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CS-200

Carbon/Sulfur
Determinator
INSTRUCTION MANUAL
Software Version DSP 2.9 Windows 1.2
Part Number 200-635
October 2003
Patents are Pending in U.S.A. and other countries
2003 LECO Corporation
Minor revisions may not be reflected in this manual.

LECO Corporation

3000 Lakeview Avenue St. Joseph, MI 49085-2396


Phone: 269-983-5531 Fax: 269-983-3850
info@leco.com www.leco.com ISO-9001 No. FM 24045
LECO is a registered trademark of LECO Corporation.

This page intentionally left blank.

12

CS-200

Introduction

Introduction

1 Introduction

Introduction
Illustrations .......................................................................18
Warranty......................................................................... 110
Symbols.......................................................................... 112
Interference to Other Devices ............................................ 114
Declaration of Conformity .................................................. 115
Major Equipment and Accessories List ................................. 118
Components and Accessories List........................................ 127
Options ........................................................................... 134
Specifications................................................................... 135

Installation
Illustrations .......................................................................22
Instrument Installation........................................................23
Facility Requirements..........................................................26
International Installation .....................................................27

Option Installation
Illustrations .......................................................................32
Balance Installation ............................................................33
Dot Matrix Printer (601-480-110) .........................................37
Deskjet (Inkjet) Printer (611-499-110)................................ 311
Installation of Optional Kits for the Autocleaner .................... 312

System Setup
Illustrations .......................................................................44
Controls and Indicators .......................................................46
Menu Organization Chart .....................................................48
Power-Up ........................................................................ 410

Introduction

CS-200

13

System Overview ............................................................. 415


System Check .................................................................. 416
System Setup .................................................................. 418
Analysis Method Menu....................................................... 432
Data Transmit.................................................................. 435
System Setup for Windows .............................................. 438
Illustrations ..................................................................... 441
Controls and Indicators ..................................................... 442
Automatically Transmit Analysis Results............................... 444
Configure Maintenance Counters......................................... 446
Configure the Analysis Report ............................................ 448
Configure the Screen ........................................................ 450
Configure the Spreadsheet................................................. 451
Method Development ........................................................ 453
Sample Templates ............................................................ 456
Standards ....................................................................... 457
System Configuration........................................................ 459
Set Barometric Pressure .................................................... 464
Transmission Formats ....................................................... 465
Preview Transmitted Data.................................................. 469
Select Language............................................................... 471
Users.............................................................................. 472

Operation
Operation Guidelines...........................................................56
Crucibles ...........................................................................59
Sample Preparation .......................................................... 510
Analyze Menu .................................................................. 511
Sample Weight Entry ........................................................ 523
Sample Analysis ............................................................... 525
Calibrate Menu................................................................. 527
Results Menu ................................................................... 538
Operation for Windows .................................................... 547
Windows Software Menus .................................................. 552
Login a Sample ................................................................ 563
Analyze a Sample ............................................................. 568

14

CS-200

Introduction

Delete a Sample............................................................... 569


Print Sample Results ......................................................... 570
Transmit Results .............................................................. 572
Recalculate Result ............................................................ 573
Calibration....................................................................... 574
Blank Calibration .............................................................. 575
Standard Calibration ......................................................... 576
Drift Correction ................................................................ 579
Data Management ............................................................ 581
Clipboard Use .................................................................. 588
Configure Result Plot......................................................... 589

Maintenance
Illustrations .......................................................................62
Periodic Maintenance Schedule .............................................63
Anhydrone Tube.................................................................64
Autocleaner .......................................................................66
Catalyst Heater Tube Packing ............................................. 611
Cellulose Filter ................................................................. 613
Combustion Tube ............................................................. 615
Combustion Zone O-rings .................................................. 616
Incoming Reagent Tube..................................................... 617
Lance and Filter Assembly ................................................. 619
Pinch Valve Tubing ........................................................... 621
Reagent Tube Screen Filter ................................................ 623
Login Periodic Maintenance ................................................ 624
View Log File ................................................................... 625
Reset Maintenance Counters .............................................. 626

Theory of Operation
Illustrations .......................................................................72
General Information............................................................73
Infrared Radiation, Absorption, and Detection.........................74
Comparator Level ...............................................................78

Introduction

CS-200

15

Diagnostics
Diagnostics........................................................................84
Ambient Monitor.................................................................85
Switch States.....................................................................88
Valve States ......................................................................89
Leak Check...................................................................... 810
Print Buffer...................................................................... 812
Plot Buffer ....................................................................... 813
System Print.................................................................... 815
Reset Memory.................................................................. 816
Diagnostics for Windows .................................................. 817
Leak Check...................................................................... 819
Ambient Monitor............................................................... 822
Switches ......................................................................... 826
Solenoids ........................................................................ 827
Comport.......................................................................... 828

Electronic Adjustments
Illustrations .......................................................................92
Barometric (PID) Pressure Regulator Adjustment ....................93
Catalyst Heater Control Card................................................96
Induction Power Control Card ...............................................98
Oven Heater Control Card.................................................. 911
IR Cell ............................................................................ 912

10

Service
Illustrations ..................................................................... 102
Combustion Pressure Adjustment ....................................... 103
Flow Controller Adjustment ................................................ 105
Safety Pressure Adjustments.............................................. 106
Vertical Crucible Alignment ................................................ 108
Gas Flows...................................................................... 1012
Valve Control States ....................................................... 1016
Notices, Errors, and Warnings .......................................... 1022
Software Upgrade........................................................... 1026

16

CS-200

Introduction

Linearization with DSP..................................................... 1030


Linearization with Windows ............................................ 1032

11

Illustrations

12

Index

Introduction

CS-200

17

Illustrations
Figure 11......... CS200 Determinator .................................. 116
Figure 12......... CS200 Determinator with Autocleaner .......... 117
Figure 2-1 ......... Wiring Diagrams ........................................ 28
Figure 2-2 ......... Interconnection Diagram ............................ 29
Figure 2-3 ......... Voltage Selection Terminal Strip .................. 211
Figure 2-4 ......... RF Shield Removal ..................................... 213
Figure 2-5 ......... Oscillator Chassis....................................... 213
Figure 2-6 ......... Anhydrone Tube ........................................ 215
Figure 2-7 ......... Reagent Tube Removal ............................... 217
Figure 2-8 ......... Reagent Tube Packing ................................ 217
Figure 2-9 ......... Combustion Tube InstallationWithout Autocleaner
....................... 219
Figure 2-10 ....... Combustion Tube InstallationWith Autocleaner
....................... 220
Figure 2-11 ....... Pedestal InstallationWithout Autocleaner .... 223
Figure 2-12 ....... Pedestal InstallationWith Autocleaner......... 224
Figure 3-1 ......... Balance Control Panel................................. 36
Figure 3-2 ......... Balance Assembly ...................................... 36
Figure 3-3 ......... Ribbon Cartridge Installation ....................... 39
Figure 3-4 ......... Paper Installation....................................... 39
Figure 41......... Controls and Indicators with Autocleaner....... 47
Figure 42......... Keypad .................................................... 411
Figure 43......... Combustion Pressure Adjustment Knob ......... 428
Figure 4-4 ......... Controls and Indicators............................... 443
Figure 61......... Anhydrone Tube ........................................ 65
Figure 62......... Autocleaner Assembly ................................ 68
Figure 63......... Catalyst Heater Tube Packing ...................... 612
Figure 64......... Cellulose Filter Packing ............................... 614
Figure 65......... Reagent Tube Removal ............................... 618
Figure 66......... Reagent Tube Packing ................................ 618
Figure 67......... Lance and Filter Assembly........................... 620
Figure 68......... Pinch Valve Assembly ................................. 622
Figure 71......... Gas Flow Diagram...................................... 76

18

CS-200

Introduction

Figure 72......... Gas Flow with Autocleaner Diagram.............. 77


Figure 91......... Barometric (PID) Pressure Regulator Card ..... 95
Figure 92......... Catalyst Heater Control Card ....................... 97
Figure 93......... Induction Power Control Card ...................... 910
Figure 94......... Oven Heater Control Card ........................... 911
Figure 95......... IR Cell Adjustment Location ........................ 913
Figure 101 ....... Combustion Pressure Adjustment Knob ......... 104
Figure 102 ....... Flow Controller Location.............................. 105
Figure 103 ....... Piston Pressure Regulator ........................... 107
Figure 104 ....... Crucible Alignment..................................... 1011
Figure 105 ....... Gas Flow Diagram...................................... 1017
Figure 106 ....... Gas Flow with Autocleaner Diagram.............. 1018
Figure 107 ....... Leak Check Flow Diagram ........................... 1019
Figure 108 ....... Leak Check Flow with Autocleaner Diagram ... 1020
Figure 109 ....... Analyze Sequence Diagram ......................... 1021
Figure 10-10...... EPROM Location......................................... 1028

Note

Introduction

The Illustrations chapter table of contents is listed on page


11-1.

CS-200

19

Warranty
Equipment manufactured by LECO Corporation, St. Joseph,
Michigan is warranted free from defect in material and
workmanship for a period of six months from the date of
installation. Equipment not manufactured by LECO is covered to
the extent of warranty provided by the original manufacturer
and this warranty does not cover any equipment, new or used,
purchased from anyone other than LECO Corporation. All
replacement parts shall be covered under warranty for a period
of thirty days from date of purchase. LECO makes no other
representation or warranty of any other kind, expressed
or implied, with respect to the goods sold hereunder,
whether as to merchantability, fitness for purpose, or
otherwise.
Expendable items such as crucibles, combustion tubes,
chemicals, and items of like nature are not covered by this
warranty.
LECO's sole obligation under this warranty shall be to repair or
replace any part or parts which, to our satisfaction, prove to be
defective upon return prepaid to LECO Corporation, St. Joseph,
Michigan. This obligation does not include labor to install
replacement parts, nor does it cover any failure due to
accident, abuse, neglect, or use in disregard of instructions
furnished by LECO. In no event shall damages for defective
goods exceed the purchase price of the goods, and LECO shall
not be liable for incidental or consequential damages
whatsoever.
All claims in regard to the parts or equipment must be made
within ten (10) days after Purchaser learns of the facts upon
which the claim is based. Authorization must be obtained from
LECO prior to returning any other parts. This warranty is voided
by failure to comply with these notice requirements.

110

CS-200

Introduction

Notice
The warranty on LECO equipment remains valid only when
genuine LECO replacement parts are employed. Since LECO has
no control over the quality or purity of consumable products not
manufactured by LECO, the specifications for accuracy of
results using LECO instruments are not guaranteed unless
genuine LECO consumables are employed in conjunction with
LECO instruments. If purchaser defaults in making payment for
any parts or equipment, this warranty shall be void and shall
not apply to such parts and equipment. No late payment or
cure of default in payment shall extend the warranty period
provided herein.
LECO Corporation is not responsible for damage to any
associated instruments, equipment, or apparatus nor will LECO
be held liable for loss of profit or other special damages
resulting from abuse, neglect, or use in disregard of
instructions. The Buyer, their employees, agents, and
successors in interest assume all risks and liabilities for the
operation, use, and/or misuse of the product(s) described
herein and agree to indemnify, hold harmless, and defend the
seller from any and all claims and actions arising from any
cause whatsoever, including seller's negligence for personal
injury incurred in connection with the use of said product(s)
and any and all damages proximately resulting therefrom.

Caution
The instrument should be operated only by technically qualified
individuals who have fully read and understand these
instructions. The instrument should be operated only in
accordance with these instructions.
The operator should follow all of the warnings and cautions set
forth in the manual and the operator should follow and employ
all applicable standard laboratory safety procedures.
LECO is a registered trademark of LECO Corporation.
Windows is a registered trademark of Microsoft Corporation.
Excel is a registered trademark of Microsoft Corporation.
Windows 95 is a trademark of Microsoft Corporation.
Windows 3.1 is a trademark of Microsoft Corporation.

Introduction

CS-200

111

Symbols

Warning and Caution


The following symbols may be found on LECO equipment or
their components. These symbols indicate the use of specific
safety guidelines. Important safety information is highlighted in
this manual by one of the following symbols as well as
WARNING and CAUTION statements. Operator and service
personnel must follow these instructions for personal safety and
to prevent damage to the equipment.

WARNING

This symbol indicates a risk of electrical shock.


Refer to the manual for specific instructions.

WARNING

This symbol indicates a high temperature


surface. Refer to the manual for specific
instructions.

!
CAUTION

This symbol indicates a caution. Refer to the


manual for specific instructions.

LECO equipment should be operated only by technically


qualified individuals who have fully read and understand the
instructions detailed in this manual. The equipment should be
operated only in accordance with these instructions.
The operator should follow all of the warnings and cautions set
forth in this manual and the operator should follow and employ
all applicable standard laboratory safety procedures.

112

CS-200

Introduction

About this Manual and the Instrument


The CS-200 can be purchased with two different user
interfaces. The first user interface has a display and keypad
built-in. Control of the instrument is from the display and
keypad. The second user interface is a Windows program
running on a PC thats interfaced with the instrument. Control
of the instrument is from the PC.
This manual contains procedures for both user interfaces. The
built-in display and keypad instrument will be refer to as the
CS-200 DSP (Display) and the instrument controlled by a PC
will be referred to as the CS-200 Windows. When a
procedure is for a specific user interface the symbols shown
below will appear next to the procedure.

User Interface (Software)

Keypad

Windows

Introduction

This symbol indicates the information is for the keypad


interface only. This instrument is referred to as the CS-200
DSP. Refer to this manual for specific instructions.

This symbol indicates the information is for the Windows


software only. This instrument is referred to as the CS-200
Windows. Refer to this manual or the electronic manual
for specific instructions.

CS-200

113

Interference to Other Devices


This equipment has been tested and found to comply with the
limits for a Class B digital device, pursuant to Part 15 of the
FCC Rules and Regulations. These limits are designed to
provide reasonable protection against harmful interference in a
residential installation. This equipment generates, uses and can
radiate radio frequency energy and, if not installed and used in
accordance with the instructions, may cause interference to
radio communications. However, there is no guarantee that
interference will not occur in a particular installation. If this
equipment does cause harmful interference to radio or
television reception, which can be determined by turning the
equipment off and on, the user is encouraged to try to correct
the interference by one or more of the following methods:

114

Reorient or relocate the radio or television receiving


antenna.

Increase the separation between the equipment and the


radio or television receiver.

Connect the equipment to an outlet on a circuit different


from that which the radio or television receiver is currently
connected.

Consult the radio or television dealer or an experienced


radio/TV technician for help.

CS-200

Introduction

Declaration of Conformity

Introduction

CS-200

115

With Keypad and Display (DSP)

Without Keypad and Display (Windows)

Figure 11
CS-200 Determinator

116

CS-200

Introduction

With Keypad and Display (DSP)

Figure 12
CS-200 Determinator with Autocleaner

Introduction

CS-200

117

Major Equipment and Accessories List

Notes

Note

Items listed below and repeated throughout this manual are


subject to revision. Please consult the packing slip received
with the instrument.

For a complete listing of all Accessory, Component,


Hazardous Material, and PC Tower packages, along with
Software Kits, see Components and Accessories List
beginning on page 127.

The following units have a Display and Keypad built into the
determinator. They do not include a PC.

CS200 Carbon/Sulfur Determinator with Display


1

617-000-100

CS-200 Determinator including:

200-635

Instruction Manual

617-010-070

Component Pack

615-426

Power Cord

607-750*

Hazardous Material Package

616-759

Accessory Pack

CS200CH High Carbon/Sulfur Determinator with Display


1

617-000-500

CS-200CH Determinator including:

200-635

Instruction Manual

617-010-070

Component Pack

1
1

607-750*

616-759

615-426

Power Cord

Hazardous Material Package


Accessory Pack

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

118

CS-200

Introduction

CS200CHH High Carbon/Sulfur Determinator with Display and Autocleaner


1

617-000-700

CS-200CH Determinator including:

200-635

Instruction Manual

617-010-070

Component Pack

615-426

Power Cord

607-750*

Hazardous Material Package

616-759

Accessory Pack

CS200CL Low Carbon/Sulfur Determinator with Display


1

617-100-300

CS-200CL Determinator including:

200-635

Instruction Manual

617-010-070

Component Pack

615-426

Power Cord

607-750*

Hazardous Material Package

616-759

Accessory Pack

CS200CLH Low Carbon/Sulfur Determinator with Display and Autocleaner


1

617-100-300

CS-200CL Determinator including:

200-635

Instruction Manual

617-010-070

Component Pack

615-426

Power Cord

607-750*

Hazardous Material Package

616-759

Accessory Pack

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

Introduction

CS-200

119

CS200CSH High Carbon/High Sulfur Determinator with Display


1

617-100-500

CS-200CSH Determinator including:

200-635

Instruction Manual

617-010-070

Component Pack

615-426

Power Cord

607-750*

Hazardous Material Package

616-759

Accessory Pack

CS200CSHH High Carbon/High Sulfur Determinator with Display and


Autocleaner
1

617-100-700

CS-200CSH Determinator including:

200-635

Instruction Manual

617-030-070

Component Pack

615-426

Power Cord

607-750*

Hazardous Material Package

616-759

Accessory Pack

CS200H Carbon/Sulfur Determinator with Display and Autocleaner


1

617-000-300

CS-200 Determinator including:

200-635

Instruction Manual

617-030-070

Component Pack

615-426

Power Cord

607-750*

Hazardous Material Package

616-759

Accessory Pack

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

120

CS-200

Introduction

CS200SH Carbon/High Sulfur Determinator with Display


1

617-200-100

CS-200SH Determinator including:

200-635

Instruction Manual

617-010-070

Component Pack

615-426

Power Cord

607-750*

Hazardous Material Package

616-759

Accessory Pack

CS200SHH Carbon/High Sulfur Determinator with Display and Autocleaner


1

617-200-300

CS-200 Determinator including:

200-635

Instruction Manual

617-030-070

Component Pack

615-426

Power Cord

607-750*

Hazardous Material Package

616-759

Accessory Pack

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

Introduction

CS-200

121

Note

The following units include a PC. They do not have a display


and keypad built into the determinator.

CS200C Carbon/Sulfur Determinator with PC


1

617-000-200

CS-200CSH Determinator including:

200-635

Instruction Manual

617-020-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

CS200HC Carbon/Sulfur Determinator with PC and Autocleaner


1

617-000-400

CS-200 Determinator including:

200-635

Instruction Manual

617-040-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

122

CS-200

Introduction

CS200CHC High Carbon/Sulfur Determinator with PC


1

617-000-600

CS-200 Determinator including:

200-635

Instruction Manual

617-020-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

CS200CHHC High Carbon/Sulfur Determinator with PC and Autocleaner


1

617-000-800

CS200CH

200-635

Instruction Manual

617-040-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

Introduction

CS-200

123

CS200CLC Low Carbon/Sulfur Determinator with PC


1

617-100-200

CS-200CL Determinator including:

200-635

Instruction Manual

617-020-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

CS200CLHC Low Carbon/Sulfur Determinator with PC and Autocleaner


1

617-100-400

CS-200CL Determinator including:

200-635

Instruction Manual

617-040-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

124

CS-200

Introduction

CS200CSHC High Carbon/High Sulfur Determinator with PC


1

617-100-600

CS-200CSH Determinator including:

200-635

Instruction Manual

617-020-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

CS200CSHHC High Carbon/High Sulfur Determinator with PC and


Autocleaner
1

617-100-800

CS-200CSH Determinator including:

200-635

Instruction Manual

617-040-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

Introduction

CS-200

125

CS200SHC Carbon/High Sulfur Determinator with PC


1

617-200-200

CS-200SH Determinator including:

200-635

Instruction Manual

617-020-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

CS-200SHHC Carbon/High Sulfur Determinator with PC and Autocleaner


1

617-200-400

CS-200SH Determinator including:

200-635

Instruction Manual

617-040-070

Component Pack

615-426

Power Cord

259-035

Software Kit

607-750*

Hazardous Material Package

616-759

Accessory Pack

686-208-2GH

PC Tower Package

1
1

609-787

701-557

Component Pack
15.00 inch Color SVGA Monitor

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

126

CS-200

Introduction

Components and Accessories List


259-035

Software Kit

159-109-100

Software Package

203-505-267

Software Registration Form

602-773

External Alarm Kit

602-773-901

External Alarm Kit Bulletin

767-228

Bag

769-299

Connector

776-118

Contact

802-151

Cable Clamp

607-750*

Hazardous Material Pack

501-171

Anhydrone 10-20 Mesh (1 lb)

502-174

Lecosorb 20-30 Mesh (500gr)

* Packed and shipped separately in the U.S.A. Not included with international shipments due
to shipping restrictions. These items are essential for operation. Contact your local LECO
distributor for quotation and delivery.

