation ring up to the sample end of the bottle.
Close V3 and bleed off the nitrogen line.
Slowly open V3 fully and bleed the remaining nitrogen from the sample bottle.
Connect nitrogen to V1 and regulate nitrogen to a maximum of 100 psi then flush across the top of
the piston and agitation ring.
Close V2 slowly and push the piston back down the sample bottle until it connects with the valve
end.
Close V1 and bleed off the nitrogen line.
Slowly open V1 fully and bleed the remaining nitrogen from the sample bottle.
Ensure valves V1 and V2 are open.
Close V3 and connect test manifold to valve port but do not tighten.
Connect water/glycol pump to manifold and flush through until all air is expelled from manifold
and nitrogen line.
Tighten manifold into bottle once all air is expelled. Pressure up manifold to maximum working
pressure of sample bottle to test manifold. (This also tests V3 in the closed position, from the
opposite direction from normal).
Upon completion of successful test, bleed off pressure from manifold.
Open V3 fully and pressure up bottle in increments stopping every 5000 psi to ensure there are no
leaks in bottle, by doing this we are testing the piston seals.
Monitor pump for any leaks and hold test for 15 minutes.
Upon completion of successful test, bleed off pressure to zero. Disconnect CEJN QRC from hose/
manifold.
Close V3 and attach nitrogen to V1 (using short 90 Nipple) and flush across top of piston and
agitation ring.
Remove slimline plug from manifold and connect 90 nipple to port in manifold
Close V2 and pressure up to 500 psi. Slowly open V3 to displace 120 cc of water/glycol from each
sample bottle in turn, close each V3 in turn.
Close V1, trapping 500 psi at sample end and bleed off nitrogen line.
Re-connect CEJN QRC from pump liner to manifold
Start pump and raise pressure to 500 psi against closed V3 on each sample bottle
Slowly open V3 fully on each sample bottle and increase pressure in increments stopping every
5000 psi until maximum working pressure is achieved.
Monitor chart for any leaks for 5 minutes.
Upon completion of successful test, bleed pressure off until 500 psi is reached.
Insert valve plugs into V1 and V2 on each sample bottle.
Fully open valves V1 and V2 and increase to maximum working pressure.
Upon completion of successful test, bleed off pressure until 500 psi is reached.
Slowly slacken valve plugs bleeding the pressure from V1 and V2.
Pump the bottle to a pressure of 5,000 psi thus ensuring the bottle is full of water/glycol.
Bleed pressure down to zero
Repeat pressure up to 5,000 psi to ensure the sample bottles are full of water/glycol (pressure
should rise immediately if no air is present in the water.
Bleed to zero and disconnect manifold

REF: OP 091
4.35
4.36
R E V: 03
DATE: 28 June 2000
PAGE 4 of 4
4.41
Close all valves (V1, V2 and V3) and plug all valve ports.
Mark the chart with serial number, the pressure it was tested, date of the test and Technicians
name.
Complete Conventional Sample Bottle Status Form 043 and place a copy in the bottle box and
original in the bottle file.
The following items should be placed in the bottle box in a plastic sealed bag,
- Inspection Release Note for Sample Cylinder
- 2 x Flammable Gas labels
- 2 x Sample Data label
- US DOT Exemption as appropriate
- UK HSE exemption to CDG-CPL2 Regulations.
Complete a green status label and attach it to the sample bottle box.
Ensure the sample bottle box is fit for purpose and presentable. Remove all rust and corrosion
and re-paint or replace affected parts.
Ensure certification database is updated. File test charts in bottle vertical file.
5.0
MARKING
4.37
4.38
4.39
4.40
With the introduction of the UK Regulations:

Health and Safety Executive SI 2092 (1996), The Carriage of Dangerous Goods (Classification, Packaging
and Labelling) and
Use of Transportable Pressure Receptacles Regulations.
It is a requirement that all oil sample bottles being shipped in the UK are marked with the following
exemption number:
-
CDGCPL2 EO 1/2000
This should be marked by vibro-engraving or chemical etching on the ID band on the sample bottle
cylinder.
WORKSHOP SERVICE OF SSB

