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Carbon/Sulfur
Determinator
INSTRUCTION MANUAL
Software Version DSP 2.9 Windows 1.2
Part Number 200-635
October 2003
Patents are Pending in U.S.A. and other countries
2003 LECO Corporation
Minor revisions may not be reflected in this manual.
LECO Corporation
12
CS-200
Introduction
Introduction
1 Introduction
Introduction
Illustrations .......................................................................18
Warranty......................................................................... 110
Symbols.......................................................................... 112
Interference to Other Devices ............................................ 114
Declaration of Conformity .................................................. 115
Major Equipment and Accessories List ................................. 118
Components and Accessories List........................................ 127
Options ........................................................................... 134
Specifications................................................................... 135
Installation
Illustrations .......................................................................22
Instrument Installation........................................................23
Facility Requirements..........................................................26
International Installation .....................................................27
Option Installation
Illustrations .......................................................................32
Balance Installation ............................................................33
Dot Matrix Printer (601-480-110) .........................................37
Deskjet (Inkjet) Printer (611-499-110)................................ 311
Installation of Optional Kits for the Autocleaner .................... 312
System Setup
Illustrations .......................................................................44
Controls and Indicators .......................................................46
Menu Organization Chart .....................................................48
Power-Up ........................................................................ 410
Introduction
CS-200
13
Operation
Operation Guidelines...........................................................56
Crucibles ...........................................................................59
Sample Preparation .......................................................... 510
Analyze Menu .................................................................. 511
Sample Weight Entry ........................................................ 523
Sample Analysis ............................................................... 525
Calibrate Menu................................................................. 527
Results Menu ................................................................... 538
Operation for Windows .................................................... 547
Windows Software Menus .................................................. 552
Login a Sample ................................................................ 563
Analyze a Sample ............................................................. 568
14
CS-200
Introduction
Maintenance
Illustrations .......................................................................62
Periodic Maintenance Schedule .............................................63
Anhydrone Tube.................................................................64
Autocleaner .......................................................................66
Catalyst Heater Tube Packing ............................................. 611
Cellulose Filter ................................................................. 613
Combustion Tube ............................................................. 615
Combustion Zone O-rings .................................................. 616
Incoming Reagent Tube..................................................... 617
Lance and Filter Assembly ................................................. 619
Pinch Valve Tubing ........................................................... 621
Reagent Tube Screen Filter ................................................ 623
Login Periodic Maintenance ................................................ 624
View Log File ................................................................... 625
Reset Maintenance Counters .............................................. 626
Theory of Operation
Illustrations .......................................................................72
General Information............................................................73
Infrared Radiation, Absorption, and Detection.........................74
Comparator Level ...............................................................78
Introduction
CS-200
15
Diagnostics
Diagnostics........................................................................84
Ambient Monitor.................................................................85
Switch States.....................................................................88
Valve States ......................................................................89
Leak Check...................................................................... 810
Print Buffer...................................................................... 812
Plot Buffer ....................................................................... 813
System Print.................................................................... 815
Reset Memory.................................................................. 816
Diagnostics for Windows .................................................. 817
Leak Check...................................................................... 819
Ambient Monitor............................................................... 822
Switches ......................................................................... 826
Solenoids ........................................................................ 827
Comport.......................................................................... 828
Electronic Adjustments
Illustrations .......................................................................92
Barometric (PID) Pressure Regulator Adjustment ....................93
Catalyst Heater Control Card................................................96
Induction Power Control Card ...............................................98
Oven Heater Control Card.................................................. 911
IR Cell ............................................................................ 912
10
Service
Illustrations ..................................................................... 102
Combustion Pressure Adjustment ....................................... 103
Flow Controller Adjustment ................................................ 105
Safety Pressure Adjustments.............................................. 106
Vertical Crucible Alignment ................................................ 108
Gas Flows...................................................................... 1012
Valve Control States ....................................................... 1016
Notices, Errors, and Warnings .......................................... 1022
Software Upgrade........................................................... 1026
16
CS-200
Introduction
11
Illustrations
12
Index
Introduction
CS-200
17
Illustrations
Figure 11......... CS200 Determinator .................................. 116
Figure 12......... CS200 Determinator with Autocleaner .......... 117
Figure 2-1 ......... Wiring Diagrams ........................................ 28
Figure 2-2 ......... Interconnection Diagram ............................ 29
Figure 2-3 ......... Voltage Selection Terminal Strip .................. 211
Figure 2-4 ......... RF Shield Removal ..................................... 213
Figure 2-5 ......... Oscillator Chassis....................................... 213
Figure 2-6 ......... Anhydrone Tube ........................................ 215
Figure 2-7 ......... Reagent Tube Removal ............................... 217
Figure 2-8 ......... Reagent Tube Packing ................................ 217
Figure 2-9 ......... Combustion Tube InstallationWithout Autocleaner
....................... 219
Figure 2-10 ....... Combustion Tube InstallationWith Autocleaner
....................... 220
Figure 2-11 ....... Pedestal InstallationWithout Autocleaner .... 223
Figure 2-12 ....... Pedestal InstallationWith Autocleaner......... 224
Figure 3-1 ......... Balance Control Panel................................. 36
Figure 3-2 ......... Balance Assembly ...................................... 36
Figure 3-3 ......... Ribbon Cartridge Installation ....................... 39
Figure 3-4 ......... Paper Installation....................................... 39
Figure 41......... Controls and Indicators with Autocleaner....... 47
Figure 42......... Keypad .................................................... 411
Figure 43......... Combustion Pressure Adjustment Knob ......... 428
Figure 4-4 ......... Controls and Indicators............................... 443
Figure 61......... Anhydrone Tube ........................................ 65
Figure 62......... Autocleaner Assembly ................................ 68
Figure 63......... Catalyst Heater Tube Packing ...................... 612
Figure 64......... Cellulose Filter Packing ............................... 614
Figure 65......... Reagent Tube Removal ............................... 618
Figure 66......... Reagent Tube Packing ................................ 618
Figure 67......... Lance and Filter Assembly........................... 620
Figure 68......... Pinch Valve Assembly ................................. 622
Figure 71......... Gas Flow Diagram...................................... 76
18
CS-200
Introduction
Note
Introduction
CS-200
19
Warranty
Equipment manufactured by LECO Corporation, St. Joseph,
Michigan is warranted free from defect in material and
workmanship for a period of six months from the date of
installation. Equipment not manufactured by LECO is covered to
the extent of warranty provided by the original manufacturer
and this warranty does not cover any equipment, new or used,
purchased from anyone other than LECO Corporation. All
replacement parts shall be covered under warranty for a period
of thirty days from date of purchase. LECO makes no other
representation or warranty of any other kind, expressed
or implied, with respect to the goods sold hereunder,
whether as to merchantability, fitness for purpose, or
otherwise.
Expendable items such as crucibles, combustion tubes,
chemicals, and items of like nature are not covered by this
warranty.
LECO's sole obligation under this warranty shall be to repair or
replace any part or parts which, to our satisfaction, prove to be
defective upon return prepaid to LECO Corporation, St. Joseph,
Michigan. This obligation does not include labor to install
replacement parts, nor does it cover any failure due to
accident, abuse, neglect, or use in disregard of instructions
furnished by LECO. In no event shall damages for defective
goods exceed the purchase price of the goods, and LECO shall
not be liable for incidental or consequential damages
whatsoever.
All claims in regard to the parts or equipment must be made
within ten (10) days after Purchaser learns of the facts upon
which the claim is based. Authorization must be obtained from
LECO prior to returning any other parts. This warranty is voided
by failure to comply with these notice requirements.
110
CS-200
Introduction
Notice
The warranty on LECO equipment remains valid only when
genuine LECO replacement parts are employed. Since LECO has
no control over the quality or purity of consumable products not
manufactured by LECO, the specifications for accuracy of
results using LECO instruments are not guaranteed unless
genuine LECO consumables are employed in conjunction with
LECO instruments. If purchaser defaults in making payment for
any parts or equipment, this warranty shall be void and shall
not apply to such parts and equipment. No late payment or
cure of default in payment shall extend the warranty period
provided herein.
LECO Corporation is not responsible for damage to any
associated instruments, equipment, or apparatus nor will LECO
be held liable for loss of profit or other special damages
resulting from abuse, neglect, or use in disregard of
instructions. The Buyer, their employees, agents, and
successors in interest assume all risks and liabilities for the
operation, use, and/or misuse of the product(s) described
herein and agree to indemnify, hold harmless, and defend the
seller from any and all claims and actions arising from any
cause whatsoever, including seller's negligence for personal
injury incurred in connection with the use of said product(s)
and any and all damages proximately resulting therefrom.
Caution
The instrument should be operated only by technically qualified
individuals who have fully read and understand these
instructions. The instrument should be operated only in
accordance with these instructions.
The operator should follow all of the warnings and cautions set
forth in the manual and the operator should follow and employ
all applicable standard laboratory safety procedures.
LECO is a registered trademark of LECO Corporation.
Windows is a registered trademark of Microsoft Corporation.
Excel is a registered trademark of Microsoft Corporation.
Windows 95 is a trademark of Microsoft Corporation.
Windows 3.1 is a trademark of Microsoft Corporation.
Introduction
CS-200
111
Symbols
WARNING
WARNING
!
CAUTION
112
CS-200
Introduction
Keypad
Windows
Introduction
CS-200
113
114
CS-200
Introduction
Declaration of Conformity
Introduction
CS-200
115
Figure 11
CS-200 Determinator
116
CS-200
Introduction
Figure 12
CS-200 Determinator with Autocleaner
Introduction
CS-200
117
Notes
Note
The following units have a Display and Keypad built into the
determinator. They do not include a PC.
617-000-100
200-635
Instruction Manual
617-010-070
Component Pack
615-426
Power Cord
607-750*
616-759
Accessory Pack
617-000-500
200-635
Instruction Manual
617-010-070
Component Pack
1
1
607-750*
616-759
615-426
Power Cord
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
118
CS-200
Introduction
617-000-700
200-635
Instruction Manual
617-010-070
Component Pack
615-426
Power Cord
607-750*
616-759
Accessory Pack
617-100-300
200-635
Instruction Manual
617-010-070
Component Pack
615-426
Power Cord
607-750*
616-759
Accessory Pack
617-100-300
200-635
Instruction Manual
617-010-070
Component Pack
615-426
Power Cord
607-750*
616-759
Accessory Pack
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
Introduction
CS-200
119
617-100-500
200-635
Instruction Manual
617-010-070
Component Pack
615-426
Power Cord
607-750*
616-759
Accessory Pack
617-100-700
200-635
Instruction Manual
617-030-070
Component Pack
615-426
Power Cord
607-750*
616-759
Accessory Pack
617-000-300
200-635
Instruction Manual
617-030-070
Component Pack
615-426
Power Cord
607-750*
616-759
Accessory Pack
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
120
CS-200
Introduction
617-200-100
200-635
Instruction Manual
617-010-070
Component Pack
615-426
Power Cord
607-750*
616-759
Accessory Pack
617-200-300
200-635
Instruction Manual
617-030-070
Component Pack
615-426
Power Cord
607-750*
616-759
Accessory Pack
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
Introduction
CS-200
121
Note
617-000-200
200-635
Instruction Manual
617-020-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
617-000-400
200-635
Instruction Manual
617-040-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
122
CS-200
Introduction
617-000-600
200-635
Instruction Manual
617-020-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
617-000-800
CS200CH
200-635
Instruction Manual
617-040-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
Introduction
CS-200
123
617-100-200
200-635
Instruction Manual
617-020-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
617-100-400
200-635
Instruction Manual
617-040-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
124
CS-200
Introduction
617-100-600
200-635
Instruction Manual
617-020-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
617-100-800
200-635
Instruction Manual
617-040-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
Introduction
CS-200
125
617-200-200
200-635
Instruction Manual
617-020-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
617-200-400
200-635
Instruction Manual
617-040-070
Component Pack
615-426
Power Cord
259-035
Software Kit
607-750*
616-759
Accessory Pack
686-208-2GH
PC Tower Package
1
1
609-787
701-557
Component Pack
15.00 inch Color SVGA Monitor
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
126
CS-200
Introduction
Software Kit
159-109-100
Software Package
203-505-267
602-773
602-773-901
767-228
Bag
769-299
Connector
776-118
Contact
802-151
Cable Clamp
607-750*
501-171
502-174
* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.
Introduction
CS-200
127
616-759
128
Accessory Pack
501-077
Chip Accelerator
501-082
Wire Brush
501-241
501-503
501-587
501-679
502-177
502-294
Accelerator Lecocel 2
502-413
528-018-500
528-043-100
602-773
605-700-087
601-920
762-058
765-976
772-520
772-738
760-138
Tweezers
761-929
Crucible Tongs
764-098
Cellulose (1 lb)
773-579
775-306
775-307
Thumb Screw
CS-200
Introduction
617-010-070
Component Pack
550-080
Insulation Sheet
601-920
605-816
605-979
608-898
Receptacle Cover
615-426
AC Power Cord
762-458
Connector Nut
765-978
772-381
Lance Cleaner
772-905
Combustion Tube
772-960
772-967
774-828
Connector
774-829
Plug Hood
783-747
789-149
Introduction
CS-200
129
617-020-070
130
Component Pack
550-080
Insulation Sheet
601-920
605-816
605-979
608-898
Receptacle Cover
615-426
AC Power Cord
616-555
Cable Assembly
762-458
Connector Nut
765-978
772-381
Cleaner Lance
772-905
Combustion Tube
772-960
772-967
774-828
Connector
774-829
Plug Hood
783-747
789-149
CS-200
Introduction
617-030-070
Component Pack
190-009
Thumb Screw
190-279
Screw
190-624
Screw
193-055
Washer
550-080
Insulation
601-920
604-126
605-814
605-816
605-979
608-898
Receptacle Cover
615-426
AC Power Cord
616-555
Cable Assembly
618-723
762-458
Connector Nut
765-978
772-381
Lance Cleaner
772-905
Combustion Tube
772-960
772-967
774-828
Connector
774-829
Hood Plug
782-603
782-604
782-880
Vacuum Filter
783-747
789-149
789-230
Vacuum Assembly
Introduction
CS-200
131
617-040-070
132
Component Pack
190-009
Thumb Screw
190-279
Screw
190-624
Screw
193-055
Washer
550-080
Insulation
601-920
605-814
605-816
605-979
608-898
Receptacle Cover
615-426
AC Power Cord
616-555
Cable Assembly
618-723
762-458
Connector Nut
765-978
772-381
Cleaner Lance
772-905
Combustion Tube
772-960
772-967
774-828
Connector
774-829
Plug Hood
782-603
782-604
782-880
Vacuum Filter
783-747
789-149
789-230
Vacuum Assembly
CS-200
Introduction
686-208-2GH
1
PC Tower Package
609-787
611-119
Receptacle
618-980
Mouse Pad
686-229
Nameplate Id
686-993
Computer Tower
Introduction
CS-200
133
Options
CF-10
501-291
605-980
Keyboard
611-499-110
614-459
614-460
616-775
616-776
616-778
616-793
616-794
616-795
616-912
616-925
616-926
616-927
616-928
616-929
766-036
751-000-120
751-300-160
751-700-120
783-690
Autocleaner Kit
783-693
783-996
134
CS-200
Introduction
Specifications
Range (at 1 gram)
CS-200C
Carbon ........................................... 4 ppm to 3.5%
Sulfur ............................................. 4 ppm to 0.4%
CS-200CLC
Carbon ........................................... 2 ppm to 0.5%
Sulfur ............................................. 4 ppm to 0.4%
CS-200CHC
Carbon ........................................... 60 ppm to 6.0%
Sulfur ............................................. 4 ppm to 0.4%
CS-200SHC
Carbon ........................................... 4 ppm to 3.5%
Sulfur ............................................. 60 ppm to 1.75%
CS-200CSHC
Carbon ........................................... 60 ppm to 6.0%
Sulfur ............................................. 60 ppm to 1.75%
Note
Introduction
CS-200
135
Precision
CS-200C
Carbon ........................................... 2 ppm or 0.5% RSD*
Sulfur ............................................. 2 ppm or 1.5% RSD*
CS-200CLC
Carbon ........................................... 1 ppm or 0.5% RSD*
Sulfur ............................................. 2 ppm or 1.5% RSD*
CS-200CHC
Carbon ........................................... 30 ppm or 0.5% RSD*
Sulfur ............................................. 2 ppm or 1.5% RSD*
CS-200SHC
Carbon ........................................... 2 ppm or 0.5% RSD*
Sulfur ............................................. 30 ppm or 1.5% RSD*
CS-200CSHC
Carbon ........................................... 30 ppm or 0.5% RSD*
Sulfur ............................................. 30 ppm or 1.5% RSD*
Chemical Reagents............................. Anhydrone Magnesium Perchlorate,
Sodium Hydroxide on an inert base,
Lecosorb,
Platinized Silica, Cellulose
Gas Required
Carrier Gas ..................................... Oxygen 99.5% pure, 40 psi (2.76 bars)
Pneumatic Gas................................. Compressed Air, Nitrogen, or Argon,
40 psi (2.76 bars),
source must be oil and water free.
Gas Flow (based on nominal analysis time)
Measure ......................................... 3 liters per analysis
Pneumatic ...................................... 1 liters per analysis
Regulators
Oxygen........................................... 501-291 Oxygen Pressure Regulator
Compressed Air ............................... 766-036 Compressed Air Regulator
Inert Gas ........................................ 764-216 Inert Gas Regulator
Furnace.............................................. Induction, 18 MHz, 2.2 kW
Data Transmit .................................... RS-232 (included)
* One Sigma, conformance tested by gas dose analysis.
136
CS-200
Introduction
Data Storage
With PC .......................................... Limited only by hard drive space
Without PC...................................... 10 Sample Weights,
50 Answers, 5 Methods
Keypad
With PC .......................................... External
Without PC...................................... Internal Membrane/External Optional
Display
With PC .......................................... 15.00 inch SVGA Monitor
Without PC...................................... Liquid Crystal (16 x 26 characters)
External PC
Computer ....................................... PentiumTM 166 MHz (min),
1.2 GB Hard Drive (min)
Monitor........................................... 15.00 inch SVGA (min)
Operating System ............................ Microsoft Windows 95 (min)
Printer
With PC .......................................... Deskjet
Without PC...................................... Dot Matrix
Dimensions
Determinator
Height ............................................ 30.50 inches (77.5 cm)
Width ............................................. 27.50 inches (70.0 cm)
Depth............................................. 23.50 inches (59.7 cm)
Weight ........................................... 300 pounds
Computer (PC based system)
Height ............................................ 17.00 inches (43.2 cm)
Width ............................................. 8.00 inches (20.3 cm)
Depth............................................. 17.00 inches (43.2 cm)
Weight ........................................... 29 pounds
Monitor (PC based system)
Height ............................................ 15.00 inches (38.1 cm)
Width ............................................. 14.00 inches (35.6 cm)
Depth............................................. 16.00 inches (40.6 cm)
Weight ........................................... 35 pounds
Shipping Weight (without PC) .............. 420 pounds
Introduction
CS-200
137
Note
138
CS-200
Introduction
Installation
2 Installation
Illustrations .......................................................................22
Instrument Installation........................................................23
Facility Requirements..........................................................26
International Installation .....................................................27
Instrument Voltage Selection ........................................ 210
Oscillator Tube Installation............................................ 212
Anhydrone Tube Packing .............................................. 214
Removal..................................................................... 214
Packing ................................................................. 214
Incoming Reagent Tube Packing .................................... 216
Removal................................................................ 216
Packing ................................................................. 216
Combustion Tube Installation ........................................ 218
Without Autocleaner................................................ 218
With Autocleaner .................................................... 218
Gas Connections.......................................................... 221
Computer Installation................................................... 222
Pedestal Installation..................................................... 223
Without Autocleaner................................................ 223
With Autocleaner .................................................... 224
Installation
CS-200
21
Illustrations
Figure 2-1 ......... Wiring Diagrams ........................................ 28
Figure 2-2 ......... Interconnection Diagram ............................ 29
Figure 2-3 ......... Voltage Selection Terminal Strip .................. 211
Figure 2-4 ......... RF Shield Removal ..................................... 213
Figure 2-5 ......... Oscillator Chassis....................................... 213
Figure 2-6 ......... Anhydrone Tube ........................................ 215
Figure 2-7 ......... Reagent Tube Removal ............................... 217
Figure 2-8 ......... Reagent Tube Packing ................................ 217
Figure 2-9 ......... Combustion Tube InstallationWithout Autocleaner
....................... 219
Figure 2-10 ....... Combustion Tube InstallationWith Autocleaner
....................... 220
Figure 2-11 ....... Pedestal InstallationWithout Autocleaner .... 223
Figure 2-12 ....... Pedestal InstallationWith Autocleaner......... 224
22
CS-200
Installation
Instrument Installation
Notes
1.
2.
WARNING
Installation
4.
5.
6.
CS-200
23
7.
!
CAUTION
Windows
9.
!
CAUTION
24
CS-200
Installation
Installation
CS-200
25
Facility Requirements
Electrical Power Requirements
Determinator................................... 230 V~, 10%, 50/60 Hz, Single phase,
15 amps max
Operating Current ....................... 12 Amps
Stand-by Current ........................ 4 Amps
Balance .......................................... 120 V~, 10%, 60 Hz, 0.5 amps max
Gas Required
Carrier Gas ..................................... Oxygen 99.5% pure, 40 psi (2.76 bars)
Pneumatic Gas................................. Compressed Air, Nitrogen, or Argon,
40 psi (2.76 bars),
source must be oil and water free.