Introduction

CS-200

127

616-759

128

Accessory Pack

501-077

Chip Accelerator

501-082

Wire Brush

501-241

Grease Vacuum (5.3 Oz)

501-503

Standard Steel Ring Sample

501-587

Platinum Silica Catalyst

501-679

Steel Pin Sample

502-177

Fine Wool Quartz (50 gr)

502-294

Accelerator Lecocel 2

502-413

Cast Iron Powdered Sample

528-018-500

Low Carbon Crucible (500 Pk)

528-043-100

Crucible Cover (100 Pk)

602-773

Alarm External Kit Connector

605-700-087

O-ring Package including:

601-920

O-ring (Combustion Tube)

762-058

O-ring (Lance Assembly)

765-976

O-ring (Anhydrone Tube)

772-520

O-ring (Reagent Tube Screen Filters)

772-738

O-ring (Reagent Tube Stationary Blocks)

760-138

Tweezers

761-929

Crucible Tongs

764-098

Cellulose (1 lb)

773-579

Scoop SST Assembly

775-306

Secondary 10micron Filter

775-307

Thumb Screw

CS-200

Introduction

617-010-070

Component Pack

550-080

Insulation Sheet

601-920

O-ring (Combustion Tube)

605-816

Pedestal Silicon Nitride

605-979

Electrical Retainer Connector

608-898

Receptacle Cover

615-426

AC Power Cord

762-458

Connector Nut

765-978

Receptacle (30A 125/250V)

772-381

Lance Cleaner

772-905

Combustion Tube

772-960

Box Crucible Assembly

772-967

Box Crucible Insulator

774-828

Connector

774-829

Plug Hood

783-747

Dust Cup Removal Assembly

789-149

EMI Gasket Ring

Introduction

CS-200

129

617-020-070

130

Component Pack

550-080

Insulation Sheet

601-920

O-ring (Combustion Tube)

605-816

Silicon Nitride Pedestal

605-979

Electrical Retainer Connector

608-898

Receptacle Cover

615-426

AC Power Cord

616-555

Cable Assembly

762-458

Connector Nut

765-978

Receptacle (30A 125/250V)

772-381

Cleaner Lance

772-905

Combustion Tube

772-960

Box Crucible Assembly

772-967

Crucible Box Insulator

774-828

Connector

774-829

Plug Hood

783-747

Dust Removal Cup Assembly

789-149

EMI Gasket Ring

CS-200

Introduction

617-030-070

Component Pack

190-009

Thumb Screw

190-279

Screw

190-624

Screw

193-055

Washer

550-080

Insulation

601-920

O-ring (Combustion Tube)

604-126

Dust Box Assembly

605-814

Pedestal Adapter Assembly

605-816

Silicon Nitride Pedestal

605-979

Electrical Retainer Connector

608-898

Receptacle Cover

615-426

AC Power Cord

616-555

Cable Assembly

618-723

Dust Box Assembly

762-458

Connector Nut

765-978

Receptacle (30A 125/250V)

772-381

Lance Cleaner

772-905

Combustion Tube

772-960

Box Crucible Assembly

772-967

Crucible Box Insulator

774-828

Connector

774-829

Hood Plug

782-603

Vacuum Cleaner Hose

782-604

Hose Vacuum Coupling

782-880

Vacuum Filter

783-747

Dust Cup Removal Assembly

789-149

EMI Gasket Ring

789-230

Vacuum Assembly

Introduction

CS-200

131

617-040-070

132

Component Pack

190-009

Thumb Screw

190-279

Screw

190-624

Screw

193-055

Washer

550-080

Insulation

601-920

O-ring (Combustion Tube)

605-814

Pedestal Adapter Assembly

605-816

Silicon Nitride Pedestal

605-979

Electrical Retainer Connector

608-898

Receptacle Cover

615-426

AC Power Cord

616-555

Cable Assembly

618-723

Dust Box Assembly

762-458

Connector Nut

765-978

Receptacle (30A 125/250V)

772-381

Cleaner Lance

772-905

Combustion Tube

772-960

Box Crucible Assembly

772-967

Crucible Box Insulator

774-828

Connector

774-829

Plug Hood

782-603

Vacuum Cleaner Hose

782-604

Hose Vacuum Coupling

782-880

Vacuum Filter

783-747

Dust Cup Removal Assembly

789-149

EMI Gasket Ring

789-230

Vacuum Assembly

CS-200

Introduction

686-208-2GH
1

PC Tower Package

609-787

Component Pack including:

611-119

Receptacle

618-980

Mouse Pad

686-229

Nameplate Id

686-993

Computer Tower

Introduction

CS-200

133

Options
CF-10

CF-10 Gas Purification System

501-291

Oxygen Pressure Regulator

605-980

Keyboard

611-499-110

Deskjet Printer Kit (for Windows packages)

614-459

Deskjet Printer Cartridge (Black)

614-460

Deskjet Printer Cartridge (Color)

616-775

PC Tower Upgrade with Monitor

616-776

Windows Upgrade Kit

616-778

Vacuum Cleaner Option

616-793

Upgrade Kit (CS-200 to CS200SH)

616-794

Upgrade Kit (CS200CH to CS200CSH)

616-795

Upgrade Kit (CS200SH to CS200CSH)

616-912

Pinch Valve Upgrade Kit (included in Autocleaner Upgrade kits)

616-925

Autocleaner Upgrade Kit (CS-200)*

616-926

Autocleaner Upgrade Kit (CS-200CL)*

616-927

Autocleaner Upgrade Kit (CS-200CH)*

616-928

Autocleaner Upgrade Kit (CS-200SH)*

616-929

Autocleaner Upgrade Kit (CS-200CSH)*

766-036

Compressed Air Regulator

751-000-120

Balance L-050 3 Place Kit

751-300-160

Balance L-250 4 Place Kit

751-700-120

Balance 5 Place PC Controlled Kit

783-690

Autocleaner Kit

783-693

Dust Removal Kit without Vacuum Cleaner

783-996

Autocleaner/Dust Removal Kit

*Includes 616-912 Pinch Valve Upgrade Kit.

134

CS-200

Introduction

Specifications
Range (at 1 gram)
CS-200C
Carbon ........................................... 4 ppm to 3.5%
Sulfur ............................................. 4 ppm to 0.4%
CS-200CLC
Carbon ........................................... 2 ppm to 0.5%
Sulfur ............................................. 4 ppm to 0.4%
CS-200CHC
Carbon ........................................... 60 ppm to 6.0%
Sulfur ............................................. 4 ppm to 0.4%
CS-200SHC
Carbon ........................................... 4 ppm to 3.5%
Sulfur ............................................. 60 ppm to 1.75%
CS-200CSHC
Carbon ........................................... 60 ppm to 6.0%
Sulfur ............................................. 60 ppm to 1.75%

Note

Reducing sample weight may extend range.

Result Readability (Display Capability)


With PCCarbon and Sulfur............... 15 digits of precision
Without PCCarbon and Sulfur .......... 0.1 ppm
Calibration
With PC .......................................... Multi-Point, Linear
Without PC...................................... Single Point, Linear
Analysis Time..................................... 45 seconds (Nominal)
Sample Size ....................................... 1 gram (Nominal)
Detection Method ............................... Solid State, Infrared Absorption,
Carbon as Carbon Dioxide
Sulfur as Sulfur Dioxide

Introduction

CS-200

135

Precision
CS-200C
Carbon ........................................... 2 ppm or 0.5% RSD*
Sulfur ............................................. 2 ppm or 1.5% RSD*
CS-200CLC
Carbon ........................................... 1 ppm or 0.5% RSD*
Sulfur ............................................. 2 ppm or 1.5% RSD*
CS-200CHC
Carbon ........................................... 30 ppm or 0.5% RSD*
Sulfur ............................................. 2 ppm or 1.5% RSD*
CS-200SHC
Carbon ........................................... 2 ppm or 0.5% RSD*
Sulfur ............................................. 30 ppm or 1.5% RSD*
CS-200CSHC
Carbon ........................................... 30 ppm or 0.5% RSD*
Sulfur ............................................. 30 ppm or 1.5% RSD*
Chemical Reagents............................. Anhydrone Magnesium Perchlorate,
Sodium Hydroxide on an inert base,
Lecosorb,
Platinized Silica, Cellulose
Gas Required
Carrier Gas ..................................... Oxygen 99.5% pure, 40 psi (2.76 bars)
Pneumatic Gas................................. Compressed Air, Nitrogen, or Argon,
40 psi (2.76 bars),
source must be oil and water free.
Gas Flow (based on nominal analysis time)
Measure ......................................... 3 liters per analysis
Pneumatic ...................................... 1 liters per analysis
Regulators
Oxygen........................................... 501-291 Oxygen Pressure Regulator
Compressed Air ............................... 766-036 Compressed Air Regulator
Inert Gas ........................................ 764-216 Inert Gas Regulator
Furnace.............................................. Induction, 18 MHz, 2.2 kW
Data Transmit .................................... RS-232 (included)
* One Sigma, conformance tested by gas dose analysis.

136

CS-200

Introduction

Data Storage
With PC .......................................... Limited only by hard drive space
Without PC...................................... 10 Sample Weights,
50 Answers, 5 Methods
Keypad
With PC .......................................... External
Without PC...................................... Internal Membrane/External Optional
Display
With PC .......................................... 15.00 inch SVGA Monitor
Without PC...................................... Liquid Crystal (16 x 26 characters)
External PC
Computer ....................................... PentiumTM 166 MHz (min),
1.2 GB Hard Drive (min)
Monitor........................................... 15.00 inch SVGA (min)
Operating System ............................ Microsoft Windows 95 (min)
Printer
With PC .......................................... Deskjet
Without PC...................................... Dot Matrix
Dimensions
Determinator
Height ............................................ 30.50 inches (77.5 cm)
Width ............................................. 27.50 inches (70.0 cm)
Depth............................................. 23.50 inches (59.7 cm)
Weight ........................................... 300 pounds
Computer (PC based system)
Height ............................................ 17.00 inches (43.2 cm)
Width ............................................. 8.00 inches (20.3 cm)
Depth............................................. 17.00 inches (43.2 cm)
Weight ........................................... 29 pounds
Monitor (PC based system)
Height ............................................ 15.00 inches (38.1 cm)
Width ............................................. 14.00 inches (35.6 cm)
Depth............................................. 16.00 inches (40.6 cm)
Weight ........................................... 35 pounds
Shipping Weight (without PC) .............. 420 pounds

Introduction

CS-200

137

Electrical Power Requirements


Determinator................................... 230 V~, 10%, 50/60 Hz, Single phase,
15 amps max
Operating Current ....................... 12 Amps
Stand-by Current ........................ 4 Amps
Computer (PC based) ....................... 115/230 V~, 10%, 50/60 Hz, 5/3 amps
Monitor (PC based)........................... 90 to 264 V~, 50/60 Hz, 1.6 amps max
Balance .......................................... 120 V~, 10%, 50/60 Hz, 0.5 amps max

Note

138

Allow a 6 inch minimum access area around all units.

CS-200

Introduction

Installation
2 Installation

Illustrations .......................................................................22
Instrument Installation........................................................23
Facility Requirements..........................................................26
International Installation .....................................................27
Instrument Voltage Selection ........................................ 210
Oscillator Tube Installation............................................ 212
Anhydrone Tube Packing .............................................. 214
Removal..................................................................... 214
Packing ................................................................. 214
Incoming Reagent Tube Packing .................................... 216
Removal................................................................ 216
Packing ................................................................. 216
Combustion Tube Installation ........................................ 218
Without Autocleaner................................................ 218
With Autocleaner .................................................... 218
Gas Connections.......................................................... 221
Computer Installation................................................... 222
Pedestal Installation..................................................... 223
Without Autocleaner................................................ 223
With Autocleaner .................................................... 224

Installation

CS-200

21

Illustrations
Figure 2-1 ......... Wiring Diagrams ........................................ 28
Figure 2-2 ......... Interconnection Diagram ............................ 29
Figure 2-3 ......... Voltage Selection Terminal Strip .................. 211
Figure 2-4 ......... RF Shield Removal ..................................... 213
Figure 2-5 ......... Oscillator Chassis....................................... 213
Figure 2-6 ......... Anhydrone Tube ........................................ 215
Figure 2-7 ......... Reagent Tube Removal ............................... 217
Figure 2-8 ......... Reagent Tube Packing ................................ 217
Figure 2-9 ......... Combustion Tube InstallationWithout Autocleaner
....................... 219
Figure 2-10 ....... Combustion Tube InstallationWith Autocleaner
....................... 220
Figure 2-11 ....... Pedestal InstallationWithout Autocleaner .... 223
Figure 2-12 ....... Pedestal InstallationWith Autocleaner......... 224

22

CS-200

Installation

Instrument Installation

Notes

The following procedure should be used for first time


installation of the instrument. This procedure assumes that
the instrument has been unpacked and positioned in its
permanent location.

The Balance and Printer are not supplied with the


instrument. They must be purchased separately. Refer to
Options, page 134, for more information.

This procedure should be used for both the Windows and


DSP instruments.

1.

Provide a work surface with convenient electrical power


and gas supplies. Refer to Facility Requirements, page 2
6, for power and gas supply requirements.

2.

Install the Instrument as shown in Figure 2-2, page 29.


Provide a minimum space of six inches around the
instrument for airflow.

WARNING

Installation

POSSIBLE SHOCK HAZARD


To avoid electrical shock, make sure the AC line
cord is disconnected from facility power before
performing this procedure.
3.

Connect the AC power cord, supplied with the instrument,


to the power connections on the rear of the instrument.
DO NOT plug it into facility power. For installation outside
the U.S.A. Refer to International Installation on page 27.

4.

Determine the facility line voltage and set the instrument


operating voltage. Refer to Instrument Voltage Selection
on page 210.

5.

Install the Oscillator tube in the furnace. Refer to Oscillator


Tube Installation, page 212.

6.

Remove the Anhydrone tube from the gas panel of the


instrument and pack it. Refer to Anhydrone Tube Packing,
page 214.

CS-200

23

7.

Remove the Incoming Reagent tube from the gas panel of


the instrument and pack it. Refer to Incoming Reagent
Tube Packing, page 216.

!
CAUTION

Windows

POSSIBLE OPERATOR INJURY


Oxygen is not recommended for use in the
pneumatic systems of LECO instruments. If a
spark is present an explosion may result.
8.

Connect the Gas connections from the gas supplies to the


oxygen and pneumatic gas connectors on the rear of the
instrument. Refer to Gas Connections, page 221.

9.

Install the Combustion Tube into the furnace. Refer to


Combustion Tube Installation, page 218.

The next step should only be performed if the instrument


was purchased with a computer.

10. If a Computer was purchased with the instrument install


the computer. Refer to Computer Installation, page 222.
11. Install the Pedestal onto the lower seal assembly. Refer to
Pedestal Installation, page 223.

!
CAUTION

POSSIBLE OPERATOR INJURY


The measure and purge flow exhaust ports must
be exhausted away from the work area and
should not be vented into the lab. Connect the
exhaust ports to the lab exhaust system or a
fume hood.
12. Connect the Measure and Purge Exhaust ports, on the rear
of the instrument, to the facility exhaust. Refer to Figure 2-2,
page 29.

24

CS-200

Installation

13. If a Balance was purchased with the instrument install the


balance. Refer to Balance Installation, page 33.
14. If a Dot Matrix Printer was purchased with the instrument
install the printer. Refer to Dot Matrix Printer (601-480-110),
page 37.
15. Plug the instrument into facility AC power DO NOT turn the
instrument on until instructed to do so.
16. This completes instrument installation. Before continuing
with operation, refer to System Setup on page 41.

Installation

CS-200

25

Facility Requirements
Electrical Power Requirements
Determinator................................... 230 V~, 10%, 50/60 Hz, Single phase,
15 amps max
Operating Current ....................... 12 Amps
Stand-by Current ........................ 4 Amps
Balance .......................................... 120 V~, 10%, 60 Hz, 0.5 amps max
Gas Required
Carrier Gas ..................................... Oxygen 99.5% pure, 40 psi (2.76 bars)
Pneumatic Gas................................. Compressed Air, Nitrogen, or Argon,
40 psi (2.76 bars),
source must be oil and water free.
Regulators
Oxygen........................................... 501-291 Oxygen Pressure Regulator
Compressed Air ............................... 766-036 Compressed Air Regulator

26

CS-200

Installation

International Installation
For international installation, a HAR approved line cord for use
in the end country must be obtained. This product requires a
disconnect device that may either be the plug of the power cord
or a disconnect device installed at the installation site if the
equipment is permanently wired.
When the plug on the power supply cord is intended to serve as
the disconnect device, the socket/outlet must be installed near
the equipment and shall be easily accessible. When the wiring
is permanently connected, a disconnect device (such as a
circuit breaker or switch) must be lockable, installed near the
equipment, and be easily accessible.

Installation

CS-200

27

POWER CORD

BROWN

POWER
NEUTRAL

220 V~

LIGHT BLUE
0 V~

GREEN/YELLOW

GROUND

CHASSIS
(CABINET)
GROUND

220 V~ 3 WIRE WIRING DIAGRAM INTERNATIONAL

PLUG

POWER

115 V~
GROUND

G
230 V~

POWER

115 V~

BLACK
T

BLACK
GREEN/YELLOW GREEN/
YELLOW G
BLACK
LIGHT BLUE

LIGHT
BLUE

X
BLACK
CHASSIS
(CABINET)
GROUND

RECEPTACLE

* BLUE WIRE IS CUT OFF INSIDE THE UNIT AND IS NON-FUNCTIONAL

230 V~ 3 WIRE WIRING DIAGRAM U.S.A.


PLUG

POWER

Y
115 V~

230 V~

GROUND

G
115 V~

POWER

0 V~
NEUTRAL

BLACK
T

BLACK
GREEN/YELLOW GREEN/
YELLOW G
BLACK
LIGHT BLUE

LIGHT
BLUE

X
BLACK
CHASSIS
(CABINET)
GROUND

RECEPTACLE

* BLUE WIRE IS CUT OFF INSIDE THE UNIT AND IS NON-FUNCTIONAL

230 V~ 4 WIRE CENTER TAPPED WIRING DIAGRAM U.S.A.

Figure 2-1
Wiring Diagrams

28

CS-200

Installation

MEASURE FLOW
EXHAUST
PNEUMATIC
INLET

DISPLAY

BALANCE

O2
40 PSI

DATA
TRANSMIT
PRINTER

BAL.