REF: OP 023
R E V: 04
DATE: 28 June 2000
PAGE 1 of 4
DO NOT PROCEED with this service until it has been established that sample cylinder and nitrogen
cylinder have at least 6 months of valid certification left.
BEFORE CONTINUING with the process of emptying and cleaning a bottle, confirm that the bottle does
not contain a sample still required by the Client. Do not proceed unless written confirmation exists to
proceed.
WARNING: The contents of the sample bottle may include poisonous and/or flammable gas. Therefore,
the bottle should be disassembled in a well ventilated area.
The contents of the sample bottle may contain poisonous and/or flammable gas. The contents should be
tested for the presence of hydrogen sulphide using a suitable meter and the appropriate steps taken to
reduce exposure to the Operator.
1.0
EMPTYING SINGLE-PHASE SAMPLE BOTTLE (SSB) Refer to DR 765 and DR 1404
1.1
1.2
Close all valves on sample bottle and double valve end.

Remove all valve plugs. Beware of any pressure trapped behind plugs. Slowly open V3 releasing
any nitrogen.
Connect bleed pipe to valve port V2 and put other end into waste container.
Slowly open V2 to allow remaining sample to escape into waste container.
Once gas pressure is bled off V2, leave bleed pipe connected to V2.
Connect nitrogen hose to V4 and use nitrogen regulator to apply 100 psi.
Open V4 and push sample piston to top of bottle, slowly opening V2 draining the remaining
sample into the container.
Once sample cylinder empty close V4 and disconnect the nitrogen hose.
Disconnect bleed pipe from V2 and connect to V4.
Connect nitrogen hose to V2 and apply 100 psi.
Open V4 slowly allowing the water/glycol to drain into the waste container, allowing piston to
move to the bottom of the cylinder.
Close V2 and bleed off and disconnect nitrogen hose.
Open V2 and V3 slowly draining remaining nitrogen.
Disconnect bleed pipe and open all valves fully. Ensure no trapped pressure remains inside SSB.
Slacken off cylinder grub screw (QT 421).
Unscrew nitrogen cylinder (AR 096) from sample chamber (AR 095), allowing excess water to drain
out into a suitable waste container.
Remove piston (QR 118) and agitation ring (QR 119) from sample chamber. Remove GT seal and
slipstrip from piston. BUR and slipstrip can be re-used if necessary.
Place nitrogen cylinder (QR 122) in the vice, slacken off grub screw and unscrew double valve block
(AR 100).
Unscrew retainer (QR 125), disassemble nitrogen piston (QR 123) and rod (QR 124) from nitrogen
cylinder.
Remove all elastomers, slipstrips and back up rings from components, keeping all separate bottle
components together.
1.3
1.4
1.5
1.6
1.7
1.8
1.9
1.10
1.11
1.12
1.13
1.14
1.15
1.16
1.17
1.18
1.19
1.20
DMW
VERIFIED BY:
DG

REF: OP 023
R E V: 04
DATE: 28 June 2000
PAGE 2 of 4
2.0
CLEANING AND REDRESS OF CONVENTIONAL SAMPLE BOTTLE (CSB)
2.1
Clean all parts thoroughly using either a designated solvent cleaning system or in the absence of
such a system use a suitable solvent such as Safety Kleen washing out the residue with a pH 7
detergent such as Decon Neutracon. Ensure that all local environmental and health regulations
are followed when disposing of waste and handling solvents and chemicals.
Dry all components thoroughly, ensure all moisture is removed from the sample areas.
Note and update sample bottle history Form (Form 058) with any changes of serial numbers on
component parts. CHECK ALL PARTS OF THE BOTTLE ARE PRESSURE RATE THE SAME ie
10K, 13K or 15K. DO NOT MIX RATINGS.
Dry all components thoroughly. Ensure all moisture is removed from sample areas.
Inspect all components for wear or damage.
Note and update Sample Bottle History (Form 058) with any changes of serial numbers on
component parts. CHECK THAT ALL PARTS OF BOTTLE ARE PRESSURE RATED THE SAME IE
10K, 13K OR 15K. DO NOT MIX RATINGS.
Inspect and reassemble bottle with new seals. Molykote silicone grease should be used to coat
elastomers. Do not apply excessively.
2.2
2.3
2.4
2.5
2.6
2.7
3.0
INSPECTION OF SSB BEFORE REDRESS
3.1
In order to ensure the correct and safe operation of the sample bottle, a through inspection of all
parts is required before redress.
NOTE: Any damage should be reported to the Workshop Supervisor.
Sample cylinder
- Cylinder bore including o-ring seal face - free of scratches or high spots.
- Internal thread - no damage or galling.
Piston
- GT seal groove - no scratches.
- Outside diameter - no high spots.
Agitation Ring
- No scratches or high spots.
By-pass Rod
- Surface finish of rod - as new.
Retainer
Thread - no damage or galling
Nitrogen Cylinder
- o-ring face - no scratches or high spots.
- Piston bore - no scratches or high spots.
- Threads - no damage or galling.
Double Valve Block
- Thread - no damage or galling.
- N-Stamp - still visible.
Autoclave Valves
- To Check Packing Torque
- Remove valve handle.
- Slacken off packing grub screws.
- Using torque wrench (35 - 40 ft/lbs) check torque on packing nut is correct.
- Tighten grub screws.
- Replace valve handle.
3.2
3.2
3.3
3.4
3.5
3.6
3.7
3.8