Regulators
Oxygen........................................... 501-291 Oxygen Pressure Regulator
Compressed Air ............................... 766-036 Compressed Air Regulator
26
CS-200
Installation
International Installation
For international installation, a HAR approved line cord for use
in the end country must be obtained. This product requires a
disconnect device that may either be the plug of the power cord
or a disconnect device installed at the installation site if the
equipment is permanently wired.
When the plug on the power supply cord is intended to serve as
the disconnect device, the socket/outlet must be installed near
the equipment and shall be easily accessible. When the wiring
is permanently connected, a disconnect device (such as a
circuit breaker or switch) must be lockable, installed near the
equipment, and be easily accessible.
Installation
CS-200
27
POWER CORD
BROWN
POWER
NEUTRAL
220 V~
LIGHT BLUE
0 V~
GREEN/YELLOW
GROUND
CHASSIS
(CABINET)
GROUND
PLUG
POWER
115 V~
GROUND
G
230 V~
POWER
115 V~
BLACK
T
BLACK
GREEN/YELLOW GREEN/
YELLOW G
BLACK
LIGHT BLUE
LIGHT
BLUE
X
BLACK
CHASSIS
(CABINET)
GROUND
RECEPTACLE
POWER
Y
115 V~
230 V~
GROUND
G
115 V~
POWER
0 V~
NEUTRAL
BLACK
T
BLACK
GREEN/YELLOW GREEN/
YELLOW G
BLACK
LIGHT BLUE
LIGHT
BLUE
X
BLACK
CHASSIS
(CABINET)
GROUND
RECEPTACLE
Figure 2-1
Wiring Diagrams
28
CS-200
Installation
MEASURE FLOW
EXHAUST
PNEUMATIC
INLET
DISPLAY
BALANCE
O2
40 PSI
DATA
TRANSMIT
PRINTER
BAL.
DATA
XMIT
OXYGEN
INLET
CONNECTOR
ASSEMBLY
(2-REQ'D)
PRI NT ER
OXYGEN
(35 PSI)
PNEU
40 PSI
MEASURE
EXHAUST
ALARM
ALARM
PURGE
EXHAUST
PURGE
EXHAUST
KEYBOARD
5 A CIRCUIT
BREAKER
PNEU. I NLET
40 PSI
VACUUM
CLEANER
BALANCE
PRINTER
EXTERNAL
KEYBOARD
VACUUM
CIRCUIT BREAKER
AUX POWER
BREAKER
VACUUM
CONNECTOR
230V~ - 50/60Hz
5.0 AMPS
AUX POWER
BREAKER
AC POWER
AC POWER
AC POWER
BALANCE
DATA
TRANSMIT
SERIAL
PORT A
BAL.
DATA
XMIT
PRINTER
OXYGEN
(35 PSI)
MEASURE
EXHAUST
PURGE
EXHAUST
PNEU. INLET
40 PSI
WINDOWS
ALARM
KEYBOARD
5 A CIRCUIT
BREAKER
VACUUM
CLEANER
BALANCE
AUX POWER
BREAKER
115
AC POWER
Figure 2-2
Interconnection Diagram
Installation
CS-200
29
Note
Note
210
1.
2.
3.
CS-200
Installation
240
220 200
COM
TERM 1
OF
K3
Figure 2-3
Voltage Selection Terminal Strip
Installation
CS-200
211
2.
3.
4.
5.
WARNING
WARNING
212
6.
7.
CS-200
Installation
Figure 2-4
RF Shield Removal
604-010
HIGH VOLTAGE
STRAP
604-009
COIL STRAP
776-008
VACUUM
CAPACITOR
771-356
PLATE
CONNECTION
776-128
CHOKE
ASSEMBLY
771-354
OSCILLATOR
TUBE
776-129
COIL
ASSEMBLY
566-002
COIL COLLET
(2-REQ'D)
Figure 2-5
Oscillator Chassis
Installation
CS-200
213
Slide the anhydrone tube upward until the bottom end can
swing free.
2.
3.
4.
Packing
214
1.
2.
3.
4.
5.
Insert the reagent stop into the top of the anhydrone tube.
Push is firmly on top of the quartz wool to hold the packing
material in place.
6.
CS-200
Installation
789-095
REAGENT STOP
765-976
O-RING
(2 REQ'D)
502-177
1/2" QUARTZ WOOL
501-171
2" ANHYDRONE
601-390
QUICK
DISCONNECT
TUBE
502-177
2" QUARTZ WOOL
775-306
SCREEN FILTER
Figure 2-6
Anhydrone Tube
Installation
CS-200
215
Slide each reagent tube upward until the bottom end can
swing free. Refer to Figure 2-7, page 217.
2.
3.
4.
Packing
216
1.
2.
Pack 1/2 inch of quartz wool into the bottom of the reagent
tube.
3.
4.
Pour Lecosorb onto the anhydrone until all but the top 1/2
inch of the reagent tube is filled, gently tapping it down.
5.
6.
CS-200
Installation
771-373
REAGENT
TUBE
Figure 2-7
Reagent Tube Removal
502-177
/2" QUARTZ WOOL
502-174
2" LECOSORB
771-373
QUICK DISCONNECT
TUBE
501-171
1" ANHYDRONE
502-177
/2" QUARTZ WOOL
775-306
SCREEN FILTER
Figure 2-8
Reagent Tube Packing
Installation
CS-200
217
Without Autocleaner
1.
2.
3.
4.
5.
Install the EMI gasket into the seal on the bottom of the
combustion tube.
6.
7.
With Autocleaner
218
1.
2.
3.
4.
5.
Install the EMI gasket into the seal on the bottom of the
combustion tube.
6.
7.
CS-200
Installation
LANCE FLOW
CONNECTION
781-420
CLEANING
HEAD
MEASURE FLOW
CONNECTION
772-905
COMBUSTION
TUBE
762-058
O-RING
772-906
COMBUSTION
TUBE RING
781-401
CLEANING HEAD
ADAPTER RING
789-149
EMI GASKET
(GASKET TO GO
AROUND OUTER
DIAMETER OF O-RING)
601-920
O-RING
605-816
PEDESTAL
Figure 2-9
Combustion Tube InstallationWithout Autocleaner
Installation
CS-200
219
604-291
AIR CYLINDER
604-272
CAP
604-268
BODY ASSEMBLY
772-905
COMBUSTION
TUBE
609-626
AUTOCLEANER
ASSEMBLY
752-058
O-RING
604-172
O-RING
773-926
PLATE
190-090
THUMBSCREWS
(2 REQ'D)
773-320
O-RING
(2 REQ'D)
789-149
EMI GASKET
(GASKET TO GO
AROUND OUTER
DIAMETER OF O-RING)
601-920
O-RING
605-816
PEDESTAL
Figure 2-10
Combustion Tube InstallationWith Autocleaner
220
CS-200
Installation
Gas Connections
Note
1.
Remove the cap plugs from the fittings on the back panel.
2.
3.
!
POSSIBLE MACHINE DAMAGE
Oxygen is not recommended for use in the
pneumatic systems of LECO instruments.
Installation
4.
5.
CS-200
221
Computer Installation
Windows
222
1.
2.
3.
4.
5.
6.
7.
CS-200
Installation
Pedestal Installation
Without Autocleaner
1.
2.
605-816
PEDESTAL
605-814
PEDESTAL
ADAPTER
ASSEMBLY
783-675
LOWER SEAL
ASSEMBLY
Figure 2-11
Pedestal InstallationWithout Autocleaner
Installation
CS-200
223
With Autocleaner
1.
2.
605-816
PEDESTAL
605-814
PEDESTAL
ADAPTER
ASSEMBLY
781-412
BARB FITTING
789-430
LOWER SEAL
ASSEMBLY
760-215
ELBOW
Figure 2-12
Pedestal InstallationWith Autocleaner
224
CS-200
Installation
Option Installation
3 Option Installation
Illustrations .......................................................................32
Balance Installation ............................................................33
Balance Interfacing ........................................................ 34
Resetting the Balance .................................................... 35
Setting the Data Output Parameter .................................. 35
Dot Matrix Printer (601-480-110) .........................................37
Printer Settings ........................................................... 310
Deskjet (Inkjet) Printer (611-499-110)................................ 311
Installation of Optional Kits for the Autocleaner .................... 312
Autocleaner ................................................................ 312
Dust Removal Kit......................................................... 312
Vacuum Cleaner Kit ..................................................... 312
System Setup
CS-200
31
Illustrations
Figure 3-1 ......... Balance Control Panel................................. 36
Figure 3-2 ......... Balance Assembly ...................................... 36
Figure 3-3 ......... Ribbon Cartridge Installation ....................... 39
Figure 3-4 ......... Paper Installation....................................... 39
32
CS-200
Option Installation
Balance Installation
Refer to the Balance Options on page 423 or the Balance Tab
on 462, to set the balance option parameters and configure
the determinator to recognize the balance. If the balance and
determinator are not programmed with the same configuration
parameter values, no weights may be transferred.
The determinator will default to the correct parameter values to
operate with the balance. If the balance does not operate
properly with the determinator, verify the balance options
parameter values set from the determinator. The correct
parameter values are shown on pages 423 and 462.
Notes
System Setup
CS-200
33
Balance Interfacing
34
1.
2.
3.
4.
5.
6.
CS-200
Option Installation
2.
3.
4.
5.
6.
Press Tare.
7.
Press CF.
8.
2.
3.
4.
5.
6.
7.
8.
Press Tare.
9.
Press CF.
10. Reposition the menu access switch to the left and reinstall
the hole plug.
System Setup
CS-200
35
TOGGLE
POWER ON
CLEAR
FUNCTION
I/O
F1
CF
INFORMATION
TARE
TARE
TARE
PRINT
F2
Figure 3-1
Balance Control Panel
MENU ACCESS
SWITCH
Figure 3-2
Balance Assembly
36
CS-200
Option Installation
Notes
Notes
The optional Dot Matrix Printer is used with the DSP and
Windows instruments. DSP all printing and Windows line
printing.
1.
2.
3.
4.
Install the platen knob by inserting the shaft into the hole
in the right side of the printer. Match the flat side of the
knob to the flat side of the platen shaft.
5.
6.
B.
C.
D.
E.
System Setup
CS-200
37
B.
C.
7.
8.
9.
10. Connect the printer interface cable to the printer and the
back of the determinator.
11. Install the paper.
Note
A.
B.
Open the access and rear covers and feed the paper
under the rear cover.
C.
Open the tractor covers and align the track feed holes
on the paper with the tractor pins. Close the tractors.
D.
E.
2)
Do not place the left edge of the paper more than 1/2 inch
from the end of the platen or the printer will signal a paper
out alarm.
12. Close the rear cover and lay the paper separator flat.
13. Open the guide wire to stop paper from curling back into
the printer.
14. Close the access cover.
15. Paper can be fed from the bottom if the printer is placed
on a stand. Refer to the printer manual for details.
16. The control panel of the printer is used to configure the
printer and its corresponding features. Refer to the
operation section of the printer manual. The Printer Settings
can be found on page 310.
38
CS-200
Option Installation
RIBBON
CARTRIDGE
TAKE-UP
KNOB
RIBBON
PLATE
RIBBON SHIELD
DO NOT REMOVE
Figure 3-3
Ribbon Cartridge Installation
ACCESS
COVER
BAIL
LEVER
TRACTOR
COVER
LOCK
LEVER
GUIDE
WIRE
PAPER
SEPARATOR
PAPER
LEVER
TRACK FEED
HOLES
PAPER
PLATEN
KNOB
PINS
STUD
ON/OFF
SWITCH
SEPARATOR
TAB
REAR
COVER
Figure 3-4
Paper Installation
System Setup
CS-200
39
Printer Settings
Group
Font
Item
Print Mode
Pitch
Style
Size
Settings
Utility
10 CPI
Normal
Single
General Control
Emulation Mode
Graphics
Paper Out Override
Print Registration
Operator Panel Functions
Reset Inhibit
Print Suppress Effective
CPU Compensation
Epson FXe
Bi-directional
No
O
Full Operation
No
Yes
Standard
Vertical Control
Line Spacing
Form Tear-Off
Skip-Over Perforation
Auto LF
Auto CR
Auto Feed XT
Page Length
6 LPI
Off
No
No
No
Invalid
11 inches
Symbol Sets
Character Set
Language Set
Zero Character
Set I
American
Slashed
Parity
Serial Data 7 or 8 Bits
Protocol
Diagnostic Test
Busy Line
Baud Rate
DSR Signal
DTR Signal
Busy Time
None
8
Ready/Busy
No
SSD9600 BPS
Valid
Ready on Power Up
200 Milliseconds
Note
310
CS-200
Option Installation
Notes
System Setup
CS-200
311
Autocleaner
Notes
!
CAUTION
Notes
Notes
312
CS-200
Option Installation
System Setup
Windows
Keypad
Keypad
4 System Setup
Illustrations .......................................................................44
Controls and Indicators .......................................................46
Menu Organization Chart .....................................................48
Power-Up ........................................................................ 410
About the Examples ..................................................... 410
Menus........................................................................ 410
Keypad ...................................................................... 411
Using the Keypad ................................................... 412
Notices and Errors ....................................................... 413
Confirmation............................................................... 414
Copyright Screen......................................................... 414
System Overview ............................................................. 415
Main Menu Overview .................................................... 415
System Check .................................................................. 416
Ambient Monitor.......................................................... 416
System Setup .................................................................. 418
System Options........................................................... 419
System Setup
CS-200
41
42
CS-200
System Setup
System Setup
CS-200
43
Illustrations
Figure 41......... Controls and Indicators with Autocleaner....... 47
Figure 42......... Keypad and Display Screen ......................... 411
Figure 43......... Combustion Pressure Adjustment Knob ......... 428
Figure 4-4 ......... Controls and Indicators............................... 443
44
CS-200
System Setup
System Setup
CS-200
45
Note
46
CS-200
System Setup
AUTOCLEANER
ASSEMBLY
ACCESS DOOR
CONTRAST
CONTROL
BRIGHTNESS
CONTROL
INCOMING
REAGENT
TUBE
DISPLAY
SCREEN
KEYPAD
782-603
VACUUM
HOSE
CATALYST
HEATER
ASSEMBLY
604-126
DUST BOX
ANHYDRONE
TUBE
MEASURE
FLOW
ROTAMETER
ANALYZER
AC POWER
ON/OFF
SWITCH
CELLULOSE
FILTER
POWER LEVEL
ADJUSTMENT
FURNACE
AC POWER
ON/OFF
SWITCH
VACUUM
CLEANER
ON/OFF
SWITCH
PISTON
UP/DOWN
SWITCH
772-960
CRUCIBLE BOX
WITH LINER
789-230
VACUUM CLEANER
Figure 41
Controls and Indicators with Autocleaner
System Setup
CS-200
47
[1] Print
[1] Print
[6] Print
[7] Transmit
[3] Calibration
[1] Print
[2] Reset Calib
[1] Print
[1] Print
[1] Print
[8] Recalculate
48
CS-200
System Setup
[4] Set-Up
[1] Print
[2] Select Method
[1] 1-Method
[2] 2-Method
[3] 3-Method
[4] 4-Method
[5] 5-Method
[1] Print
[1] Print
[1] Print
[2] Test Balance
[3] Test Tare
[1] Print
[9] More
[5] Diagnostics
[2] Switches
[3] Valves
[4] Leak Check
[1] Print
System Setup
CS-200
49
Power-Up
1.
2.
3.
4.
5.
6.
7.
Menus
When pressing the menu key, a menu will appear displaying
different choices. When a menu appears, only options within
the menu are selectable. To remove a menu from the display
screen, press exit.
410
CS-200
System Setup
Keypad
The keypad used on the determinator is a matrix of switches,
referred to as keys, which must be pressed to activate a
selection, see Figure 42, below. This type of keypad is referred
to as a 'membrane keypad'. When activating a selection, press
the middle of the key until the microcomputer and display
screen recognize the selection.
PREVIOUS
NEXT
SELECT
MENU
ABC
DEF
GHI
JKL
MNO
PQR
STU
VWX
YZ
NO
YES
+
.% #,
RESET
DEL
EXIT
START
Figure 42
Keypad
System Setup
CS-200
411
412
CS-200
System Setup
System Setup
CS-200
413
Confirmation
Any operation that can cause information to be deleted will
display a confirmation box. Press yes to confirm the operation
or no to abort the delete command.
Copyright Screen
Upon power-up and exit from the main menu, the copyright
screen will be displayed. When this screen is displayed, wait a
few seconds, the screen will disappear and the main menu will
appear in its place.
414
CS-200
System Setup
System Overview
Analyze
Results
Calibrate
Setup
Diagnostics
System Setup
CS-200
415
System Check
Notes
Ambient Monitor
Notes
If the determinator has just been turned on, wait one hour
before checking the ambient monitor for the system to
stabilize.
1.
2.
Carbon IR Cell
Sulfur IR Cell
Oven Temp
Catalyst Heater
System Pressure
Plate Current
Grid Current
Note
416
8.500 v
8.500 v
48oC
350oC
762 mm
480 mA
100 mA
CS-200
System Setup
3.
Range
Units
Carbon IR Cell
Parameters
8.5
7.5 to 9.2
Sulfur IR Cell
8.5
7.5 to 9.2
Oven Temp
48
46 to 50
Catalyst Heater
350
325 to 357
System Pressure
762
740 to 790
Plate Current
460*
420 to 500
mA
Grid Current
100*
80 to 120
mA
V
C
C
mmHg
* Nominal values during analysis only. When furnace power is off, the
plate and grid current should be zero.
4.
5.
System Setup
6.
7.
8.
9.
CS-200
417
System Setup
Notes
418
Analysis Method
System Options
Transmit Options
Balance Options
System Clock
Set Barometer
More
CS-200
System Setup
System Options
Note
1.
15
Con
350
No
No
Short
1
MM-DD-YY
Yes
2.
3.
Enter the value from the keypad or press the right or left
arrow keys to move the cursor into position to change a
value.
4.
[1] Print
System Setup
5.
6.
CS-200
419
420
CS-200
System Setup
Transmit Options
Note
Yes
Comma
CRLF
SOH/EOT
9600
None
8
1
Option:
Yes
Yes/No
1.
2.
3.
4.
5.
[1] Print
System Setup
6.
7.
CS-200
421
422
CS-200
System Setup
Balance Options
Notes
4
Auto Tare
Esc T
1200
Odd
7
1
Option:
Yes
Yes/No
1.
2.
3.
4.
5.
[1] Print
[2] Test Balance
[3] Test Tare
System Setup
CS-200
423
6.
7.
8.
9.
424
CS-200
System Setup
System Setup
CS-200
425
System Clock
Notes
Enter Time
426
HH:MM:SS
10:24:39
Enter Date
MM-DD-YY
01-01-00
1.
2.
Press the left or right arrow keys to move the cursor into
position to set the time or press Select to set the date. The
enter date prompt will appear below the time.
3.
4.
CS-200
System Setup
Set Barometer
Note
1.
Pressure is Stabilizing
740 mm Hg
2.
Pressure (mm/Hg)
743
System Setup
3.
Press the right or left arrow keys to move the cursor into
position and change the barometric pressure to the correct
value with the number keys.
4.
5.
6.
CS-200
427
Combustion Pressure
Note
1.
2.
3.
4.
5.
ADJUSTMENT
KNOB
PRESSURE
REGULATOR
Figure 43
Combustion Pressure Adjustment Knob
428
CS-200
System Setup
Operation
1.
From the main menu, press Menu. The quick access menu
will be displayed.
Quick Menu
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]
[9]
System Setup
Analyze
Results
Calibrate
Analysis Method
Set Barometer
Leak Check
Print Buffer
Plot Buffer
Ambient Monitor
2.
3.
CS-200
429
Defining
Note
1.
1
2
3
4
5
6
7
8
9
Analyze
Results
Calibrate
Analysis Method
Set Barometer
Leak Check
Print Buffer
Plot Buffer
Ambient Monitor
Option:
Yes
Yes/No
2.
3.
4.
[1] Print
430
5.
6.
CS-200
System Setup
Change Password
Notes
1.
USER DIALOG
Enter Password
[
2.
USER DIALOG
Verify Password
[
System Setup
3.
4.
5.
CS-200
431
Notes
1.
432
1-Method
No
15
0
4
4.0
1.0
1.000
0.000
2.
3.
4.
CS-200
System Setup
5.
[1] Print
[2] Select Method
[3] Copy Method To
6.
7.
8.
[1]
[2]
[3]
[4]
[5]
9.
System Setup
1-Method
2-Method
3-Method
4-Method
5-Method
CS-200
433
434
CS-200
System Setup
Data Transmit
Notes
System Setup
1.
2.
3.
4.
5.