DATA
XMIT

OXYGEN
INLET

CONNECTOR
ASSEMBLY
(2-REQ'D)

PRI NT ER

OXYGEN
(35 PSI)

PNEU
40 PSI

MEASURE
EXHAUST

ALARM

ALARM

PURGE
EXHAUST

PURGE
EXHAUST

KEYBOARD

5 A CIRCUIT
BREAKER

PNEU. I NLET
40 PSI

VACUUM
CLEANER

BALANCE

PRINTER

EXTERNAL
KEYBOARD
VACUUM
CIRCUIT BREAKER
AUX POWER
BREAKER

VACUUM
CONNECTOR
230V~ - 50/60Hz
5.0 AMPS

AUX POWER
BREAKER

AC POWER

AC POWER

AC POWER

CONNECTION DIAGRAM OF INSTRUMENT WITH INTERNAL DISPLAY AND KEYPAD (DSP)

BALANCE

DATA
TRANSMIT
SERIAL
PORT A

BAL.

DATA
XMIT

PRINTER

OXYGEN
(35 PSI)

MEASURE
EXHAUST

PURGE
EXHAUST

PNEU. INLET
40 PSI

WINDOWS

ALARM

KEYBOARD

5 A CIRCUIT
BREAKER

VACUUM
CLEANER

BALANCE

AUX POWER
BREAKER

115

CONNECTION DIAGRAM OF WINDOWS INSTRUMENT (PC CONTROL)

AC POWER

NOTES: THE DESKJET PRINTER OPTION CONNECTS TO THE PC.


THE DOT MATRIX PRINTER CONNECTS TO THE INSTRUMENT
(FOR SINGLE LINE PRINTING). DATA TRANSMIT CONNECTS TO
THE PC (SECOND RS-232 SERIAL PORT). GAS CONNECTIONS
ARE THE SAME AS ABOVE.

Figure 2-2
Interconnection Diagram

Installation

CS-200

29

Instrument Voltage Selection

Note

The determinator is setup at the factory to operate from


230 V~. If the AC line voltage is different, perform the
procedure below.

POSSIBLE SHOCK HAZARD


To avoid electrical shock, make sure the AC line
cord is disconnected from facility power before
performing this procedure.

Note

210

1.

Remove the cover panel from the oscillator power supply,


located on the right side of the unit.

The gray wires referred to in step 2 are only shown as gray


in Figure 2-3, page 211. The wires may be blue or white in
the determinator. Make sure when changing the voltage
taps the correct wires are moved. If the correct wires to
move cannot be determined, contact the LECO service
department for help.

2.

Locate the voltage selection terminal strip and move the


gray voltage selection wires, and varistor terminal
connected to the gray wire, to the tap that most closely
matches the actual line voltage. Refer to Figure 2-3, page
211.

3.

Tighten the terminal strip screws and reinstall the cover


panel.

CS-200

Installation

240

220 200

COM

TERM 1
OF
K3

Figure 2-3
Voltage Selection Terminal Strip

Installation

CS-200

211

Oscillator Tube Installation


1.

Remove the RF shield side panel of the oscillator chassis,


located on the right side of the furnace. Refer to Figure 2-4
and Figure 2-5 on page 213.

2.

Install the oscillator tube.

3.

Secure the plate connector to the top of the oscillator


tube.

4.

Install the RF choke.

5.

Install the vacuum capacitor.

WARNING

ELECTRICAL SHOCK HAZARD


The capacitors on the oscillator chassis store a
lethal amount of energy and must be discharged
to avoid electric shock . Contact the LECO service
department for more information before
servicing the oscillator chassis.

WARNING

HIGH VOLTAGE HAZARD


After the power has been turned on, both the
oscillator and the furnace power supply produce
lethal voltages. Contact the LECO service
department for more information. Contact the
LECO service department for more information
before servicing the power supply.

212

6.

Replace the RF shield side panel and tighten all screws.

7.

Replace the right side panel.

CS-200

Installation

Figure 2-4
RF Shield Removal

604-010
HIGH VOLTAGE
STRAP

604-009
COIL STRAP

776-008
VACUUM
CAPACITOR

771-356
PLATE
CONNECTION

776-128
CHOKE
ASSEMBLY

771-354
OSCILLATOR
TUBE

776-129
COIL
ASSEMBLY
566-002
COIL COLLET
(2-REQ'D)

Figure 2-5
Oscillator Chassis

Installation

CS-200

213

Anhydrone Tube Packing


Removal
1.

Slide the anhydrone tube upward until the bottom end can
swing free.

2.

Tilt out the free anhydrone tube end.

3.

Pull the anhydrone tube downward off the top port.

4.

To reinstall the anhydrone tube, push the top end of the


anhydrone tube over the top port, tilt it inward and pull it
down, pushing it over the bottom port.

Packing

214

1.

Insert a screen filter into the bottom of the anhydrone


reagent tube. Refer to Figure 2-6, page 215. Position the
o-ring towards the bottom and push the screen filter up
onto the anhydrone tube 1/4 inch.

2.

Pack 2 inches of quartz wool into the bottom of the


anhydrone tube.

3.

Pour 2 inches of anhydrone onto the quartz wool and


gently tap it down. Add anhydrone as necessary to
maintain a level of 2 inches.

4.

Pack 1/2 inch of quartz wool on top of the anhydrone


leaving a 1 inch opening at the top of the anhydrone tube.

5.

Insert the reagent stop into the top of the anhydrone tube.
Push is firmly on top of the quartz wool to hold the packing
material in place.

6.

Reinstall the packed anhydrone tube into the lower left


reagent tube port blocks on the front panel.

CS-200

Installation

789-095
REAGENT STOP
765-976
O-RING
(2 REQ'D)
502-177
1/2" QUARTZ WOOL

501-171
2" ANHYDRONE

601-390
QUICK
DISCONNECT
TUBE

502-177
2" QUARTZ WOOL

775-306
SCREEN FILTER

Figure 2-6
Anhydrone Tube

Installation

CS-200

215

Incoming Reagent Tube Packing


Removal
1.

Slide each reagent tube upward until the bottom end can
swing free. Refer to Figure 2-7, page 217.

2.

Tilt out the free reagent tube end.

3.

Pull the reagent tube downward off the top port.

4.

To reinstall the reagent tube, push the top end of the


reagent tube over the top port, tilt it inward and pull it
down, pushing it over the bottom port.

Packing

216

1.

Insert a screen filter into the bottom of each reagent tube.


Position the o-ring towards the bottom and push the
screen filter up into the reagent tube 1/4 inch. Refer to
Figure 2-8, page 217.

2.

Pack 1/2 inch of quartz wool into the bottom of the reagent
tube.

3.

Pour 1 inch of anhydrone onto the quartz wool and gently


tap it down. Add anhydrone as necessary to maintain a
level of 1 inch.

4.

Pour Lecosorb onto the anhydrone until all but the top 1/2
inch of the reagent tube is filled, gently tapping it down.

5.

Firmly pack 1/2 inch of quartz wool on top of the Lecosorb


filling the bubble in the reagent tube.

6.

Reinstall the packed reagent tube into the lower left


reagent tube port blocks on the front panel.

CS-200

Installation

771-373
REAGENT
TUBE

Figure 2-7
Reagent Tube Removal

502-177
/2" QUARTZ WOOL

502-174
2" LECOSORB

771-373
QUICK DISCONNECT
TUBE
501-171
1" ANHYDRONE

502-177
/2" QUARTZ WOOL
775-306
SCREEN FILTER

Figure 2-8
Reagent Tube Packing

Installation

CS-200

217

Combustion Tube Installation

Without Autocleaner
1.

Lift the lance access door.

2.

Insert the combustion tube o-ring into the cleaning head


adapter ring. Refer to Figure 2-9, page 219.

3.

Install the combustion tube into the furnace, fitting it into


the combustion tube ring.

4.

Install the o-ring around the bottom of the combustion


tube.

5.

Install the EMI gasket into the seal on the bottom of the
combustion tube.

6.

Insert the cleaning head into the cleaning head adapter


ring and turn the cleaning head to lock it in place.

7.

Connect the measure flow and lance flow tubing to the


cleaning head. Refer to Autocleaner Assembly, Figure 2-9,
page 219, for flow tubing locations.

With Autocleaner

218

1.

Lift the lance access door.

2.

Insert the combustion tube o-ring into the autocleaner


assembly. Refer to Figure 2-10, page 220.

3.

Install the combustion tube into the furnace, fitting it into


the combustion tube ring. Refer to Figure 2-9, page 219.

4.

Install the o-ring around the bottom of the combustion


tube.

5.

Install the EMI gasket into the seal on the bottom of the
combustion tube.

6.

Insert the autocleaner assembly into the furnace. Tighten


thumbscrews. Refer to Figure 2-10, page 220.

7.

Connect the measure flow and lance flow tubing to the


autocleaner assembly. Refer to Figure 2-10, page 220.

CS-200

Installation

LANCE FLOW
CONNECTION

781-420
CLEANING
HEAD

MEASURE FLOW
CONNECTION

(SHOW UPSIDE DOWN


TO VIEW O-RING)

772-905
COMBUSTION
TUBE
762-058
O-RING

772-906
COMBUSTION
TUBE RING

781-401
CLEANING HEAD
ADAPTER RING

789-149
EMI GASKET
(GASKET TO GO
AROUND OUTER
DIAMETER OF O-RING)

601-920
O-RING

605-816
PEDESTAL

Figure 2-9
Combustion Tube InstallationWithout Autocleaner

Installation

CS-200

219

604-291
AIR CYLINDER

604-272
CAP

604-268
BODY ASSEMBLY

772-905
COMBUSTION
TUBE

(SHOWN UPSIDE DOWN


TO VIEW O-RINGS)

609-626
AUTOCLEANER
ASSEMBLY

752-058
O-RING

604-172
O-RING

773-926
PLATE

190-090
THUMBSCREWS
(2 REQ'D)

773-320
O-RING
(2 REQ'D)

789-149
EMI GASKET
(GASKET TO GO
AROUND OUTER
DIAMETER OF O-RING)
601-920
O-RING

605-816
PEDESTAL

Figure 2-10
Combustion Tube InstallationWith Autocleaner

220

CS-200

Installation

Gas Connections

Note

Refer to Figure 2-2 on page 29 for more information

1.

Remove the cap plugs from the fittings on the back panel.

2.

Fasten the connector attached to the oxygen supply line to


the regulator on the oxygen supply.

3.

Attach the connector on the other end of the supply line to


the OXY INLET connector on the rear panel of the unit.

!
POSSIBLE MACHINE DAMAGE
Oxygen is not recommended for use in the
pneumatic systems of LECO instruments.

Installation

4.

Fasten the connector attached to the pneumatic supply


line to the regulator on the pneumatic supply.

5.

Attach the other end of the connector to the PNEU INLET


connector on the rear panel or the unit.

CS-200

221

Computer Installation

Windows

222

This procedure should only be used if the instrument was


purchased with a computer.

1.

Install the Computer System. Refer to the manual supplied


with the computer.

2.

Connect one end of the Computer Interface Cable to the


data transmit connector on the instrument. Refer to
Figure 2-2, page 29.

3.

Connect the other end of the Computer Interface Cable to


the serial interface connector COM 1 on the computer.

4.

Connect the Video Cable from the monitor to the monitor


connector on the rear of the computer.

5.

Connect the cables from the keyboard and mouse to the


computer.

6.

If an optional Ink Jet Printer was purchased with the


instrument connect the printer cable to the printer port on
the rear of the computer. If may be necessary to install
the printer software on the computer. Wait until the
complete system is installed and then follow the
instructions supplied with the printer to install it.

7.

Connect the AC power cables from the computer, monitor,


balance and printer to facility AC power. DO NOT turn the
computer on until instructed to do so.

CS-200

Installation

Pedestal Installation

Without Autocleaner
1.

Install the pedestal adapter onto the lower seal assembly,


see Figure 2-11 below). The pedestal adapter should only
be hand-tightened.

2.

Set the pedestal onto the pedestal adapter. The crucible


will rest on the pedestal.

605-816
PEDESTAL

605-814
PEDESTAL
ADAPTER
ASSEMBLY

783-675
LOWER SEAL
ASSEMBLY

Figure 2-11
Pedestal InstallationWithout Autocleaner

Installation

CS-200

223

With Autocleaner
1.

Install the pedestal adapter onto the lower seal assembly,


see Figure 2-12 below). The pedestal adapter should only
be hand-tightened.

2.

Set the pedestal onto the pedestal adapter. The crucible


will rest on the pedestal.

605-816
PEDESTAL

605-814
PEDESTAL
ADAPTER
ASSEMBLY

781-412
BARB FITTING

789-430
LOWER SEAL
ASSEMBLY

760-215
ELBOW

Figure 2-12
Pedestal InstallationWith Autocleaner

224

CS-200

Installation

Option Installation
3 Option Installation

Illustrations .......................................................................32
Balance Installation ............................................................33
Balance Interfacing ........................................................ 34
Resetting the Balance .................................................... 35
Setting the Data Output Parameter .................................. 35
Dot Matrix Printer (601-480-110) .........................................37
Printer Settings ........................................................... 310
Deskjet (Inkjet) Printer (611-499-110)................................ 311
Installation of Optional Kits for the Autocleaner .................... 312
Autocleaner ................................................................ 312
Dust Removal Kit......................................................... 312
Vacuum Cleaner Kit ..................................................... 312

System Setup

CS-200

31

Illustrations
Figure 3-1 ......... Balance Control Panel................................. 36
Figure 3-2 ......... Balance Assembly ...................................... 36
Figure 3-3 ......... Ribbon Cartridge Installation ....................... 39
Figure 3-4 ......... Paper Installation....................................... 39

32

CS-200

Option Installation

Balance Installation
Refer to the Balance Options on page 423 or the Balance Tab
on 462, to set the balance option parameters and configure
the determinator to recognize the balance. If the balance and
determinator are not programmed with the same configuration
parameter values, no weights may be transferred.
The determinator will default to the correct parameter values to
operate with the balance. If the balance does not operate
properly with the determinator, verify the balance options
parameter values set from the determinator. The correct
parameter values are shown on pages 423 and 462.

Notes

System Setup

To insure proper balance operation, balance interfacing,


resetting the balance and setting the data output parameter
procedures, beginning on the next page, must be
performed.

The following information is for the LECO four-place


balance. If another balance is used, follow the instructions
provided with the balance.

CS-200

33

Balance Interfacing

34

1.

Unpack the balance and assemble it as shown in the


balance operation manual.

2.

Plug the AC adapter, supplied with the balance, into facility


power. Connect the AC adapter cable to the power input
jack on the rear of the balance. Refer to Figure 2-2, page
29.

3.

Adjust the balance feet to level the balance. The level


bubble should be inside the circle when the balance is
level. The level bubble is located on the rear of the
balance.

4.

Locate the balance connector on the rear panel of the


determinator and connect one end of the balance interface
cable to the balance connector. Connect the other end of
the cable to the rear of the balance. Refer to Figure 2-2,
page 29.

5.

To properly interface the balance with the determinator,


perform the Resetting the Balance procedure, page 35,
to reset the balance to the factory defaults.

6.

After the balance is reset, do not change any of the


configuration codes except the one shown in this manual.
The balance codes can be changed to custom configure the
balance, if desired, after this procedure is completed.

CS-200

Option Installation

Resetting the Balance


1.

Remove the hole plug on the lower front right corner of


the balance and move the menu access switch to the right.
Refer to Figure 3-2, page 36.

2.

Turn the AC power on to the balance by pushing the power


on button, Figure 3-1, page 36. As soon as all the
segments on the display light up, push the Tare button.
The display will be blank for a few seconds and then
display the menu code settings.

3.

Press F1 to display 9 in the left digit.

4.

Press Print to skip the center digit.

5.

Press F1 to display 1 as the right digit.

6.

Press Tare.

7.

Press CF.

8.

Turn the AC power off to the balance.

Setting the Data Output Parameter


1.

Set the data output parameter to "Auto print regardless of


stability" code 614 using this procedure.

2.

Turn the AC power on to the balance by pushing the power


on button. As soon as all segments on the display light up,
push the Tare button. The display will be blank for a few
seconds and then display the menu code settings.

3.

Press F1 to display 6 in the left digit.

4.

Press Print to display the center digit.

5.

Press F1 to display 1 as the center digit.

6.

Press Print to display the right digit.

7.

Press F1 to display 4 as the right digit.

8.

Press Tare.

9.

Press CF.

10. Reposition the menu access switch to the left and reinstall
the hole plug.

System Setup

CS-200

35

TOGGLE

POWER ON
CLEAR
FUNCTION

I/O

F1

CF

INFORMATION

TARE

TARE

TARE
PRINT

F2

Figure 3-1
Balance Control Panel

MENU ACCESS
SWITCH

Figure 3-2
Balance Assembly

36

CS-200

Option Installation

Dot Matrix Printer (601-480-110)

Notes

Notes

Refer to Figure 3-3 and Figure 3-4 on page 39 when


following these procedures.

The optional Dot Matrix Printer is used with the DSP and
Windows instruments. DSP all printing and Windows line
printing.

1.

Unpack the printer. Locate the separate printer manual in


the printer box and check the contents of the box against
the manual list.

2.

Remove any tape, bags, or styrofoam from the printer.


Remove the platen knob from the styrofoam before
discarding.

3.

Remove the shipping retainer located inside the printer


(save it in case the printer needs to be shipped).

4.

Install the platen knob by inserting the shaft into the hole
in the right side of the printer. Match the flat side of the
knob to the flat side of the platen shaft.

After extended periods of printing, allow time for the


printhead to cool before touching it.

Turn off the power before moving the printhead.

5.

6.

Install the ribbon cartridge.


A.

Open the access cover.

B.

Position the printhead between bail rollers and push


the bail lever back.

C.

Place the flat end of the ribbon cartridge, knob facing


up, into the ribbon plate, then lower the other end
over the printhead and snap it into place.

D.

Turn the knob clockwise to take up ribbon slack.

E.

The headgap lever can be adjusted for one or two


part forms (position 1), three or four part forms
(position 2), or envelopes, and extra-thick paper
(position 3).

Install the paper separator.


A.

System Setup

Lift the rear cover.

CS-200

37

B.

Hold the legs against the separator and place the


separator tabs over the studs on the sides of the rear
cover.

C.

Close the rear cover.

7.

Set the printer next to the determinator and the paper


tray behind the printer.

8.

Attach the printer power cord to the printer. Connect the


other end to the facility power source.

9.

The printer should be off.

10. Connect the printer interface cable to the printer and the
back of the determinator.
11. Install the paper.

Note

A.

Move the paper lever and bail lever forward.

B.

Open the access and rear covers and feed the paper
under the rear cover.

C.

Open the tractor covers and align the track feed holes
on the paper with the tractor pins. Close the tractors.

D.

Turn the platen knob to feed the paper around the


platen. Be sure the paper feeds underneath the black
tabs in front of the tractors.

E.

To adjust the tractors:


1)

Lift the lock levers on both sides.

2)

Slide the tractors into position. Reference marks


on the printer show the recommended left edge
position for the two most common paper sizes.