REF: OP 023
R E V: 04
DATE: 28 June 2000
PAGE 3 of 4
4.0
REDRESSING AND ASSEMBLING OF SSB
4.1
Before redressing, check all serial numbers are updated on the Bottle History Form (Form 058) and
any changes of component parts or numbers noted.
Replace seals are follows. Refer to DR 765 and DR 1404.
Light smear of silicon grease on all o-rings and tee seals.
Light covering of copper slip on all threads, except autoclave port.
Place bypass tube in double valve block.
NOTE: On some of the bottles a rod-spacer is required. This can be positioned after the nitrogen
cylinder is in position.
Screw on nitrogen cylinder.
Push nitrogen piston onto rod and screw on retainer.
Place sample cylinder in vice and insert agitation ring.
Insert piston into cylinder and push in carefully.
Screw nitrogen cylinder onto sample cylinder or double valve block to ensure sample ports are at
90 to nitrogen and water/glycol ports.
4.2
4.3
4.4
4.5
4.6
4.7
4.8
5.0
ROUTINE PRESSURE TEST FOR SSB
SAFETY NOTE
All pressure testing shall take place in a designated pressure test bay ensuring the pump is situated
outside the test bay. On no account should any unauthorised personnel enter the test bay when high
pressure is applied to the assembly. Use only fully rated and traceable pressure fittings and hoses. Do
not over-tighten high pressure metal to metal sealed fittings and connections.
Inspect all pressure equipment and fittings prior to carrying out testing.
All pressure tests should be recorded on a calibrated chart recorder (six month re-calibration interval)
5.1
5.2
5.3
5.4
5.5
5.6
5.7
5.8
5.9
5.10
5.11
5.12
5.13
5.14
5.15
5.16
5.17
5.18
Open all valves on bottle (V1, V2, V3, and V4).

Close V2 and connect nitrogen to V1, regulate nitrogen pressure to 100 psi and push sample piston
and agitation ring to the bottom of the bottle, then open V2 fully to bleed off nitrogen and
disconnect.
Connect nitrogen to V3, regulate nitrogen pressure to 100 psi and push nitrogen piston to the top of
the nitrogen sub. Bleed off nitrogen and disconnect from V3.
Close V4 and connect manifold to valve port, but do not tighten.
Connect water/glycol pump to manifold and flush with water/glycol.
Tighten manifold into bottle once all air is expelled. Pressure up manifold to maximum working
pressure to test manifold (this will test V4 in the closed position from the opposite direction from
normal). Monitor chart.
Upon completion of successful test, bleed off pressure from manifold.
Open V4 fully and pressure up bottle in increments stopping every 5,000 psi to ensure there are no
leaks evident in bottle, thereby testing the piston seals and nitrogen sub seal.
Monitor chart for any leaks and hold test for 15 minutes.
Upon completion of successful test, bleed off pressure to zero. Disconnect CEJN QRC from hose/
manifold.
Remove slimline plug from end of test manifold.
Close V4 and attach nitrogen to V3 (using short 90 Nipple) and pressure up to 500 psi.
Slowly open V4 to displace water/glycol from each sample bottle nitrogen sub in turn, close each
V3 in turn trapping 500 psi of nitrogen in nitrogen cylinder chamber.
Close V4 and attach nitrogen to V1, slowly flush across the sample end of the bottle, approx 50 psi.
Close V2.
Slowly open V4 and remove 120 cc water from each bottle in turn, close each V4 in turn.
Increase nitrogen pressure to 500 psi.
Close V1, trapping 500 psi nitrogen, bleed off nitrogen line and disconnect.
Replace the slimline plug into the test manifold.