CS-200
435
ACK
BEL
BS
CAN
CR
DC1
DC2
DC3
DC4
DEL
DLE
Acknowledge
Bell, or alarm
Backspace
Cancel
Carriage return
Device control 1
Device control 2
Device control 3
Device control 4
Delete
Data link escape
EM
ENQ
EOT
ESC
ETB
ETX
FF
FS
GS
HT
LF
End of Medium
Enquiry
End of transmission
Escape
End of transmission block
End of text
Form feed
File separator
Group separator
Horizontal tab
Line feed
NAK
NUL
RS
SI
SO
SOH
SP
STX
SUB
SYN
US
VT
Negative acknowledge
Null, or all zeros
Record separator
Shift in
Shift Out
Start of heading
Space
Start of text
Substitute
Synchronous idle
Unit separator
Vertical Tab
*American Standard Code for Information Interchange (ASCII) X3.4 - 1967 for use on tape
1967 USA Standards Institute. Reprinted by permission.
436
CS-200
System Setup
Sample ID Code
FS
Weight
FS
00
01
02
03
04
05
06
07
08
09
0A
0B
0C
0D
0E
0F
10
11
12
SOH
"
"
FS
FS
01
22
41
30
30
30
30
30
30
31
22
1C
31
2E
30
30
30
30
30
1C
14
15
16
17
18
19
1A
1B
1C
1D
1E
1F
20
21
22
23
24
25
26
27
"
"
FS
22
31
2D
4D
45
54
48
4F
44
22
1C
31
2E
30
30
37
36
20
20
1C
28
29
39
3A
Method
FS
Carbon Calib.
2A
2B
FS
2C
2D
Carbon Results
Carbon Blank
2E
2F
30
31
13
32
33
FS
34
35
FS
FS
Time
36
37
FS
38
FS
FS
FS
31
2E
30
30
30
30
1C
30
2E
30
30
30
30
30
1C
30
34
30
1C
Peak
FS
3D
3E
3F
40
Sulfur Result
41
42
43
3C
1
FS
20
31
35
33
37
1C
31
2E
30
30
37
36
Sulfur Blank
51
52
53
54
44
45
FS
3B
FS
55
56
57
58
46
5A
4A
4B
49
FS
FS
20
20
1C
31
2E
30
30
30
30
1C
FS
5B
5C
FS
FS
30
2E
30
30
30
30
30
1C
30
34
30
1C
4C
4D
4E
64
65
66
67
31
30
3A
32
33
System Setup
68
20
4F
Peak
5F
50
FS
5D
5E
60
FS
20
31
35
33
37
1C
FS
48
Time
59
Sulfur Calib.
47
61
RS
62
EOT
69
6A
6B
6C
6D
6E
6F
70
71
72
RS
EOT
30
31
2D
32
38
2D
39
39
1E
04
CS-200
437
Keypad
Windows
Keypad
Illustrations .......................................................................44
Controls and Indicators .......................................................46
Menu Organization Chart .....................................................48
Power-Up ........................................................................ 410
About the Examples ..................................................... 410
Menus........................................................................ 410
Keypad ...................................................................... 411
Using the Keypad ................................................... 412
Notices and Errors ....................................................... 413
Confirmation............................................................... 414
Copyright Screen......................................................... 414
System Overview ............................................................. 415
Main Menu Overview .................................................... 415
System Check .................................................................. 416
Ambient Monitor.......................................................... 416
System Setup .................................................................. 418
System Options........................................................... 419
Definitions, Ranges, and Defaults.............................. 420
Transmit Options ......................................................... 421
Definitions, Ranges, and Defaults.............................. 422
438
CS-200
System Setup
System Setup
CS-200
439
440
CS-200
System Setup
Illustrations
Figure 41......... Controls and Indicators with Autocleaner....... 47
Figure 42......... Keypad and Display Screen ......................... 411
Figure 43......... Combustion Pressure Adjustment Knob ......... 428
Figure 4-4 ......... Controls and Indicators............................... 443
System Setup
CS-200
441
Note
442
CS-200
System Setup
AUTOCLEANER
ASSEMBLY
ACCESS DOOR
CONTRAST
CONTROL
BRIGHTNESS
CONTROL
INCOMING
REAGENT
TUBE
782-603
VACUUM
HOSE
CATALYST
HEATER
ASSEMBLY
604-126
DUST BOX
ANHYDRONE
TUBE
MEASURE
FLOW
ROTAMETER
ANALYZER
AC POWER
ON/OFF
SWITCH
CELLULOSE
FILTER
POWER LEVEL
ADJUSTMENT
FURNACE
AC POWER
ON/OFF
SWITCH
VACUUM
CLEANER
ON/OFF
SWITCH
PISTON
UP/DOWN
SWITCH
772-960
CRUCIBLE BOX
WITH LINER
789-230
VACUUM CLEANER
Figure 4-4
Controls and Indicators
System Setup
CS-200
443
444
CS-200
System Setup
System Setup
2.
3.
4.
5.
6.
7.
8.
9.
CS-200
445
Example
446
1.
2.
3.
4.
5.
6.
Click OK to close.
CS-200
System Setup
System Setup
CS-200
447
448
1.
2.
3.
4.
Click the Report Format drop down box and select the
desired report type.
5.
Click the Statistics drop down box and select the desired
statistics report type.
CS-200
System Setup
6.
B.
D.
Select the font name, text style, text size and color.
E.
F.
Line Printing
Note
I.
J.
7.
8.
9.
System Setup
CS-200
449
Tool Bar
This procedure hides or displays the Toolbar. When displayed
the tool bar is located at the top of the screen and is a quick
way to perform menu functions without accessing the menus.
1.
2.
Status Bar
This procedure hides or displays the Status Bar. When
displayed the Status Bar is located at the bottom of the screen
and displays operational functions of the instrument as they're
currently in progress.
450
1.
2.
CS-200
System Setup
Displayed Fields
Font Name
Font Style
Font Size
Font Color
Font Effects
Line Width
Plot Elements
Reporting Units
Significant Digits
Precision
Line Width
1.
System Setup
CS-200
451
2.
3.
4.
5.
6.
Click Font to change the font name, style, size, color and
effects.
7.
8.
9.
452
CS-200
System Setup
Method Development
A method is a set of analytical parameters used to control the
instrument during analysis and calculation of the final result.
Before analysis, a method must be created. Refer to the
method definitions below to help create a method for a specific
application.
In addition to creating a method, the methods screen also lists
methods that have been created and saved. If it is desired to
switch methods, or use an old method for a new application, a
method can be selected from this list during the sample login
procedure. Refer to Login a Sample on page 563.
Note
System Setup
1.
2.
3.
CS-200
453
454
4.
5.
6.
7.
8.
9.
Click OK.
CS-200
System Setup
System Setup
CS-200
455
Sample Templates
Sample Templates is a quick way for the operator to login a
sample and enter a method, comment and description. After a
Sample Template has been created refer to Login using a
Sample Template on page 567.
456
1.
2.
Double click on the last empty cell under the Name column
and enter the template name. The cursor must appear
before text can be entered.
3.
Double click in the other cells to the right of the name cell
to enter a method, comment and description into those
cells.
4.
5.
CS-200
System Setup
Standards
A Calibration Standard is a sample of known type and value.
Standards are used to calibrate the instrument for best
accuracy. Since calibration standards are usually purchased and
their value remains consistent, a list of standard samples and
associated information can be stored and accessed when
needed.
Standards creates a list of calibration standards for use during
calibration. This list can be accessed and found under the
Configuration menu.
Notes
System Setup
1.
2.
3.
4.
5.
CS-200
457
Standards Definitions
Standard NameThis is the name of the Standard defined by
the operator. The part number or lot number of the standard
can be used in place of the name.
(Element) PercentThe value of the standard. This is the
carbon or sulfur value taken from the label.
458
CS-200
System Setup
System Configuration
System Configuration sets the overall instrument operating
settings and parameter values. In addition, the settings for the
Serial Port, Balance and Language can be changed. The
settings and parameters are listed under system configuration
definitions.
System Setup
1.
2.
3.
4.
CS-200
459
460
CS-200
System Setup
System Setup
CS-200
461
Balance Tab
The Balance Tab is used to configure the balance serial port for
communications with an external balance. The serial port used
by the balance is COM 2.
462
1.
2.
3.
4.
CS-200
System Setup
Balance Definitions
Baud RateSelect the data transmission speed between the
computer and the balance. Selection: 1200 through 19200 bits
per second (bps). Default: 1200 bps.
Data BitsSelects the number of transmitted data bits per
byte. Selection: 6 through 8. Default: 7.
ParitySelects the method of error checking. Selection: Even,
Odd or None. Default: Even.
Stop BitsSelects the number of data bits that are used to
signal the end of transmitted data. Selections: 1 or 2. Default:
1.
Tare CommandThe command sent from the instrument that
causes the balance to tare. Selections are <ESC T>, T,
T<CR>LF>.
Send Command The command sent from the instrument that
causes the balance send a mass value back to the instrument.
Selections are <ESC>P<CR><LF>, S<CR><LF>,
SI<CR><LF>, P0<CR><LF>, and P1<CR><LF>.
Readability (Significant Digits)The number of significant digits
to the right of the mass value transferred from the balance and
entered into the spreadsheet. Range 3 to 6. Default: 4.
System Setup
CS-200
463
Note
464
1.
2.
Click Next.
3.
4.
5.
Click Next
6.
CS-200
System Setup
Transmission Formats
Transmission Formats permits the operator to select sample
and data transmission parameters to send to the host
computer. These include:
Note
Define Fields
Define Delimiters
Transmit Automation
Define Fields
Note
System Setup
7.
8.
CS-200
465
9.
466
CS-200
System Setup
Define Delimiters
Note
System Setup
1.
2.
CS-200
467
Note
3.
4.
Click the radio buttons and select the Field delimiter, Start
of Transmission delimiter, End of Transmission delimiter
and Text Format.
5.
468
CS-200
System Setup
System Setup
1.
2.
3.
CS-200
469
470
4.
5.
CS-200
System Setup
Select Language
Notes
System Setup
1.
2.
Select the desired language and click OK. The display text
will appear in the language selected.
CS-200
471
Users
The system manager can assign users (operators), passwords
and grant permissions from Users. This adds security to the
system and prevents unauthorized operation that could cause
damage or inaccurate result data.
Add a User
472
1.
2.
3.
4.
CS-200
System Setup
Add Password
System Setup
1.
2.
3.
4.
5.
CS-200
473
Note
1.
2.
3.
4.
474
CS-200
System Setup
Operation
Windows
Keypad
Keypad
5 Operation
Operation Guidelines...........................................................56
Before an Analysis ......................................................... 57
After an Analysis ........................................................... 58
After Use...................................................................... 58
Crucibles ...........................................................................59
Sample Preparation .......................................................... 510
Sample Size................................................................ 510
High Sulfur Samples .................................................... 510
Blank Samples ....................................................... 510
Analyze Menu .................................................................. 511
Screen Description....................................................... 511
Delete Weight ............................................................. 513
Insert Weight.............................................................. 514
Print Weights .............................................................. 515
System Controls .......................................................... 516
Definitions and Ranges ............................................ 517
Clean Switch............................................................... 518
Operation
CS-200
51
52
CS-200
Operation
Fill........................................................................ 554
Cut....................................................................... 554
Copy..................................................................... 554
Paste .................................................................... 554
View Menu.................................................................. 555
Tool Bar ................................................................ 555
Status Bar ............................................................. 555
First Row............................................................... 555
Analysis Row.......................................................... 555
Last Row ............................................................... 555
Samples Menu ............................................................ 556
Login .................................................................... 556
Balance ................................................................. 556
Analyze ................................................................. 556
Reset/Abort ........................................................... 556
Recalculate ............................................................ 557
Transmit ............................................................... 557
Delete................................................................... 557
Configuration Menu...................................................... 558
Calibrations ........................................................... 558
Blank .................................................................... 558
Drift ..................................................................... 558
Linearizations......................................................... 558
Standards.............................................................. 559
Methods ................................................................ 559
Counters ............................................................... 559
Sample Templates .................................................. 559
System ................................................................. 559
Users .................................................................... 559
Transmission Formats ............................................. 560
Select Language ..................................................... 560
Auto Widths ........................................................... 560
Display.................................................................. 560
Hardware Calibrations ............................................. 560
Diagnostics Menu ........................................................ 561
Leak Check ............................................................ 561
Operation
CS-200
53
Ambients............................................................... 561
Switches ............................................................... 561
Solenoids .............................................................. 561
Comport................................................................ 561
Maintenance Menu....................................................... 562
Login .................................................................... 562
View Log File.......................................................... 562
Login a Sample ................................................................ 563
Sample Login Definitions .............................................. 565
Balance Login ............................................................. 566
Login using a Sample Template ..................................... 567
Analyze a Sample ............................................................. 568
Delete a Sample............................................................... 569
Print Sample Results ......................................................... 570
Transmit Results .............................................................. 572
Recalculate Result ............................................................ 573
Calibration....................................................................... 574
Blank Calibration ......................................................... 574
Standard Calibration .................................................... 574
Drift Correction ........................................................... 574
Blank Calibration .............................................................. 575
Standard Calibration ......................................................... 576
Standard Calibration Definitions................................ 578
Drift Correction ................................................................ 579
Drift Correction ........................................................... 580
Data Management ............................................................ 581
Insert Data into the Spreadsheet ................................... 581
Insert a Sample Out-of-Sequence .................................. 582
Fill Selected Cells with the Same Values.......................... 582
Select First Row in the Spreadsheet ............................... 583
Select the Analysis Row in the Spreadsheet..................... 583
Select Last Row in the Spreadsheet................................ 583
Import Sample Data .................................................... 583
Export Sample ............................................................ 584
Export Sample Definitions ........................................ 586
Export Buffer .............................................................. 587
54
CS-200
Operation
Operation
CS-200
55
Operation Guidelines
Listed below are guidelines that should be followed before
analysis, after analysis and after use. By using this information,
along with the procedures in the Operation Chapter, the
operator will be able to obtain the best possible performance
from this instrument.
Note
56
CS-200
Operation
Before an Analysis
Before a sample can be analyzed and an accurate result
obtained, the instrument must be prepared for analysis. This
includes inspecting and cleaning the combustion system orings, performing a system leak check, selecting or creating a
method, performing a blank calibration and then performing a
standard calibration.
Note
1.
B.
C.
2.
3.
4.
5.
6.
7.
8.
9.
Operation
CS-200
57
After an Analysis
When an analysis is complete, the furnace automatically shuts
OFF, a signal sounds, and the spreadsheet shows the final
result. If Line Printing and Automatically Print After Each
Analysis is selected, the printer will print the analysis result.
Refer to Configure the Analysis Report, page 448.
After Use
The AC power to the instrument should remain on at all times.
If the power to the instrument is switched off for any reason a
one-hour warm-up is necessary before analyzing samples.
The instrument automatically switches to conservation (low gas
flow) after an amount of time specified by the Conservation
Time-out in System Configuration, page 459.
Remove the crucible from the furnace after use.
Note
58
CS-200
Operation
Crucibles
When analyzing for low carbon (<0.1%) or low sulfur
(<0.01%), burned off crucibles yield the best results.
Crucibles are burned off by firing them at 1350oC (2500oF) for
at least 20 minutes in a TF-1 or TF-10 Tube Furnace, then
cooling them in a desiccator. Crucibles must be used within four
hours of being burned off or the procedure must be done again.
!
CAUTION
Operation
CS-200
59
Sample Preparation
!
CAUTION
Sample Size
The nominal sample weight is 1.0 gram. The lower and upper
limits will depend on the sample material analyzed.
510
CS-200
Operation
Analyze Menu
Access the analyze screen by pressing [1] Analyze from the
main menu.
Analyze
0.01010% Carbon
0.02020% Sulfur
Plate
Grid
[
[
] 0mA
] 0mA
Method
ID Code
Weight
1-Method
A0000001
1.0000
1 2 3
Screen Description
The mode of operation is displayed on the top line.
The second line is the result window. The results of the last
analysis (or current analysis if one is in progress) is displayed,
followed by the element type. After each analysis, the result is
placed at the end of the results list and displayed in the results
window. The results list stores up to 50 analyses.
The center block displays the plate current and grid current
readings during an analysis.
The lower block displays the current active method, sample ID
code and sample weight. On the left side the parameter name
is displayed and on the right side the value.
The bottom line displays the number of sample weights that
have been entered. The highlight indicates the position
currently displayed in the weight list.
Note
Operation
CS-200
511
512
CS-200
Operation
Delete Weight
Notes
1.
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]
Operation
Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method
2.
3.
CS-200
513
Insert Weight
Note
0.01010% Carbon
0.02020% Sulfur
Plate
Grid
[
[
] 0mA
] 0mA
Method
ID Code
Weight
1-Method
A0000001
1.0000
1 2 3
Note
514
1.
2.
3.
Enter the weight from the keypad, or press the arrow keys
to move the cursor to the digit to edit and enter the value
from the keypad.
CS-200
Operation
Print Weights
Notes
1.
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]
2.
Operation
Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method
CS-200
515
System Controls
Notes
1.
Analysis Mode
Carrier Gas
Clean Counter
Clean Interval
Auto
Off
17
10
2.
3.
Enter the value from the keypad or press the arrow keys
to move the cursor into position to change a digit value.
4.
[1] Print
516
5.
6.
CS-200
Operation
Operation
CS-200
517
Clean Switch
The clean switch function has two modes of operation; with
autocleaner installed or without autocleaner installed. The clean
switch can be used in either mode to close the furnace without
starting an analysis.
During the cleaning process, the vacuum cleaner will
automatically turn on if the autocleaner is installed. If the
autocleaner is not installed, the vacuum cleaner must be turned
on manually.
If the autocleaner is installed, refer to clean counter and
furnace clean interval. These parameters will determine when
the combustion tube is automatically cleaned.
With Autocleaner
Note
518
1.
2.
3.
4.
5.
After the cleaning, pressing the piston switch will close the
furnace and start an analysis automatically if a weight is
entered in the weight list.
CS-200
Operation
Without Autocleaner
1.
2.
3.
4.
Remove the lance flow fitting and filter cap from the filter
head assembly.
5.
6.
Turn the vacuum cleaner off and press the piston switch to
release the cleaning cup.
7.
8.
9.
10. Press [5] Clean Switch to raise the lower seal assembly
without starting an analysis.
11. After the cleaning, pressing the piston switch will close the
furnace and start an analysis automatically if a weight is
entered in the weight list.
Note
Operation
CS-200
519
Balance Weight
Notes
1.
2.
3.
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]
4.
520
Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method
CS-200
Operation
Transmit Last
Notes
1.
2.
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]
3.
Operation
Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method
CS-200
521
Select Method
Notes
1.
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]
2.
Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method
[1]
[2]
[3]
[4]
[5]
3.
522
Method
Method
Method
Method
Method
1
2
3
4
5
CS-200
Operation
Notes
1.
There are four types of weight entry that can be used. The
following procedures describe the use of each entry.
A.
B.
C.
Operation
2)
2)
2)
CS-200
523
D.
2.
Note
524
2)
3.
4.
CS-200
Operation
Sample Analysis
Notes
1.
Note
For best results, turn the power off only if the instrument
malfunctions. This eliminates the warm-up time delay.
2.
3.
0.01010% Carbon
0.02020% Sulfur
Plate
Grid
[
[
] 0mA
] 0mA
Method
ID Code
Weight
1-Method
A0000001
1.0000
1 2 3
Operation
4.
5.
CS-200
525
Note
Note
6.
Place the crucible and sample onto the pedestal and press
Piston Up/Down. If the determinator is configured for
automatic operation, the sample will be loaded into the
furnace and analysis will begin. If the determinator is
configured for manual operation, press Start to begin the
analysis after the piston rises and the sample is loaded
into the furnace.
7.
8.
9.
WARNING
526
CS-200
Operation
Calibrate Menu
Notes
1.
Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031
0 Selected
1 of 7
2.
3.
4.
5.
6.
Carbon
Record Format
List Format
Clear Selections
Calculate Calib
Edit Calibration
Calculate Blank
Edit Blank
Recalculate
0 Selected
Operation
Sulfur
0.00169
0.00796
0.00855
0.00654
0.00776
0.00528
0.00487
CS-200
1 of 7
527
Notes
1.
Note
2.
3.
Note
4.
528
Results
Calib.
Blank
Time
Peak
A0000001
1.0000
1-Method
Carbon
Sulfur
0.8921
0.0034
0.7863
1.3017
0.0000
0.0000
40
44
16462
149
0 Selected:
1 of 7
CS-200
Operation
Clear Selection
Note
1.
Record Format
List Format
Clear Selections
Calculate Calib
Edit Calibration
Calculate Blank
Edit Blank
Recalculate
0 Selected
2.
Operation
Carbon
1 of 7
CS-200
529
Calculate Calibration
Notes
1.
Carbon
Standard
Yes
0.35400
Sulfur
Standard
Yes
0.05400
Option:
Yes
Y/N
2.
3.
530
Carbon
Standard
Yes
0.35400
Sulfur
Standard
Yes
0.05400
Option:
Yes
CS-200
Y/N
Operation
4.
[1] Print
[2] Reset Calib.
5.
Operation
A.
B.
CS-200
531
Edit Calibration
Notes
1.
1.0512
1.1617
Sulfur
Old Calib
New Calib
1.0033
1.0055
2.
3.
[1] Print
532
4.
5.
CS-200
Operation
Calculate Blank
Notes
1.
Carbon
Standard
0.0000
Sulfur
Standard
0.0000
2.
3.
Press Yes to calculate the new blank value, and display the
blank calculation screen.
Blank Results
Operation
Carbon
Old Blank
New Blank
0.0000
0.0012
Sulfur
Old Blank
New Blank
0.0000
0.0010
CS-200
533
4.
[1] Print
534
5.
6.
CS-200
Operation
Edit Blank
Notes
1.
Press [7] Edit Blank from the calibrate menu to display the
edit blank screen.
Edit Blank
Carbon
Old Blank
New Blank
0.0000
0.0012
Sulfur
Old Blank
New Blank
0.0000
0.0010
2.