Do not place the left edge of the paper more than 1/2 inch
from the end of the platen or the printer will signal a paper
out alarm.

12. Close the rear cover and lay the paper separator flat.
13. Open the guide wire to stop paper from curling back into
the printer.
14. Close the access cover.
15. Paper can be fed from the bottom if the printer is placed
on a stand. Refer to the printer manual for details.
16. The control panel of the printer is used to configure the
printer and its corresponding features. Refer to the
operation section of the printer manual. The Printer Settings
can be found on page 310.

38

CS-200

Option Installation

RIBBON
CARTRIDGE

TAKE-UP
KNOB

RIBBON
PLATE

RIBBON SHIELD
DO NOT REMOVE

Figure 3-3
Ribbon Cartridge Installation

ACCESS
COVER

BAIL
LEVER

TRACTOR
COVER

LOCK
LEVER

GUIDE
WIRE

PAPER
SEPARATOR

PAPER
LEVER
TRACK FEED
HOLES
PAPER
PLATEN
KNOB

PINS
STUD
ON/OFF
SWITCH
SEPARATOR
TAB

REAR
COVER

Figure 3-4
Paper Installation

System Setup

CS-200

39

Printer Settings
Group
Font

Item
Print Mode
Pitch
Style
Size

Settings
Utility
10 CPI
Normal
Single

General Control

Emulation Mode
Graphics
Paper Out Override
Print Registration
Operator Panel Functions
Reset Inhibit
Print Suppress Effective
CPU Compensation

Epson FXe
Bi-directional
No
O
Full Operation
No
Yes
Standard

Vertical Control

Line Spacing
Form Tear-Off
Skip-Over Perforation
Auto LF
Auto CR
Auto Feed XT
Page Length

6 LPI
Off
No
No
No
Invalid
11 inches

Symbol Sets

Character Set
Language Set
Zero Character

Set I
American
Slashed

Serial I/F Option

Parity
Serial Data 7 or 8 Bits
Protocol
Diagnostic Test
Busy Line
Baud Rate
DSR Signal
DTR Signal
Busy Time

None
8
Ready/Busy
No
SSD9600 BPS
Valid
Ready on Power Up
200 Milliseconds

Note

310

To restore the menu to its original factory settings, turn the


printer off, hold down the Sel and Mode buttons, then turn
the printer on again.

CS-200

Option Installation

Deskjet (Inkjet) Printer (611-499-110)

Notes

System Setup

The optional Deskjet Printer is only used with the Windows


controlled instrument. It connects directly to the PC. Refer
to the Figure 2-2 on page 29.

To install the Deskjet Printer refer to the Installation Manual


supplied with the printer.

CS-200

311

Installation of Optional Kits for the Autocleaner

Autocleaner

Notes

For part number and ordering information, refer to Options


on page 134.

Follow instructions provided in the kit for current installation


instructions.

!
CAUTION

For the autocleaner kit to function properly, the


Dust Removal Kit, page 312, must be installed.

Dust Removal Kit

Notes

For part number and ordering information, refer to Options


on page 134.

Follow instructions provided in the kit for current installation


instructions.

The instructions are applicable for the dust removal kit as


well as the autocleaner/dust removal kit.

Vacuum Cleaner Kit

Notes

312

For part number and ordering information, refer to Options


on page 134.

Follow instructions provided in the kit for current installation


instructions.

CS-200

Option Installation

System Setup

Windows

Keypad

Keypad

4 System Setup

For instruments using Windows software refer to the


instructions listed on page 438.

For instruments using DSP software refer to the instructions


listed below.

Illustrations .......................................................................44
Controls and Indicators .......................................................46
Menu Organization Chart .....................................................48
Power-Up ........................................................................ 410
About the Examples ..................................................... 410
Menus........................................................................ 410
Keypad ...................................................................... 411
Using the Keypad ................................................... 412
Notices and Errors ....................................................... 413
Confirmation............................................................... 414
Copyright Screen......................................................... 414
System Overview ............................................................. 415
Main Menu Overview .................................................... 415
System Check .................................................................. 416
Ambient Monitor.......................................................... 416
System Setup .................................................................. 418
System Options........................................................... 419

System Setup

CS-200

41

Definitions, Ranges, and Defaults.............................. 420


Transmit Options ......................................................... 421
Definitions, Ranges, and Defaults.............................. 422
Balance Options .......................................................... 423
Definitions and Selections ........................................ 425
System Clock .............................................................. 426
Set Barometer ............................................................ 427
Combustion Pressure ................................................... 428
Quick Access Menu ...................................................... 429
Operation .............................................................. 429
Defining ................................................................ 430
Change Password ........................................................ 431
Analysis Method Menu....................................................... 432
Definitions, Ranges, and Defaults................................... 434
Data Transmit.................................................................. 435
Data Transmit Format .................................................. 437
System Setup for Windows .............................................. 438
Windows

Illustrations ..................................................................... 441


Controls and Indicators ..................................................... 442
Automatically Transmit Analysis Results............................... 444
Configure Maintenance Counters......................................... 446
Maintenance Counter Definitions.................................... 447
Configure the Analysis Report ............................................ 448
Select the Fields ..................................................... 449
Select the Font....................................................... 449
Configure the Plot................................................... 449
Line Printing .......................................................... 449
Configure the Screen ........................................................ 450
Tool Bar ..................................................................... 450
Status Bar .................................................................. 450
Configure the Spreadsheet................................................. 451
Configure Plot Definitions.............................................. 452
Method Development ........................................................ 453
Method Parameter Definitions........................................ 455

42

CS-200

System Setup

Sample Templates ............................................................ 456


Create a Sample Template ............................................ 456
Standards ....................................................................... 457
Standards Definitions ................................................... 458
System Configuration........................................................ 459
System Configuration Definitions ................................... 460
System Tab ........................................................... 460
Serial Port Tab ....................................................... 461
Balance Tab ........................................................... 462
Balance Definitions ................................................. 463
Set Barometric Pressure .................................................... 464
Transmission Formats ....................................................... 465
Define Fields ............................................................... 465
Define Delimiters......................................................... 467
Preview Transmitted Data.................................................. 469
Select Language............................................................... 471
Users.............................................................................. 472
Add a User ................................................................. 472
Add Password ............................................................. 473
Assign User Functions .................................................. 474

System Setup

CS-200

43

Illustrations
Figure 41......... Controls and Indicators with Autocleaner....... 47
Figure 42......... Keypad and Display Screen ......................... 411
Figure 43......... Combustion Pressure Adjustment Knob ......... 428
Figure 4-4 ......... Controls and Indicators............................... 443

44

CS-200

System Setup

This page intentionally left blank.

System Setup

CS-200

45

Controls and Indicators

Note

Refer to Figure 41 on page 47, for locations of the items


listed below.

Determinator Power On/Off SwitchSwitches power on and off


to the determinator. Also acts as a circuit breaker on the
incoming facility line power.
Measure Flow RotameterIndicates the oxygen flow rate in lpm
(liters per minute). Nominal indication is 3.0 lpm.
KeypadThe keypad is used as a communications link between
the operator and the determinator. Operation of the
determinator is controlled from the keypad.
Display ScreenThe display screen provides a visual link
between the operator and determinator.
BrightnessThe brightness control, on top of unit, adjusts the
brightness of the display screen. This control should be
adjusted by the operator for the amount of brightness desired.
ContrastThe contrast control, on top of unit, adjusts the
contrast of the display screen. This control should be adjusted
by the operator for the best display contrast and is usually
adjusted after the brightness control has been properly set.
Printer (not shown)The printer is used to print out analysis
data, information presented on the display, and buffer or
screen plots.
Furnace Power On/Off SwitchSwitches power on and off to
the furnace. Also acts as a circuit breaker on the incoming
facility line power.
Power Lever AdjustmentControls oscillator maximum power
output by adjusting the plate current for approximately 100 mA
(idling current) to 500 mA (full power). The overload protection
is reset by turning the adjustment fully counterclockwise until it
clicks and then turning it clockwise.
Vacuum Cleaner On/Off SwitchTurns the optional vacuum
cleaner on or off. The vacuum cleaner can be used to clear
dust and debris from the combustion area and furnace shelf.
Piston Up/Down SwitchThis switch controls the movement of
the piston, either up or down. During operation, the piston
raises the crucible and sample into the furnace for analysis.
This switch is also used to control the piston during furnace
cleaning.

46

CS-200

System Setup

AUTOCLEANER
ASSEMBLY
ACCESS DOOR

CONTRAST
CONTROL

BRIGHTNESS
CONTROL
INCOMING
REAGENT
TUBE
DISPLAY
SCREEN
KEYPAD

782-603
VACUUM
HOSE

CATALYST
HEATER
ASSEMBLY

604-126
DUST BOX
ANHYDRONE
TUBE
MEASURE
FLOW
ROTAMETER

ANALYZER
AC POWER
ON/OFF
SWITCH
CELLULOSE
FILTER

POWER LEVEL
ADJUSTMENT

FURNACE
AC POWER
ON/OFF
SWITCH

VACUUM
CLEANER
ON/OFF
SWITCH

PISTON
UP/DOWN
SWITCH

772-960
CRUCIBLE BOX
WITH LINER

789-230
VACUUM CLEANER

Figure 41
Controls and Indicators with Autocleaner

System Setup

CS-200

47

Menu Organization Chart


[1] Analyze

[1] Delete Weights


[2] Insert Weight
[3] Print Weights
[4] System Controls

[1] Print

[5] Clean Switch


[6] Balance Weight
[7] Transmit Last
[2] Results

[1] Record Format


[2] List Format
[3] Clear Selections
[4] Delete
[5] Statistics

[1] Print

[6] Print
[7] Transmit
[3] Calibration

[1] Record Format


[2] List Format
[3] Clear Selections
[4] Calculate Calib

[1] Print
[2] Reset Calib

[5] Edit Calibration

[1] Print

[6] Calculate Blank

[1] Print

[7] Edit Blank

[1] Print

[8] Recalculate

[1] Re-Calc. Todays


[2] Re-Calc. Select

48

CS-200

System Setup

[4] Set-Up

[1] Analysis Method

[1] Print
[2] Select Method

[1] 1-Method
[2] 2-Method
[3] 3-Method
[4] 4-Method
[5] 5-Method

[3] Copy Method To


[2] System Options

[1] Print

[3] Transmit Options

[1] Print

[4] Balance Option

[1] Print
[2] Test Balance
[3] Test Tare

[5] System Clock


[6] Set Barometer

[1] Print

[9] More

[1] Quick Option Menu


[2] Linearization
[3] Change Password

[5] Diagnostics

[1] Ambient Monitor

[1] Display Units


[2] Display Volts
[3] Print

[2] Switches
[3] Valves
[4] Leak Check

[1] Entire System


[2] Bypass Furnace

[5] Print Buffer


[6] Plot Buffer

[1] Print

[7] System Print


[8] Reset Memory

System Setup

CS-200

49

Power-Up
1.

The power switches for both the determinator and furnace


should be set to the off positions.

2.

Connect the determinator to a proper electrical power


source.

3.

Turn on the gas supplies and set the oxygen pressure to


40 psi and the pneumatic pressure to 40 psi.

4.

Turn the determinator and furnace power switches on.

5.

After a short delay, the main menu should appear on the


display screen.

6.

Turn the gas ON. Refer to the System Controls procedure,


page 516.

7.

Allow the determinator to warm-up for one hour before


performing a system check or sample analysis.

About the Examples


The numbers used for the screen examples in this manual are
only to illustrate operation and may or may not be applicable to
specific procedures.

Menus
When pressing the menu key, a menu will appear displaying
different choices. When a menu appears, only options within
the menu are selectable. To remove a menu from the display
screen, press exit.

410

CS-200

System Setup

Keypad
The keypad used on the determinator is a matrix of switches,
referred to as keys, which must be pressed to activate a
selection, see Figure 42, below. This type of keypad is referred
to as a 'membrane keypad'. When activating a selection, press
the middle of the key until the microcomputer and display
screen recognize the selection.

PREVIOUS

NEXT

SELECT

MENU

ABC

DEF

GHI

JKL

MNO

PQR

STU

VWX

YZ

NO

YES
+

.% #,

RESET

DEL

EXIT

START

Figure 42
Keypad

System Setup

CS-200

411

Using the Keypad


NextMoves the cursor to the next sample. When the analyze
screen is displayed, it is used to select a sample from the
sample weight list. When the calibrate and results screens are
displayed, it is used to select sample results. It is also used to
move the cursor to the next line when editing.
PreviousMoves the cursor to the previous sample. A beep will
sound when the cursor cannot be advanced further. When the
analyze screen is displayed, previous is used to select a sample
from the sample weight list. When the calibrate and results
screens are displayed, it is used to select sample results and
also used for editing.
SelectMoves the cursor to the next selection within a menu or
screen. Permits the operator to scroll through selections and
select sample results. Acts as an enter key to advance to the
next line.
MenuDisplays a menu of selections available for the current
screen.
ResetStops an analysis in progress. The operator is permitted
to abort, reset, or continue.
StartIn the manual mode, after a weight has been entered
and the furnace closed, press start to begin analysis of a
sample. In the automatic mode, closing the furnace causes
analysis to begin.
DELUsed to delete a character at the cursor's position. When
no more characters are left to delete, a beep will sound.
ExitUsed to remove a menu or screen and return to the
previous menu or screen.
Left/Right Arrow KeysUsed to move the cursor one position
to the left or right. Refer to the Number/Letter Keys definition
below.
Yes/NoUsed to select a result. These keys are used to include
(yes) or exclude (no) a sample. They are also used to enable or
disable a menu option, respond to a confirmation screen, and
permit the user to scroll through selections.
1STU, 2VWX, 3YZ, 4JKL, 5MNO, 6PQR, 7ABC, 8DEF, 9GHI,
0SymbolThese keys are used to enter data during operation
or editing, select a procedure, or select a menu option. By
repeatedly pressing the key, the operator is permitted selection
of the number or letter shown on the key. Use the left/right
arrow keys to move the cursor and continue entering or
editing data.

412

CS-200

System Setup

Notices and Errors


A notice or error is a message that appears on the display
screen that warns the operator of a condition that could yield
an incorrect result. Notices or errors may be caused by
operator error or component failure. Operator problems are
most likely to occur after a manual procedure or a change in
the setup, method, or system control parameters. If a notice or
error occurs, refer to page 1022 for corrective action.

System Setup

CS-200

413

Confirmation
Any operation that can cause information to be deleted will
display a confirmation box. Press yes to confirm the operation
or no to abort the delete command.

Copyright Screen
Upon power-up and exit from the main menu, the copyright
screen will be displayed. When this screen is displayed, wait a
few seconds, the screen will disappear and the main menu will
appear in its place.

414

CS-200

System Setup

System Overview

Main Menu Overview


LECO CS-200
V 2.xx
Carbon/Sulfur Determinator
[1]
[2]
[3]
[4]
[5]

Analyze
Results
Calibrate
Setup
Diagnostics

HeadlineAfter power-up, the main menu appears and displays


the headline. The headline contains the model number of the
determinator, the software version installed, and the type of
determinator. It is important to note the version of software
when contacting the LECO Corporation.
Center WindowDuring operation, display screens and menus
will appear in the center window. When the determinator is
powered up, the main menu appears providing the operator
with five selections, [1] Analyze, [2] Results, [3] Calibrate, [4]
Setup, and [5] Diagnostics. The number in brackets refers to
the key number to press on the keypad. When making a
selection from the main menu, a screen or menu will always
appear. For more information concerning the main menu
selections, refer to the Setup and Operation chapters.
Bottom LineThe information on this line will appear under a
menu or screen. During analysis, the bottom line will display
the weight list. During setup and system configuration, this line
will display the range and/or selections available. When the
main menu is displayed, this line is blank.

System Setup

CS-200

415

System Check

Notes

All steps in the installation and initial power-up sections


must be completed before performing these procedures.

The gas supplies must be on, the oxygen regulator set to 40


psi and the pneumatic regulator set to 40 psi.

The determinator AC power must be on.

Ambient Monitor

Notes

The ambient monitor is used to display system parameters


during operation or servicing of the determinator.

If the determinator has just been turned on, wait one hour
before checking the ambient monitor for the system to
stabilize.

1.

The ambient monitor is accessed from the diagnostics


menu. From the main menu, press [5] Diagnostics.

2.

Press [1] Ambient Monitor to display the ambient monitor.


Ambient Monitor

Carbon IR Cell
Sulfur IR Cell
Oven Temp
Catalyst Heater
System Pressure
Plate Current
Grid Current

Note

416

8.500 v
8.500 v
48oC
350oC
762 mm
480 mA
100 mA

The ambient monitor will continuously update as the


operator views it.

CS-200

System Setup

3.

Check that all system parameters, temperatures and


voltages fall within the range limits shown below. If any
values are out of range refer to the setup, operation or
service sections for correction procedures.
Nominal Value

Range

Units

Carbon IR Cell

Parameters

8.5

7.5 to 9.2

Sulfur IR Cell

8.5

7.5 to 9.2

Oven Temp

48

46 to 50

Catalyst Heater

350

325 to 357

System Pressure

762

740 to 790

Plate Current

460*

420 to 500

mA

Grid Current

100*

80 to 120

mA

V
C
C

mmHg

* Nominal values during analysis only. When furnace power is off, the
plate and grid current should be zero.

4.

Press Select to toggle the displayed parameters between


voltages and units.

5.

Press Menu to display the ambient monitor menu.


Ambient Monitor

[1] Display Units


[2] Display Voltages
[3] Print

System Setup

6.

Press [1] Display Units to display the system parameters


in voltages, temperatures and pressure.

7.

Press [2] Display Voltages to display the a/d output


voltages.

8.

Press [3] Print to create a hardcopy printout of the


ambient monitor parameters.

9.

Press Exit to remove the ambient monitor menu and


display the ambient monitor screen.

CS-200

417

System Setup

Notes

The following procedures are all located under the system


setup menu. To access this menu, press [4] Setup from the
main menu.

Analysis method is described in the Operation and


Diagnostics chapters.
Setup
[1]
[2]
[3]
[4]
[5]
[6]
[9]

418

Analysis Method
System Options
Transmit Options
Balance Options
System Clock
Set Barometer
More

CS-200

System Setup

System Options

Note

1.

This procedure allows the operator to set the system


operating conditions used for analysis.
Access the system options screen by choosing [2] System
Options from the setup menu.
System Options
Gas Conservation (min)
Gas Conservation Mode
Catalyst Heater (DegC)
Enable Auto Cleaner
Enable Door Option
Result Format
Blank Lines
Date Format
Pressure Control

15
Con
350
No
No
Short
1
MM-DD-YY
Yes

2.

Press Select to scroll through the system option


parameters. Refer to Definitions, Ranges, and Defaults on
page 420.

3.

Enter the value from the keypad or press the right or left
arrow keys to move the cursor into position to change a
value.

4.

Press Menu to display the system option menu.


System Options

[1] Print

System Setup

5.

Press [1] Print to receive a printout of the system option


parameters on the system printer.

6.

Press Exit to exit the system option menu and return to


the system option screen.