REF: OP 023
5.19
5.20
5.21
R E V: 04
DATE: 28 June 2000
PAGE 4 of 4
5.40
Re-connect CEJN QRC from pump liner to manifold.

Start pump and raise pressure to 500 psi against closed V4 on each sample bottle.
Once 500 psi is achieved slowly open V4 fully on each sample bottle and increase pressure in
increments stopping every 5,000 psi until maximum working pressure of sample bottle is achieved.
Insert valve plugs into V1, V2 and V3.
Fully open valves V1, V2 and V3 and increase to maximum working pressure of bottle.
Monitor chart for any leaks and hold for 5 minutes.
Slowly slacken valve plugs bleeding the nitrogen pressure from V1, V2 and V3.
Pump the bottle up to a pressure of 5,000 psi, thus ensuring the bottle is full of water/glycol.
Bleed pressure down to zero.
Repeat the pressure up to 5,000 psi to ensure each sample bottle is full of water. (Pressure should
rise immediately if there is no air present in the water).
Bleed pressure down to zero.
Close V4 and disconnect manifold.
Close all valves (V1, V2, V3 and V4) and plug all valve ports.
Mark the chart with serial number, the pressure it was tested, date of the test and Technician's
name.
Complete Singlephase Sample Bottle Status (Form 042) and place a copy in the bottle box and
original in the bottle vertical file.
The following items should be placed in the bottle box in a plastic sealed bag
Inspection Release Note for Sample Cylinder and Nitrogen Cylinder
2 x Flammable Gas labels
2 x Sample Data label
US DOT Exemption as appropriate
UK HSE exemption to CDG-CPL2 Regulations
Complete a green status label and attach it to the sample bottle box.
Ensure the sample bottle box is fit for purpose and presentable. Remove all rust and corrosion and
re-paint or replace affected parts.
Ensure certification database is updated. File test charts in bottle vertical file.
6.0
MARKING
5.22
5.23
5.24
5.25
5.26
5.27
5.28
5.29
5.30
5.31
5.32
5.33
5.34
5.35
5.36
5.37
5.38
5.39
With the introduction of the UK Regulations:

Health and Safety Executive SI 2092 (1996), The Carriage of Dangerous Goods (Classification, Packaging
and Labelling) and
Use of Transportable Pressure Receptacles Regulations.
It is a requirement that all oil sample bottles being shipped in the UK are marked with the following
exemption number:
-
CDGCPL2 EO 1/2000
This should be marked by vibro-engraving or chemical etching on the ID band on the sample bottle
cylinder.
GAS SAMPLE CYLINDER CLEAN AND TEST PROCEDURE

REF: OP 077
R E V: 01
D A T E : 3 November 1995
PAGE 1 of 1
1 . Log the following information from the gas sample bottle:a)

b)
c)
d)
e)
f)
g)
Cylinder serial no
Date of original certification
Date of last certification
Volume of cylinder
Cylinder type
Valve type
Valve outlet
A copy of this information and work to be carried out must be returned to Oilphase prior to work
commencing.
2 . Dump contents if any, take the necessary safety precautions. Remove valves.
3 . Clean cylinder thoroughly both internally and externally.
4 . Dry cylinder completely.
5 . Inspect cylinder walls, threads for damage. If a 5 year recertification is necessary Bureau Veritas
Surveyor should be present.
6 . Fill bottle with fluid and pressure test to maximum working pressure or test pressure for
duration as applicable.
7 . Upon completion of satisfactory test drain fluid and dry cylinder thoroughly, particularly
internally.
8 . Refit valves and draw a vacuum of <1 mBar, plug valves.
9 . Ensure transit box is clean and fit for purpose. Label cylinder and box. Arrange shipment with
the following documentation enclosed:-
2
2
1
1
x
x
x
x
Sample labels
Flammable gas labels
Bureau Veritas release note
Gas bottle service form
DM
VERIFIED BY:
CD
A P P R O V E D B Y : KM
ROUTINE PRESSURE TEST OF GAS SAMPLE CYLINDER