3.
[1] Print
Operation
4.
5.
CS-200
535
Recalculate Results
Notes
1.
Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031
0 Selected
1 of 7
Sulfur
0.044
0.051
0.047
0.050
0.051
0.046
0.045
2.
3.
4.
A.
B.
Carbon
2 Selected
536
CS-200
1 of 7
Operation
Operation
5.
6.
7.
CS-200
537
Results Menu
Notes
1.
538
ID Code
A0000001
A0000002
A0000003
A0000004
A0000005
A0000006
>A0000007
Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031
0 Selected
1 of 7
Sulfur
0.044
0.051
0.047
0.050
0.051
0.046
0.045
2.
3.
B.
CS-200
Operation
4.
5.
Operation
Carbon
Record Format
List Format
Clear Selections
Delete
Statistics
Print
Transmit
CS-200
539
Notes
1.
2.
3.
540
Result
Calib
Blank
Time
Peak
A0000001
0.1452
1-Method
Carbon
Sulfur
0.8921
0.0322
0.7863
0.9309
0.00000 0.00000
40
44
16462
149
0 Selected
1 of 7
CS-200
Operation
Clear Selections
Note
1.
2.
Operation
Record Format
List Format
Clear Selections
Delete
Statistics
Print
Transmit
CS-200
541
0 Selected
542
1 of 7
2.
3.
CS-200
Operation
Statistics
1.
Carbon
Average
Std. Dev.
RSD
Points
Sulfur
Average
Std. Dev.
RSD
Points
0.311
0.001
0.039
3
0.0354
0.0003
0.73
3
Statistics
[1] Print
Operation
2.
3.
4.
CS-200
543
Definitions
AverageThe average value of the selected results.
Standard DeviationThe amount of deviation, from the average
value, where 67% of the measured results range. The standard
deviation calculation uses n-1" degrees of freedom.
Relative Standard DeviationThe standard deviation compared
to the average value expressed as a percentage.
(STD DEV/AVG) x 100.
PointsThe number of selected results used to calculate the
average value and standard deviation.
544
CS-200
Operation
Operation
ID Code
A0000001
A0000002
A0000003
A0000004
A0000005
A0000006
>A0000007
Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031
0 Selected
1 of 2
CS-200
Sulfur
0.044
0.051
0.047
0.050
0.051
0.046
0.045
545
546
ID Code
A0000001
A0000002
A0000003
A0000004
A0000005
A0000006
>A0000007
Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031
0 Selected
1 of 2
CS-200
Sulfur
0.044
0.051
0.047
0.050
0.051
0.046
0.045
Operation
Keypad
Windows
Keypad
Operation Guidelines...........................................................56
Before an Analysis ......................................................... 57
After an Analysis ........................................................... 58
After Use...................................................................... 58
Crucibles ...........................................................................59
Sample Preparation .......................................................... 510
Sample Size................................................................ 510
High Sulfur Samples .................................................... 510
Blank Samples ....................................................... 510
Analyze Menu .................................................................. 511
Screen Description....................................................... 511
Delete Weight ............................................................. 513
Insert Weight.............................................................. 514
Print Weights .............................................................. 515
System Controls .......................................................... 516
Definitions and Ranges ............................................ 517
Clean Switch............................................................... 518
With Autocleaner .................................................... 518
Without Autocleaner................................................ 519
Balance Weight ........................................................... 520
Transmit Last.............................................................. 521
Operation
CS-200
547
548
CS-200
Operation
CS-200
549
CS-200
Operation
Operation
CS-200
551
Note
File Menu
This menu permits the operator to configure and print data on
the system printer, import data from another application
software and export data to a floppy disk.
Click File to display this menu.
Print
Select Print to access the report settings dialog box and print
selected sample results on the system printer. Refer to Print
Sample Results on page 570.
Print Preview
Select Print Preview to access the report settings dialog box
and preview how selected samples would print on the system
printer. Refer to Configure the Analysis Report on page 448.
Print Setup
Select Print Setup to access the printer setup dialog box and
configure the system printer settings.
552
CS-200
Operation
Import
Select Import to transfer sample data from another software
application. Refer to Import Sample Data on page 583.
Export
Select Export to transfer sample data to another storage
location like a floppy disk. Refer to Export Sample on page 5
84.
Exit
Select Exit to stop using the CS-200 application program and
return to the Windows Operating System.
Operation
CS-200
553
Edit Menu
This menu permits the operator to insert a sample out of
sequence into the spreadsheet, fill a group of cells in the
spreadsheet with the same data, cut and move data to other
cells, copy data to other cells and paste data to other cells.
Click Edit to display this menu.
Insert
Select Insert to insert a sample out of sequence, between
unanalyzed samples, into the spreadsheet for analysis. Refer to
Data Management on page 581.
Fill
Select Fill to quickly fill a group of cells in the spreadsheet with
the same data value. Refer to Data Management on page 581.
Cut
Select Cut to move data from an entire row in the spreadsheet
to the clipboard. Refer to Clipboard Use on page 588.
Copy
Select Copy to transfer data from an entire row in the
spreadsheet to the clipboard. Refer to Clipboard Use on page
588.
Paste
Select Paste to insert data from the clipboard to a selected row
in the spreadsheet. Refer to Clipboard Use on page 588.
554
CS-200
Operation
View Menu
This menu permits the operator to turn the tool bar and status
bar ON or OFF and select the first row, last row or analysis row
in the spreadsheet.
Click View to display this menu.
Tool Bar
Select Tool Bar to display or hide the toolbar. Refer to
Configure the Screen on page 450.
Status Bar
Select Status Bar to display or hide the status Bar. Refer to
Configure the Screen on page 450.
First Row
Select the First Row of analysis data in the spreadsheet. Refer
to Data Management on page 581.
Analysis Row
Select the Analysis Row that contains the next sample to be
analyzed in the spreadsheet. Refer to Data Management on
page 581.
Last Row
Select the Last Row of analysis data in the spreadsheet. Refer
to Data Management on page 581.
Operation
CS-200
555
Samples Menu
This menu permits the operator to log sample data into the
spreadsheet, analyze a sample, abort an analysis, recalculate
results, transmit results and delete a sample from the
spreadsheet.
Click Samples to display this menu.
Login
Select Login to enter a sample and sample data into the
spreadsheet. Refer to Login a Sample on page 563.
Balance
Select Balance to enter a mass from the balance into the
sample login screen. Refer to Balance Login on page 566.
Analyze
Select Analyze to login and analyze a sample or analyze a
standard. Refer to Analyze a Sample on page 568.
Reset/Abort
Select Abort to stop an analysis in progress. Refer to Analyze a
Sample on page 568.
556
CS-200
Operation
Recalculate
After an analysis is complete, Recalculate Results can be used
to recalculate the result if the extraction data or calibration has
changed. Refer to Recalculate Result on page 573.
Transmit
Select Transmit to transfer selected sample results to a host
computer. Refer to Transmit on page 572.
Delete
Select Delete to remove a selected sample from the
spreadsheet. Refer to Delete a Sample on page 569.
Operation
CS-200
557
Configuration Menu
This menu is used for instrument calibration, to configure the
instrument hardware, to create a method, to configure the
software and for maintenance configuration.
Click Configuration to display this menu.
Calibrations
Select Calibrations to set the accuracy of the instrument to that
of known calibration standard samples. Refer to Calibration on
page 574.
Blank
Select Blank to calculate the system blank and compensate for
it when calculating the analysis result. Refer to Blank
Calibration on page 575.
Drift
Select Drift to compensate standard calibration and account for
variances or Drift in the instrument hardware that can slightly
change the calibration. Refer to Drift Correction on page 579.
Linearizations
Select Linearizations to enter the IR cell reference and
saturation values. Breaks and slopes are not typically set, they
are provided for those who wish to modify the linearity of the
instrument. Refer to Linearization on page 1032.
558
CS-200
Operation
Standards
Select Standards to create a list of standard calibration
samples. Refer to Standards on page 457.
Methods
Select Method to create a set of analysis parameter values for
analysis. Refer to Method Development on page 453.
Counters
Select Counters to automatically determine when periodic
maintenance is necessary. Maintenance data that was entered
into Login Periodic Maintenance is used by the counters to
determine when maintenance is necessary. Refer to Login
Periodic Maintenance on page 624.
Sample Templates
Sample Templates is a quick way for the operator to login a
sample and enter a method, comment and description. Select
Sample Template to develop a specific sample template. After a
sample template is developed, use Login Using a Sample
Template to login a sample with predetermined sample analysis
data. Refer to Sample Templates on page 456.
System
Select System Configuration to set the overall instrument
operating settings and configure the instrument for a specific
application or set of applications. Refer to System Configuration
on page 459.
Users
Select Users to assign an operator and give them access to use
the instrument. Select Assign User Password to add security to
the system by requiring a password to log on to the instrument.
Select Assign User Functions to grant permissions that a user
can use while operating the instrument. Refer to Users on page
472.
Operation
CS-200
559
Transmission Formats
Before data can be transmitted to a host computer, the
transmitted data format must be configured to match. Use
Transmission Formats to Configure Data Transmission. Refer to
Transmission Formats on page 465.
Select Language
Select Language to determine and change the language of text
display by the software. Refer to Select Language on page 4
71.
Auto Widths
Select Auto Widths to automatically adjust the width of each
cell to fit the text. Refer to Configure the Spreadsheet on page
451.
Display
Select Display to set the desktop characteristics as viewed on
the computer monitor. Refer to Configure the Spreadsheet on
page 451.
Hardware Calibrations
Hardware Calibration permits the operator and service person
to calibrate the Back Pressure Controller, Catalyst Heaters, and
Oxygen Flow Rate. Refer to Hardware Calibrations on page 103.
560
CS-200
Operation
Diagnostics Menu
This menu is used to perform a leak check, monitor the
instrument operating parameters, toggle the solenoid valves,
monitor the electrical switch states and check communications
between the instrument and PC.
Click Diagnostics to display this menu.
Leak Check
Select Leak Check to check and determine if the instrument has
an oxygen or pneumatic gas leak. Refer to Leak Check on page
819.
Ambients
Select Ambients to monitor the system operating parameters
and display the ambient monitor. All parameters can be
displayed. Refer to Ambient Monitor on page 822.
Switches
Select Switches to view the electrical switch states. None of the
states can be changed from this screen. Refer to Switches on
page 826.
Solenoids
Select Solenoids to toggle the solenoid valves to check
operation, diagnose instrument problems and perform periodic
maintenance. Refer to Solenoids on page 827.
Comport
Select Comport to check the transfer of data between the PC
and the instrument. Refer to Comport on page 828.
Operation
CS-200
561
Maintenance Menu
This menu permits the operator to login periodic maintenance
and view the maintenance log file.
Click Maintenance to display this menu.
Login
Select Login to login periodic maintenance after it was
performed. Refer to Login Periodic Maintenance on page 624.
View Log File
The system will automatically keep a record of various
procedures that were performed and error conditions. The
record can be viewed using View Log File. Refer to View Log File
on page 625.
562
CS-200
Operation
Login a Sample
Login a Sample is used by the operator to enter sample
information into the spreadsheet. This procedure is called
Sample Login. Using Sample Login the operator can login a
Blank Sample, Standard Sample, Gas Dose Sample or an
Unknown Sample for analysis.
Before a sample is analyzed, the sample type and information
associated with it must be entered into the spreadsheet. A
sample that has been logged in may be analyzed later.
In addition to Sample Login, a sample can be logged in using
Balance Login, page 566, Login using a Sample Template,
page 567, or directly into the Spreadsheet by clicking on the
next available line and typing in the sample data. The sample
name and method can be inserted using the drop-down menu.
1.
Operation
CS-200
563
564
2.
3.
4.
CS-200
Operation
Operation
CS-200
565
Balance Login
Balance automatically enters a row at the spreadsheet. The
sample ID and method will be entered into the row along with
the mass. The sample ID and method will be the same as those
in the previous row. The mass will be the value read on the
balance.
Before the mass can be automatically transferred to the
spreadsheet, the balance must be interfaced with the
instrument. Refer to Balance on page 33 for instructions.
1.
566
CS-200
Operation
Operation
1.
2.
Click the drop down arrow to the right of sample name and
enter the desired sample name from the drop down list.
The sample name, mass, method, comments, description,
operator will automatically be entered into the
spreadsheet.
3.
CS-200
567
Analyze a Sample
After a sample is logged in it can be analyzed. Analyze a
Sample starts an analysis. Analysis will start with the first
unanalyzed sample in the spreadsheet. Analyzing will appear in
the date column as the analysis is in progress.
Abort an Analysis will stop an analysis in progress.
Note
WARNING
SERIOUS BURNS
After analysis use crucible tongs to remove the
hot crucibles from the pedestal and place them in
the crucible bucket to cool.
1.
Notes
Note
568
2.
If the furnace did not start before abort was selected the
analysis will be reset and can be restarted.
CS-200
Operation
Delete a Sample
A sample that has been logged in or analyzed can be deleted
from the spreadsheet. This may be a sample that was logged in
error or a sample that was improperly analyzed.
Operation
1.
2.
CS-200
569
570
1.
2.
3.
Click File and select Print. The Report Settings screen will
appear.
CS-200
Operation
Operation
CS-200
571
Transmit
Analysis Results can be transmitted or transferred to a host
computer. This permits another person to analyze data as
samples are being analyzed. It can also be used to save
selected results at another location.
572
1.
2.
CS-200
Operation
Recalculate Result
After a sample is analyzed, the result can be recalculated if
sample data has changed. The mass, method or calibration may
have changed, or need to be changed, to obtain the desired
result.
Operation
1.
2.
CS-200
573
Calibration
Calibration is the process that adjusts the instrument to
produce an analysis result to equal that of a known calibration
standard with the same concentration. First a Blank Calibration
is performed, then Standard Calibration and then as daily
maintenance both a Blank Calibration and Drift Correction.
Single point calibration calibrates the instrument to one
calibration point. Multi-point calibration calibrates the
instrument to a set of calibration points over an expected range
of concentrations.
Blank Calibration
Blank Calibration is used to calculate the system blank or
baseline. Sometimes this is called the blank area. Blank
calibration calculates the system blank and compensates for it
when calculating the analysis result. The system blank should
be determined every day by performing a blank calibration
before analysis. Refer to Blank Calibration on page 575.
Standard Calibration
Standard Calibration is used to calibrate the instrument with
known calibration standards. A single point or multi-point
calibration can be performed and the curve type selected
although, LECO recommends multipoint, linear calibrations that
employ 1/certified weighting. Additionally a blank calibration
should be completed prior to performing a standard calibration.
Since Standard Calibration is saved with each method, each
method must be calibrated after it is created. Refer to Standard
Calibration on page 576.
Drift Correction
Drift Correction is used to compensate standard calibration and
account for variances in the instrument hardware that can
slightly change the calibration. Drift correction should be
performed at the start of every day. This insures accurate
calibration and analysis results. Refer to Drift Correction on
page 579.
574
CS-200
Operation
Blank Calibration
Blank calibration calculates the system blank and compensates
for it when calculating the analysis result. Refer to Calibration
on page 574 for more information.
Note
Note
Operation
1.
2.
3.
4.
5.
CS-200
575
Standard Calibration
Standard Calibration is used to calibrate the instrument with
known calibration standards. Refer to Calibration on page 574
for more information.
Notes
576
1.
2.
3.
CS-200
Operation
4.
Click the arrow in the drop down box and Select a Cell
(detector) to calculate a calibration for. A separate
calibration can be calculated for each cell.
5.
Click the arrow in the drop down box and Select a Curve
Type. LECO recommends that multipoint linear calibration
that employs 1/certified weighting be used for standard
calibration.
6.
7.
Click the arrow in the drop down box and Select the
desired Weighting. LECO recommends that multipoint
linear calibration that employs 1/certified weighting be
used for standard calibration.
8.
9.
10. Repeat the process for each cell, carbon high, carbon low,
and sulfur.
11. Click OK to exit the calibration procedure and save the
calibration curve.
Operation
CS-200
577
578
CS-200
Operation
Drift Correction
Drift Correction is used to compensate standard calibration and
account for variances in the instrument hardware over a period
of time that can slightly change the calibration. Drift correction
should be performed at the start of each day. This insures
accurate calibration and analysis results.
Perform standard calibration and choose the drift standards
before performing a drift calibration. Refer to Calibration on
page 574 for more information.
Note
Operation
CS-200
579
Drift Correction
Note
Note
580
1.
2.
3.
4.
5.
CS-200
Operation
Data Management
Data Management is a group of procedures that permits the
operator to move sample data from one area of the
spreadsheet to another, move data into the spreadsheet and
move data out of the spreadsheet and store it on a floppy disk.
The following procedures are grouped under Data Management.
Operation
1.
Click and drag the mouse pointer to select the cells to fill
with the same data.
2.
3.
4.
CS-200
581
Note
1.
2.
Click Edit and select Insert. A row will be inserted into the
spreadsheet before the selected row.
582
1.
2.
Click Edit and select Fill. The Fill screen will appear.
3.
4.
CS-200
Operation
Operation
1.
2.
CS-200
583
Export Sample
Export Sample permits the operator to select sample data and
data transmission parameters and transfer them to a file for
storage. More than one configuration can be defined and
selected.
584
1.
2.
Click File and select Export. The Export screen will appear.
3.
4.
5.
CS-200
Operation
6.
7.
8.
For each field to transmit, select the Field from the fields
list box and click Add.
9.
Operation
CS-200
585
586
CS-200
Operation
Export Buffer
Export Buffer permits the operator to select a sample and
transfer the plot buffer data contents to a file.
Operation
1.
2.
Click File and select Export. The Export screen will appear.
3.
4.
5.
CS-200
587
Clipboard Use
The Clipboard is a temporary storage space for data. Data can
be moved into and out of the clipboard by cutting, copying or
pasting. By using the clipboard cell data can be moved
throughout the spreadsheet.
1.
2.
Click the Edit menu and select Cut. The data will be
removed from the spreadsheet and moved to the
clipboard.
1.
2.
Click the Edit menu and select Copy. The data will be
copied from the spreadsheet to the clipboard.
588
1.
2.
Click the Edit menu and select Paste. The data will be
moved from the clipboard to the spreadsheet.
CS-200
Operation
2.
3.
Selection Procedures
Zoom In (not a menu selection)Position the pointer (mouse
pointer) over the area to zoom in on. Hold the left mouse
button down and draw a box. The area inside the box will be
magnified. Draw another box to zoom in farther. Zoom In
cannot be used if the sample being analyzed is displayed. Wait
until analysis is complete and then zoom in on the plot.
Zoom OutClick Zoom Out to remove all steps of
magnification.
Zoom Out One LevelClick Zoom Out to remove the last step
of magnification.
Label PointsWhen result points are selected and displayed,
the points can be numbered to show their relationship to the
samples selected. The first sample selected is labeled number 1
and the remaining samples selected are numbered as they
were selected from the spreadsheet. The number displayed on
the plot is not the sample number displayed on the
spreadsheet. Multiple samples and statistics (below) must be
selected before this feature can be used.
Operation
CS-200
589
From the Properties screen you can select the Reporting Units,
Significant Digits, Plot Pattern and Plot Color. You can also Hide
the Baseline and Plot if desired.
590
CS-200
Operation
Maintenance
6 Maintenance
Illustrations .......................................................................62
Periodic Maintenance Schedule .............................................63
Anhydrone Tube.................................................................64
Removal....................................................................... 64
Packing ........................................................................ 64
Autocleaner .......................................................................66
Autocleaner Assembly .................................................... 67
Autocleaner Mesh Filter .................................................. 69
Autocleaner O-rings ..................................................... 610
Catalyst Heater Tube Packing ............................................. 611
Cellulose Filter ................................................................. 613
Removal..................................................................... 613
Packing ...................................................................... 613
Combustion Tube ............................................................. 615
Combustion Zone O-rings .................................................. 616
Incoming Reagent Tube..................................................... 617
Removal..................................................................... 617
Packing ...................................................................... 617
Lance and Filter Assembly ................................................. 619
Pinch Valve Tubing ........................................................... 621
Reagent Tube Screen Filter ................................................ 623
Login Periodic Maintenance ................................................ 624
View Log File ................................................................... 625
Reset Maintenance Counters .............................................. 626
Maintenance
CS-200
61
Illustrations
Figure 61......... Anhydrone Tube ........................................ 65
Figure 62......... Autocleaner Assembly ................................ 68
Figure 63......... Catalyst Heater Tube Packing ...................... 612
Figure 64......... Cellulose Filter Packing ............................... 614
Figure 65......... Reagent Tube Removal ............................... 618
Figure 66......... Reagent Tube Packing ................................ 618
Figure 67......... Lance and Filter Assembly........................... 620
Figure 68......... Pinch Valve Assembly ................................. 622
62
CS-200
Maintenance
Replacement/Cleaning
Schedule
Inspection Schedule
Anhydrone Tube
Inspect daily.
Replace as needed.
Autocleaner
Daily.
Refer to page 66.
Disassemble
and clean daily.
Daily.
Refer to page 69.
Inspect monthly.
Clean if flow is restricted.
Autocleaner O-rings
Daily.
Refer to page 610.
Inspect monthly.
Grease or replace
as necessary.
Replace packing
every six months.
Refer to page 611.
Cellulose Filter
Replace cellulose.
Inspect o-rings.
Clean or grease
as necessary.
Combustion Tube
Brush every
five to ten analysis.
