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Composites: Part B
journal homepage: www.elsevier.com/locate/compositesb
a r t i c l e
i n f o
Article history:
Received 4 December 2008
Received in revised form 25 January 2009
Accepted 6 February 2009
Available online 7 May 2009
Keywords:
B. Creep
A. Particle reinforcement
C. Micro-mechanics
B. Thermomechanical Functionally graded
material (FGM)
a b s t r a c t
An integrated micromechanical-structural framework is presented to analyze coupled heat conduction
and deformations of functionally graded materials (FGM) having temperature and stress dependent viscoelastic constituents. A through-thickness continuous variation of the thermal and mechanical properties of the FGM is approximated as an assembly of homogeneous layers. Average thermo-mechanical
properties in each homogeneous medium are computed using a simplied micromechanical model for
particle reinforced composites. This micromechanical model consists of two isotropic constituents. The
mechanical properties of each constituent are timestresstemperature dependent. The thermal properties (coefcient of thermal expansion and thermal conductivity) of each constituent are allowed to vary
with temperature. Sequentially coupled heat transfer and displacement analyses are performed, which
allow analyzing stress/strain behaviors of FGM having time and temperature dependent material properties. The thermo-mechanical responses of the homogenized FGM obtained from micromechanical
model are compared with experimental data and the results obtained from nite element (FE) analysis
of FGMs having microstructural details. The present micromechanical-modeling approach is computationally efcient and shows good agreement with experiments in predicting time-dependent responses
of FGMs. Our analysis forecasts a better design for creep resistant materials using particulate FGM
composites.
2009 Elsevier Ltd. All rights reserved.
1. Introduction
Functionally graded materials (FGMs) are composite materials
in which the physical and mechanical properties of the materials
vary spatially along specic directions over the entire domain.
Changes in the composition of the constituents result in a nonuniform microstructure leading to gradual variations of the macroscopic material properties. Structures made of FGMs are often
subjected to high temperature gradient loadings. Under such conditions, the properties of the constituents can vary signicantly
with temperature accompanied by a non-negligible time-dependent response. For example, FGMs composed of metal and ceramic
constituents tend to creep at high temperatures. In addition, nonuniform temperature elds and mismatch in the properties of the
constituents in FGMs generate thermal/residual stresses that affect
overall performance of FGMs. Therefore, understanding nonlinear
thermo-viscoelastic behavior of FGMs plays a signicant role in
evaluating the performance of structures made from such materials. This study investigates the non-linear viscoelastic behavior of
FGMs during transient heat conduction process. The thermal and
* Corresponding author. Tel.: +1 979 458 3579; fax: +1 979 845 3081.
E-mail address: amuliana@neo.tamu.edu (A.H. Muliana).
1359-8368/$ - see front matter 2009 Elsevier Ltd. All rights reserved.
doi:10.1016/j.compositesb.2009.02.003
512
a) Functionally graded
material idealization
b) Microstructure
details
c) Microstructure
Idealization
d) RVE
e) Unit Cell
513
DSijkl wt ws
Z
0
dn
arn aT
ws ws
Z s
0
dn
arn aT
where utj
@T t
;
@xj
where qti and utj are the heat ux and temperature gradient. K tij is
the temperature dependent thermal conductivity. K tij is also called
the consistent tangent thermal conductivity, which varies with
temperature at current time t.
2.2. Effective thermo-viscoelastic properties
By satisfying the displacement and traction continuities at the
interfaces during thermo-viscoelastic deformations, the expression
for the effective time dependent stiffness matrix and coefcient of
thermal expansion are formulated. This formulation leads to an
effective timetemperaturestress-dependent coefcient of thermal expansion. The effective thermal conductivity is formulated
by imposing heat ux and temperature continuities at the subcell
interfaces.