R E F : OP021
R E V: 02
DATE: 10 March 1994
PAGE 1 of 2
Lay gas sample cylinder on its side. Open then close both valves to check there is no pressure in
the cylinder.
Connect vacuum pump to valve A.
Ensure valve B is closed.
Open valve A and evacuate cylinder to < 2 mm Hg.
When vacuum has been achieved close cylinder valve A.
Disconnect vacuum pump and connect nitrogen hose from FTU to valve A. (Leave connection to
valve A finger tight).
Flush hose from FTU to gas sample cylinder with OFN before tightening connection into valve A.
Open valve A to fill cylinder with OFN.
Boost OFN pressure with FTU nitrogen booster to maximum working pressure of cylinder (200 bar;
2900 psig).
10
When pressure has stabilised hold for 30 mins.
11
Using Snoop check for leaks paying particular attention to:

threaded connection of valves to cylinder body.
Stem packings of valve A.
Valve port B.
12
If pressure test is successful (no leaks, stable pressure) plug valve port B and open the valve. (If
necessary boost OFN to re-establish test pressure).
13
Close valve A and bleed off hose pressure at FTU.
14
Disconnect FTU nitrogen hose and adapter from cylinder.
15
Using snoop check for leaks paying particular attention to:

Stem packings of valve B.
Valve port A.
16
If no leaks are found during 30 mins monitoring period open valve A to carefully bleed off OFN
pressure from cylinder.
17
Re-connect vacuum pump to valve A and evacuate cylinder to < 2 mm Hg.
18
When vacuum has been achieved close valves A and B.

This document has been issued as an "Uncontrolled" document
and shall not be subject to amendment or update unless
overstamped "Controlled Copy" in red ink.
CF
VERIFIED BY:
GD
ROUTINE PRESSURE TEST OF GAS SAMPLE CYLINDER

R E F : OP021
R E V: 02
DATE: 10 March 1994
PAGE 2 of 2
19
Plug valve A.
20
Complete form 044 and place copy in self-sealing plastic bag inside gas sample cylinder box. File
original form 044 in gas cylinder status file. Copy form 044 to Operations Manager who will
update the bottle status board and the bottle files.
21
Write out green label and attach to cylinder box as per OP010.
22
Place gas sample cylinder in serviced equipment area in its transportation box.
USE OF WELKER SAMPLE CYLINDER CP7MA

REF: OP 110
1.0
R E V: 01
DATE: 17 July 1996
PAGE 1 of 2
INTRODUCTION
This procedure is specific for the CPA-1000MA cylinder but is applicable to generally most Welker
piston sample cylinder. This procedure describes how to introduce a sample into the cylinder and
how to mix the sample prior to analysis.
2.0
DESCRIPTION
The Welker cylinder is a piston cylinder with two flanges or end cap labelled "product inlet" and
"precharge end" plus a protruding indicator rod from the precharge end. The cylinder is usually
equipped with valves at each end and bursting discs at each end. The cylinder also has facilities for
mixing the sample via an internal rod and paddle inside the indicator rod.
3.0
SAFETY
As with all sample cylinders the working pressure and ratings of valves, fittings and tubing and
bursting disc have to be applicable for the job in hand. When handling pressurised cylinder and
samples the proper safety clothing and equipment should be used. This procedure should only be
carried out by a suitably experienced and trained individual.
4.0
SAMPLING
PROCEDURE
4.1
Prepare the cylinder by pressurising it at the precharge end to a pressure equal to or slightly
above the sampling pressure.
4.2
Connect the sampling point valve to the product inlet valve via a suitable pipe, liner or tube.
An additional pressure gauge is advised somewhere along this pipe.
4.3
To purge the lines of sample either:a)
Open the sampling point valve and purge at the pipe to product inlet valve fitting
for 3 - 5 times the volume of the pipe volume.
or
b)
Open the sampling point valve and purge 3 - 5 times the pipe volume via an
additional valve on a "T" piece just prior to the product inlet valve, if fitted.
or
c)
Open the sampling point valve and the product inlet valve and purge via an
additional valve on the product inlet end cap or flange, if fitted.
4.4
Let the sample fill the cylinder by gradually releasing precharge end fluid via an additional
valve and pressure gauge. Ensure that the pressure at the product inlet and the precharge
end do not vary greatly.
4.5
When the indicator rod reaches the indicator cap close the valves at the precharge end then
close the product inlet valve. Finally close the sampling point valve. The cylinder should
now contains 800 cc of sample. If applicable create a gas cap by bleeding 80 cc from the
precharge end.
PREPARED BY:
DD
VERIFIED BY:
GD
USE OF WELKER SAMPLE CYLINDER CP7MA