Refer to page 615.
Replace if damaged.
Refer to page 616.
Daily.
Refer to page 619.
Inspect monthly.
Replace as necessary.
Replace if damaged.
Refer to page 623.
Inspect monthly.
Clean or replace
if flow is restricted.
Maintenance
CS-200
63
Anhydrone Tube
Removal
1.
Slide the anhydrone tube upward until the bottom end can
swing free. Refer to Figure 65, page 618.
2.
3.
4.
Packing
64
1.
2.
3.
4.
5.
6.
7.
CS-200
Maintenance
789-095
REAGENT STOP
765-976
O-RING
(2 REQ'D)
502-177
1/2" QUARTZ WOOL
501-171
2" ANHYDRONE
601-390
QUICK
DISCONNECT
TUBE
502-177
2" QUARTZ WOOL
775-306
SCREEN FILTER
Figure 61
Anhydrone Tube
Maintenance
CS-200
65
Autocleaner
Notes
Keypad
Windows
66
CS-200
Maintenance
Autocleaner Assembly
Maintenance
1.
2.
3.
Clean the inside of the lance using the lance cleaning rod.
4.
Inspect the brushes for wear. Remove the o-rings from the
filter and replace them.
5.
CS-200
67
604-291
AIR CYLINDER
806-214
FITTING
(2) REQD
604-519
EXTENSION
807-261
FITTING
(2) REQD
193-143
LOCKWASHER
610-735
SLOTTED
BRUSH
807-196
TUBING
(2) REQD
604-517
RETAINER
604-516
FITTING
773-320
O-RING
(2 REQD)
789-115
LANCE TUBE
604-268
BODY
ASSEMBLY
193-164
LOCKWASHER
(2 REQD)
604-172
O-RING
604-274
SHAFT
604-163
BRUSH
762-058
O-RING
190-228
SCREW
(2 REQD)
604-159
PLUNGER
604-273
BUSHING
ADAPTOR
604-272
CAP
190-757
SCREW
(4) REQD
604-168
LOCK
MOUNT
771-991
O-RING
778-703
SPACER
(4) REQD
778-596
FILTER
190-090
THUMBSCREW
(2 REQD)
762-058
O-RING
773-926
PLATE
190-431
SCREW
(2) REQD
762-058
O-RING
773-577
PISTON RING
Figure 62
Autocleaner Assembly
68
CS-200
Maintenance
Note
Note
1.
2.
3.
4.
Reach into the body assembly and pull the metal filter out.
5.
6.
7.
8.
9.
B.
10. After the filter has been cleaned, remove it from the tank
and rinse it for two minutes under clean running water,
then dry with warm air.
11. Wipe clean and lubricate the o-rings with silicone grease.
Reinstall the o-rings.
12. Install the filter in the body assembly and reassemble the
cleaning brush assembly if necessary.
13. Reconnect the gas lines.
Maintenance
CS-200
69
Autocleaner O-rings
Note
1.
2.
3.
4.
Unscrew the four screws from the air cylinder and remove
the cylinder from the autocleaner cap.
5.
6.
7.
8.
610
A.
B.
Slide the autocleaner cap over the rod and screw the
shaft into the rod.
C.
D.
E.
CS-200
Maintenance
WARNING
1.
2.
3.
4.
5.
6.
Insert 3/4 inch of quartz wool into the catalyst heater tube
and position it at the bottom of the bubble in the catalyst
heater tube.
7.
8.
Insert 3/4 inch of quartz wool into the catalyst heater tube
and position it on top of the platinized silica gel.
9.
Maintenance
CS-200
611
772-694
MOVABLE
BLOCK
KNOB
614-316
MOVABLE
BLOCK
772-520
O-RING
772-739
TUBE
502-177
/4" QUARTZ
WOOL
501-587
1" PLATINUM
SILICA CATALYST
502-177
/4" QUARTZ
WOOL
Figure 63
Catalyst Heater Tube Packing
612
CS-200
Maintenance
Cellulose Filter
Notes
Removal
1.
Slide the cellulose filter tube upward until the bottom end
can swing free.
2.
3.
4.
5.
Packing
1.
Notes
Maintenance
Leave 1/2 inch of the cellulose filter tube open at both ends
for reinstallation onto the unit. Refer to Figure 64, page 6
14.
2.
CS-200
613
764-098
CELLULOSE
771-030
QUICK
DISCONNECT
TUBE
Figure 64
Cellulose Filter Packing
614
CS-200
Maintenance
Combustion Tube
Notes
Keypad
Note
Maintenance
1.
2.
CS-200
615
616
CS-200
Maintenance
Removal
1.
Slide each reagent tube upward until the bottom end can
swing free. Refer to Figure 65, page 618.
2.
3.
4.
Packing
Maintenance
1.
2.
3.
4.
Pack 1/2 inch of quartz wool into the bottom of the reagent
tube.
5.
6.
Pour Lecosorb onto the anhydrone until all but the top 1/2
inch of the reagent tube is filled, gently tapping it down.
7.
8.
CS-200
617
771-373
REAGENT
TUBE
Figure 65
Reagent Tube Removal
502-177
/2" QUARTZ WOOL
502-174
2" LECOSORB
771-373
QUICK DISCONNECT
TUBE
501-171
1" ANHYDRONE
502-177
/2" QUARTZ WOOL
775-306
SCREEN FILTER
Figure 66
Reagent Tube Packing
618
CS-200
Maintenance
Notes
Note
Maintenance
1.
Loosen the connection on the lance flow inlet 1/4 turn and
disconnect the line.
2.
Unscrew the filter cap. Scrape and remove the dust and
soot from inside the filter cap. Refer to Figure 67, page
620.
3.
4.
5.
6.
Replace the filter cap and reconnect the lance flow line.
7.
CS-200
619
773-311
FILTER
781-422
FILTER CAP
781-424
O-RING
762-058
O-RING
*772-704
FITTING
781-421
FILTER
HOUSING
*773-136
FITTING
781-663
LANCE
GUARD
789-118
LANCE TUBE
ASSEMBLY
771-991
O-RING
781-423
ADAPTOR TUBE
BUSHING
772-381
LANCE
CLEANING
ROD
762-058
O-RING
773-577
PISTON
RING
190-431
SCREW
(4) REQD
781-425
FILTER END
PLATE
190-258
SCREW
(2) REQD
LANCE
TUBE
762-068
O-RING
*781-401
ADAPTER
RING
NOTE: * NOT PART OF ASSEMBLY
Figure 67
Lance and Filter Assembly
620
CS-200
Maintenance
Note
1.
Remove the dust box and vacuum hose from the right side
of the furnace and remove the right side furnace panel.
2.
3.
4.
5.
6.
7.
8.
9.
10. Replace the dust box and vacuum hose then restore
pneumatic pressure.
Maintenance
CS-200
621
616-892
BRACKET
190-246
SCREW
(2 REQ'D)
589-182
FITTING
774-612
HOUSING
774-613
O-RING
769-973
ROLL PIN
(2 REQ'D)
774-610
PISTON
772-909
PINCH VALVE
ASSEMBLY
776-093
CAP
190-246
SCREW
(2 REQ'D)
501-110-019
SILICONE
TUBE
Figure 68
Pinch Valve Assembly
622
CS-200
Maintenance
Note
Maintenance
1.
2.
CS-200
623
624
1.
2.
3.
4.
Click OK.
CS-200
Maintenance
Maintenance
Network Errors
Sample Aborted
Sample Deleted
1.
Click Maintenance and select View Log File the Log File
screen will appear.
2.
3.
CS-200
625
Note
626
1.
2.
3.
Click OK.
CS-200
Maintenance
4.
5.
6.
Maintenance
The Confirm dialog box for the first maintenance item will
appear.
A.
B.
C.
B.
C.
CS-200
627
Theory of Operation
7 Theory of Operation
Illustrations .......................................................................72
General Information............................................................73
Infrared Radiation, Absorption, and Detection.........................74
Comparator Level ...............................................................78
Theory of Operation
CS-200
71
Illustrations
Figure 71 Gas Flow Diagram............................................... 76
Figure 72 Gas Flow with Autocleaner Diagram....................... 77
72
CS-200
Theory of Operation
General Information
The CS-200 Carbon/Sulfur Determinator is a microprocessor
based, software driven instrument for measurement of carbon
and sulfur content in metals, ores, ceramics, and other
inorganic materials. The CS-200 uses an induction furnace and
measures carbon and sulfur by infrared absorption.
Analysis begins by weighing out a sample (1 g nominal) into a
ceramic crucible on a balance. Accelerator material is added,
the crucible is placed on the loading pedestal, and the analyze
key is pressed. Furnace closure is performed automatically,
then the combustion chamber is purged with oxygen to drive
off residual atmospheric gases. After purging, oxygen flow
through the system is restored and the induction furnace is
turned on. The inductive elements of the sample and
accelerator couple with the high frequency field of the furnace.
The pure oxygen environment and the heat generated by this
coupling cause the sample to combust. During combustion,
carbon bearing elements are reduced, releasing the carbon,
which immediately binds with the oxygen to form CO and CO2,
the majority being CO2. Also, sulfur-bearing elements are
reduced, releasing sulfur, which binds with oxygen to form SO2.
Sample gases are swept into the carrier stream. Sulfur is
measured as sulfur dioxide in the first IR cell. A small amount
of carbon monoxide is converted to carbon dioxide in the
catalytic heater assembly; SO2 is converted to SO3, while sulfur
trioxide is removed from the system in a cellulose filter. Carbon
is measured as carbon dioxide in the IR cell as gases flow
through the IR cells.
The optional automatic autocleaner is ideal for high volume
applications and reduces operator time. The autocleaner
brushes the filter screen and combustion tube at intervals
specified in System Configuration.
Theory of Operation
CS-200
73
74
CS-200
Theory of Operation
Theory of Operation
CS-200
75
BAROM
PRESSURE
TRANSDUCER
BAROM
CTRL
VALVE
PT
OVEN
FM
EXHAUST
FLOW
CONTROLLER
TRANSDUCER &
REGULATOR
ASSEMBLY
MEASURE
FLOW
ROTAMETER
SO3
TRAP
CELLULOSE
FILTER
SV3
CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE
PS
RESTRICTOR
PRESSURE
SWITCH
WIRE MESH
FILTER
PS
O2 IN
40 PSI
LECOSORB/ANH
PARTICLE
FILTER
SO2
IR
CELL
CO 2
IR CELL
SV1
SV2
QUARTZ
WOOL
C
NO
ANH
PRESSURE
REGULATOR
NC
SV9
INCOMING
PRESSURE
GUAGE
RESTRICTOR
EXH
SV5
PS
PRESSURE
SWITCH
SV11
NC
NO
4 PSI
PRESSURE
SWITCH
PS
SV12
NC
NO
PS
25 PSI
PS
SV7
PNEUMATIC
PRESSURE
40 PSI
4 PSI
DOWN
SV10
NC
PARTICLE
FILTER
UP
NO
SAFETY
PRESSURE
REGULATOR
Figure 71
Gas Flow Diagram
76
CS-200
Theory of Operation
BAROM
PRESSURE
TRANSDUCER
BAROM
CTRL
VALVE
PT
OVEN
FM
EXHAUST
FLOW
CONTROLLER
TRANSDUCER &
REGULATOR
ASSEMBLY
SO2
IR
CELL
CO 2
IR CELL
MEASURE
FLOW
ROTAMETER
SO3
TRAP
CELLULOSE
FILTER
CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE
PS
SV3
MEASURE FLOW
QUARTZ
WOOL
PRESSURE
SWITCH
RESTRICTOR
ANH
PS
O2 IN
40 PSI
LECOSORB/ANH
PARTICLE
FILTER
PRESSURE
REGULATOR
SV1
SV9
PS
PRESSURE
SWITCH
SV5
DOWN
RESTRICTOR
SV10
NC
NO
UP
NO
FURNACE NC
BYPASS FLOW
SV11
NC
NO
DOOR SOL.
(OPTIONAL)
4 PSI
PRESSURE
SWITCH
PS
SV12
NC
AUTO CLEANER
(OPTIONAL)
NO
PS
25 PSI
PS
4 PSI
SV7
PNEUMATIC
PRESSURE
40 PSI
DUST
EJECT
PINCH VALVE
PARTICLE
FILTER
SAFETY
PRESSURE
REGULATOR
NC
SV6
NO
Figure 72
Gas Flow with Autocleaner Diagram
Theory of Operation
CS-200
77
SV2
Comparator Level
Note
78
CS-200
Theory of Operation
START OF
ANALYSIS
COMPARATOR
LEVELEND OF ANALYSIS
DETECTOR OUTPUT
COLLECTED
START OF
ANALYSIS
COMPARATOR
LEVELEND OF ANALYSIS
DETECTOR OUTPUT
COLLECTED
2.
3.
Theory of Operation
CS-200
79
DETECTOR
OUTPUT
COLLECTED
SIGNIFICANT
DETECTOR
OUTPUT
EXCLUDED
COMPARATOR LEVEL
(SET TOO LOW)
INSIGNIFICANT
DETECTOR
OUTPUT
DETECTOR
OUTPUT
COLLECTED
710
CS-200
Theory of Operation
Diagnostics
Windows
Keypad
Keypad
8 Diagnostics
Diagnostics........................................................................84
Ambient Monitor.................................................................85
Ambient Monitor Definitions ............................................ 87
Switch States.....................................................................88
Valve States ......................................................................89
Leak Check...................................................................... 810
Definitions .................................................................. 811
Print Buffer...................................................................... 812
Plot Buffer ....................................................................... 813
System Print.................................................................... 815
Reset Memory.................................................................. 816
Windows
Diagnostics
CS-200
81
82
CS-200
Electronic Adjustments
Diagnostics
CS-200
83
Diagnostics
This procedure permits the operator to view and print the
ambient monitor, view the digital input switch states, view and
change the solenoid valve states, and perform system leak
checks.
Note
84
Ambient Monitor
Switches
Valves
Leak Check
Print Buffer
Plot Buffer
CS-200
Electronic Adjustments
Ambient Monitor
Notes
If the determinator has just been turned on, wait one to two
hours for the system to stabilize.
1.
From the main menu, press [5] Diagnostics then press [1]
Ambient Monitor to display the ambient monitor.
Ambient Monitor
Carbon IR Cell
Sulfur IR Cell
Oven Temp
Catalyst Heater
System Pressure
Plate Current
Grid Current
2.
8.500 V
8.500 V
48oC
350oC
725 mm
480 mA
100 mA
Parameter
Nominal Value
Range
Units
Carbon IR Cell
8.5
7.5 to 9.2
Sulfur IR Cell
8.5
7.5 to 9.2
Oven Temp
48
46 to 50
Catalyst Heater
350
325 to 375
System Pressure
750
Elevation Dependent
Plate Current*
460
420 to 500
mA
Grid Current*
100
80 to 120
mA
V
C
C
mmHg
*Nominal values during analysis only. When furnace power is off, the
plate and grid current should be zero.
Diagnostics
CS-200
85
3.
4.
86
5.
6.
7.
CS-200
Electronic Adjustments
Diagnostics
CS-200
87
Switch States
Notes
1.
2.
88
State
Closed
Open
Closed
Closed
Open
Open
Closed
Closed
Open
CS-200
Electronic Adjustments
Valve States
Notes
1.
Diagnostics
State
> Off
Off
Off
Off
Off
Off
Off
Off
Off
2.
3.
4.
5.
6.
7.
CS-200
89
Leak Check
Note
1.
Note
810
2.
From the leak check menu, select one of the two choices:
A.
B.
CS-200
Electronic Adjustments
Notes
3.
Definitions
System PressureThe operating pressure of the system before
it is pressurized. The system pressure will not change as the
system is being pressurized.
Initial PressureThe system pressure at the start of system
pressurization. Normally, initial pressure is the same value as
system pressure.
Current PressureThe system pressure at the current time.
The current pressure changes rapidly as the system is being
pressurized.
Change PressureThe difference between the initial pressure
and the current pressure. A negative number indicates an
increase in system pressure. A positive number indicates a
decrease in system pressure.
TimeThe length of time, in seconds, that the test has been
running. Normally, after 60 seconds the test is complete.
Diagnostics
CS-200
811
Print Buffer
From the diagnostics menu, choose [5] Print Buffer to receive a
printout from the system printer of the buffer contents from the
last carbon analysis and then return to the diagnostics menu.
812
CS-200
Electronic Adjustments
Plot Buffer
Notes
The area between the base line and plotted curve is the
integrated concentration of sample gas as it passes through
the IR cell.
1.
Diagnostics
X-axis
Start
End
0
48
Y-axis
Start
End
0
6000
2.
3.
4.
5.
CS-200
813
6.
[1] Print
7.
814
CS-200
Electronic Adjustments
System Print
Notes
Diagnostics
1.
2.
CS-200
815
Reset Memory
Notes
816
1.
2.
3.
CS-200
Electronic Adjustments
Keypad
Windows
Keypad
Diagnostics........................................................................84
Ambient Monitor.................................................................85
Ambient Monitor Definitions ............................................ 87
Switch States.....................................................................88
Valve States ......................................................................89
Leak Check...................................................................... 810
Definitions .................................................................. 811
Print Buffer...................................................................... 812
Plot Buffer ....................................................................... 813
System Print.................................................................... 815
Reset Memory.................................................................. 816
Windows
Diagnostics
CS-200
817
818
CS-200
Electronic Adjustments
Leak Check
This procedure automatically check the measurement system of
the instrument for a gas leak. The entire system can be
checked or the operator can by-pass the furnace to isolate the
leak.
During a system leak check the system is pressured to 500 mm
Hg above current system pressure and sealed. It is then
permitted to equilibrate. For the next 60 seconds the system
pressure is measured. If the pressure remains within 5 mm Hg
of the pressurized value the system passes the leak check (for
system check only). If the pressure changes more than 5 mm
Hg of the pressurized value the leak check fails.
In the Leak Check Progress box the status of the leak check is
displayed. If a leak check fails it may be caused by gas leaking
into or out of the system.
If Change in Pressure has increased the incoming valve SV6
may be malfunctioning or the catalyst heater tubes are not at a
steady temperature. If Change in Pressure has decreased gas
is leaking out of the system.
If a leak is present, "Leak Check Failed" appears next to Leak
Check Status. If there isn't a leak " Leak Check Passed"
appears. If the system fails a leak check and a leak is detected,
perform a by-pass the furnace leak check to isolate the leak.
Before a leak check is performed the instrument should warm
up for at least for 30 minutes and the catalyst heater tubes
must be at a steady temperature. It is recommended that a
leak check be performed after autocleaner maintenance,
furnace maintenance or anytime a reagent tube is removed or
replaced.
Diagnostics
CS-200
819
Leak Check
820
1.
2.
3.
4.
5.
CS-200
Electronic Adjustments
Diagnostics
CS-200
821
Ambient Monitor
This procedure permits the operator to view and print the
ambient monitor parameter values.
Refer to Ambient Monitor Definitions, on page 824, for
Ambient Monitor Definitions.
822
CS-200
Electronic Adjustments
Ambients
Diagnostics
1.
2.
3.
4.
5.
CS-200
823
824
CS-200
Electronic Adjustments
Note
This symbol
will appear next to the parameter name, on
the ambient monitor screen, if the parameter value is out of
minimum or maximum range.
Parameter
Nominal Value
Range
Units
Oven Temp
48
46 to 50
System Pressure
750
Elevation Dependent
Catalyst Heater
350
325 to 375
Plate Current*
460
420 to 500
mA
Grid Current*
100
80 to 120
mA
Carbon IR Cell
8.5
7.5 to 9.2
Sulfur IR Cell
8.5
7.5 to 9.2
mmHg
o
* The values shown for these parameters are typical values during an analysis.
Diagnostics
CS-200
825
Switches
Switches are used throughout the instrument as sensors to
determine the status of a condition. Theyre not only used to
control the instrument, they're used for safety to prevent the
instrument from damage and the operator from harm.
The Switch screen is a diagnostic status screen. None of the
switch states can be changed from this screen. View the screen
to determine the switch status. Refer to Switch Conditions to
determine the meaning of each condition.
826
1.
2.
CS-200
Electronic Adjustments
Solenoids
The Solenoids screen permits the service technician or operator
to toggle the solenoid valves either on or off. It is also used to
test operation of the Batch Loader (autoloader).
By using the valve state drop down box the service technician
or operator can determine which valves should be turned per
valve state. To determine what each valve may affect refer to
the Flow Diagram Figure 105, on page 1017.
After this procedure is closed the solenoid valve states will
automatically be set to their default states.
Diagnostics
1.
2.
3.
CS-200
827
Comport
Comport is a diagnostic utility that can be used by the service
technician, operator and software engineer to troubleshoot the
instrument. In some cases it may be of advantage to the
service person and LECO to analyze the data collected by this
utility for diagnostic and trouble shooting purposes. Comport
must be used with direction from a LECO engineer.
Note
828
1.
2.
Click the Pause Check Box to stop the data scrolling in the
communications data window.
3.
4.
CS-200
Electronic Adjustments
Electronic Adjustments
9 Electronic Adjustments
Illustrations .......................................................................92
Barometric (PID) Pressure Regulator Adjustment ....................93
Catalyst Heater Control Card................................................96
Induction Power Control Card ...............................................98
Oven Heater Control Card.................................................. 911
IR Cell ............................................................................ 912
Electronic Adjustments
CS-200
91
Illustrations
Figure 91......... Barometric (PID) Pressure Regulator Card ..... 95
Figure 92......... Catalyst Heater Control Card ....................... 97
Figure 93......... Induction Power Control Card ...................... 910
Figure 94......... Oven Heater Control Card ........................... 911
Figure 95......... IR Cell Adjustment Location ........................ 913
92
CS-200
Electronic Adjustments
Notes
1.