CS-200

419

Definitions, Ranges, and Defaults


Gas Conservation (Min)The time in minutes, after analysis,
when the determinator automatically switches to the gas
conservation mode. Range: 0 to 600 minutes, Default: 15
minutes
Gas Conservation ModeThe oxygen flow settings used as gas
conservation. Normal oxygen flow is 3 liters per minute.
Conservation mode changes the oxygen flow to 1 liter per
minute. Off turns the oxygen flow completely off. Settings: Off
or Con. Default: Con
Catalyst Heater TemperatureThe set operating temperature of
the catalyst heater. Range 0 to 900oC, Default 350oC
Enable Auto CleanerSelects operation of the optional
autocleaner. Select yes if the autocleaner is installed, or no if
the autocleaner is not installed. Default: No
Enable Door OptionSelects operation of the optional
combustion system cleaning door. Select yes if the cleaning
door is installed, or no if the cleaning door is not installed.
Refer to Dust Removal Kit on page 312. Default: No
Results FormatSelects the desired answer format. Short
format prints time, date, sample weight, and result. Long
format prints time, date, sample weight, result, calibration,
blank, time, and peak. Table format prints the long format
parameters in tabular form. Default: Long
# Blank LinesThe number of blank lines between analysis
results printed on the system printer. Range: 0 to 2 lines.
Default: 0
Date FormatSelects the date format displayed on the display
screen and printer on the system printer. Selections: MM-DDYY (Month-Day-Year), or DD-MM-YY (Day-Month-Year).
Default: MM-DD-YY
Pressure ControlThis parameter is set by the operator and
determined by the hardware installed in the determinator. If
the determinator has the electronic barometric pressure control
installed, select yes. If the determinator does not have the
electronic barometric pressure control installed, select no.

420

CS-200

System Setup

Transmit Options

Note

This procedure configures the determinator for


communications with a data transmit peripheral.
Transmit Options
Enable
Field Separator
Record Separator
Head/Tail
Baud Rate
Parity
Data Bits
Stop Bits

Yes
Comma
CRLF
SOH/EOT
9600
None
8
1

Option:

Yes

Yes/No

1.

Access transmit options by choosing [3] Transmit Options


from the setup menu.

2.

Press Select to move the cursor to the next line. Refer to


Definitions, Ranges, and Defaults on page 422.

3.

Press No to scroll through the transmit options


parameters.

4.

Press Yes to affirm the selection and move the cursor


down one line.

5.

Press Menu to display the transmit options menu.


Transmit Options

[1] Print

System Setup

6.

Press [1] Print to receive a printout of the transmit option


parameters on the system printer.

7.

Press Exit to remove the transmit options menu.

CS-200

421

Definitions, Ranges, and Defaults


EnableEnables or disables data transmit operation. Select
yes to enable data transmit, or no to disable data transmit.
Default: No
Field SeparatorSelects the data character used to separate
fields of data. Selections: Comma, Space, or FS (field
separator). Default: Comma
Record SeparatorSelects the data character(s) used to
separate records of data. Selections: CRLF (carriage return and
line feed), CR (carriage return), LF (line feed), or RS (record
separator). Default: CRLF
Head/TailDetermines the data character(s) used to start and
end the frame of data sent during data transmit. Selections:
None, SOH/EOH, or CTRL Z. Refer to the Data Transmit section
on page 435. Default: SOH/EOH
NoneNo starting or ending data character.
SOH/EOHStarting data character is 01 (hex), start of
header, and the ending data character is 04 (hex), end
of header.
CTRL ZNo starting data character. Ending data
character is 01A (hex).
Baud RateSets the data transmission speed in bits per
second. Selections: 1200, 2400, 4800, and 9600 bps.
Default: 9600
ParitySets the method of error checking used. Selections:
Even, Odd, or None. Default: Even
Data BitsUsed to select the number of bits per byte for data
that will be transmitted. Selections: 5 to 8. Default: 8
Stop BitsUsed to select the number of bits that are used to
signal the end of a transmitted data byte. Selections: 1 or 2.
Default: 1

422

CS-200

System Setup

Balance Options

Notes

This procedure configures the determinator for use with an


external balance.

The balance options parameters must match the


configuration of the balance. Refer to Setting the Data
Output Parameter, page 35.
Balance Options
Readability
Weight Entry
Tare Command
Baud Rate
Parity
Data Bits
Stop Bits

4
Auto Tare
Esc T
1200
Odd
7
1

Option:

Yes

Yes/No

1.

Access balance options by choosing [4] Balance Options


from the setup menu.

2.

Press Select to move the cursor to the next line. Refer to


Definitions and Selections on page 425.

3.

Pressing No scrolls through the accepted balance options


parameters (except for readability). Enter the desired
number for the readability parameter.)

4.

Press Yes to move the cursor down one line.

5.

Press Menu to display the balance options menu.


Balance Option

[1] Print
[2] Test Balance
[3] Test Tare

System Setup

CS-200

423

6.

Press [1] Print to receive a printout of the balance option


parameters on the system printer.

7.

Press [2] Test Balance to determine if the interfaced


balance will communicate with the determinator. The test
balance screen will be displayed.
Test Balance

Weight String From Balance


0.000g

Any Key to Continue

8.

The weight displayed on the balance should be displayed


on the test balance screen. If the display is not correct,
recheck the balance options parameters and balance
programming.

9.

Press any key to return to the balance options.

10. Press [3] Test Tare to determine if the determinator can


tare the interfaced balance. The weight displayed on the
balance should indicate zero. If the display is not correct,
recheck the balance options parameters and balance
programming.
11. Press Exit to escape the balance option menu and return
to the setup menu.

424

CS-200

System Setup

Definitions and Selections


ReadabilityThe number of significant places to the right of the
decimal point transferred from the balance to the determinator
during sample weight entry. Range: 3 to 5. Default: 4.
Weight EntrySelections are Remote (weight is entered from
the balance), Normal (weight is entered from the
determinator), Auto Tare (automatic tare for weights over 15 g,
weight is entered from the determinator), or None (manual
weight entry only). Refer to Sample Weight Entry, page 523.
Default: None
Tare CommandThe command from the determinator that the
balance reads to Tare. Selections are 'T', 'ESC T', or 'T, CR, LF'.
For LECO supplied balances, set the command to 'T, CR, LF'.
Baud RateSets the data transmission speed in bits per
second. Selections: 1200, 2400, 4800, and 9600 bps. For LECO
supplied balances, set baud rate to 1200 bps.
ParitySets the method of error checking used. Selections:
Even, Odd, or None. For LECO supplied balances, set parity to
Odd.
Data BitsUsed to select the number of bits per byte for data
that will be transmitted. Selections: 5 to 8. For LECO supplied
balances, set data bits to 7.
Stop BitsUsed to select the number of bits that are used to
signal the end of a transmitted data byte. Selections: 1 or 2.
For LECO supplied balances, set stop bits to 1.

System Setup

CS-200

425

System Clock

Notes

The system clock procedure permits the operator to set the


determinator's internal real-time clock.

The feasibility of the entered time and date are checked


before the operator is allowed to exit this procedure.
System Clock

Enter Time

426

HH:MM:SS

10:24:39

Enter Date
MM-DD-YY

01-01-00

1.

Access the system clock procedure by choosing [5]


System Clock from the setup menu. The enter time
prompt will appear on the screen.

2.

Press the left or right arrow keys to move the cursor into
position to set the time or press Select to set the date. The
enter date prompt will appear below the time.

3.

If the time was set in step 2, press Select to move the


cursor into position to set the date. The enter date prompt
will appear below the time.

4.

After setting the time and/or date, press Exit to return to


the main menu.

CS-200

System Setup

Set Barometer

Note

1.

The local barometric pressure must be known before the


barometric pressure can be set.
Access the set barometric pressure procedure by choosing
[6] Set Barometer from the setup menu.
Set Barometer

Pressure is Stabilizing
740 mm Hg

2.

In a short period of time the screen will change and the


Set Barometer

Pressure (mm/Hg)

743

barometric pressure value will be highlighted.

System Setup

3.

Press the right or left arrow keys to move the cursor into
position and change the barometric pressure to the correct
value with the number keys.

4.

Press Menu to display the barometric pressure menu.

5.

Press [1] Print to receive a printout of the edited


barometric pressure on the system printer.

6.

Press Exit to return to the setup menu.

CS-200

427

Combustion Pressure

Note

The Set Barometer procedure, page 427, should be


completed before the combustion pressure is set.

1.

Remove the left side panel of the determinator.

2.

From the Main menu, press [1] Analyze then Menu to


display the analysis menu.

3.

Press [4] System Controls. Set carrier gas to on.

4.

Adjust the pressure regulator for 12 psi as shown on the


pressure gauge, see Figure 43, below.

5.

After this procedure is completed, replace the left side


panel.

ADJUSTMENT
KNOB

PRESSURE
REGULATOR

Figure 43
Combustion Pressure Adjustment Knob

428

CS-200

System Setup

Quick Access Menu


The quick access menu is a list of user-defined selections that
can be programmed by the operator. By defining and using the
quick access menu, the instrument will be both faster and
easier to use.

Operation
1.

From the main menu, press Menu. The quick access menu
will be displayed.
Quick Menu
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]
[9]

System Setup

Analyze
Results
Calibrate
Analysis Method
Set Barometer
Leak Check
Print Buffer
Plot Buffer
Ambient Monitor

2.

Press the number on the keypad to the left of the desired


selection. The determinator will immediately display the
menu selection.

3.

To return to the main menu, press Exit.

CS-200

429

Defining

Note

When a system password is being used, the operator must


enter the password to exit the quick access menu and
return to the main menu.

1.

Access the quick access menu options procedure by


pressing [9] More then [1] Quick Menu Option from the
setup menu. The quick menu options screen will be
displayed.
Quick Menu Options
Item
Item
Item
Item
Item
Item
Item
Item
Item

1
2
3
4
5
6
7
8
9

Analyze
Results
Calibrate
Analysis Method
Set Barometer
Leak Check
Print Buffer
Plot Buffer
Ambient Monitor

Option:

Yes

Yes/No

2.

Press Select to move the highlight and select the item to


change.

3.

At the highlight, press no to change the item and select


the desired item function. Selections: Analyze, Results,
Calibrate, Analysis Method, Set Barometer, Leak Check,
Print Buffer, Plot Buffer, and Ambient Monitor.

4.

Press Menu to display the quick menu options menu.


Quick Menu Options

[1] Print

430

5.

Press [1] Print to receive a printout of the quick menu


options Items on the system printer.

6.

Press Exit to remove the quick menu options menu and


return to the setup menu.

CS-200

System Setup

Change Password

Notes

Change password protects selections under the setup menu


from being accessed by unauthorized operators.

To clear an entered password and permit use of the


determinator without securing the setup menu, press Select
twice from the enter password screen.

1.

Access change password by pressing [9] More then [3]


Change Password from the setup menu.
Change Password

USER DIALOG
Enter Password
[

2.

From the user dialog screen, enter a six-digit password


and press Select. The verify password screen will be
displayed.
Change Password

USER DIALOG
Verify Password
[

System Setup

3.

From the verify password screen, enter the same


password as entered in step 2.

4.

Press Select to accept the password and return to the


setup menu.

5.

Press Exit to return to the main menu. In order to return


to the setup menu, the password entered in step 2 must
be entered when the enter password screen appears.

CS-200

431

Analysis Method Menu

Notes

Analysis method permits the operator to set the analysis


parameters used in the analysis of a sample.

Up to five analysis methods can be defined from the


analysis method menu and stored.

Each analysis method can be calibrated separately. Refer to


the Calibration menu.

1.

To access the analysis method screen, choose [4] Setup


from the main menu. From the setup menu, choose [1]
Analysis Method. The analysis method screen will appear.
Analysis Method
Method Name
Secure Method
Purge Time
Delay Time
Significant Figures
Minimum Time Out
Comparator Level
Calibration
Blank

432

1-Method
No
15
0
4
4.0
1.0
1.000
0.000

2.

Press Select to scroll through and select the parameters to


edit. Refer to the Definitions, Ranges, and Defaults on
page 434.

3.

If the parameter to be edited is a number, enter the value


from the keyboard, or press the arrow keys to move the
cursor to a digit and enter the value with the keypad.

4.

If a parameter to be edited is selectable text, press No to


scroll through the selections or Yes to accept the selection
and move to the next parameter.

CS-200

System Setup

5.

Press Menu to display the analysis method menu.


Analysis Method

[1] Print
[2] Select Method
[3] Copy Method To

6.

Press [1] Print to receive a printout of the analysis method


parameters.

7.

Press [2] Select Method to display the analysis method


selection menu and select the analysis method to edit.

8.

Press [3] Copy Method To to copy the current method to a


selected method.
Select Method

[1]
[2]
[3]
[4]
[5]

9.

System Setup

1-Method
2-Method
3-Method
4-Method
5-Method

Press Exit to remove the analysis method selection menu


and return to the analysis method screen.

CS-200

433

Definitions, Ranges, and Defaults


Analysis MethodPermits the operator to assign a specific
name to an analysis method. Up to eight characters can be
entered.
Secure MethodWhen set to yes, the operator is prompted to
type in the password before the method can be changed. If set
to no, the current method is used and no prompt will appear.
Selections: Yes or No. Default: No.
Purge TimeThe amount of time the determinator permits
carrier gas flows through the combustion system before
analysis, clearing it of atmosphere that may have entered when
the furnace was open during crucible loading. Range: 0 to 60
seconds. Default: 1 second.
Delay TimeThe amount of time permitted to elapse after
purge time and before analysis. This time period helps establish
a stable baseline reference for detection. Range: 0 to 60
seconds. Default: 0 seconds.
Significant FiguresThe number of digits displayed in the
element result. This includes digits to the left and right of the
decimal point. Range: 0 to 5. Default: 5.
Minimum Time-OutThe minimum time permitted for analysis.
Range: 10 to 225 seconds. Default: 40 seconds.
Comparator LevelAn area of the analysis plot, less than peak
height, measured as a percentage of peak height that will stop
analysis. Refer to Comparator Level, page 78. Range: 0 to 100
percent. Default: 1.0% carbon.
CalibrationThe linear multiplier value used to adjust the
detector output of a standard to its known value. This value
is automatically determined during calibration. Refer to
Calibrate Menu, page 527. Range: 0.0100 to 10.0000.
Default: 1.0000.
BlankThe percentage of element (based on a 1 gram nominal
sample size) measured by the system that is not caused by
combustion of the analyte. Crucible contamination and the
accelerator primarily cause this value. This value is
automatically subtracted from the result by the determinator.
Refer to Calculate Blank, page 533. Range: - 1.00000 to
+1.00000. Default: 0.00000.
Answer FormatAutomatically converts the element result to
the selected answer format. Selections for Carbon: % carbon,
% C[CO2] and % CaCO3. Default: % carbon. Selections for
Sulfur: % sulfur, % S[SO3] and S[SO4]. Default: % sulfur.

434

CS-200

System Setup

Data Transmit

Notes

System Setup

The transmit data output is RS-232.

All character generation is coded in ASCII format.

Special characters (such as expanded print characters) are


filtered out.

1.

Place the on/off power switch to the off position.

2.

Connect the data transmit serial port, on the rear panel of


the determinator, to the serial connector on the peripheral
device using the supplied cable. Refer to Figure 2-2, page
29.

3.

Configure the determinator's output to match the


peripheral device. Refer to Transmit Options, page 421,
for the configuration procedure.

4.

To transmit the results, stored in the results database,


refer to Transmit Selected Results, page 546.

5.

Switch the power on.

CS-200

435

ASCII Character Definition Table

ACK
BEL
BS
CAN
CR
DC1
DC2
DC3
DC4
DEL
DLE

Acknowledge
Bell, or alarm
Backspace
Cancel
Carriage return
Device control 1
Device control 2
Device control 3
Device control 4
Delete
Data link escape

EM
ENQ
EOT
ESC
ETB
ETX
FF
FS
GS
HT
LF

End of Medium
Enquiry
End of transmission
Escape
End of transmission block
End of text
Form feed
File separator
Group separator
Horizontal tab
Line feed

NAK
NUL
RS
SI
SO
SOH
SP
STX
SUB
SYN
US
VT

Negative acknowledge
Null, or all zeros
Record separator
Shift in
Shift Out
Start of heading
Space
Start of text
Substitute
Synchronous idle
Unit separator
Vertical Tab

*American Standard Code for Information Interchange (ASCII) X3.4 - 1967 for use on tape
1967 USA Standards Institute. Reprinted by permission.

436

CS-200

System Setup

Data Transmit Format


Line 1:
SOH

Sample ID Code

FS

Weight

FS

00

01

02

03

04

05

06

07

08

09

0A

0B

0C

0D

0E

0F

10

11

12

SOH

"

"

FS

FS

01

22

41

30

30

30

30

30

30

31

22

1C

31

2E

30

30

30

30

30

1C

14

15

16

17

18

19

1A

1B

1C

1D

1E

1F

20

21

22

23

24

25

26

27

"

"

FS

22

31

2D

4D

45

54

48

4F

44

22

1C

31

2E

30

30

37

36

20

20

1C

28

29

39

3A

Method

FS

Carbon Calib.
2A

2B

FS
2C

2D

Carbon Results

Carbon Blank

2E

2F

30

31

13

32

33

FS
34

35

FS
FS

Time

36

37

FS

38

FS

FS

FS

31

2E

30

30

30

30

1C

30

2E

30

30

30

30

30

1C

30

34

30

1C

Peak

FS

3D

3E

3F

40

Sulfur Result
41

42

43

3C
1

FS

20

31

35

33

37

1C

31

2E

30

30

37

36

Sulfur Blank
51

52

53

54

44

45

FS

3B

FS

55

56

57

58

46

5A

4A

4B

49
FS

FS

20

20

1C

31

2E

30

30

30

30

1C

FS
5B

5C

FS

FS

30

2E

30

30

30

30

30

1C

30

34

30

1C

4C

4D

4E

64

65

66

67

31

30

3A

32

33

System Setup

68
20

4F

Peak
5F

50

FS

5D

5E

60

FS

20

31

35

33

37

1C

Time and Date


63

FS

48

Time
59

Sulfur Calib.

47

61

RS

62

EOT

69

6A

6B

6C

6D

6E

6F

70

71

72

RS

EOT

30

31

2D

32

38

2D

39

39

1E

04

CS-200

437

System Setup for Windows

Keypad

Windows

Keypad

For instruments using DSP software refer to the instructions


listed on page 41.

For instruments using Windows software refer to the


instructions listed below.