The method of volume averaging is used to evaluate the effective response of a unit-cell (micromechanical model). The average
stresses and strains are dened by:
N Z
N
1X
1X
a a
a
r
xk dV a
V a rij and
ij
V a1 V a
V a1
N Z
N
1X
1X
a
eij
eija xka dV a
V a eij ;
V a1 V a
V a1
r ij
4
5
where an over bar indicates average material quantities. The superscript a denotes the subcells number and N is the number of suba
a
cells. Stress rij and strain eij are the average stress and strain in
each subcell. The unit-cell volume V is:
N
X
V a ;
N 4:
a1
The superscript t indicates a variable at time t. Sijkl 0 are the components of the instantaneous elastic compliance, DSijkl wt ws are
the components of the transient compliances, and aij are the components of coefcient of thermal expansion (CTE) tensor. The
parameters T t and T 0 are the current and reference temperatures.
The linear coefcient of thermal expansion, a, also varies with temperatures. w is the reduced-time (effective time) given by:
wt wt
Z t
s ; T s rskl
d g 2 r
dDT s
aij T t
ds:
ds
dsds
0
for solving the stress tensor using the incremental strains. An iterative scheme is included in order to minimize residual from the linearization. A detailed discussion about the non-linear parameters
and recursive algorithm formulation of Eq. (1) can be found in
Haj-Ali and Muliana [10] and Muliana and Khan [16]. An outline
of the recursiveiterative algorithm for the nonlinear isotropic viscoelastic material is given Appendix A.
The conduction mode of heat transfer is considered. The Fourier
law of heat conduction with temperature dependent thermal conductivity is used and can be expressed as:
7
8
and DT t;a DT t
The micromechanical model is designed to be compatible with displacement based FE software, in which the incremental strains are
chosen as independent variable. We introduce a strain interaction
t;a
matrix Bt;a , which relates the subcell average strains, Deij , to
t
the unit-cell average strain, Deij , and it is written as:
a
a;t
Det;
Bijkl Detkl
ij
10
514
The average heat ux equation for a homogeneous composite medium is expressed by the Fourier law of heat conduction as:
N
h
i
1X
a;t
a;t
a;t
tij
Dr
V a C ijkl Bklrs Detrs akl DT t
V a1
tkl DT t
C tijkl Detkl a
ti K tij u
tj
q
11
From the above equation, the effective tangent stiffness matrix, C tijrs ,
is:
C tijrs
N
1X
a;t a;t
V a C ijkl Bklrs ;
V a1
12
a;t
a tij
1;t N
X
C ijkl
a;t
a;t
V a C klmn amn
;
13
a tij a t dij
1;t h
i
C ijkl
A;t
4;t
3 3;t 3;t
C klmn amn V 4 C klmn a4;t
V A C klmn aA;t
mn V
mn ;
V
14
aA;t
aA;t dij
ij
X 1;t
ijkl
where
X tijkl
i
1 h 1 1;t
2 2;t
; and
V
a
V
a
ij
ij
VA
15
16
1 h
VA
11;t
C ijkl
21;t
C ijkl
17
The effective CTE in Eq. (14) depends on the moduli and CTE of each
constituent. Thus, for the stress, temperature and time dependent
constituent mechanical and thermal properties, the effective CTE
also varies with stress, temperature and time. A detailed formulation for the effective coefcient of thermal expansion can be found
in Appendix B.
2.3. Effective thermal conductivity
A volume averaging method based on spatial variation of the
temperature gradient in each subcell is adopted to determine the
effective thermal conductivity of particle reinforced composites.
The average heat ux and temperature gradient are:
N Z
N
1X
1X
a
a
a
qi xk dV a
V a qi ; and
V a1 V a
V a1
N Z
N
1X
1X
a
i
u
uia xka dV a
V a u i :
V a1 V a
V a1
i
q
dT t
:
dx j
20
K tik
4
1X
a;t
a;t
V a K ij Mjk ;
V a1
21
where, the Ma;t matrix is the concentration tensor that relates the
average subcell temperature gradient with the overall temperature
gradient across the unit-cell. A detailed formulation of Ma;t tensor
and the effective thermal conductivity can be found in Appendix B.