2.
B.
R27Set to 9.
B.
R28Set to 2.
C.
R29Set to 5.
3.
4.
5.
From the main menu, press [4] Setup and then [6] Set
Barometer. Set the barometric pressure to the current
value at the location of the determinator.
Electronic Adjustments
CS-200
93
6.
94
From the main menu, press [1] Analyze and then Menu to
display the analysis menu.
CS-200
Electronic Adjustments
7.
8.
From the main menu, press [5] Diagnostics and then [1]
Ambient Monitor. Monitor the system pressure.
9.
B.
R1
R2
J038A
CR3
CR4
C11
C17
R26
J038B
C14
TP4
R27
5
J3
1
R30
C13
C12
J2
1
TP5
D
J2
R30
R27
10
C15
C18
R29
R28
J4
1
10
J038C
C16
U4
J1
U3
10
C20
C19
TP3
R25
C5
C21
R12
R14
R13
R15
R16
C8
R11
TP2
R7
C6
R23
C10
J1
C9
C7
C3
R6
R10
Q4
R8
R9
U1
C4
C2
Q2 Q3 TP1
R17
R18
R19
R20
R21
R22
Q1
R3
R4
R5
C1
COPYRIGHT C 1993
ALL RIGHTS RESERVED
LECO CORPORATION
ST, JOSEPH, MI U.S.A.
LED1 J038
CR1
R24
Q2
J3
R28
R29
Figure 91
Barometric (PID) Pressure Regulator Card
Electronic Adjustments
CS-200
95
WARNING
Notes
Note
96
1.
2.
3.
4.
5.
6.
7.
CS-200
Electronic Adjustments
8.
9.
C3
C2
U1
CR1
C4
C9
C7
R11
R10
R8
R7
R6
C5
R5
U2
C10
R9
R4
R3
C8
R2
C6
J078A
+ C1
R1
J078A
COPYRIGHT C 1993
ALL RIGHTS RESERVED
LEC O CORPORATION
ST. JOSEPH, MI U.S.A.
J078
U4
R13
U4
Figure 92
Catalyst Heater Control Card
Electronic Adjustments
CS-200
R16
C13
R15
R14
C12
TB1
U3
R13
R12
C11
R16
97
Note
1.
2.
3.
Turn off the service switch and verify that the plate and
grid currents go to zero.
4.
5.
6.
7.
Note
98
CS-200
Electronic Adjustments
8.
Note
9.
Note
A.
B.
C.
11. Adjust the overload control, R32, down until the furnace
power trips. Be sure the power has actually tripped and
that the power has not merely turned off because the
analysis has ended. Verification can be accomplished by
observing that LED1 is lighted.
12. Turn the overload control back approximately 11/2 turns to
ensure that the furnace will go into overload just above
the full-scale current setting of 500mA.
13. Reset the overload by turning the power level control to
reset and then back to max. Now the furnace should not
go into overload when the power level control is returned
to max.
Electronic Adjustments
CS-200
99
TP1 TP2
TP3
TP4
C1
J112A
C11
C10
R12
R18
R1 6
R17
R28
Q10
R25
R27
R29
LED1
R32
R33
SCR1
R39
R40
COPYRIGHT C 1995
ALL RIGHTS RESERVED
LECO CORPORATION
ST. JOSEPH, MI U.S.A
C22
C23
J112B
R32
R26
C16
R20
R2 2
R21
C19
C21
J1
LED1
U3
C18
Q8
R38
C20
R35
R34
R37
R36
C17
R29
Q6
Q9
CR 3
Q11
R31
R30
C14
U2
R24
C15
R23
R19
Q7
R13
C13
R15
C12
Q5
J1
Q3
CR2
Q2
R14
R11
J112
R10
C9
Q4
C6
C7
C8
Q1
C4 C5
U1
R6
R7
R8
R9
BR1
R1
R4
R3
R5
CR1
R2
C2
C3
J112C
Figure 93
Induction Power Control Card
910
CS-200
Electronic Adjustments
2.
3.
4.
5.
6.
7.
U5
CS-200
C5
J224
C7
C6
C4
R12
TEMP
TP3
R4
R5
R9
U3
U1
U2
R1
C2
C3
U4
R3
Figure 94
Oven Heater Control Card
Electronic Adjustments
C1R8
R7
R6
J224C
J224B
J224A
R2
R14
COPYRIGHT C 1997
ALL RIGHTS RESERVED
LECO CORPORATION
ST, JOSEPH, MI U.S.A.
K1
R14
TEST
TP1
TP1
TP2
CR1
TP2
GND
1.
R10
R11
Notes
TP3
911
IR Cell
Notes
1.
Note
Notes
2.
3.
4.
5.
Note
912
CS-200
Electronic Adjustments
6.
Note
7.
CO2 IR CELL
R3
GAIN
J-152
CONNECTOR
R24
ZERO
ADJUST
R3
GAIN
R24
ZERO
ADJUST
OVEN HEATER
CONTROL CARD
J-152A
CONNECTOR
SO 2 IR CELL
Figure 95
IR Cell Adjustment Location
Electronic Adjustments
CS-200
913
10
Service
10 Service
Service
CS-200
101
Illustrations
Figure 101 ....... Combustion Pressure Adjustment Knob ......... 104
Figure 102 ....... Flow Controller Location.............................. 105
Figure 103 ....... Piston Pressure Regulator ........................... 107
Figure 104 ....... Crucible Alignment..................................... 1011
Figure 105 ....... Gas Flow Diagram...................................... 1017
Figure 106 ....... Gas Flow with Autocleaner Diagram.............. 1018
Figure 107 ....... Leak Check Flow Diagram ........................... 1019
Figure 108 ....... Leak Check Flow with Autocleaner Diagram ... 1020
Figure 109 ....... Analyze Sequence Diagram ......................... 1021
Figure 10-10...... EPROM Location......................................... 1028
102
CS-200
Service
Note
1.
Keypad
Windows
Service
2.
3.
CS-200
103
ADJUSTMENT
KNOB
PRESSURE
REGULATOR
Figure 101
Combustion Pressure Adjustment Knob
104
CS-200
Service
2.
3.
From the main menu, press [1] Analyze to turn the gas on
and then [4] System Controls.
4.
5.
FLOW CONTROL
ASSEMBLY
ACCESS HOLE
602-454
REGULATOR
FLOW CONTROL
ASSEMBLY
666-224-110
OVEN HEATER
CARD
782-067-110
SO2 IR-CELL
778-574-120
CO2 IR CELL
Figure 102
Flow Controller Location
Service
CS-200
105
WARNING
Notes
1.
2.
Remove the left side panel and locate the piston pressure
regulator. Refer to Figure 11-1, page 11-3.
3.
106
2)
3)
4)
5)
CS-200
Service
B.
2)
3)
4)
5)
!
CAUTION
FIRE HAZARD
Oxygen increases the flammability of materials.
Always use caution when adjusting or operating
units using oxygen supplies. LECO recommends
routine leak check procedures to reduce the
possibility of fire hazards.
620-611 W/AC
620-120 WO/AC
MANIFOLD
ASSEMBLY
SAFETY
PRESSURE
REGULATOR
KNOB
Figure 103
Piston Pressure Regulator
Service
CS-200
107
Note
WARNING
WARNING
1.
2.
3.
WARNING
108
CS-200
Service
B.
C.
D.
E.
WARNING
WARNING
F.
!
CAUTION
Service
CS-200
109
1)
2)
3)
1010
a)
b)
c)
b)
c)
d)
e)
f)
G.
H.
I.
4.
5.
CS-200
Service
528-018
CRUCIBLE
605-814
PEDESTAL
ADAPTER
ASSEMBLY
INDUCTION
COIL
EMPTY
CRUCIBLE
605-816
PEDESTAL
LOWER SEAL
ASSEMBLY
METAL
SCREEN
FRONT
COVER
Figure 104
Crucible Alignment
Service
CS-200
1011
Gas Flows
Analysis
Analyze Valve StateIn this valve state, oxygen flows through
both the furnace and the determinator system.
When the gas is turned on, oxygen, regulated at 35 psi at its
source, enters the determinator through the O2 inlet port on the
cabinet back panel. Oxygen flow is then filtered through a 6
inch bubble tube (located on the front of the furnace)
containing Lecosorb and anhydrone. Carbon dioxide is removed
from the oxygen flow using Lecosorb reagent and moisture is
removed in the anhydrone reagent. Oxygen, with all impurities
removed, serves as the carrier gas in the system.
After all impurities have been removed from the carrier gas, the
flow is divided into two paths; one path, the lance flow, is
directed through solenoid valve 3 and into the top of the
combustion tube. During an analysis, lance flow is held
constant and is directed into the sample to assist carbonbearing components to convert into CO or CO2. The second
path is directed through solenoid valve 5 into the bottom of the
combustion tube; this flow rate varies (2 to 3 lpm) in
accordance with each valve state.
The carrier gas flows from the combustion tube sweeping
released gases from the combustion tube through a screen
filter, then through a 4 inch filter tube containing anhydrone to
remove water. The carrier gas, regulated by a flow controller in
the oven, flows through the catalyst heater. A small percentage
of the carbon is present as carbon monoxide, which is
converted to carbon dioxide as the gas flows through the
platinized silica gel in the heater. Sulfur trioxide is removed in a
cellulose trap. Gas then flows through the cellulose trap, CO2 IR
cell and solenoid valve 15. It is then exhausted out the back of
the unit.
Furnace Open 1 Valve StateIn this valve state, the
combustion tube is depressurized so that residual dust can be
ejected.
Lance flow remains the same as in the analyze valve state, but
the measure flow is bypassed through both solenoid valve 9
and solenoid valve 2. Flow through solenoid valve 9 is briefly
purged through the combustion chamber while flow from
solenoid valve 2 passes through the cellulose trap and IR cell as
previously described for the measure flow. Pneumatic gas flows
through the safety pressure regulator. With solenoid valve 9
open, the lance and purge flow (through solenoid valve 9)
ejects residual dust from the combustion tube.
1012
CS-200
Service
Service
CS-200
1013
1014
CS-200
Service
Autocleaner
After a programmed number of analyses, the furnace must be
cleaned, either manually or automatically, to prevent excessive
residue buildup. The following procedure generally describes
both manual and automatic cleaning cycle flows; however, in
system controls, several autoclean options can be selected.
Refer to the System Controls procedure on page 516 and
System Configuration on page 459, for details.
In each of the three clean valve states, oxygen flow is bypassed
through the IR cell, the piston is down, and the door is closed.
Differences in these valve states include vacuum cleaner on or
off and brush up or down.
A clean cycle is begun by pressing [5] Clean from the analyze
menu. If the cup is up, the combustion tube is depressurized
(Furnace Open 1 Valve State) and the lance pressure switch
opens. If the piston switch is down, Clean 1 Valve State is
signaled and the furnace door closes.
If an autocleaner has been installed, the vacuum turns on, the
brush moves down (Clean 2 Valve State) and up (Clean 1 Valve
State), and then the cycle repeats 2 times. If manually
cleaning, the vacuum switch shuts off automatically (Clean 3
Valve State) and the vacuum switch is pressed manually to
begin cleaning. After cleaning the filter and combustion tube,
the vacuum switch is shut off manually. Then [5] Clean is
pressed and the furnace door opens (Furnace Open 3 Valve
State).
The cycle is completed when atmospheric gases are purged
from the system (gas flows for each valve state have been
previously discussed). After cleaning, the vacuum is shut off
(Furnace Open 3 Valve State), the clean switch is pressed, and
the cup moves up under low pressure (Furnace Closed 1 Valve
State). The cup then goes to high pressure, sealing the piston
against the o-ring. Atmospheric gases are purged from the
combustion tube (Furnace Closed 2 Valve State) and after a
purge delay, the combustion tube is pressurized. Finally, after a
two second delay, oxygen flows through both the furnace and
determinator (Post Analyze Valve State).
Service
CS-200
1015
Oxygen Solenoid
Bypass Solenoid
Lance Solenoid
Safety Solenoid
Doser Solenoid
Purge Solenoid
Piston Solenoid
Door Solenoid
Brush Solenoid
SV
1
SV
2
SV
3
SV
4
SV
5
SV
6
SV
7
SV
8
SV
9
SV
10
SV
11
SV
12
SV
13
SV
14
SV
15
SV
16
Gas Off
00
Standby
Analyze
Furnace Open 1
Furnace Open 2
Furnace Open 3
Furnace Closed 1
Furnace Closed 2
Furnace Closed 3
Post Analyze
Leak Check 1
Leak Check 2
Leak Check 3
Leak Check 4
Barometric
Clean 1
Clean 2
Clean 3
CS-200
Valve State
Notes
1016
CS-200
Service
BAROM
PRESSURE
TRANSDUCER
BAROM
CTRL
VALVE
PT
OVEN
FM
EXHAUST
FLOW
CONTROLLER
TRANSDUCER &
REGULATOR
ASSEMBLY
MEASURE
FLOW
ROTAMETER
SO3
TRAP
CELLULOSE
FILTER
SV3
CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE
PS
RESTRICTOR
PRESSURE
SWITCH
WIRE MESH
FILTER
PS
O2 IN
40 PSI
LECOSORB/ANH
PARTICLE
FILTER
SO2
IR
CELL
CO 2
IR CELL
SV1
SV2
QUARTZ
WOOL
C
NO
ANH
PRESSURE
REGULATOR
NC
SV9
INCOMING
PRESSURE
GUAGE
RESTRICTOR
EXH
SV5
PS
PRESSURE
SWITCH
SV11
NC
NO
4 PSI
PRESSURE
SWITCH
PS
SV12
NC
NO
PS
25 PSI
PS
SV7
PNEUMATIC
PRESSURE
40 PSI
4 PSI
DOWN
SV10
NC
PARTICLE
FILTER
UP
NO
SAFETY
PRESSURE
REGULATOR
Figure 105
Gas Flow Diagram
Service
CS-200
1017
BAROM
PRESSURE
TRANSDUCER
BAROM
CTRL
VALVE
PT
OVEN
FM
EXHAUST
FLOW
CONTROLLER
TRANSDUCER &
REGULATOR
ASSEMBLY
SO2
IR
CELL
CO 2
IR CELL
MEASURE
FLOW
ROTAMETER
SO3
TRAP
CELLULOSE
FILTER
CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE
PS
SV3
MEASURE FLOW
QUARTZ
WOOL
PRESSURE
SWITCH
RESTRICTOR
ANH
PS
O2 IN
40 PSI
LECOSORB/ANH
PARTICLE
FILTER
PRESSURE
REGULATOR
SV1
SV9
PS
PRESSURE
SWITCH
SV5
DOWN
RESTRICTOR
SV10
NC
NO
UP
NO
FURNACE NC
BYPASS FLOW
SV11
NC
NO
DOOR SOL.
(OPTIONAL)
4 PSI
PRESSURE
SWITCH
PS
SV12
NC
AUTO CLEANER
(OPTIONAL)
NO
PS
25 PSI
PS
4 PSI
SV7
PNEUMATIC
PRESSURE
40 PSI
DUST
EJECT
PINCH VALVE
PARTICLE
FILTER
SAFETY
PRESSURE
REGULATOR
NC
SV6
NO
Figure 106
Gas Flow with Autocleaner Diagram
1018
CS-200
Service
SV2
BAROM
PRESSURE
TRANSDUCER
BAROM
CTRL
VALVE
PT
OVEN
FM
EXHAUST
FLOW
CONTROLLER
TRANSDUCER &
REGULATOR
ASSEMBLY
MEASURE
FLOW
ROTAMETER
SO3
TRAP
CELLULOSE
FILTER
SV3
PRESSURE
SWITCH
CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE
PS
RESTRICTOR
WIRE MESH
FILTER
PS
O2 IN
40 PSI
LECOSORB/ANH
PARTICLE
FILTER
SO2
IR
CELL
CO2
IR CELL
SV1
SV2
QUARTZ
WOOL
C
NO
ANH
PRESSURE
REGULATOR
NC
SV9
INCOMING
PRESSURE
GUAGE
RESTRICTOR
EXH
SV5
PS
PRESSURE
SWITCH
SV11
NC
NO
4 PSI
PRESSURE
SWITCH
PS
SV12
NC
NO
PS
25 PSI
PS
SV7
PNEUMATIC
PRESSURE
40 PSI
4 PSI
DOWN
SV10
NC
PARTICLE
FILTER
UP
NO
SAFETY
PRESSURE
REGULATOR
Figure 107
Leak Check Flow Diagram
Service
CS-200
1019
BAROM
PRESSURE
TRANSDUCER
BAROM
CTRL
VALVE
PT
OVEN
FM
EXHAUST
FLOW
CONTROLLER
TRANSDUCER &
REGULATOR
ASSEMBLY
SO2
IR
CELL
CO 2
IR CELL
MEASURE
FLOW
ROTAMETER
SO3
TRAP
CELLULOSE
FILTER
CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE
PS
SV3
MEASURE FLOW
QUARTZ
WOOL
PRESSURE
SWITCH
RESTRICTOR
ANH
PS
O2 IN
40 PSI
LECOSORB/ANH
PARTICLE
FILTER
PRESSURE
REGULATOR
SV1
SV9
PS
PRESSURE
SWITCH
SV5
RESTRICTOR
DOWN
SV10
NC
NO
UP
FURNACE
NC
NO
SV2
BYPASS FLOW
SV11
NC
NO
DOOR SOL.
(OPTIONAL)
4 PSI
PRESSURE
SWITCH
PS
SV12
NC
AUTO CLEANER
(OPTIONAL)
NO
PS
25 PSI
DUST
EJECT
PS
4 PSI
SV7
PNEUMATIC
PRESSURE
40 PSI
PINCH VALVE
PARTICLE
FILTER
SAFETY
PRESSURE
REGULATOR
NC
SV6
NO
Figure 108
Leak Check Flow with Autocleaner Diagram
1020
CS-200
Service
Figure 109
Analyze Sequence Diagram
Service
CS-200
1021
YES
FURNACE OPEN
3 VALVE STATE
YES
DELAY
1 SECOND
YES
LANCE
PRESSURE
SWITCH
OPEN
?
YES
FURNACE OPEN
1 VALVE STATE
YES
PISTON
CONTROL
YES
ANALYZE
V5
YES
PNEUMATIC
PRESSURE
+ 25 PSI
YES
O2
PRESSURE
+ 25 PSI
TURN
GAS ON
NO PNEUMATIC
PRESSURE
DUST CLOG IN
FLOW SYSTEM
YES
HAVE
2 SECONDS
ELAPSED
?
NO
NO
MEASURED FLOW
BY-PASSES FURNACE.
TUBE DEPRESSURIZED.
SOME DUST PURGED
THRU PINCH VALVE.
O2 FLOW THRU
FURNACE AND
ANALYTICAL SYSTEM
NO
YES
PRE-ANALYZE
PURGE DELAY
FURNACE
CLOSED 2
VALVE STATE
YES
YES
YES
PISTON
UP LIMIT
SWITCH
FURNACE
CLOSED 1
VALVE STATE
YES
YES
PISTON
CONTROL
YES
LOAD CRUCIBLE
AND SAMPLE
YES
NO
PISTON
NO
DOWN LIMIT
SWITCH
EDITABLE THRU
ANALYSIS METHOD
CUP CHANGES TO
HIGH PRESSURE.
PURGE ATMOSPHERIC
GASES OUT OF
COMBUSTION TUBE.
NO PISTON
UP LIMIT SWITCH
YES
HAVE
5 SECONDS
ELAPSED
?
NO
CUP MOVES UP
UNDER LOW PRESSURE
NO PISTON
DOWN LIMIT SWITCH
YES
HAVE
3 SECONDS
ELAPSED
?
NO
YES
TAKE
IR ZEROS
YES
750mV
< IR <
9500mV
RANGE
CHECK
COMBUSTION
PRESSURE
575L=PRESS
=625
YES
YES
PRE-ANALYZE
DELAY
LANCE
PRESSURE
SWITCH
CLOSED
?
YES
YES
ANALYZE
VALVE STATE
HAS SAMPLE
WEIGHT BEEN
ENTERED
?
YES
YES
DELAY
2 SECONDS
FURNACE
CLOSED 3
VALVE STATE
YES
ENTER
WEIGHT
O2 FLOW
THRU FURNACE
AND ANALYTICAL
SYSTEM
NO COMBUSTION
TUBE PRESSURE
NO
IR CELL
OUT OF RANGE
WARNING
COMBUSTION
PRESSURE
NO
EDITABLE THRU
ANALYSIS METHOD
ALL ATMOSPHERIC GASES
PURGED FROM SYSTEM.
WAITING FOR GOOD
STABLE IR BASELINE.
NO
NO
COMBUSTION TUBE
IS PURGED AND
PRESSURIZED
NO
DISPLAY
CARBON
ANSWER
YES
YES
SAVE AND
PRINT
ANSWERS
MINIMUM
SULFUR
TIME
?
YES
POST ANALYZE
VALVE STATE
NO
NO
LANCE FLOW
IS OFF
LOW PLATE
CURRENT
OR
LOW GRID
CURRENT
DISPLAY
SULFUR
ANSWER
YES
SULFUR
COMPARATOR
LEVEL
?