Illustrations .......................................................................44
Controls and Indicators .......................................................46
Menu Organization Chart .....................................................48
Power-Up ........................................................................ 410
About the Examples ..................................................... 410
Menus........................................................................ 410
Keypad ...................................................................... 411
Using the Keypad ................................................... 412
Notices and Errors ....................................................... 413
Confirmation............................................................... 414
Copyright Screen......................................................... 414
System Overview ............................................................. 415
Main Menu Overview .................................................... 415
System Check .................................................................. 416
Ambient Monitor.......................................................... 416
System Setup .................................................................. 418
System Options........................................................... 419
Definitions, Ranges, and Defaults.............................. 420
Transmit Options ......................................................... 421
Definitions, Ranges, and Defaults.............................. 422

438

CS-200

System Setup

Balance Options .......................................................... 423


Definitions and Selections ........................................ 425
System Clock .............................................................. 426
Set Barometer ............................................................ 427
Combustion Pressure ................................................... 428
Quick Access Menu ...................................................... 429
Operation .............................................................. 429
Defining ................................................................ 430
Change Password ........................................................ 431
Analysis Method Menu....................................................... 432
Definitions, Ranges, and Defaults................................... 434
Data Transmit.................................................................. 435
Data Transmit Format .................................................. 437
System Setup for Windows .............................................. 438
Windows

Illustrations ..................................................................... 441


Controls and Indicators ..................................................... 442
Automatically Transmit Analysis Results............................... 444
Configure Maintenance Counters......................................... 446
Maintenance Counter Definitions.................................... 447
Configure the Analysis Report ............................................ 448
Select the Fields ..................................................... 449
Select the Font....................................................... 449
Configure the Plot................................................... 449
Line Printing .......................................................... 449
Configure the Screen ........................................................ 450
Tool Bar ..................................................................... 450
Status Bar .................................................................. 450
Configure the Spreadsheet................................................. 451
Configure Plot Definitions.............................................. 452
Method Development ........................................................ 453
Method Parameter Definitions........................................ 455
Sample Templates ............................................................ 456
Create a Sample Template ............................................ 456
Standards ....................................................................... 457

System Setup

CS-200

439

Standards Definitions ................................................... 458


System Configuration........................................................ 459
System Configuration Definitions ................................... 460
System Tab ........................................................... 460
Serial Port Tab ....................................................... 461
Balance Tab ........................................................... 462
Balance Definitions ................................................. 463
Set Barometric Pressure .................................................... 464
Transmission Formats ....................................................... 465
Define Fields ............................................................... 465
Define Delimiters......................................................... 467
Preview Transmitted Data.................................................. 469
Select Language............................................................... 471
Users.............................................................................. 472
Add a User ................................................................. 472
Add Password ............................................................. 473
Assign User Functions .................................................. 474

440

CS-200

System Setup

Illustrations
Figure 41......... Controls and Indicators with Autocleaner....... 47
Figure 42......... Keypad and Display Screen ......................... 411
Figure 43......... Combustion Pressure Adjustment Knob ......... 428
Figure 4-4 ......... Controls and Indicators............................... 443

System Setup

CS-200

441

Controls and Indicators

Note

Refer to Figure 4-4, on page 443, for locations of the items


listed below.

Determinator Power On/Off SwitchSwitches power on and off


to the determinator. Also acts as a circuit breaker on the
incoming facility line power.
Measure Flow RotameterIndicates the oxygen flow rate in lpm
(liters per minute). Nominal indication is 3.0 lpm.
Computer (not shown)Used to control the instrument and
process sample data.
Printer (not shown)The printer is used to print out analysis
data, information presented on the display, and buffer or
screen plots.
Furnace Power On/Off SwitchSwitches power on and off to
the furnace. Also acts as a circuit breaker on the incoming
facility line power.
Power Lever AdjustmentControls oscillator maximum power
output by adjusting the plate current for approximately 100 mA
(idling current) to 500 mA (full power). The overload protection
is reset by turning the adjustment fully counterclockwise until it
clicks and then turning it clockwise.
Vacuum Cleaner On/Off SwitchTurns the optional vacuum
cleaner on or off. The vacuum cleaner can be used to clear
dust and debris from the combustion area and furnace shelf.
Piston Up/Down SwitchThis switch controls the movement of
the piston, either up or down. During operation, the piston
raises the crucible and sample into the furnace for analysis.
This switch is also used to control the piston during furnace
cleaning.

442

CS-200

System Setup

AUTOCLEANER
ASSEMBLY
ACCESS DOOR

CONTRAST
CONTROL

BRIGHTNESS
CONTROL
INCOMING
REAGENT
TUBE

782-603
VACUUM
HOSE

CATALYST
HEATER
ASSEMBLY

604-126
DUST BOX
ANHYDRONE
TUBE
MEASURE
FLOW
ROTAMETER

ANALYZER
AC POWER
ON/OFF
SWITCH
CELLULOSE
FILTER

POWER LEVEL
ADJUSTMENT

FURNACE
AC POWER
ON/OFF
SWITCH

VACUUM
CLEANER
ON/OFF
SWITCH

PISTON
UP/DOWN
SWITCH

772-960
CRUCIBLE BOX
WITH LINER

789-230
VACUUM CLEANER

Figure 4-4
Controls and Indicators

System Setup

CS-200

443

Automatically Transmit Analysis Results


Using this procedure the operator can automatically transmit
analysis results after each new analysis.
1.

444

Click Configuration and select Transmission Formats. The


Transmission Formats screen will appear.

CS-200

System Setup

System Setup

2.

Select a Format by clicking on it.

3.

Click the Properties tab. The Transmission Properties


screen will appear.

4.

Click the Automation tab. The Automation screen will


appear.

5.

Click the Check Box to select Transmit Data Automatically


after each analysis.

6.

Click the Fields tab to select the information to be


transmitted.

7.

Click the Delimiters tab to select the character to separate


fields.

8.

Click the Serial Port tab to configure the serial port.

9.

Click OK to close the Automation screen.

CS-200

445

Configure Maintenance Counters


Maintenance Counters is a list of components and assemblies,
within the instrument, that have been determined to require
periodic maintenance. An analyses counter will determine when
periodic maintenance is needed and alert the operator. After
maintenance, a history log of maintenance performed is
automatically generated. The counters should not be reset from
this procedure. To reset the counters see Reset Maintenance
Counters on page 626.
Note

Example

446

The Furnace Counter sets the autocleaner clean interval.

To clean after every analysis set the Furnace Counter to


Analyses and Stop to 1. To clean after every other analysis
set the Furnace Counter to Analyses and Stop to 2.

1.

Click Configuration and select Counters. The Counters


screen will appear.

2.

Click Add to define a maintenance counter

3.

Enter the information required in the dialog box. Refer to


maintenance counter definitions.

4.

To remove a counter, select the counter and click Delete.


You can only remove a counter that you added.

5.

Click Print to print a listing of the maintenance counters


and their parameter values on the system printer.

6.

Click OK to close.

CS-200

System Setup

Maintenance Counter Definitions


NameA name or description of the component or assembly
that requires periodic maintenance.
TypeAn operation, period or amount selected by the operator
that is counted. Selections: Analyses, Hours, Days. Default:
Analyses.
Count BlanksDetermines if blanks are to be includes as an
analysis count. Selections: Yes or No.
CountThe number of times an operation, period or amount
occurs before it is reset. An operation, period or amount is
defined by type. Examples: hours, days or analyses.
WarningThe determined number of analyses that the analyses
counter can reach, before a warning message is displayed,
alerting the operator that periodic maintenance is necessary.
Analysis will not stop when this counter limit is reached. To turn
this function off, enter 0.
StopThe determined number of analyses that the analyses
counter can reach, before the instrument will automatically stop
and prevent continued analysis. To turn this function off, enter
0.
ResetsThe number of times that the maintenance item was
serviced. The resets counter is incremented every time a
maintenance item is checked in the maintenance dialog box.
ResetDisplays the date and time the maintenance counter
was reset.
CommentsA place for the operator to add notes or comments
concerning maintenance.

System Setup

CS-200

447

Configure the Analysis Report


A report of analysis results can be generated and printed on the
system printer. Before the report is printed the printed format
should be determined. Configuration is the process of
formatting the report.
Report Configuration permits the operator to select a tabular
report or a report with plots, title the report, select the field to
include in the report, select the text font and color and
configure the plot.

448

1.

Select the Analysis Results that will be included in the


report.

2.

Click File and select Print Preview. The Report Settings


Screen will appear.

3.

Select the Reports tab.

4.

Click the Report Format drop down box and select the
desired report type.

5.

Click the Statistics drop down box and select the desired
statistics report type.

CS-200

System Setup

6.

Enter a Heading Text to title the report.

Select the Fields


Note

To print fields as they appear on the spreadsheet do not


select Define Reports Fields.
A.

Select the Fields tab. If the Field tab is not shown


check Define Reports Field.

B.

Select the fields to display in the report. To show an


invisible field, select the field to display and click
Show. To hide a visible field, select the field to hide
and click Hide

Select the Font


C.

Select the Font tab.

D.

Select the font name, text style, text size and color.

E.

Click Strikeout to draw a line through the text.

F.

Click Underline to draw a line under the text.

Configure the Plot


G.

Select the Plot tab to format the report plot. Refer to


Configure the Spreadsheet, on page 451, for
Configure Plot Definitions.

Line Printing
Note

Line Printing permits the operator to print an analysis result


on a single line instead on an entire page. To use Line
Printing a dot matrix printer should be selected.
H.

Select the Reports Tab.

I.

Check Line Printing to print the selected samples as a


line of text across the page.

J.

Check Automatically Print After Each Analysis to print


the analysis result after each sample has been
analyzed.

7.

Click OK to save the report style changes.

8.

Click OK to preview the print format.

9.

Click Print to print the report. The Printer Configuration


screen will appear.

10. Configure the printer if necessary and click OK to print the


report on the system printer.

System Setup

CS-200

449

Configure the Screen

Tool Bar
This procedure hides or displays the Toolbar. When displayed
the tool bar is located at the top of the screen and is a quick
way to perform menu functions without accessing the menus.
1.

Click View and select Toolbar. A check indicates the


toolbar is displayed.

2.

The spreadsheet will automatically display with the Toolbar


hidden or with it displayed.

Status Bar
This procedure hides or displays the Status Bar. When
displayed the Status Bar is located at the bottom of the screen
and displays operational functions of the instrument as they're
currently in progress.

450

1.

Click View and select Status Bar. A check indicates the


Status Bar is displayed.

2.

The spreadsheet will automatically display with the Status


Bar hidden or with it displayed.

CS-200

System Setup

Configure the Spreadsheet


Configure Spreadsheet customizes the spreadsheet as desired
by the operator. The following items of the spreadsheet can be
changed.

Displayed Fields

Font Name

Font Style

Font Size

Font Color

Font Effects

Line Width

Plot Elements

Reporting Units

Significant Digits

Precision

Line Width

1.

System Setup

Click Configuration and select Display. The Display


Configuration screen will appear.

CS-200

451

2.

Click Fields to display or hide a spreadsheet field.

3.

To show an invisible field, select the field to display and


click Show.

4.

To hide a visible field, select the field to hide and click


Hide.

5.

To change the order of fields shown on the spreadsheet,


select the Field to move, in the fields list box, and click
promote or demote.

6.

Click Font to change the font name, style, size, color and
effects.

7.

Click Element to change the Elements, Reporting Units,


Significant Digits, Plot Color, Plot Pattern, and show or
hide the Baseline.

8.

Click OK to close the Display Configuration screen.

9.

To automatically adjust the cell width to fit the data, click


Configuration and select Auto Widths. The cell widths will
be automatically adjusted.

Configure Plot Definitions


Reporting UnitsPermits the operator to select the result units.
This will determine the displayed and printed units. Selections:
Percent, Milligrams, Area and Parts Per Million.
Significant DigitsThe number of significant digits displayed in
the result above the plot. Selections: 1 - 6. For PPM the number
of significant digits will be limited to the instrument's
measurement capability.

452

CS-200

System Setup

Method Development
A method is a set of analytical parameters used to control the
instrument during analysis and calculation of the final result.
Before analysis, a method must be created. Refer to the
method definitions below to help create a method for a specific
application.
In addition to creating a method, the methods screen also lists
methods that have been created and saved. If it is desired to
switch methods, or use an old method for a new application, a
method can be selected from this list during the sample login
procedure. Refer to Login a Sample on page 563.

Note

System Setup

This procedure should be performed before a sample is


analyzed.

1.

Click Configuration and select Methods, the Method screen


will appear.

2.

Click Add to create a method. A row will be added to the


bottom of the spreadsheet.

3.

Click a row and enter a method name.

CS-200

453

454

4.

Click Properties. The Method Properties screen will appear.

5.

Enter the desired method parameter values for the


parameters listed. It will be necessary to select all the
parameter types, analysis, element, gas dose and furnace

6.

Click OK to close the method properties screen.

7.

Select a method and click Clone to copy a method and


save it as a different method name. This permits the
operator to edit the new method creating a different one.

8.

Select a method and click Delete to remove a method,

9.

Click OK.

CS-200

System Setup

Method Parameter Definitions


Purge TimeThe time before analysis when the furnace is
closed and atmosphere is purged from the combustion area.
Oxygen is flushed into the combustion area to purge
atmospheric gas. Default 1 second.
Delay TimeThe amount of time permitted to elapse between
purge time and analysis. This time period helps establish a
stable baseline reference for detection. Default 8 seconds.
Minimum TimeoutThe minimum time permitted for analysis.
The analysis will last at least this long. Range 10 to 300
seconds. Default 40 seconds.
Comparator LevelAn area of the analysis plot, less than peak
height, measured as a percentage of peak height that will stop
analysis. Refer to Comparator Level, page 78. Range 0 to 100
percent. Default 1 percent.
Significant DigitsThe number of digits displayed in the
analysis result. This includes digits to the right and left of the
decimal point. Range 0 to 5. Default 3 digits.

System Setup

CS-200

455

Sample Templates
Sample Templates is a quick way for the operator to login a
sample and enter a method, comment and description. After a
Sample Template has been created refer to Login using a
Sample Template on page 567.

Create a Sample Template

456

1.

Click the Configuration menu and select Sample Templates


the Sample Templates screen will appear.

2.

Double click on the last empty cell under the Name column
and enter the template name. The cursor must appear
before text can be entered.

3.

Double click in the other cells to the right of the name cell
to enter a method, comment and description into those
cells.

4.

Click Add to save the sample template.

5.

Click OK to close the sample template screen.

CS-200

System Setup

Standards
A Calibration Standard is a sample of known type and value.
Standards are used to calibrate the instrument for best
accuracy. Since calibration standards are usually purchased and
their value remains consistent, a list of standard samples and
associated information can be stored and accessed when
needed.
Standards creates a list of calibration standards for use during
calibration. This list can be accessed and found under the
Configuration menu.

Notes

System Setup

A Standard can be used to perform automatic calibration


checks if the upper and lower control limits are set and Yes
is selected for standard check.

A Standard cannot be used to calibrate or drift correct a


method until it is defined as a Standard.

1.

Click Configuration and select Standards. The standards


screen will appear.

2.

Click Add to list a standard. A row will be added to the


bottom of the spreadsheet.

3.

Click the row and enter a standard name, lot number,


value and control limit.

4.

Click OK to list the standard.

5.

If it becomes necessary to delete a standard select the


standard to delete and click Delete.

CS-200

457

Standards Definitions
Standard NameThis is the name of the Standard defined by
the operator. The part number or lot number of the standard
can be used in place of the name.
(Element) PercentThe value of the standard. This is the
carbon or sulfur value taken from the label.

458

CS-200

System Setup

System Configuration
System Configuration sets the overall instrument operating
settings and parameter values. In addition, the settings for the
Serial Port, Balance and Language can be changed. The
settings and parameters are listed under system configuration
definitions.

System Setup

1.

Click Configuration and select the System. The System


Configuration screen will appear.

2.

Click the desired configuration tab.

3.

Click the edit box next to the right of desired parameter to


change and enter the new setting. To select a language
from the language tab, click the edit box and select a
language.

4.

Click OK to save the changes or Cancel to retain the


original system configuration.

CS-200

459

System Configuration Definitions


System Tab
Significant DigitsThe number of digits displayed in all fields of
the spreadsheet except the mass and analysis result. The
number of digits in the mass field is determined from balance
configuration and the number of digits in the result field is
determined by the analysis method.
Reduction Heater (Catalyst) TemperatureThe set operating
temperature of the Measure Flow Catalyst Heater. Range 0900oC. Default 350oC.
Gas Conservation TimeoutThe time in minutes, after analysis,
when the instrument automatically switches to the gas
conservation mode. Range 0 to 600 minutes. Default 15
minutes.
Gas Conservation ModeThe oxygen flow settings used as gas
conservation. Normal oxygen flow is 3 liters per minute.
Conservation mode changes the oxygen flow to 1 liter per
minute. Off turns the oxygen flow completely OFF. Selections
are OFF or Conservation.
AutocleanerConfigures the instrument for use with the
optional autocleaner. Selections: Enabled (an autocleamer is
installed), Disabled (an autocleaner is not installed).
Door OptionConfigures the instrument for use with the
optional dust eject door. Selections: Enabled (a dust eject door
is installed), Disabled (a dust eject door is not installed).
Increment Sample NamesIf enabled, and the sample name
ends in a number, the number will be automatically
incremented by one every time a sample is entered. If there is
no number in the sample name one will be added, starting with
2 on the second sample with that name. Standards do not
increment. Selections are Enable or Disable.
Nominal MassThis is the mass automatically entered when
performing blank and gas dose analysis. The nominal value is
usually 1.000 gram.

460

CS-200

System Setup

Serial Port Tab


Serial Port Configuration is not available. The serial port is used
by the PC to communicate with the instrument during
Windows operation.

System Setup

CS-200

461

Balance Tab
The Balance Tab is used to configure the balance serial port for
communications with an external balance. The serial port used
by the balance is COM 2.

462

1.

Click Configuration and select Balance. The Balance


Configuration screen will appear.

2.

Click the desired configuration tab.

3.

Click the edit box next to the right of desired parameter to


change and enter the new setting. To select a language
from the language tab, click the edit box and select a
language.

4.

Click OK to save the changes or Cancel to retain the


original system configuration.

CS-200

System Setup

Balance Definitions
Baud RateSelect the data transmission speed between the
computer and the balance. Selection: 1200 through 19200 bits
per second (bps). Default: 1200 bps.
Data BitsSelects the number of transmitted data bits per
byte. Selection: 6 through 8. Default: 7.
ParitySelects the method of error checking. Selection: Even,
Odd or None. Default: Even.
Stop BitsSelects the number of data bits that are used to
signal the end of transmitted data. Selections: 1 or 2. Default:
1.
Tare CommandThe command sent from the instrument that
causes the balance to tare. Selections are <ESC T>, T,
T<CR>LF>.
Send Command The command sent from the instrument that
causes the balance send a mass value back to the instrument.
Selections are <ESC>P<CR><LF>, S<CR><LF>,
SI<CR><LF>, P0<CR><LF>, and P1<CR><LF>.
Readability (Significant Digits)The number of significant digits
to the right of the mass value transferred from the balance and
entered into the spreadsheet. Range 3 to 6. Default: 4.

System Setup

CS-200

463

Set Barometric Pressure

Note

464

The local barometric pressure must be known before the


barometric pressure can be set.

1.

Click Configuration and select Hardware Calibration. The


Barometric Calibration screen will appear displaying the
last barometric calibration date.

2.

Click Next.

3.

Wait for the system to stabilize and a barometric pressure


reading to appear.

4.

Enter the current barometric pressure obtained from a


local source.

5.

Click Next

6.

Click Finished to exit the barometric pressure calibration


procedure.

CS-200

System Setup

Transmission Formats
Transmission Formats permits the operator to select sample
and data transmission parameters to send to the host
computer. These include:

Note

Define Fields

Define Delimiters

Transmit Automation

Serial Port Configuration

Preview screen for previewing the transmit data format.

More than one Transmission Format can be defined and


selected when desired.

Define Fields
Note

System Setup

A field is a block of transmitted data. Use this procedure to


select the fields to transmit.

7.

Click Configuration and select Transmission Formats. The


Transmission Formats screen will appear.

8.

Click Add to create a data transmission format. A row will


be added to the bottom of the spreadsheet

CS-200

465

9.

Click a row and enter a format name.

10. Click Properties. The Transmission Formats Properties


screen will appear.

11. Select the Fields tab.


12. For each field to transmit, select the field from the fields
list box and click Add to add a field or click Remove to
remove a field.
13. Click OK to close the Transmission Formats Properties
screen.