REF: OP 110
R E V: 01
DATE: 17 July 1996
PAGE 2 of 2
4.6
Disconnect all pipes and gauges taking care of residual pressure and sample in the pipes and
plug the valves on the cylinder.
4.7
Take a note of final pressure of the sample, temperature, sampling point, time and date of
sampling, duration of sampling and any other available data for the sample sheet.
4.8
Box and label the cylinder for shipping to storage or the laboratory for analysis or as directed.
5.0
PREPARATION OF SAMPLE FOR ANALYSIS
5.1
Ensure the cylinder serial number corresponds correctly to client instructions and/or delivery
ticket and any sampling sheet. Record the serial number on Sample Volume Tracking (Form
087).
5.2
Check all fittings for leaks and if any leaks are found record this on Form 087. Seal the leaks if
possible.
5.3
Ensure the cylinder is secure and safe for the following steps.
5.4
Measure the opening pressure and cylinder temperature on Form 087 by connecting a water
pump and calibrated pressure gauge to the precharge end and by the use of a calibrated
temperature probe.
5.5
Decide on a working pressure for the sample. This pressure should be as low as possible
below any bursting disc rating but much higher than the samples bubble point or sampling
pressure.
5.6
Pressure the sample to the working pressure by pumping into the precharge end.
5.7
Mix the sample by removing the indicator rod cap and screwing in firmly the mixing rod and
handle. Stoke the mixing rod handle 3 - 5 times maintaining a firm grasp on the handle at all
times.
5.8
Isolate pump and drain water from the precharge end. Measure the volume of water and
record this on Form 087. Sample volume is 1,000 minus the drained water volume.
5.9
Repeat 5.6 and 5.7 until the pressure in the cylinder is stable and remove the mixing rod and
handle and replace the indicator rod cap.
5.10
The sample is now ready for transfer or flashing as required by the Client.
WSM WELLSITE SAMPLING MODULE (PR 2111)

OPERATING PROCEDURES
REF: OP 193
1.0
REV: 02
DATE: 28 February 2001
PAGE 1 of 3
INTRODUCTION
The Wellsite Sampling Module (WSM) allows high temperature/pressure wellhead samples to be taken
safely, by the use of hard piping on all liners and high temperature rated valves. The module allows the
fitment of up to six SSBs or CSBs. The option to use test gauges to monitor the sample pressure also
exists. A removable drain/purge tank is fitted to the module. Optional transport wheels that can be
fitted to the module (see DR2399).
During sampling operations, correct safety procedures should be observed, all operators must wear the
appropriate PPE: disposable lab coat/coveralls, hard hat, safety glasses/face shield, safety shoes, etc.
Wear breathing apparatus if appropriate. Protective gloves should be worn when handling all chemicals.
The sample bottles should be prepared as per normal Oilphase practice and have green tags etc.
2.0
SETUP
PROCEDURE (REFER TO DR2397 FOR SCHEMATIC VIEW)
2.1
The WSM, as shipped, should have the end panels removed. Check that the drain/purge
tank is empty before commencing (a suitable place should be found for the effluent, observing
any local QHSE policy and/or local environmental regulations).
2.2
The sample bottles should be mounted to the module with the sample end of the bottle to the
sample end of the WSM. Leave the clamps unsecured for now. The WSM can have either SSB or
CSB fitted and the correct set of 1/8" water/glycol liners should be used (longer liners are for the
SSB, shorter for the CSB).
2.3
The blanking plugs should be removed and stored from the bottles and the liners to connect to the
WSM fitted to the bottles. There are two liners for the sample end and one for the water/glycol
end. The liners at the sample end should be 180 apart with the port at the water/glycol end at 90
to these. When fitting the liners at the water end an adapter is required from the 1/8" Taperseal to
the " slimline autoclave connection of the bottle. These can be tricky to fit and care should be
taken when doing so. Once the liners are all fitted and tightened the clamps can be secured.
2.4
If required, test gauges for the sample and water/glycol can be fitted to the top of the module to
monitor the pressures more accurately than the panel mounted gauges. The fittings for the test
gauges are very similar to those found on FTU, etc and have to be folded out and adjusted to
support the gauge correctly.
PREPARED BY: MI
VERIFIED BY: DG
APPROVED BY: JB