YES
YES
FURNACE
OFF
NO
MONITOR
GRID & PLATE
CURRENT
CARBON
COMPARATOR
LEVEL
?
YES
MINIMUM
CARBON
TIME
?
YES
MONITOR GRID
AND
PLATE CURRENT
YES
LIVE ANSWER
DISPLAY
YES
FURNACE
ON
YES
START
INTEGRATION
Cause
Probable Solution
Data transmit
option is disabled.
No Results Available
No results are
stored in result list.
Run analysis
to obtain results.
No Results Selected
No results selected
from the result list.
No Weights Entered
No weights have
been entered into
the weight stack.
Password Mismatch
The incorrect
password was entered.
Enter the
correct password.
Reset Memory
Sample Weight
Out Of Range
Enter correct
sample weight.
1022
CS-200
Service
Warnings
Message
Cause
Probable Solution
Combustion Pressure
Pressure outside of
575mm to 625mm range.
Perform a combustion
pressure adjustment.
Service
CS-200
1023
Errors
Message
Cause
Probable Solution
Balance port
will not initialize.
Hardware problem.
Contact the LECO
service department.
Data Transmit
[Port Disabled,
Buffer Is Full,
Buffer Is Empty,
String Is Too Long,
Not Enough Room]
Hardware problem.
Contact the LECO
service department.
IR cell voltage
exceeds range limits.
Combustion system
cannot pressurize.
Gross leak in
combustion system.
Check furnace o-rings
and outer combustion
tube for possible cracks.
No Combustion
Tube Pressure
1024
CS-200
Service
Message
Cause
Probable Solution
No Oxygen Pressure
Check pneumatic
pressure. Check to see if
crucible is jammed.
No Pneumatic Pressure
Pneumatic pressure is
turned off or gas bottle is
empty.
Hardware problem.
Contact the LECO
service department.
Pneumatic supply
is turned off.
Possible gross
leak in system.
Unable To Pressurize
Service
CS-200
1025
Software Upgrade
A major portion of the determinator's functions are defined and
controlled by a software program that may be updated. Most
updates do not affect the physical design of the determinator,
but can improve performance and make operation easier.
Therefore, an identification system for program changes called
'Program Version' is used in the CS-200 Carbon and Sulfur
Determinator and other LECO instruments.
A three-digit number identifies program version levels. The first
generation of a program is version '1.00'. Each time a program
is changed, the version number is increased.
Keypad
Note
1.
WARNING
1026
CS-200
Service
2.
WARNING
Note
Service
3.
Locate the program EPROMs IC3 and IC4. With a small flat
tip screwdriver, pry the old EPROMs from their sockets.
Discard the EPROMs.
4.
5.
6.
7.
8.
9.
CS-200
1027
IC3
IC4
C1
C2
R7
U1
U9
C123
U10
C46
PD1A
PD2A
C54
IC4
PD2
IC3
J1
U30
C6
PD4
PD1 C5
R42
U14
U13
CR3
C49
CR1
+
C110
C109
C122
CR2 + U31
C121
U29
C25 C26
C72
C108
C73
C71
C48
R13
R28
U12
U11
C44
C45
C47
U27
C68
R29
C69
U28
C107
R33
C111
C114
C7
U3
C9
PD5
C10
RN1
C30
PD8
C11
Y1
C31
U17
C58
C87
U36
COPYRIGHT C 1994-95
ALL RIGHTS RESERVED
LECO CORPORATION
ST. JOSEPH, MI U. S. A.
C56
C8
C57
U34
C85 C86
U35
R8
R9
R10
CR4 R11
R12
U33
C55
PD6
U15
U2
J859A
C27
U16
C80
U32
C113
J859K
PD9
C59
C88
C12
U4
C32
U18
U39
C60
IC39
C115
C90
C89
U19
TP1
TP2
TP3
C66
U37
U38
J859I
+
C4
C20
C21
C3
C23
C24
+
J859H
1
C67
19
C106
C13
J859B
13
U5
U45
U41
C92
U22
J859C
C16
U23
C93
R3
R2 R4
RN2
C95
C96
C97
C98
C63
C17
R1
U46
R34
U42
C117
U7
Y2 C62
C34
C35
J859H
C116
C61
C33
U6
U20
U44
U40
C91
U21
C15
19
C14
A1
B1
C1
A32
B32
C32
C118
C18
J859D
U8
R24
R25
R26
R27
U24
L1
U43
Y3
PD3
IC9
J859F
1
1
Q1
C19
R6
C103
C65
+ C43
C42
R5
U26
C101
TP5
TP6
TP7
U48
C120
SW1
+
C104
+
C105
+ C102
U25
C124
1
J859E
C64
C41
+
C99
C100
C94
PD7
U47
J859N
C119
1
1
1
R19
R20
R21
R22
R23
CPU BOARD
C28
R43
C29
J859G
J859J
J859L
Service
CS-200
1028
C76
C36
C37
C38
C39
C40
R35
R36
R37
R38
R39
R40
R41
C78
C79
C82
C83
C84
C74
C75
C51
C52
C53
C77
C81
C112
R14
R15
R32 R30
R16
C70
R31
C22
Figure 10-10
EPROM Location
Windows
Service
1.
2.
3.
4.
5.
6.
7.
CS-200
1029
Keypad
Notes
1.
Note
1030
Adj Bk
1.0000
565
1125
2326
3898
6677
9612
12873
16821
19493
21776
Slope
1.0466
1.0381
1.0299
1.0534
1.0348
1.0344
1.0822
1.0921
1.1001
0 - 52000
CS-200
Service
Service
2.
3.
4.
Press the left or right arrow keys to move the cursor and
edit a digit using the keypad.
5.
6.
After all break and slope values have been entered, press
Exit to return to the setup menu. The determinator will
calculate the adjusted break value.
CS-200
1031
Windows
The Break and Slope values are not used by LECO but can
be used by the operator to customize their instrument. Click
on the table to enter a break and slope value.
1.
1032
CS-200
Service
Service
2.
Click the arrow in the Select Cell drop down box and select
the IR cell to linearize. Selections are Carbon Low Range,
Carbon High Range or Sulfur.
3.
Click on the table and enter the break and slope values. The
determinator will calculate the adjusted break value.
4.
CS-200
1033
11
Illustrations
11-1
CS-200
Illustrations
Illustrations
CS-200
11-2
620-611 W/AC
620-612 WO/AC
MANIFOLD
ASSEMBLY
666-147
CELL POWER
SUPPLY CARD
614-833
FAN
ASSEMBLY
606-466
FILTER
666-339-xxx
CPU CARD
666-004*
BRIGHT / CONTRAST
ADJUSTMENT CARD
773-383
REGULATOR
777-836*
POWER SUPPLY
LCD
777-759
OVEN
INTERFACE
CARD
604-727*
LCD DISPLAY
666-112
INDUCTION
POWER CARD
777-504
CHOPPER
MOTOR
CARD
777-899-101
16 POSITION
SOLENOID
INTERFACE
CARD
608-399
SPEAKER
ASSEMBLY
666-038
PID PRESSURE
REGULATOR
CARD
666-042
DUAL SWITCH
INTERFACE
CARD
666-078-101
CATALYST
HEATER
CONTROL
CARD
777-923
POWER
DISTRIBUTION
CARD
666-034
FILTERED
D-SHELL
775-296
ISOLATION
CARD A
608-497
RELAY
781-165
RELAY
769-370
RELAY
603-818
FAN & PLATE
ASSEMBLY
602-454
REGULATOR
FLOW CONTROL
ASSEMBLY
666-224-110
OVEN HEATER
CARD
782-067-110
SO2 IR-CELL
778-574-120
CO2 IR CELL
Figure 11-1
CS-200 Left Side View
11-3
CS-200
Illustrations
776-008
VACUUM CAPACITOR
604-001
OSCILLATOR
ASSEMBLY
781-420
LANCE AND FILTER
ASSEMBLY
( NOT ON UNITS
WITH AUTOCLEANER)
771-354
OSCILLATOR
TUBE
550-048
GRID CHOKE
775-298
ISOLATION
CARD B
616-718
FILAMENT
TRANSFORMER
616-705
POWER
SUPPLY
CHASSIS
762-066
RECTIFIER
(4) REQD
789-410
BRACKET &
RECTIFIER
ASSEMBLY
604-155
LIMIT SWITCH
(2 REQ'D)
614-465
HIGH VOLTAGE
TRANSFORMER
607-157
RELAY FURNACE
INTERLOCK
771-986
AC FILTER
779-270
SAFETY
INTERLOCK
SWITCH
770-990
VOLTAGE
SELECTION
TERMINAL
STRIP
781-165
RELAY
Figure 11-2
CS-200 Right Side View
Illustrations
CS-200
11-4
776-008
VACUUM CAPACITOR
604-001
OSCILLATOR
ASSEMBLY
609-626
AUTOCLEANER
ASSEMBLY
771-354
OSCILLATOR
TUBE
550-048
GRID CHOKE
775-298
ISOLATION
CARD B
616-718
FILAMENT
TRANSFORMER
616-705
POWER
SUPPLY
CHASSIS
762-066
RECTIFIER
(4 REQD)
789-410
BRACKET &
RECTIFIER
ASSEMBLY
604-155
LIMIT SWITCH
(2 REQ'D)
614-465
HIGH VOLTAGE
TRANSFORMER
616-893
PINCH VALVE
ASSEMBLY
607-157
RELAY FURNACE
INTERLOCK
771-986
AC FILTER
779-270
SAFETY
INTERLOCK
SWITCH
770-990
VOLTAGE
SELECTION
TERMINAL
STRIP
781-165
RELAY
Figure 11-3
CS-200 with Autocleaner Right Side View
11-5
CS-200
Illustrations
604-291
AIR CYLINDER
806-214
FITTING
(2) REQD
604-519
EXTENSION
807-261
FITTING
(2) REQD
193-143
LOCKWASHER
610-735
SLOTTED
BRUSH
807-196
TUBING
(2) REQD
604-517
RETAINER
604-516
FITTING
773-320
O-RING
(2 REQD)
789-115
LANCE TUBE
604-268
BODY
ASSEMBLY
193-164
LOCKWASHER
(2 REQD)
604-172
O-RING
604-274
SHAFT
604-163
BRUSH
762-058
O-RING
190-228
SCREW
(2 REQD)
604-159
PLUNGER
604-273
BUSHING
ADAPTOR
604-272
CAP
190-757
SCREW
(4) REQD
604-168
LOCK
MOUNT
771-991
O-RING
778-703
SPACER
(4) REQD
778-596
FILTER
190-090
THUMBSCREW
(2 REQD)
762-058
O-RING
773-926
PLATE
190-431
SCREW
(2) REQD
762-058
O-RING
773-577
PISTON RING
Figure 11-4
609-626 Autocleaner Assembly
Illustrations
CS-200
11-6
CATALYST HEATER
TUBE
781-364
CATALYST HEATER
ASSEMBLY
772-725
ENCLOSURE
772-694
KNOB
772-738
O-RING
614-316
MOVABLE
BLOCK
614-319
STATIONARY
BLOCK
190-229
SCREW
(3 REQ'D)
192-004
SCREW
(4 REQ'D)
772-737
INSULATOR
768-798
PLUG
193-008
WASHER
(6 REQ'D)
782-042
TOP
INSULATOR
772-729
CORE
INSULATOR
614-411
BLOCK
772-520
O-RING
(4 REQ'D)
190-278
SCREW
(6 REQ'D)
614-412
LOWER BLOCK
781-365
CATALYST HEATER
ELEMENT
781-366
THERMOCOUPLE
TYPE K
616-767
PANEL
762-664
CHROMAL
WIRE
772-730
BOTTOM
INSULATOR
772-736
CATALYST
HEATER
CAP
Figure 11-5
616-771 Catalyst Heater Panel
11-7
CS-200
Illustrations
610-754
SWITCH
MEMBRANE
783-741
BRACKET
614-290
CONDUCTIVE
SHIELD
783-757
SLEEVE
(4 REQUIRED)
194-105
NUT
(4 REQUIRED)
777-836
LCD POWER
CARD
614-294
GASKET
J836C
604-727
DISPLAY
J836G
604-744
STUD EXTENSION
(4 REQUIRED)
CONDUCTIVE SIDE OF
614-290 HAS TO BE
PLACED AGAINST THE
BRACKET 783-741
Figure 11-6
614-492 Display
Illustrations
CS-200
11-8
783-791
VALVE
ASSEMBLY
617-246
PRESSURE
SENSOR
537-165
ELBOW
FITTING
604-316
FITTING
761-784
FITTING
193-054
WASHER
(2-REQ'D)
190-227
SCREW
(2-REQ'D)
783-792
BRACKET
602-581
STANDOFF
(4-REQ'D)
666-038
PID PRESSURE
REGULATOR CARD ASSEMBLY
Figure 11-7
617-248 Barometric Flow Controller
11-9
CS-200
Illustrations
616-771
CATALYST
ASSEMBLY
772-458
FITTING
(2 REQ'D)
194-056
NUT
(6 REQ'D)
193-055
WASHER
(6 REQ'D)
614-414
UPPER
BLOCK
190-698
SCREW
(2 REQ'D)
783-689
BRACKET
194-056
NUT
(2 REQ'D)
789-349
BLOCK
765-976
O-RING
773-383
REGULATOR
772-520
O-RING
(3 REQ'D)
803-431
FITTING
(2 REQ'D)
614-413
LOWER
BLOCK
(2 REQ'D)
190-277
SCREW
(4 REQ'D)
193-008
WASHER
(4 REQ'D)
193-008
WASHER
(8 REQ'D)
616-891
BRACKET
194-056
NUT
(2 REQUIRED)
606-650
3 WAY
SOLENOID
VALVE
190-278
SCREW
(8 REQ'D)
772-702
FITTING TEE
(2 REQ'D)
616-768
PANEL
772-458
FITTING
(4 REQ'D)
NOTE:
616-896 ASSEMBLY IS AS SHOWN;
FOR 616-897 ASSEMBLY USE 614-931
PANEL INSTEAD OF 616-771 CATALYST
ASSEMBLY.
606-649
2 WAY
SOLENOID
VALVE
Figure 11-8
616-896 Gas Panel Assembly
Illustrations
CS-200
11-10
Figure 11-9
604-080-110 CO2 IR Cell
11-11
CS-200
Illustrations
783-040
PREAMP
COVER
193-006
WASHER
(4 REQ'D)
190-227
SCREW
(4 REQ'D)
777-818
PREAMP
CARD
783-038
HEX SPACER
(4 REQ'D)
770-838
THERMAL
RESISTOR
193-104
WASHER
190-227
SCREW
(4 REQ'D)
783-127
EXTENSION
(2 REQ'D)
781-637
FOAM PAD
783-124
COVER SEAL
783-037
MOUNT
190-866
SET SCREW
768-944
O-RING
190-766
SCREW
781-941
SOURCE
END CAP
190-295
SCREW
(4 REQ'D)
781-949
GUARD
FEEDTHRU
190-247
SCREW
(2 REQ'D)
772-560
CHOPPER MOTOR
781-943
SOURCE
PLATE
190-174
SCREW
(2 REQ'D)
781-945
LECOSORB
CYLINDER
772-561
IR SOURCE AND
REFLECTOR PLATE
190-766
SCREW
772-563
IR SOURCE
ASSEMBLY
782-063
CONE IR DETECTOR 768-974
ASSEMBLY
CHOPPER
BLADE
604-096
END DETECTOR BODY
ASSEMBLY
782-697
INNER
GASKET
193-054
WASHER
(4 REQ'D)
Figure 11-10
778-574-120 CO2 IR Cell
Illustrations
CS-200
11-12
783-040
PREAMP
COVER
193-006
WASHER
(4 REQ'D)
190-227
SCREW
(4 REQ'D)
777-818
PREAMP
CARD
783-038
SPACER
(4 REQ'D)
770-838
THERMAL
RESISTOR
193-104
WASHER
190-227
SCREW
(4 REQ'D)
783-127
EXTENSION
(2 REQD)
781-637
FOAM PAD
783-124
COVER SEAL
783-037
MOUNT
190-766
SCREW
772-563
IR SOURCE
ASSEMBLY
190-866
SET SCREW
782-063
768-974
CONE IR DETECTOR CHOPPER
ASSEMBLY
BLADE
772-809
BLOCK & WINDOWS
ASSEMBLY
782-697
INNER
GASKET
193-054
WASHER
(4 REQ'D)
190-766
SCREW
772-561
IR SOURCE AND
REFLECTOR PLATE
768-944
O-RING
781-941
SOURCE
END CAP
190-247
SCREW
(2 REQ'D)
190-295
SCREW
(4 REQ'D)
781-949
GUARD
FEEDTHRU
772-560
CHOPPER MOTOR
781-943
SOURCE
PLATE
190-174
SCREW
(2 REQ'D)
781-945
LECOSORB
CYLINDER
Figure 11-11
782-723-110 CO2 IR Cell
11-13
CS-200
Illustrations
190-247
SCREW
(2-REQ'D)
772-560
MOTOR
768-944
O-RING
190-295
SCREW
(4-REQ'D)
190-766
SCREW
190-174
SCREW
(2-REQ'D)
781-945
ASSY CYLINDER
ASCARITE
781-987
SOURCE
CAP ASSEMBLY
190-866
SCREW
190-601
SCREW
(4 REQ'D)
772-806
PLATE
(2 REQ'D)
768-974
CHOPPER MOTOR
BLADE
190-820
SCREW
(6-REQ'D)
190-766
SCREW
781-942
IR SOURCE
AND
772-561
REFLECTOR
783-038
STANDOFF
(4 REQ'D)
190-227
SCREW
(4 REQ'D)
193-104
WASHER
770-838
THERMAL
RESISTER
782-697
GASKET
781-992
CELL
BODY
ASSEMBLY
190-227
SCREW
(4 REQ'D)
781-637
FOAM PAD
777-818
PREAMP CARD
ASSEMBLY
783-040
193-006
COVER
WASHER
(4 REQ'D) ASSEMBLY
783-037
MOUNT
782-063
CONE DETECTOR
ASSEMBLY
Figure 11-12
616-706 SO2 IR Cell
Illustrations
CS-200
11-14
783-040
PREAMP
COVER
193-006
WASHER
(4 REQ'D)
190-227
SCREW
(4 REQ'D)
777-818
PREAMP
CARD
783-038
HEX SPACER
(4 REQUIRED)
770-838
THERMAL
RESISTOR
193-104
WASHER
190-227
SCREW
(4 REQ'D)
783-127
EXTENSION
(2 REQD)
781-637
FOAM PAD
783-124
COVER SEAL
783-037
MOUNT
782-065
CONE IR
DETECTOR
ASSEMBLY
190-866
SET SCREW
768-944
O-RING
190-766
SCREW
781-941
SOURCE
END CAP
190-295
SCREW
(4 REQ'D)
781-949
GUARD
FEEDTHRU
190-247
SCREW
(2 REQ'D)
772-560
CHOPPER MOTOR
781-943
SOURCE
PLATE
190-174
SCREW
(2 REQ'D)
781-945
LECOSORB
CYLINDER
772-561
IR SOURCE AND
REFLECTOR PLATE
190-766
SCREW
772-563
IR SOURCE
ASSEMBLY
768-974
CHOPPER
BLADE
781-992
END DETECTOR BODY
ASSEMBLY
782-697
INNER
GASKET
193-054
WASHER
(4 REQ'D)
Figure 11-13
782-067-110 SO2 IR Cell
11-15
CS-200
Illustrations
783-040
PREAMP
COVER
193-006
LOCKWASHER
(4 REQUIRED)
770-838
THERMAL
RESISTOR
783-038
HEX SPACER
(4 REQUIRED)
777-817
PREAMP
CARD
193-104
WASHER
190-227
SCREW
(4 REQUIRED)
783-127
EXTENSION
(2 REQUIRED)
190-227
SCREW
(4 REQUIRED)
781-637
FOAM PAD
783-124
COVER SEAL
783-037
MOUNT
782-697
INNER
GASKET
190-820
SCREW
(3 REQUIRED)
193-054
WASHER
(4 REQUIRED)
781-849-010
DETECTOR
BLOCK
12
782-056
TUBE CELL BODY
ASSEMBLY
109-601
SCREW
(4 REQUIRED)
190-866
SET SCREW
768-974
CHOPPER BLADE
190-766
SCREW
772-563
IR SOURCE
ASSEMBLY
772-806
PLATE
(2 REQUIRED)
781-990
0-RING
(3 REQUIRED)
190-820
SCREW
(3 REQUIRED)
781-991-010
SOURCE
BLOCK
777-066
TUBE BODY
772-520
0-RING
(2 REQUIRED)
775-795
SPACER
(2 REQUIRED)
772-804
GOLD PLATED
GLASS TUBE
772-557
TUBE
(2 REQUIRED)
190-766
SCREW
772-561
IR SOURCE
REFLECTOR
PLATE
768-944
O-RING
190-295
SCREW
(4 REQUIRED)
781-941
SOURCE
END CAP
781-949
GUARD
FEEDTHRU
190-247
SCREW
(2 REQUIRED)
772-560
CHOPPER MOTOR
781-943
SOURCE
PLATE
190-174
SCREW
(2 REQUIRED)
781-945
LECOSORB CYLINDER
773-311
FILTER
781-422
FILTER CAP
781-424
O-RING
762-058
O-RING
*772-704
FITTING
781-663
LANCE
GUARD
781-421
FILTER
HOUSING
*773-136
FITTING
789-118
LANCE TUBE
ASSEMBLY
771-991
O-RING
772-381
LANCE
CLEANING
ROD
781-423
ADAPTOR TUBE
BUSHING
762-058
O-RING
LANCE
TUBE
773-577
PISTON
RING
190-431
SCREW
(4) REQD
781-425
FILTER END
PLATE
190-258
SCREW
(2) REQD
762-058
O-RING
*781-401
ADAPTER
RING
NOTE: * NOT PART OF ASSEMBLY
Figure 11-14
781-420 Lance and Filter Assembly
Illustrations
CS-200
11-16
Figure 11-15
620-612 Manifold Assembly
11-17
CS-200
Illustrations
S2
Safety Pressure
Regulator
S5
Oxygen
SV1
S14
S14
Bypass
SV2
Furnace
SV6
Lance
SV3
No Hole indicates
2-way valve.