466

CS-200

System Setup

Define Delimiters

Note

System Setup

A delimiter is a character that separates fields of data. Use


this procedure to select the delimiters to transmit.

1.

Click Configuration and select Transmission Formats. The


Transmission Formats screen will appear.

2.

Click the Properties tab. The Transmission Properties


screen will appear.

CS-200

467

Note

3.

Click the Delimiters tab. The Delimiters screen will appear.

4.

Click the radio buttons and select the Field delimiter, Start
of Transmission delimiter, End of Transmission delimiter
and Text Format.

5.

468

Click the radio button to select Other and enter an


undefined delimiter.
Click OK to close the Delimiters screen.

CS-200

System Setup

Preview Transmitted Data


This screen permits the operator to preview the Transmitted
Data Format after it is setup. If changes are necessary they can
be done before closing this procedure.

System Setup

1.

Click Configuration and select Transmission Formats. The


Transmission Formats screen will appear.

2.

Select a Transmission Format.

3.

Click the Properties tab. The Transmit Data Properties


screen will appear.

CS-200

469

470

4.

Click the Preview tab. The Transmit Data Preview screen


will appear with the transmitted data shown.

5.

Click OK to close the Transmit Data Preview screen.

CS-200

System Setup

Select Language

Notes

System Setup

Select Language permits the operator to change the


language of the text displayed in the software.

Select Language will not change the language of the text


displayed in the electronic manual.

1.

Click the Configuration menu and select Select Language


the Select Language screen will appear.

2.

Select the desired language and click OK. The display text
will appear in the language selected.

CS-200

471

Users
The system manager can assign users (operators), passwords
and grant permissions from Users. This adds security to the
system and prevents unauthorized operation that could cause
damage or inaccurate result data.

Add a User

472

1.

Click Configuration and select Users. The Users screen will


appear.

2.

Click Add and enter a user name to assign a user. A new


user will be added to the bottom of the list.

3.

To edit a user name click the name of a user and enter


any changes.

4.

Click OK to enter the user name.

CS-200

System Setup

Add Password

System Setup

1.

From the User Screen select an operator. This will be the


operator that a password will be assigned to.

2.

Click Properties to display the User Properties screen.

3.

Click the box to the right of the password and enter a


password.

4.

If the password must match the user name during login,


check The Users Name must match. If this is not
checked any password entered into the system can be
used to log onto the system.

5.

Click OK to enter the password.

CS-200

473

Assign User Functions

Note

1.

From the User Screen select an operator. This will be the


operator to assign permissions in the following steps.

2.

Click Properties to display the User Properties screen.

3.

Click the desired permission check boxes to select the


functions the user can or cannot access. A check indicates
access is granted.

4.

474

If you do not want this operator to edit (or change) user


permissions do not check Edit Users.
Click OK to enter the user permissions.

CS-200

System Setup

Operation

Windows

Keypad

Keypad

5 Operation

For instruments using Windows software refer to the


instructions listed on page 547.

For instruments using DSP software refer to the instructions


listed below.

Operation Guidelines...........................................................56
Before an Analysis ......................................................... 57
After an Analysis ........................................................... 58
After Use...................................................................... 58
Crucibles ...........................................................................59
Sample Preparation .......................................................... 510
Sample Size................................................................ 510
High Sulfur Samples .................................................... 510
Blank Samples ....................................................... 510
Analyze Menu .................................................................. 511
Screen Description....................................................... 511
Delete Weight ............................................................. 513
Insert Weight.............................................................. 514
Print Weights .............................................................. 515
System Controls .......................................................... 516
Definitions and Ranges ............................................ 517
Clean Switch............................................................... 518

Operation

CS-200

51

With Autocleaner .................................................... 518


Without Autocleaner................................................ 519
Balance Weight ........................................................... 520
Transmit Last.............................................................. 521
Select Method ............................................................. 522
Sample Weight Entry ........................................................ 523
Sample Analysis ............................................................... 525
Calibrate Menu................................................................. 527
Calibration Results Format Selection............................... 528
Clear Selection ............................................................ 529
Calculate Calibration .................................................... 530
Edit Calibration ........................................................... 532
Calculate Blank ........................................................... 533
Edit Blank................................................................... 535
Recalculate Results ...................................................... 536
Results Menu ................................................................... 538
Results Format Selection .............................................. 540
Clear Selections .......................................................... 541
Delete Selected Results ................................................ 542
Statistics .................................................................... 543
Definitions ............................................................. 544
Print Selected Results .................................................. 545
Transmit Selected Results............................................. 546
Windows

Operation for Windows .................................................... 547


Windows Software Menus .................................................. 552
File Menu ................................................................... 552
Print ..................................................................... 552
Print Preview ......................................................... 552
Print Setup ............................................................ 552
Import .................................................................. 553
Export................................................................... 553
Exit ...................................................................... 553
Edit Menu ................................................................... 554
Insert ................................................................... 554

52

CS-200

Operation

Fill........................................................................ 554
Cut....................................................................... 554
Copy..................................................................... 554
Paste .................................................................... 554
View Menu.................................................................. 555
Tool Bar ................................................................ 555
Status Bar ............................................................. 555
First Row............................................................... 555
Analysis Row.......................................................... 555
Last Row ............................................................... 555
Samples Menu ............................................................ 556
Login .................................................................... 556
Balance ................................................................. 556
Analyze ................................................................. 556
Reset/Abort ........................................................... 556
Recalculate ............................................................ 557
Transmit ............................................................... 557
Delete................................................................... 557
Configuration Menu...................................................... 558
Calibrations ........................................................... 558
Blank .................................................................... 558
Drift ..................................................................... 558
Linearizations......................................................... 558
Standards.............................................................. 559
Methods ................................................................ 559
Counters ............................................................... 559
Sample Templates .................................................. 559
System ................................................................. 559
Users .................................................................... 559
Transmission Formats ............................................. 560
Select Language ..................................................... 560
Auto Widths ........................................................... 560
Display.................................................................. 560
Hardware Calibrations ............................................. 560
Diagnostics Menu ........................................................ 561
Leak Check ............................................................ 561
Operation

CS-200

53

Ambients............................................................... 561
Switches ............................................................... 561
Solenoids .............................................................. 561
Comport................................................................ 561
Maintenance Menu....................................................... 562
Login .................................................................... 562
View Log File.......................................................... 562
Login a Sample ................................................................ 563
Sample Login Definitions .............................................. 565
Balance Login ............................................................. 566
Login using a Sample Template ..................................... 567
Analyze a Sample ............................................................. 568
Delete a Sample............................................................... 569
Print Sample Results ......................................................... 570
Transmit Results .............................................................. 572
Recalculate Result ............................................................ 573
Calibration....................................................................... 574
Blank Calibration ......................................................... 574
Standard Calibration .................................................... 574
Drift Correction ........................................................... 574
Blank Calibration .............................................................. 575
Standard Calibration ......................................................... 576
Standard Calibration Definitions................................ 578
Drift Correction ................................................................ 579
Drift Correction ........................................................... 580
Data Management ............................................................ 581
Insert Data into the Spreadsheet ................................... 581
Insert a Sample Out-of-Sequence .................................. 582
Fill Selected Cells with the Same Values.......................... 582
Select First Row in the Spreadsheet ............................... 583
Select the Analysis Row in the Spreadsheet..................... 583
Select Last Row in the Spreadsheet................................ 583
Import Sample Data .................................................... 583
Export Sample ............................................................ 584
Export Sample Definitions ........................................ 586
Export Buffer .............................................................. 587
54

CS-200

Operation

Clipboard Use .................................................................. 588


Cut Data to the Clipboard ............................................. 588
Copy Data to the Clipboard ........................................... 588
Paste Data from the Clipboard ....................................... 588
Configure Result Plot......................................................... 589
Display the Menu......................................................... 589
Selection Procedures ............................................... 589

Operation

CS-200

55

Operation Guidelines
Listed below are guidelines that should be followed before
analysis, after analysis and after use. By using this information,
along with the procedures in the Operation Chapter, the
operator will be able to obtain the best possible performance
from this instrument.

Note

56

Do not turn the AC power off to the instrument unless it


malfunctions or it's not going to be used for an extended
period of time.

If the gas is turned off for eight hours or more, do not


perform an analysis until the gas has been turned on for at
least one hour.

The piston should be left up with the crucible removed when


the furnace is not in use.

Refer to Before Analysis for before analysis guidelines.

Refer to After Analysis for after analysis guidelines.

Refer to After Use for after use guidelines.

CS-200

Operation

Before an Analysis
Before a sample can be analyzed and an accurate result
obtained, the instrument must be prepared for analysis. This
includes inspecting and cleaning the combustion system orings, performing a system leak check, selecting or creating a
method, performing a blank calibration and then performing a
standard calibration.
Note

1.

This procedure prepares the instrument for analysis, not the


sample. Refer to Sample Preparation on page 510 for
sample preparation procedures.
Perform daily maintenance before the start of analysis.
A.

Inspect and grease the Combustion O-rings. Refer to


Combustion Zone O-rings, page 616.

B.

Clean the Autocleaner and Mesh Filter. Refer to


Autocleaner, page 66.

C.

Perform a Leak Check. Refer to page 810.

2.

Verify that the gas is turned on.

3.

Verify that the oven is on and reached the proper


temperature. Refer to Ambient Monitor, page 85.

4.

Select or create a Method to use for analysis. Reference


application notes to determine the method parameter
values to enter. Refer to Method Development page 453.

5.

Analyze 3 to 5 blank conditioning samples. This will purge


the system before analysis.

6.

Analyze 3 to 5 blanks and perform a Blank Calibration.


This will set the blank calibration value. Refer to Blank
Calibration page 575.

7.

Analyze a Blank Check Sample to determine if the blank


value was set properly. Refer to Login a Sample page 5
63.

8.

Perform a Drift Correction and analyze 3 to 5 standard


samples. This will set the drift correction value. Refer to
Drift Correction page 579.

9.

Analyze a Standard Check Sample to determine if the drift


value was set properly. Refer to Drift Correction page 5
79.

10. At this point the instrument is ready for Sample Analysis.


Refer to Analyze a Sample on page 568.

Operation

CS-200

57

After an Analysis
When an analysis is complete, the furnace automatically shuts
OFF, a signal sounds, and the spreadsheet shows the final
result. If Line Printing and Automatically Print After Each
Analysis is selected, the printer will print the analysis result.
Refer to Configure the Analysis Report, page 448.

After Use
The AC power to the instrument should remain on at all times.
If the power to the instrument is switched off for any reason a
one-hour warm-up is necessary before analyzing samples.
The instrument automatically switches to conservation (low gas
flow) after an amount of time specified by the Conservation
Time-out in System Configuration, page 459.
Remove the crucible from the furnace after use.

Note

58

The furnace should be closed except when loading and


unloading samples or when maintenance is being
performed. If the furnace is left open for an extended period
of time, analyze 3 to 5 conditioner samples before resuming
normal operation.

CS-200

Operation

Crucibles
When analyzing for low carbon (<0.1%) or low sulfur
(<0.01%), burned off crucibles yield the best results.
Crucibles are burned off by firing them at 1350oC (2500oF) for
at least 20 minutes in a TF-1 or TF-10 Tube Furnace, then
cooling them in a desiccator. Crucibles must be used within four
hours of being burned off or the procedure must be done again.

!
CAUTION

Operation

After the crucibles have been burned off handle


them with 761-929 crucible tongs to avoid
burning your fingers or contaminating the
crucibles.

CS-200

59

Sample Preparation

!
CAUTION

DO NOT touch the crucibles or sample material.


Touching them or letting dust accumulate on
them will adversely affect analytical results.

Sample Size
The nominal sample weight is 1.0 gram. The lower and upper
limits will depend on the sample material analyzed.

High Sulfur Samples


Reduced sample mass is required for samples with 40% or
more sulfur content. For these samples use one scoop Iron Chip
and one scoop Lecocel to ensure complete coupling of the
sample and RF field.
Blank Samples
Blank samples should be 1 scoop Iron Chip and 1 scoop
Lecocel.

510

CS-200

Operation

Analyze Menu
Access the analyze screen by pressing [1] Analyze from the
main menu.
Analyze

0.01010% Carbon
0.02020% Sulfur
Plate
Grid

[
[

] 0mA
] 0mA

Method
ID Code
Weight

1-Method
A0000001
1.0000

1 2 3

Screen Description
The mode of operation is displayed on the top line.
The second line is the result window. The results of the last
analysis (or current analysis if one is in progress) is displayed,
followed by the element type. After each analysis, the result is
placed at the end of the results list and displayed in the results
window. The results list stores up to 50 analyses.
The center block displays the plate current and grid current
readings during an analysis.
The lower block displays the current active method, sample ID
code and sample weight. On the left side the parameter name
is displayed and on the right side the value.
The bottom line displays the number of sample weights that
have been entered. The highlight indicates the position
currently displayed in the weight list.

Note

Operation

Before analyzing any samples, select the appropriate


analysis method parameter values. Refer to Select Method,
page 522, for more details.

CS-200

511

Weight is the sample weight value in grams. Nominal sample


weight is 1 gram. Samples to be analyzed are taken in the
same order as they were placed in the sample weight list. The
operator must identify and arrange the samples to match the
order of the sample weight entries. The sample weight list will
store up to 10 sample weights in the order in which the
samples were entered.
ID Code assigns a specific label to an analyzed sample for
identification.

512

CS-200

Operation

Delete Weight

Notes

Delete weight removes the highlighted sample weight and


ID code from the sample weights list.

To delete a weight, the cursor must highlight the weight to


be deleted on the bottom line of the analyze screen.

1.

While in the sample weights list, press Next/Previous to


select the weight to be deleted.
Analyze

[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]

Operation

Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method

2.

Access the analyze menu by pressing Menu from the


analyze screen.

3.

Press [1] Delete Weight to delete the weight from the


weight list.

CS-200

513

Insert Weight

Note

Insert weight inserts a sample weight and ID code before


the position highlighted in the sample weight list.
Analyze

0.01010% Carbon
0.02020% Sulfur
Plate
Grid

[
[

] 0mA
] 0mA

Method
ID Code
Weight

1-Method
A0000001
1.0000

1 2 3

Note

514

1.

Press Next/Previous to move along the bottom line of the


screen and select the position in the weight list to insert a
weight.

2.

From the analyze menu, press [2] Insert Weight to insert


a weight into the weight list. The analyze screen will
appear with the weight block highlighted.

3.

Enter the weight from the keypad, or press the arrow keys
to move the cursor to the digit to edit and enter the value
from the keypad.

It is also possible to use the balance for automatic weight


entry.

CS-200

Operation

Print Weights

Notes

Print weights permits the operator to receive a printout of


the ID code and sample weight list.

If there are no weights in the sample weights list, the


printer will not print when print weights is selected.

Weights cannot be printed while an analysis is in progress.

1.

To select print weights, the analyze menu must be


displayed.
Analyze

[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]

2.

Operation

Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method

From the analyze menu, press [3] Print Weights. The


operator will receive a printout of the ID codes and sample
weights in the weight list. After the weights are printed,
the analyze screen will appear.

CS-200

515

System Controls

Notes

System controls permits the operator to manually select the


analysis mode and change the carrier gas flow status, or set
the clean counter value and the clean interval value.

Although the carrier gas flow status can be set by system


controls, it will automatically change as determined by the
gas conservation time. Refer to System Configuration.

1.

From the analyze menu, press [4] System Controls. The


System Controls screen will appear.
System Controls

Analysis Mode
Carrier Gas
Clean Counter
Clean Interval

Auto
Off
17
10

2.

Press Select to scroll through the system controls


parameters. Refer to the Definitions and Ranges, on
page 517.

3.

Enter the value from the keypad or press the arrow keys
to move the cursor into position to change a digit value.

4.

Press Menu to display the system controls menu.


System Controls

[1] Print

516

5.

Press [1] Print to receive a printout of the system control


parameters.

6.

Press Exit to remove the system controls menu and return


to the setup menu.

CS-200

Operation

Definitions and Ranges


Analysis ModeSelects the analysis mode of operation, either
automatic or manual. In the automatic mode, analysis begins
when the piston is raised. In the manual mode, analysis begins
when the piston is raised and the start button is pressed.
Default: Auto
Carrier GasSelects the oxygen flow: On, Off, or Conserve.
Oxygen flow can be monitored by observing the oxygen flow
rotameter located on the front panel of the instrument.
Default: Off
Clean CounterThis parameter keeps track of the number of
analyses performed before a cleaning cycle. The counter resets
to zero after each cleaning cycle. If the furnace is cleaned
manually before the preset interval, reset the counter to zero
before operation begins. Default: 0
Furnace Clean IntervalThe number of analyses performed
before cleaning the furnace. The message Cleaning Time prints
when the interval has elapsed. If the autocleaner is installed,
the autoclean cycle is initiated when the interval elapses.
Default: 20

Operation

CS-200

517

Clean Switch
The clean switch function has two modes of operation; with
autocleaner installed or without autocleaner installed. The clean
switch can be used in either mode to close the furnace without
starting an analysis.
During the cleaning process, the vacuum cleaner will
automatically turn on if the autocleaner is installed. If the
autocleaner is not installed, the vacuum cleaner must be turned
on manually.
If the autocleaner is installed, refer to clean counter and
furnace clean interval. These parameters will determine when
the combustion tube is automatically cleaned.

With Autocleaner

Note

518

1.

From the analyze menu, choose [5] Clean Switch. The


piston will drop to the sample load position and the dust
eject door will close.

2.

As the process continues, the vacuum cleaner will turn on


and the autocleaner will brush the lance filter and
combustion area. Dirt left from the combustion process
will flow down the combustion tube and be sucked into the
vacuum cleaner.

3.

After the cleaning process is complete, the determinator


will beep.

4.

Press [5] Clean Switch to raise the lower seal assembly


without starting an analysis. At this point, the next sample
can be loaded.

5.

After the cleaning, pressing the piston switch will close the
furnace and start an analysis automatically if a weight is
entered in the weight list.

The operator should load the next sample on the pedestal


before pressing the piston switch.

CS-200

Operation

Without Autocleaner
1.

From the analyze menu, choose [5] Clean Switch. The


piston will drop to the sample load position.

2.

Remove the pedestal from the lower seal assembly.

3.

Attach the vacuum cleaner hose to the cleaning cup,


position the cleaning cup onto the lower seal assembly,
and press the piston switch. The cleaning cup and lower
seal assembly will rise.

4.

Remove the lance flow fitting and filter cap from the filter
head assembly.

5.

Turn the vacuum cleaner on and brush the filter and


combustion area with the wire brush. The dirt left from the
combustion process will flow down the combustion tube
and be sucked into the vacuum cleaner.

6.

Turn the vacuum cleaner off and press the piston switch to
release the cleaning cup.

7.

Use the wire lance cleaner to clean the lance.

8.

Remove the cleaning cup, replace the filter cap, and


reinstall the lance flow fitting and pedestal.

9.

Press the piston switch to close the lower seal assembly.

10. Press [5] Clean Switch to raise the lower seal assembly
without starting an analysis.
11. After the cleaning, pressing the piston switch will close the
furnace and start an analysis automatically if a weight is
entered in the weight list.

Note

Operation

The operator should load the next sample on the pedestal


before pressing the piston switch.

CS-200

519

Balance Weight

Notes

Balance weight permits the operator to enter a weight from


the balance when the determinator is in the manual weight
entry mode.