In the following sections, Eqs. (12), (14) and (21) are used to
determine the variations of effective time dependent stiffness matrix, coefcient of linear thermal expansion, and thermal conductivity along the graded direction of FGMs.
a1
The previously developed micromechanical relations for the effective viscoelastic response of particle reinforced composite (Muliana
and Kim [15]) is modied to determine the effective CTE. Using the
micromechanical relations and thermo-viscoelastic constitutive
relations for the particle and matrix subcells, the effective CTE for
the isotropic nonlinear responses can be expressed as:
A;t
C ijkl
tj
where u
18
19
515
Poisson ratio t
Ni3 Al
TiC
Al-6061 (T6)
SiC
Si
Al
199
460
70.3
400
112.4
72
0.295
0.19
0.34
0.20
0.42
0.33
11.90
7.20
23.40
3.4
3.0
23.6
173
120
100
234
500
200
400
300
200
Experimental Data Zhai et. al. (1993)
180
Km = Thermal Conductivity of Al
160
140
120
Experimental Data Geiger and Jackson (1989)
Micromechanical Model
Present Model
100
0
0.2
0.4
0.6
0.8
100
0
0.1
0.2
0.3
0.4
0.5
0.6
Fig. 2. Comparison of Youngs modulus for FGM consisting of TiC and Ni3 Al.
3E-005
Aluminum with Silicon inclusions
-1
Kp/Km = 120:173
2E-005
simulations are performed using the ABAQUS FE software. The results obtained from the micromechanical model are compared
with the ones from FE analysis of the FGM model having microstructural details. The FGM panel of 16 mm length 10 mm
height 1 mm depth is studied. The volume fraction of inclusions
varies along the length direction. A 2D FE model of FGM having a
gradation of the particle in one direction is shown in Fig. 5(a)
and (b). The particles in the form of circles are dispersed randomly
with a gradient of volume fractions of particle from 0% to 40%. In
Fig. 5(a), large diameter particles are distributed while Fig. 5(b)
contains small size particles. Small size particles show more uniform distribution as compare to the ones with large size particle.
Fig. 5(c) illustrates the simplied piece-wise homogenized model
with sixteen (16) layers. Each layer represents the macroscopic
material point with homogeneous properties varying with the gradient of volume fraction of the particles. The heat transfer thermal
analysis is rst performed to obtain the temperature distribution
along the graded direction. Using the temperature distribution,
the stress analyses are carried out to determine the timetemperature dependent deformations of FGM along the graded directions.
In order to obtain the temperature proles, the equation governing
the heat conduction in an FGM body needs to be solved. This equation is written as:
1E-005
qcxk T qi;i i; k 1; 2; 3
Experimental Data Geiger and Jackson (1989)
Micromechanical Model
0.1
0.2
0.3
0.4
0.5
22
where qcxk is the effective heat capacity that depends on the composition, density, and specic heat of the two constituents in the
FGM body. The effective heat capacity is obtained using a volume
average method.
The FGM consisting of Ti6Al4V and ZrO2 is rst considered.
The temperature dependent mechanical and physical properties
of these materials are given in Table 2. The properties are taken
from Praveen et al. [21]. First, a transient heat transfer analysis is
516
(a)
(b)
(c)
Fig. 5. Illustration of the geometry of the nite element models for a volume fraction that varies from 0% to 40%. (a) Coarse and (b) ne microstructural details; (c) piece-wise
homogeneous macroscopic layers.
1200
Ti6Al-4v with Zr0 2 inclusions
1000
Temperature (K)
Micromechanical Model
t =15s
800
t =10s
t =5s
600
t =3s
t =1s
400
Volume fraction varies from 0 to 40%
with maximum at distance 16 mm.
200
0
12
16
Distance (mm)
Fig. 6. Temperature proles at different times along the graded direction of FGM
having constituents with temperature dependent thermal conductivities, for Ti
6Al4V/ZrO2.
shown by the deviation in the two responses in Fig. 8. As time progresses, the temperature gradient decreases which reduces thermal stresses and for a zero temperature gradient both results
agree quite well.
Next, coupled heat conduction and deformation analysis is performed to investigate the effect of viscoelastic constituents on the
overall thermo-mechanical responses of FGMs. The time-dependent behavior of metal-matrix composites is of importance at high
temperatures. The creep behavior of Al with silicon carbide inclusions is thus numerically studied as an example. The temperature
dependent elastic modulus of aluminum is taken from Kaufman
[11]. The properties of SiC are taken from Geiger and Jackson [8].