S2 and S5
Autocleaner
Door
Safety
Cylinder
SV7
604-009
COIL STRAP
604-010
HIGH VOLTAGE
STRAP
764-640
CAPACITOR
(2-REQ'D)
776-008
VACUUM
CAPACITOR
771-356
PLATE
CONNECTOR
550-047
CHOKE
ASSEMBLY
776-129
COIL
ASSEMBLY
771-354
OSCILLATOR
TUBE
566-002
COIL COLLET
(2-REQ'D)
550-187
CAPACITOR
500
100
200
200
771-487
STANDOFF
(4 REQ'D)
200
764-641
CAPACITORS
(4-REQ'D)
604-008
SUPPRESSOR
773-066
CERAMIC
STANDOFF
(5 REQ'D BUT
NOT SHOWN)
521-037
TERMINAL BLOCK
773-572
GROMMET
776-175
5K RESISTOR
(UNDER SHELF)
550-048
RF CHOKE
Figure 11-16
604-001 Oscillator
Illustrations
CS-200
11-18
616-892
BRACKET
190-246
SCREW
(2 REQ'D)
589-182
FITTING
774-612
HOUSING
774-613
O-RING
769-973
ROLL PIN
(2 REQ'D)
774-610
PISTON
772-909
PINCH VALVE
ASSEMBLY
776-093
CAP
190-246
SCREW
(2 REQ'D)
501-110
SILICONE
TUBE
Figure 11-17
616-893 Pinch Valve Assembly
11-19
CS-200
Illustrations
190-227
SCREW
(4 REQD)
777-923
ASSY CARD
900-537
STANDOFF
(4 REQD)
190-231
SCREW
(8 REQD)
190-277
SCREW
(3 REQD)
193-006
WASHER
(4 REQD)
602-407
COVER
193-008
WASHER
(11 REQD)
190-277
SCREW
(11 REQD)
193-008
WASHER
(3 REQD)
194-055
NUT
(4 REQD)
193-006
WASHER
(6 REQD)
615-728
ASSY HARNESS
190-277
SCREW
(7 REQD)
190-004
SCREW
(4 REQD)
194-055
NUT
(8 REQD)
602-439
PLATE
193-008
WASHER
(7 REQD)
609-081
ASSY HARNESS
602-410
PANEL
782-746
FILTER
604-709
GUARD
194-055
NUT
(2 REQD)
194-105
NUT
(4 REQD)
608-386
FAN
194-055
NUT
(4 REQD)
193-006
WASHER
(4 REQD)
190-239
SCREW
(4 REQD)
TB101
608-604
POWER SUPPLY
190-232
SCREW
(2 REQD)
190-424
SCREW
(2 REQD)
615-574
RECEPTACLE
190-229
SCREW
(4 REQD)
194-059
NUTS
(4 REQD)
194-105
NUT
(2 REQD)
190-277
SCREW
(22 REQD)
193-008
WASHER
(22 REQD)
194-056
NUT
(2 REQD)
193-008
WASHER
(2 REQ'D)
750-155-106
TERMINAL
BLOCK
616-707
TRANSFORMER
ASSEMBLY
750-155-100
JUMPER
616-714
BOX
778-951
CIRCUIT
BREAKER
190-381
SCREW
(4 REQD)
602-410
PLATE
602-409
BRACKET
Figure 11-18
616-715 Power Supply
Illustrations
CS-200
11-20
190-752
SCREW
(4 REQ'D)
193-108
WASHER
(4 REQ'D)
616-718
TRANSFORMER
193-008
WASHER
(3 REQ'D)
190-277
SCREW
(3 REQ'D)
802-340
INSULATOR
589-275
TERMINAL
BLOCK
190-231
SCREW
(2 REQ'D)
190-277
SCREW
(2 REQ'D)
773-666
SNUBBER
190-279
SCREW
(2 REQ'D)
190-227
SCREW
(2 REQ'D)
616-701
BRACKET
770-991
INSULATOR
190-279
SCREW
(2 REQ'D)
770-990
TERMINAL
BLOCK
193-008
WASHER
(2 REQ'D)
190-282
SCREW
(2 REQ'D)
190-479
SCREW
(2 REQ'D)
616-702
CHASSIS
781-165
RELAY
572-037
GROMMET
193-108
WASHER
(4 REQ'D)
194-059
NUT
(4 REQ'D)
771-986
FILTER
194-056
NUT
(2 REQ'D)
Figure 11-19
616-705 Power Supply Chassis
11-21
CS-200
Illustrations
SCREW
(2-REQ'D)
RETAINER
PLATE
RETAINER
CAP
O-RING
SEAT RING
INNER VALVE
ASSEMBLY PLUG
DIAPHRAGM
REGULATOR
BODY
ADJUSTMENT
NUT
METAL
BAND
SPACER
SCREW
(4-REQ'D)
(2-REQ'D)
SPRING
SPRING
SEAT
SPRING
HOUSING
SCREW
(4-REQ'D)
KNOB
Figure 11-20
773-383 Pressure Regulator
STEM
REGULATOR
BODY
SPRING
VALVE
Figure 11-21
782-839 Pressure Regulator
Illustrations
CS-200
11-22
783-772
PRESSURE
SWITCH
778-523
FITTING
767-866
FITTING
767-866
FITTING
778-246
RESTRICTOR
604-154
FITTING
805-063
TEE BLOCK
Figure 11-22
602-491 Pressure Switch and Restrictor
11-23
CS-200
Illustrations
SCREW
(2-REQ'D)
SCREW
(2-REQ'D)
CAP
WASHER
(2-REQ'D)
ARMATURE
SPRING
HOUSING
SEAL
O-RING
(3-REQ'D)
O-RING
(3-REQ'D)
PIN
SCREW
(2-REQ'D)
Figure 11-23
604-059 Solenoid Valve
VALVE
BODY
O-RING
ARMATURE
SPRING ARMATURE
HOUSING
SPACER
HOUSING
&
COIL
NUT
Figure 11-24
606-649 Solenoid Valve
Illustrations
CS-200
11-24
O-RING
O-RING
STEM
SPACER
HOUSING &
COIL
NUT
Figure 11-25
606-651 Solenoid Valve
NUT
HOUSING
&
COIL
SPACER
STEM
O-RING
O-RING
Figure 11-26
606-652 Solenoid Valve
11-25
CS-200
Illustrations
616-732
VACUUM DOOR
MOUNT
190-174
SCREW
(2-REQ'D)
194-105
NUT
(3-REQ'D)
616-731
BRACKET
789-366
TWIN ROD
CYLINDER
190-174
SCREW
(2-REQ'D)
602-427
TWIN ROD
MOUNT
190-008
SCREW
(3-REQ'D)
773-661
BARB FITTING
(2-REQ'D)
789-367
SENSOR
ASSEMBLY
J203
CONNECTOR
Figure 11-27
616-764 Twin Rod Cylinder
Illustrations
CS-200
11-26
TO
CATALYST HEATER
TOP
TO
CATALYST HEATER
BOTTOM
TO
SV2 FRONT
GAIN
J-152
CONNECTOR
TO
ROTAMETER
BOTTOM
ZERO
ADJUST
GAIN
ZERO
ADJUST
J-152A
CONNECTOR
782-067-110
SO2 IR-CELL
Figure 11-28
CS-200 and CS-200CH Series Oven Tubing Diagram
11-27
CS-200
Illustrations
TO
CATALYST HEATER
TOP
TO
CATALYST HEATER
BOTTOM
782-723-110
CO2 IR CELL
SV2 FRONT
GAIN
ZERO
ADJUST
GAIN
782-067-110
SO2 IR CELL
Figure 11-29
CS-200CL Series Oven Tubing Diagram
Illustrations
CS-200
11-28
TO
ROTAMETER
BOTTOM
TO SV2
604-080-110
CO2 IR CELL
GAIN
ZERO
ADJUST
ZERO
ADJUST
616-706
SO2 IR CELL
Figure 11-30
CS-200CSH Series Oven Tubing Diagram
11-29
CS-200
Illustrations
TO
ROTAMETER
BOTTOM
TO
CATALYST HEATER
TOP
TO
SV2 BOTTOM
GAIN
778-574-120
CO2IR CELL
TO
CATALYST HEATER
BOTTOM
ZERO
ADJUST
GAIN
ZERO
ADJUST
616-706
SO2 IR CELL
Figure 11-31
CS-200SH Series Oven Tubing Diagram
Illustrations
CS-200
11-30
12
Index
12 Index
A
Abort ......................................................................... 556
About the Examples ..................................................... 410
Add a User ................................................................. 472
Add Password ............................................................. 473
After Use, what to do ..................................................... 58
Ambient Monitor.......................................................... 416
Ambient Monitor Definitions ................................... 87, 824
Ambient Monitor Ranges............................................... 825
Ambient Monitor, DSP .................................................... 85
Ambient Monitor, Windows............................................ 822
Ambients.................................................................... 561
Analysis Gas Flow States ............................................ 1012
Analysis Menu Definitions and Ranges ............................ 517
Analysis Method Menu .................................................. 432
Analysis Row .............................................................. 555
Analysis Valve State, Gas Flow Analysis ........................ 1013
Analyze...................................................................... 556
Analyze a Sample ............................................... 525, 568
Analyze Menu ............................................................. 511
Analyze Sequence Diagram ......................................... 1021
Analyze Valve State, Gas Flow Analysis......................... 1012
Anhydrone.............................................................63, 64
Anhydrone Tube ............................................23, 214, 64
ASCII Character Definition Table.................................... 436
Assign User Functions .................................................. 474
Auto Widths................................................................ 560
Autocleaner ......................................................... 312, 66
Autocleaner Assembly .................................................... 67
Index
CS-200
121
B
Balance............................................................... 33, 556
Balance Configuration Definitions ................................... 463
Balance Definitions ...................................................... 463
Balance Installation ....................................................... 33
Balance Interfacing ........................................................ 34
Balance Login ............................................................. 566
Balance Options .......................................................... 423
Balance Tab................................................................ 462
Balance Weight ........................................................... 520
Balance Weight, Analyze Menu ...................................... 520
Balance, Resetting the ................................................... 35
Balance, Setting the Data Output Parameter ..................... 35
Barometric (PID) Pressure Regulator Adjustment ............... 93
Barometric Pressure..................................................... 464
Blank ......................................................................... 558
Blank Calibration ......................................................... 575
Blank Samples ............................................................ 510
Blank Samples defined ................................................. 510
Buffer ........................................................................ 587
Buffer, Plot ................................................................. 813
Buffer, Print................................................................ 812
C
Calculate Blank ........................................................... 533
Calculate Calibration .................................................... 530
Calibrate Menu ............................................................ 527
Calibration.................................................................. 574
Calibration Format ....................................................... 528
Calibration Results Format Selection............................... 528
Calibrations ................................................................ 558
122
CS-200
Index
CS-200
123
D
Data Management ....................................................... 581
Data Transmit ............................................................. 435
Data Transmit Format .................................................. 437
Declaration of Conformity ............................................. 115
Define Delimiters......................................................... 467
Define Fields ............................................................... 465
Defining, Quick Access Menu ......................................... 430
Definitions and Ranges, Analyze Menu ............................ 517
Definitions and Selections, Balance Options ..................... 425
Definitions, Leak Check ................................................ 811
Definitions, Linearization ............................................ 1033
Definitions, Ranges, and Defaults, Analysis Method Menu .. 434
Definitions, Ranges, and Defaults, System Options ........... 420
Definitions, Ranges, and Defaults, Transmit Options ......... 422
Definitions, Statistics ................................................... 544
Delete........................................................................ 557
Delete a Sample .......................................................... 569
Delete Selected Results ................................................ 542
Delete Weight ............................................................. 513
Delete Weight, Analyze Menu ........................................ 513
Delimiters .................................................................. 467
Deskjet (Inkjet) Printer ................................................ 311
Diagnostics for DSP ....................................................... 81
Diagnostics for Windows ............................................... 817
Diagnostics Menu ........................................................ 561
Diagnostics Procedure, DSP ............................................ 84
Diagnostics, Comport ................................................... 828
Diagnostics, Solenoid Valves ......................................... 827
Display ...................................................................... 560
124
CS-200
Index
E
Edit Blank, Calibration Menu ......................................... 535
Edit Calibration ........................................................... 532
Edit Menu ................................................................... 554
Enter Sample Weight .......................................... 425, 523
Enter Standards .......................................................... 457
Error Messages ......................................................... 1024
Errors ...................................................................... 1024
Exit ........................................................................... 553
Export ....................................................................... 553
Export Buffer .............................................................. 587
Export Sample ............................................................ 584
Export Sample Definitions............................................. 586
F
Facility Requirements ..................................................... 26
Facility Voltage Selection .............................................. 210
Fields......................................................................... 465
File Menu ................................................................... 552
Fill............................................................................. 554
Fill Selected Cells with the Same Values.......................... 582
Filter, Cellulose ........................................................... 613
Filter, Lance Assembly....................................63, 66, 619
First Row.................................................................... 555
Flow Controller Adjustment ........................................... 105
Format Results............................................................ 540
Index
CS-200
125
G
Gas Connections.......................................................... 221
Gas Flow Diagram .............................................. 76, 1017
Gas Flow States ........................................................ 1012
Gas Flow with Autocleaner Diagram ...................... 77, 1018
General Information, Theory of Operation ......................... 73
Gudelines Before an Analysis........................................... 57
Guidelines After an Analysis ............................................ 58
Guidelines for Operation ................................................. 56
H
Hardware Calibration ................................................... 464
Hardware Calibrations .................................................. 560
High Sulfur Samples .................................................... 510
I
Illustrations List ............................................................ 18
Import ....................................................................... 553
Import Sample Data .................................................... 583
Incoming Reagent Tube....................................... 216, 617
Induction Power Control Card Adjustment ......................... 98
Infrared Radiation, Absorption, and Detection.................... 74
Insert ........................................................................ 554
Insert a Sample Out-of-Sequence .................................. 582
Insert Data into the Spreadsheet ................................... 581
Insert Weight.............................................................. 514
Insert Weight, Analyze Menu......................................... 514
Installation of Optional Kits for the Autocleaner................ 312
Instrument Installation................................................... 23
Interference to Other Devices........................................ 114
International Installation ................................................ 27
126
CS-200
Index
K
Keypad ...................................................................... 411
L
Lance and Filter Assembly............................................. 619
Language .......................................................... 471, 560
Last Row .................................................................... 555
Leak Check................................................................. 561
Leak Check Definitions ........................................ 811, 821
Leak Check Gas Flow Diagram..................................... 1019
Leak Check Gas Flow with Autocleaner Diagram............. 1020
Leak Check Procedure, DSP .......................................... 810
Leak Check Procedure, Windows .................................... 819
Linearization with DSP................................................ 1030
Linearization with Windows ......................................... 1032
Linearizations.............................................................. 558
Log File ...................................................................... 562
Log File, View ............................................................. 625
Login ................................................................ 556, 562
Login a Sample ........................................................... 563
Login Periodic Maintenance ........................................... 624
Login using a Sample Template ..................................... 567
Login, Balance ............................................................ 566
M
Main Menu Overview .................................................... 415
Maintenance ................................................................. 63
Maintenance Counters, Reset ........................................ 626
Maintenance Menu....................................................... 562
Maintenance Schedule.................................................... 63
Major Equipment ......................................................... 118
Memory, Reset............................................................ 816
Menu Organization Chart ................................................ 48
Menu,Calibrate DSP ..................................................... 527
Menus............................................................... 410, 552
Mesh Filter, Autocleaner ................................................. 69
Index
CS-200
127
N
Notice, Operator.......................................................... 111
Notices .................................................................... 1022
Notices and Errors ....................................................... 413
Notices, Errors, and Warnings ..................................... 1022
O
Operation for DSP.......................................................... 51
Operation for Windows ................................................. 547
Operation Guidelines...................................................... 56
Operation, Quick Access Menu....................................... 429
Optional Equipment ..................................................... 134
Options ...................................................................... 134
O-rings, Autocleaner .................................................... 610
O-rings, Combustion .................................................... 616
Oscillator Tube ............................................................ 212
Oven Heater Control Card Adjustment ............................ 911
P
Packing, Anhydrone Tube ...................................... 214, 64
Packing, Cellulose Filter ................................................ 613
Packing, Incoming Reagent Tube .......................... 216, 617
Paste ................................................................ 554, 588
Pedestal Installation..................................................... 223
Periodic Maintenance Schedule ........................................ 63
Periodic Maintenance, Login .......................................... 624
Pinch Valve Assembly, Illustration .................................. 622
Pinch Valve Tubing ...................................................... 621
Plot Buffer .................................................................. 813
Plot Configuration ........................................................ 589
Points, Statistics.......................................................... 544
Post-Analyze Valve State, Gas Flow Analysis.................. 1014
Power Adjustment, Induction .......................................... 98
128
CS-200
Index
Q
Quick Access Menu ...................................................... 429
R
Reagent Tube Screen Filter ........................................... 623
Reagent Tube, Incoming............................................... 617
Recalculate ................................................................. 557
Recalculate Result ....................................................... 573
Recalculate Results, Calibration Menu ............................. 536
Relative Standard Deviation, Statistics............................ 544
Removal, Anhydrone Tube ..................................... 214, 64
Removal, Cellulose Filter .............................................. 613
Removal, Incoming Reagent Tube ......................... 216, 617
Reset......................................................................... 556
Reset Maintenance Counters ......................................... 626
Reset Memory............................................................. 816
Resetting the Balance .................................................... 35
Result Plot Menu ......................................................... 589
Result, Recalculate ...................................................... 573
Results Format Selection .............................................. 540
Results Menu .............................................................. 538
Results, Transmit ........................................................ 572
Index
CS-200
129
S
Safety Pressure Adjustments......................................... 106
Sample ...................................................................... 568
Sample Analysis ................................................. 525, 568
Sample Login .............................................................. 563
Sample Login Definitions .............................................. 565
Sample Preparation ..................................................... 510
Sample Results, Print ................................................... 570
Sample Size................................................................ 510
Sample Template, Login ............................................... 567
Sample Templates .............................................. 456, 559
Sample Weight Entry ................................................... 523
Samples Menu ............................................................ 556
Screen Description, Analyze Menu.................................. 511
Screen Filter ............................................................... 623
Select First Row in the Spreadsheet ............................... 583
Select Language................................................. 471, 560
Select Last Row in the Spreadsheet................................ 583
Select Method ............................................................. 522
Select Method, Analyze Menu ........................................ 522
Select the Analysis Row in the Spreadsheet..................... 583
Serial Port Tab ............................................................ 461
Set Barometer ............................................................ 427
Setting the Data Output Parameter, Balance ..................... 35
Shutdown After Use ....................................................... 58
Software Upgrade Procedure ....................................... 1026
Solenoid Valve Control States...................................... 1016
Solenoid Valve States..................................................... 89
Solenoid Valves, ................................................. 561, 827
Solenoids ................................................................... 561
Specifications.............................................................. 135
Standard Calibration .................................................... 576
Standard Calibration Definitions..................................... 578
Standard Deviation, Statistics........................................ 544
Standards ......................................................... 457, 559
1210
CS-200
Index
T
Theory of Operation ....................................................... 73
Tool Bar ............................................................ 450, 555
Transmission Formats ......................................... 465, 560
Transmit .................................................................... 557
Transmit Last.............................................................. 521
Transmit Last, Analyze Menu......................................... 521
Transmit Options ......................................................... 421
Transmit Results ......................................................... 572
Transmit Selected Results............................................. 546
Transmitted Data ........................................................ 469
Tubing, Pinch Valve ..................................................... 621
Index
CS-200
1211
U
User Functions ............................................................ 474
User Password ............................................................ 473
Users................................................................ 472, 559
Using the Keypad ........................................................ 412
V
Vacuum Cleaner Kit ..................................................... 312
Valve Control States .................................................. 1016
Valve States ................................................................. 89
Vertical Crucible Alignment ........................................... 108
View Log File ..................................................... 562, 625
View Menu.................................................................. 555
W
Warnings.................................................................. 1023
Warranty.................................................................... 110
Windows Diagnostics.................................................... 817
Windows Operation...................................................... 547
Windows Sample Analysis ............................................. 568
Windows Software Menus ............................................. 552
Windows System Configuration...................................... 459
Windows System Configuration Definitions ...................... 460
Windows System Setup ................................................ 438
Windows Software Upgrade Procedure ........................ 1029
With Autocleaner, Pedestal Installation ........................... 224
Without Autocleaner, Pedestal Installation....................... 223
1212
CS-200
Index