REF: OP 193
3.0
REV: 02
PRESSURE TEST WATER/GLYCOL SYSTEM
PAGE 2 of 3
(REFER TO DR2395)
Using a transfer bench or similar pump, connect the water/glycol liner to the CEJN quick connect fitting
mounted on the WSM, marked "Water/Glycol Inlet". Ensure that all the isolation valves for the water/
glycol side are closed and that all the valves on the bottles are closed.
3.1
Open isolation valve and purge the gauge with the water/glycol.
3.2
Pressure up the water/glycol system to the expected Wellhead Pressure (WHP) plus 4,000 psig, to a
maximum of 15,000 psig. Check the system holds pressure.
3.3
One at a time, the isolation valve and the bottle water/glycol valve should be opened, and the
bottle pressured up to the same test pressure. Observe for leaks. Close isolation valve for each
bottle, leaving the valve in the bottle fully open to avoid washout. Repeat for the remaining bottles.
Bleed off the liner pressure.
3.4
Remove the water liner from the WSM.
4.0
PRESSURE TEST SAMPLE SYSTEM (REFER TO DR2396)
Using the nitrogen supply and gas booster if required, the sample side of the WSM should be tested up to
the drain valve, to the same test pressure as the water/glycol side. Connect the liner to the "Sample Test"
bulkhead, on the bleed down line. The liner to the wellhead should ideally not have a valve fitted in line
to minimize risk of backing off, etc. The customer could test this liner up to the first isolation valve of the
WSM, with water, along with the wellhead.
4.1
Purge the line of air, up to and including the test gauge if fitted, with oxygen-free nitrogen.
4.2
Open the bottle valves and isolation valves for each bottle in turn, but not the upstream isolation to
the wellhead, or the drain valves (the drain pipe work is rated to 3,000 psig only, and is open ended
anyway).
4.3
Pressure up the system to the same test pressure as before and check for leaks, one bottle at a time.
4.4
Repeat for remaining bottles.
4.5
Bleed off the nitrogen test pressure slowly. Failure to do so could result in damage to the drain/
purge tank. This tank is vented, but cannot sustain the volumetric flow of dumping the test gas
from 15, 000 psi if done quickly. Close all isolation valves, leaving the bottle valves fully open to
avoid risk of washout of these valves. Remove the nitrogen liner from the WSM.

REF: OP 193
5.0
OPERATING PROCEDURE
REV: 02
PAGE 3 of 3
(REFER TO SCHEMATIC DR2397)
5.1
The sample valves and the water/glycol valve on each CSB or SSB should now be fully open, with
water/glycol side of each, pressurised to expected WHP plus 4,000 psig (to a maximum of 15,000
psig). All the isolation valves are closed.
5.2
Open the sample isolation valve for the sample bottle to be filled.
5.3
Open the sample drain valve (slowly) for the same bottle, and estimate purge of 2 - 3 liners volume.
There is no provision to check the actual volume at present, so the Field Engineer should satisfy
themselves that adequate volume has been purged through. Close drain valve.
5.4
Open isolation valve to water/glycol side of bottle.
5.5
Open purge/drain valve from water/glycol system slowly to avoid dropping pressure below WHP,
to a measuring cylinder and drain out 600 cc of water and close valve. The time taken to sample
should be the same as for conventional surface sampling.
5.6
Close all isolation and bottle valves for the bottle just filled, take care that when the sample cools,
pressure will drop. Ensure that the pressure is maintained above WHP.
5.7
Record the closing pressure, bottle number and time.
5.8
Repeat for each remaining bottle as and when required, from step 5.2.
5.9
When sampling is complete, close the upstream isolation valve of the WSM.
5.10
Using the sample test isolation valve, allow the trapped pressure in the line to bleed off in to a
suitable container and be disposed of according to local QHSE policy and /or local environmental
regulations.
5.11
Sample bottles can now be removed or replaced by empty bottles for further sampling. Remember
to replace the blanking plugs to the bottle valve ports. The samples should be labelled, etc in
accordance with Operating Procedure OP 019 Surface Sampling.