The temperature dependent mechanical and physical properties
of Al and SiC are given in Table 3. The present model requires
the creep parameters which can be obtained from a series of experimental data performed at constant stress and different temperatures. Because of the unavailability of such data, creep properties
of aluminum at 573 K and 28.5 MPa are taken from the experimental work of Tjong and Ma [28]. The time dependent and non-linear
temperature dependent parameters of Al are given in Table 4.
Table 2
Temperature dependent mechanical and physical properties of materials of Ti6Al4V and ZrO2 .
Property
Young modulus (E), Pa
Poisson ratio t
Coefcient of thermal expansion a 106 ; 1=K
Thermal conductivity (K), W/m/K
Specic heat (C), J/kg K
Density q kg=m3
T is temperature in K.
Ti6Al4V
11
Zirconia ZrO2
6
1:23 10 56:457 10 T
0.3
7:58 106 4:927 109 T 2:388 1012 T 2
1.2095 + 0.01686T
625:2969 0:264T 4:49 104 T 2
4429
517
Table 4
Prony series coefcients and non-linear temperature dependent parameters for Al.
0.0008
Steady State Time = 159 seconds
Displacement (mm)
0.0006
0.0004
kn s1
Dn 106 MPa1
1
2
3
4
5
6
1
101
102
103
104
105
0.1
0.15
20
30
160
1100
2
0
g T0 exp 0:36 TT
;
T0
t =40s
g T1 g T2 aT 1
t =30s
0.0002
t =20s
t =5s
0
0
12
16
Distance (mm)
Fig. 7. Variations of displacement eld at different times along the graded direction
of FGM having constituents with temperature dependent elastic properties, for Ti
6Al4V/ZrO2.
0.2
Detail Microstructural Model
Micromechanical Model
Displacement (mm)
0.15
Ti6Al-4v with Zr0 2 inclusions
t =159s
t =50s
0.1
t =40s
t =30s
0.05
t =20s
0
0
12
16
Distance (mm)
Fig. 8. Variations of displacement eld at different times along the graded direction
of FGM having constituents with temperature dependent elastic and thermal
properties, for Ti6Al4V/ZrO2.
Moreover, DiCarlo and Yun [5] reported that the SiC does not show
any creep up to 1073 K. This temperature is far above the temperatures considered in this study. Therefore, SiC is assumed to behave linearly elastic. The axial creep data of pure aluminum is
shown in Fig. 9. The axial creep of composites and FGMs consisting
of aluminum and SiC is computed using the micromechanical model. A constant stress of 28.5 MPa is applied at one end followed by
holding for 12,000 s at a constant temperature of 573 K. The
boundary conditions of the specimens are shown in Fig. 9. Composites having a uniform distribution and linear gradation of SiC along
Table 3
Temperature dependent mechanical and physical properties of materials of Al and SiC.
Property
Aluminum (Al)
406,783 22.61T
0.2
183.78 0.1569T
750
3210
3 106 3 109 T 6 1013 T 2
T is temperature in K.
518
0.01
Pure Aluminum Experimental Creep Data ( Tjong and Ma,1999)
0.008
0.006
Acknowledgements
A
0.004
T(K)
(MPa)
T= 573
0.002
=28.5
Appendix A
12000
12000
0
0
4000
8000
12000
Time (seconds)
Fig. 9. Comparison of axial creep deformations for Al, Al/SiC composite and FGM.
1
3
1
1
t ; T t J0 Stij g 1 r
t; Tt
etij g 0 r
2
2
t =3s
500
t =2s
t =0.5s
400
t =0.1s
300
4
12
16
Distance (mm)
J 0 21 tD0
DJ
Fig. 10. Temperature proles at different times along the graded direction of FGM
having constituents with temperature dependent thermal conductivities, for Al/SiC.
0.04
wt
=28.5
t
A
t =2000s
0.02
t =1000s
Micromechanical Model
Al with SiC inclusions
t =350s
0.01
t =14.8s
t =0.5s
0
0
DBw 31 2tDDw
A:2
Here D0 and DD are the instantaneous elastic and transient compliances under uniaxial (extensional) creep loading. The uniaxial transient compliance, DD, is expressed in terms of Prony series as:
DDw
N
X
Dn 1 expkn wt
A:3
n1
0.03
2000
B0 31 2tD0
21 tDDw
(MPa)
h
i
s ; T s Ssij
d g 2 r
where eM;t
and eT;t
ij
ij are the total mechanical and thermal strains,
respectively. The superscript t indicates a variable at time t. The
parameters J0 and B0 are the instantaneous elastic shear and bulk
compliances, respectively. The terms DJ and DB are the time-dependent shear and bulk compliances, respectively. The corresponding
linear elastic Poissons ratio, t, is assumed to be time independent,
which allows expressing the shear and bulk compliances as:
t =1s
DJwt ws
ds
ds
Z t
s
s
; T rskk
d g r
1
1
etkk g 0 r t ; T t B0 rtkk g 1 r t ; T t DBwt ws 2
ds
ds
3
3
0
A:1
Micromechanical Model
Temperature (K)
1
3
600
This appendix outline the basic concepts of solving the Eq. (1)
using the recursiveiterative algorithm. For isotropic materials,
the total strain in Eq. (1) can be written as:
12
16
Distance (mm)
Fig. 11. Variations of axial creep deformations of FGM having constituents with
temperature dependent elastic and thermal properties, for Al/SiC.
519
Fig. A1. Recursiveiterative algorithm for the nonlinear isotropic viscoelastic material.
given in 3.3 of Fig. A1. Finally, the consistent tangent stiffness matrix is dened by taking the inverse of the partial derivative of the
incremental strain with respect to the incremental stress at the end
of the current time step. The consistent tangent stiffness, C tijkl , at
the converged state, are:
C tijkl
@drtij
M;t
kl
@de
"
@Rtij
@drtkl
#1
;
Rtij
! 0
A:5
Eq. (A.5) denes material properties at current time t for each subcell
in the micromechanical model. The components of the consistent
tangent stiffness tensor vary with time, temperature, and stress.
uxi xk ui
Appendix B
This appendix outlines the basic concepts require in formulating the effective thermal properties of the homogenized composite
medium having spherical particle inclusions. The detailed micromechanical formulations are presented in the manuscript Khan
and Muliana [12] which is currently under review.
B.1. Periodic boundary conditions
To reduce complexity in the micromechanical formulation, a
composite having a periodic microstructure is assumed. A representative volume element (RVE) is then dened by a single particle
Xi;i xk x
~xi xk
u
u
k
B:1
a
Xi;i x0k xaki
uxi x0k uxi xki u
txi x0k
a
t xi xki
txi
x
ij nj
B:2
B:3
520
x2
a1
(*)
f Re g AM
1
a2
121
8 1 9
e >
>
>
>
> 2 >
i <
e =
1224
x1
>
e3 >
>
>
>
;
: 4 >
x3
Fig. B1. Representative volume element of the periodic microstructure.