003.0 Surface Sampling Operating Procedures

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SURFACE SAMPLING - GENERAL GUIDELINES

SURFACE SAMPLING - GENERAL GUIDELINES

LIQUID SURFACE SAMPLING using the Oilphase Conventional Bottle

Close V4 and disconnect pump.

Ensure all valves are closed.

Pressure up liner by opening valve V1.

SURFACE SAMPLING - GENERAL GUIDELINES

1/2" NPT (m) x 1/4" JIC (m) adapter

SURFACE SAMPLING - GENERAL GUIDELINES

LIQUID SURFACE SAMPLING using the Oilphase Single-phase Sample Bottle

Place sample bottle in stand. See Figure 2.

1/2" NPT (m) x 1/4" SL Autoclave (m) adapter

SURFACE SAMPLING - GENERAL GUIDELINES

Close V4 and remove pump.

Ensure all valves are closed (except for SSB V3).

Pressure up liner by opening valve on sampling point V1.

Connect glycol/water pump to valve CSB V3.

Close CSB V1. Bleed OFN and rig down liner.

SURFACE SAMPLING - GENERAL GUIDELINES

1/2" NPT (m) x 1/4" JIC (m) adapter

SURFACE SAMPLING - GENERAL GUIDELINES

When bottle is full close valves V2 and GSB V1.

Open V2 to restore separator pressure to bottle.

If possible, measure and record the pH and temperature of the sample.

SURFACE SAMPLING - GENERAL GUIDELINES

PRODUCED WATER SAMPLING (for dissolved organics)

Use clean glass bottles, not polyethylene.

Fill through a tube as above but do not overflow.

ATMOSPHERIC OIL SAMPLING

SURFACE SAMPLING - GENERAL GUIDELINES

The sample should be labelled as per Section 1.6 of this procedure.

WORKSHOP SERVICE OF CSB

DATE: 28 June 2000

EMPTYING CONVENTIONAL SAMPLE BOTTLE (CSB)

N O T E : ALL CSB COMPONENTS SHOULD BE KEPT TOGETHER DURING CLEANING AND

WORKSHOP SERVICE OF CSB

DATE: 28 June 2000

CLEANING AND REDRESS OF CONVENTIONAL SAMPLE BOTTLE (CSB)

INSPECTION OF CSB BEFORE REDRESS

WORKSHOP SERVICE OF CSB

DATE: 28 June 2000

ROUTINE PRESSURE TEST FOR CSB

WORKSHOP SERVICE OF CSB

DATE: 28 June 2000

With the introduction of the UK Regulations:

WORKSHOP SERVICE OF SSB

DATE: 28 June 2000

EMPTYING SINGLE-PHASE SAMPLE BOTTLE (SSB) Refer to DR 765 and DR 1404

Close all valves on sample bottle and double valve end.

WORKSHOP SERVICE OF SSB

DATE: 28 June 2000

CLEANING AND REDRESS OF CONVENTIONAL SAMPLE BOTTLE (CSB)

INSPECTION OF SSB BEFORE REDRESS

WORKSHOP SERVICE OF SSB

DATE: 28 June 2000

REDRESSING AND ASSEMBLING OF SSB

ROUTINE PRESSURE TEST FOR SSB

Open all valves on bottle (V1, V2, V3, and V4).

WORKSHOP SERVICE OF SSB

DATE: 28 June 2000

Re-connect CEJN QRC from pump liner to manifold.

With the introduction of the UK Regulations:

GAS SAMPLE CYLINDER CLEAN AND TEST PROCEDURE

1 . Log the following information from the gas sample bottle:a)