T x xk T x; T i;i xk xk Te xk
B:4
0
i
T x x0k T x xki T X
i;i xk xk
B:5
a
qxi xki ni
B:6
1;t
ij
V de
V
V 1 V 2
for i j; i; j 1; 2; 3
2;t
ij
de
3;t
ij
de
4;t
ij
de
h
fRr g AM;t
2
121
8 1 9
>
>
>e >
=
< e2 >
i>
>
e3 >
>
>
>
;
: 4 >
1224
V 1
I
V A
6 33
6
6
6 0
0
6
M
A1 6 33 33
6 0
0
6 33 33
6
4
0
V 1 I
A;t
drij
d tij
1;t
drij
1;t
ij
r dr
3;t
4;t
2;t
drij
dr
2;t
ij
33
AM;t
2
C1
ax
6 33
6
6
6 0
6 33
6
6
6 0
6 33
6
6
4
0
33
33
33
33
33
33
33
33
V 2 I
33
33
33
33
V 3 I
33
7
7
7
0 7
33 7
7
0 7
7
33 7
5
V 4 I
33
33
33
33
33
33
33
C2
ax
33
33
C
Csh
33
33
33
1
Csh
33
33
Csh
33
33
1
sh
33
33
33
33
33
33
33
33
33
3
C sh
33
33
33
33
33
0
0
33
for i j
33 7
7
7
0 7
33 7
7
7
0 7
7
33 7
7
4 5
C sh
33
B:14
where:
V 4 drij
33
B:13
V 3 drij
V 2
I
V A
33
33
for ij
B:8
A;t
B:12
126 61
33
tij V 1 V 2 drij
dr
O feg
241
B:7
2;t
3;t
4;t
tij V 1 dc1;t
dc
V 2 dcij V 3 dcij V 4 dcij
ij
B:11
61
where Re is the residual vector arising from imposing strain compatibility relations. In the case of linear elastic responses are exhibited for all subcells, the vector Re is zero. The second sets of
equations are formed based on traction continuity relations. The
equations based on the traction continuity relations within
subcells:
33
dtij
126
241
a3
qxi x0k ni
h i
DM
feg
1
B:9
C 1111
C 1122
C 3311
C 2222
C 3322
6
Cax 4 C 2211
C 1133
C 1212
7
6
C 2233 5 Csh 4 0
C 3333
0
0
C 1212
0
7
0
5
C 1212
B:15
dr
3;t
ij
4;t
ij
dr
for ij
B:10
33
DM
1
6
6 I
6 33
6
6
6 I
6 33
4
0
33
33
7
0 7
7
7
0 7
33 7
5
I
33 7
B:16
33
a;t
The B
matrices in Eq. (10) are then formed using Eqs. (B.11) and
(B.12), which in linearized relations are.
i
Ba;t
24x6
"
AM
1
AM;t
2
24x24
1
"
DM
1
O
24x6
B:17
1 h
ti
du
ti
dq
A;t
2;t
v 1 du1;t
v 2 dui
i
3;t
dui
i
1 h A A;t
4;t
v dqi v 3 dq3;t
v 4 dqi
i
V
1;t
dqi
dqi
2;t
dqi
4;t
dui
B:18
B:19
B:20
where the total volume of subcells 1 and 2 in Eqs. (B.18) and (B.19)
2
is V A V 1 V : .
We introduce a concentration tensor that relates the average
subcells temperature gradient with the overall temperature gradient across the unit-cell. Let Ma;t be the concentration tensor of the
temperature gradient. The temperature gradient in each subcell is
expressed by:
a;t
dui
a;t
tj
Mij du
B:21
a;t
To formulate the M
matrix, the micromechanical relations and
the constitutive equations are imposed. The present micromodel
consists of four (4) subcells with three (3) components of heat ux
need to be determined for every subcell. This requires forming
twelve (12) equations based on the temperature and heat ux continuities at the interface of each subcell which are written as:
8
1;t 9
dui >
>
>
>
>
>
>
=
< du2;t >
i
ti g
A1
D1 fdu
3;t
>
> du
912 >
93
31
>
>
>
i
>
>
:
4;t ;
dui
B:22
121
8
1;t 9
dui >
>
>
>
>
>
>
>
=
t < du2;t
i
ti g
A2
O fdu
3;t >
>
13
d
u
31
>
112 >
>
>
i
>
>
:
4;t ;
dui
B:23
121
By substituting Eq. (B.21) to Eqs. (B.22) and (B.23), the Ma;t matrix
can be determined, which is:
h
i A1 D
1
1
Ma;t
At2
O
121
124
B:24
41
The matrix O is the zero matrix and the components of matrix A1 ; At2
and D1 are given as follows:
3
2
V 1
I VV A I
0
0
V A
33
33 7
6 33
33
7
6
7
6
A1 6 0
0
I
0 7
6 33 33 33 33 7
5
4
0
0
0
I
33
33
33
33
h 1;t
i
2;t
I
0
0
At2 K33I K
33
33
33
3
2
I
6 33 7
6 I 7
6 33 7
7
6
D1 6
7
6 I 7
6 33 7
5
4
I
2
33
B:25
B:26
B:27
521
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