If a key is pressed from the analyze screen to edit a


parameter, the determinator will automatically switch to the
manual weight entry mode.

1.

Before using balance weight, be certain that the proper


position in the weight stack is selected. The current weight
in the weight stack will be overwritten.

2.

Normal or remote must be selected for the balance mode.


If None is selected, balance weight will not appear on the
analyze menu. Refer to Balance Options, page 423.

3.

From the analyze screen, press Menu. The analyze menu


will be displayed.
Analyze

[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]

4.

520

Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method

From the analyze menu, press [6] Balance Weight. If the


normal mode was selected the weight displayed on the
balance will be displayed on the instrument. Remote is
displayed if the balance was set to the remote mode.

CS-200

Operation

Transmit Last

Notes

Transmit last permits the operator to transmit the results of


the last analysis to a peripheral device.

To configure data transmit for operation with a specific


peripheral device, refer to the System Setup chapter.

Transmit enable must be set to no.

1.

To select transmit last, the analyze menu must be


displayed.

2.

From the analyze screen, press Menu. The analyze menu


will be displayed.
Analyze

[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]

3.

Operation

Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method

From the analyze menu, press [7] Transmit Last. The


results of the last analysis will be transmitted to a
peripheral device. After the results are transmitted the
analyze screen will be displayed.

CS-200

521

Select Method

Notes

Select method permits the operator to quickly select an


defined analysis method.

Up to five Analysis Methods can be defined from the


analysis method menu and selected from this menu.

Each analysis method can be calibrated separately. Refer to


Calibrate Menu, page 527.

1.

From the analyze screen, press Menu. The analyze menu


will be displayed.
Analyze

[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]

2.

Delete Weight
Insert Weight
Print Weights
System Controls
Clean Switch
Balance Weight
Transmit Last
Select Method

From the analyze menu, press [8] Select Method. The


select method menu will be displayed.
Analyze

[1]
[2]
[3]
[4]
[5]

3.

522

Method
Method
Method
Method
Method

1
2
3
4
5

Select the desired method. The analyze screen will be


displayed.

CS-200

Operation

Sample Weight Entry

Notes

Up to 10 sample weights can be stored in the sample


weight list.

A highlight without a weight position number indicates the


sample weight must be entered.

The optional balance must be configured to match the


selected balance weight mode. Refer to the Options on page
134.

1.

There are four types of weight entry that can be used. The
following procedures describe the use of each entry.
A.

B.

C.

Operation

NoneWithout Optional Balance.


1)

Sample weight(s) are entered using the keypad.

2)

The next key is used after a sample weight has


been entered to advance the cursor for the next
sample.

RemoteWith Optional Balance.


1)

Place the crucible on the balance pan and press


Tare on the balance.

2)

Add the sample material. When the balance


stabilizes, press Print on the balance to enter the
sample weight in the sample weight list. The
system will automatically advance to the next
sample each time the print key on the balance is
pressed. Press print only once for each weight to
be entered.

NormalWith Optional Balance.


1)

Place the crucible on the balance pan and press


Tare on the balance.

2)

Add the sample material. When the balance


stabilizes, press Next on the determinator keypad
to enter the sample weight in the sample weight
list.

CS-200

523

D.

2.

Note

524

Auto TareWith Optional Balance.


1)

Place the crucible on the balance pan. The


balance will automatically tare for weights over
15 grams.

2)

Add the sample material. When the balance


stabilizes press Next on the determinator keypad
to enter the sample weight in the sample weight
list.

The select key can be used to move the cursor (highlight)


to edit the sample ID code.

The ID code will advance as weights are entered.

3.

A number key can be pressed at anytime to manually


enter a weight into a highlighted sample weight position.

4.

The operator can return to the auto-weigh mode by


selecting menu [6] Balance Weight.

CS-200

Operation

Sample Analysis

Notes

All steps in Installation, Initial Power-up, System Check,


and System Setup should be completed before analyzing
samples.

Accurate analysis results are only obtained after the


instrument has been calibrated. Refer to the Calibrate
Menu, page 527.

Before analysis, set the analysis method, system options


and system control parameters. Refer to Analysis Method
Menu, page 432, System Setup, page 418, and System
Controls, page 516.

1.

Note

The gas supplies should be on.

For best results, turn the power off only if the instrument
malfunctions. This eliminates the warm-up time delay.

2.

Carrier gas should be on. Refer to System Controls,


page 516.

3.

Choose [1] Analyze from the main menu to display the


analyze screen.
Analyze

0.01010% Carbon
0.02020% Sulfur
Plate
Grid

[
[

] 0mA
] 0mA

Method
ID Code
Weight

1-Method
A0000001
1.0000

1 2 3

Operation

4.

Load one scoop of Lecocel 2 Accelerator and a Steel Ring


Standard into the Ceramic Crucible.

5.

In the analyze screen, enter the sample weight. Then


press Select and enter the ID code. Or, after entering the
sample weight, pressing Next will enter the sample weight.

CS-200

525

Note

Note

Up to 10 sample weights may be stored in the weight list.

6.

Place the crucible and sample onto the pedestal and press
Piston Up/Down. If the determinator is configured for
automatic operation, the sample will be loaded into the
furnace and analysis will begin. If the determinator is
configured for manual operation, press Start to begin the
analysis after the piston rises and the sample is loaded
into the furnace.

7.

Adjust the furnace power control for the proper plate


current that varies maximum induction power. Maximum
plate current should be limited to 500 mA to extend the
oscillator tube life.

8.

After the sample is analyzed, the results are displayed on


the analyze screen and stored in the results list. Press
Piston Up/Down to lower the piston and remove the
crucible.

9.

The results list stores the last 50 sample results analyzed.


Repeat this procedure for five samples. Refer to the
Calibrate Menu, page 527, and calculate a new calibration
factor.

10. Load one scoop of Lecocel 2 Accelerator into the ceramic


crucible. From the keypad, enter a weight of 1 grams. Run
five blanks. Refer to Calculate Blank, page 533, to
determine the blank value.

WARNING

526

HIGH TEMPERATURE HAZARD


After the sample burns, the crucible is very hot.
Use tongs to remove the crucible from the
furnace and pedestal. Allow the crucible to cool
before touching the crucible.

CS-200

Operation

Calibrate Menu

Notes

Calibration is generally accomplished using standard


samples (samples with known elemental concentrations).
The operator must run at least three analyses of a standard
reference material with a known elemental concentration.

The calibration value is the slope of a linear calibration while


the blank is the intercept of the linear calibration.

1.

From the main menu, press [3] Calibrate. The calibrate


results screen will appear.
Select Results
Select Results
ID Code
A0000001
A0000002
A0000003
A0000004
A0000005
A0000006
>A0000007

Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031

0 Selected

1 of 7

2.

Press the Next/Previous keys to move the cursor down and


up the list of results.

3.

Press Select to include a sample and move the cursor up.

4.

Press Yes to include a sample. The included sample(s) will


remain highlighted.

5.

Press No to exclude a sample. The excluded sample(s) will


not be highlighted.

6.

Press Menu to display the calibrate menu.


Select Results
ID Code
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]

Carbon

Record Format
List Format
Clear Selections
Calculate Calib
Edit Calibration
Calculate Blank
Edit Blank
Recalculate

0 Selected

Operation

Sulfur
0.00169
0.00796
0.00855
0.00654
0.00776
0.00528
0.00487

CS-200

1 of 7

527

Calibration Results Format Selection

Notes

There are two calibration result formats to select from:


Record Format and List Format.

See the Results Menu, page 538, for more information on


Record Format, List Format, and Clear Selections
commands.

1.

Note

Press [1] Record Format from the results menu to display


the selected results in the record format.

The record format is the same as the select results screen


which can display up to eleven results at a time.

2.

Press Menu to return to the select results screen.

3.

Press [2] List Format to display the selected results in the


list format. The list format screen will appear with the
sample result indicated, by an arrow on the record format
screen, displayed.
Select Results
ID Code
Weight
Method Name

Note

4.

528

Results
Calib.
Blank
Time
Peak

A0000001
1.0000
1-Method
Carbon
Sulfur
0.8921
0.0034
0.7863
1.3017
0.0000
0.0000
40
44
16462
149

0 Selected:

1 of 7

The list format displays one result at a time with more


information provided per result.
Press Menu to return to the results menu.

CS-200

Operation

Clear Selection

Note

1.

Clear Selection removes the highlight from selected results


quickly, giving the operator the opportunity to select other
results.
With results selected in the select results screen, press the
Menu key. The calibration menu will be displayed.
Select Results
ID Code
[1]
[2]
[3]
[4]
[5]
[6]
[7]
[8]

Record Format
List Format
Clear Selections
Calculate Calib
Edit Calibration
Calculate Blank
Edit Blank
Recalculate

0 Selected

2.

Operation

Carbon

1 of 7

Press [3] Clear Selections to remove the highlight from all


selected results. The select results screen will be
displayed.

CS-200

529

Calculate Calibration

Notes

Calculate calibration allows the operator to calibrate the


instrument based upon a previously analyzed standard.

A minimum of three to five analyses of a known standard


should be completed before calculate calibration is
performed.

Standard sample results must be selected from the select


results screen before calculate calibration is attempted.

1.

Press [4] Calculate Calibration from the calibrate menu to


display the calculate calibration screen.
Calculate Calib

Carbon
Standard

Yes
0.35400

Sulfur
Standard

Yes
0.05400

Option:

Yes

Y/N

2.

To edit the standard value, enter the value from the


keyboard, or press the arrow keys to move the cursor to a
digit position and enter the digit value with the keypad.

3.

Press Yes to continue and display the calibration results


screen.
Calibrate Results

530

Carbon
Standard

Yes
0.35400

Sulfur
Standard

Yes
0.05400

Option:

Yes

CS-200

Y/N

Operation

4.

Press Menu to display the calibration results menu, or Exit


to return to the select results screen and save the new
calibration values.
Calibration Results

[1] Print
[2] Reset Calib.

5.

Operation

A.

Press [1] Print to receive a printout of the calibration


values on the system printer. The new calibration
values will be saved, and the calibration results
screen displayed.

B.

Press [2] Reset Calibration to reset the new


calibration values and return to the old calibration
values.

Press Exit to return to the select results screen. The new


calibration value will be saved. If reset calibration was
selected, the old calibration value will be saved.

CS-200

531

Edit Calibration

Notes

Edit calibration permits the operator to change the


calibration by entering the calibration value.

This procedure can be used to enter a predetermined value


or used to replace a calibration value that was lost.

1.

Choose [5] Edit Calibration from the calibrate menu to


display the edit calibration screen.
Edit Calibration
Carbon
Old Calib
New Calib

1.0512
1.1617

Sulfur
Old Calib
New Calib

1.0033
1.0055

2.

To edit the calibration value, enter the value from the


keyboard, or press the arrow keys to move the cursor to a
digit and enter the digit value with the keypad.

3.

Press Menu to display the calibration results menu, or Exit


to return to the select results screen and save the new
calibration values.
Edit Calibration

[1] Print

532

4.

Press [1] Print to receive a printout of the calibration


values on the system printer. The new calibration values
will be saved and the calibration results screen displayed.

5.

Press Exit to return to the select results screen and save


the new calibration values.

CS-200

Operation

Calculate Blank

Notes

Calculate blank permits the operator to take into account


the carbon content in the accelerator or contamination in
the system or carrier gas. Refer to Definitions, Ranges, and
Defaults, page 434.

Blank sample results must be selected from the select


results screen before calculate blank is attempted.

Use a sample weight of 1.0000 gram.

1.

Press [6] Calculate Blank from the calibrate menu to


display the edit blank standard screen.
Calculate Blank

Carbon
Standard

0.0000

Sulfur
Standard

0.0000

2.

To edit the blank value, enter the value from the


keyboard, or press the arrow keys to move the cursor to a
digit and enter the digit value with the keypad.

3.

Press Yes to calculate the new blank value, and display the
blank calculation screen.
Blank Results

Operation

Carbon
Old Blank
New Blank

0.0000
0.0012

Sulfur
Old Blank
New Blank

0.0000
0.0010

CS-200

533

4.

Press Menu to display the blank results menu.


Blank Results

[1] Print

534

5.

Press [1] Print to receive a printout of the new blank


calibration values.

6.

Press Exit to return to the select results screen and save


the calculated blank results.

CS-200

Operation

Edit Blank

Notes

Edit blank permits the operator to change the blank


calibration value by entering a new blank value.

This procedure can only be used to enter a predetermined


value. Normal blank calibration should be performed using
calculate blank.

1.

Press [7] Edit Blank from the calibrate menu to display the
edit blank screen.
Edit Blank

Carbon
Old Blank
New Blank

0.0000
0.0012

Sulfur
Old Blank
New Blank

0.0000
0.0010

2.

To edit the calibration value, enter the value from the


keyboard, or press the arrow keys to move the cursor to a
digit and enter the digit value with the keypad.

3.

Press Menu to display the blank results menu.


Edit Blank

[1] Print

Operation

4.

Press [1] Print to receive a printout of the new blank


calibration values.

5.

Press Exit to return to the select results screen and save


the edited blank results.

CS-200

535

Recalculate Results

Notes

Recalculate results permits the operator to recalculate


previous results based on a new calibration value.

Operator must select the results to be recalculated when


using option [2].

1.

Press [3] Calibration from the main menu. The select


results screen will be displayed.
Select Results
ID Code
A0000001
A0000002
A0000003
A0000004
A0000005
A0000006
>A0000007

Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031

0 Selected

1 of 7

Sulfur
0.044
0.051
0.047
0.050
0.051
0.046
0.045

2.

Press the Next/Previous keys to move the cursor down and


up the list of results.

3.

Press Select to move the cursor up and include a sample.

4.

A.

Press Yes to include a sample. The included sample


will be highlighted.

B.

Press No to exclude a sample. The excluded sample


will not be highlighted.

Press [8] Recalculate from the calibration menu to display


the recalculate results menu.
Select Results
ID Code

Carbon

[1] Re-calc Today's


[2] Re-calc Select

2 Selected

536

CS-200

1 of 7

Operation

Operation

5.

Press [1] Re-calc Todays to recalculate todays results


based on the recorded date corresponding to the results.

6.

Press [2] Re-calc Select to recalculate the results that


were previously selected.

7.

Press Exit to recalculate the selected results and return to


the main menu.

CS-200

537

Results Menu

Notes

The results menu displays the list of analysis results.

Through this procedure, analysis results can be transmitted


to a data transmit peripheral, used to generate statistics,
printed out, and/or deleted.

The number of selected results will be displayed on the


bottom line of each results screen.

1.

To access the results screen, press [2] Results from the


main menu. The results screen will appear.
Selected Results

538

ID Code
A0000001
A0000002
A0000003
A0000004
A0000005
A0000006
>A0000007

Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031

0 Selected

1 of 7

Sulfur
0.044
0.051
0.047
0.050
0.051
0.046
0.045

2.

Press the Next/Previous keys to move the cursor either


down or up.

3.

Press Select to move the cursor up and include a sample.


A.

Press Yes to include a sample. The included sample


will be highlighted.

B.

Press No to exclude a sample. The excluded sample


will not be highlighted.

CS-200

Operation

4.

Press the Menu key to display the results menu.


Select Results
ID Code
[1]
[2]
[3]
[4]
[5]
[6]
[7]

5.

Operation

Carbon

Record Format
List Format
Clear Selections
Delete
Statistics
Print
Transmit

Press Exit to return to the results screen.

CS-200

539

Results Format Selection

Notes

The record format is the same as the select results screen


that can display up to eleven results at a time.

The list format displays one result at a time with more


information provided per result.

1.

Press [1] Record Format from the results menu to display


the selected results in the record format. The record
format is the same as the select results screen shown
under step 1.

2.

Press Menu to return to the select results screen.

3.

Press [2] List Format to display the selected results in the


list format. The list format screen will appear with the
sample result indicated by an arrow on the record format
screen.
Select Results
ID Code
Weight
Method Name

540

Result
Calib
Blank
Time
Peak

A0000001
0.1452
1-Method
Carbon
Sulfur
0.8921
0.0322
0.7863
0.9309
0.00000 0.00000
40
44
16462
149

0 Selected

1 of 7

CS-200

Operation

Clear Selections

Note

1.

Clear selections removes the highlight from selected results


quickly giving the operator the opportunity to select other
results.
With results selected on the select results screen, press
the Menu key. The results menu will be displayed.
Select Results
ID Code
Carbon
[1]
[2]
[3]
[4]
[5]
[6]
[7]

2.

Operation

Record Format
List Format
Clear Selections
Delete
Statistics
Print
Transmit

Press [3] Clear Selections to remove the highlight from all


selected results. The select results screen will be
displayed.

CS-200

541

Delete Selected Results


1.

Press [4] Delete from the results menu to delete selected


results. The delete results confirmation screen will appear.
Select Results
ID Code
Carbon
Confirmation
Delete Results
Yes/No

0 Selected

542

1 of 7

2.

Press Yes to delete the selected results and return to the


results screen.

3.

Press No to return to the results screen without deleting


selected results.

CS-200

Operation

Statistics
1.

Press [5] Statistics from the results menu to calculate


statistics based on selected results. The statistics screen
will appear.
Statistics

Carbon
Average
Std. Dev.
RSD
Points
Sulfur
Average
Std. Dev.
RSD
Points

0.311
0.001
0.039
3
0.0354
0.0003
0.73
3

Statistics

[1] Print

Operation

2.

Press Menu to display the statistics menu.

3.

Press [1] Print to receive a printout of the calculated


statistics.

4.

Press Exit to return to the statistics screen.

CS-200

543

Definitions
AverageThe average value of the selected results.
Standard DeviationThe amount of deviation, from the average
value, where 67% of the measured results range. The standard
deviation calculation uses n-1" degrees of freedom.
Relative Standard DeviationThe standard deviation compared
to the average value expressed as a percentage.
(STD DEV/AVG) x 100.
PointsThe number of selected results used to calculate the
average value and standard deviation.

544

CS-200

Operation

Print Selected Results


Press [6] Print from the results menu to receive a printout on
the system printer of the selected results. The select results
screen will appear.
Select Results

Operation

ID Code
A0000001
A0000002
A0000003
A0000004
A0000005
A0000006
>A0000007

Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031

0 Selected

1 of 2

CS-200

Sulfur
0.044
0.051
0.047
0.050
0.051
0.046
0.045

545

Transmit Selected Results


Press [7] Transmit from the results menu to transmit selected
results from the determinator to a peripheral device or
computer. The select results screen will appear.
Select Results

546

ID Code
A0000001
A0000002
A0000003
A0000004
A0000005
A0000006
>A0000007

Carbon
0.030
0.033
0.032
0.033
0.034
0.030
0.031

0 Selected

1 of 2

CS-200

Sulfur
0.044
0.051
0.047
0.050
0.051
0.046
0.045

Operation

Operation for Windows

Keypad

Windows

Keypad

For instruments using DSP software refer to the instructions


on page 51.

For instruments using Windows software refer to the


instructions listed below.

Operation Guidelines...........................................................56
Before an Analysis ......................................................... 57
After an Analysis ........................................................... 58
After Use...................................................................... 58
Crucibles ...........................................................................59
Sample Preparation .......................................................... 510
Sample Size................................................................ 510
High Sulfur Samples .................................................... 510
Blank Samples ....................................................... 510
Analyze Menu .................................................................. 511
Screen Description....................................................... 511
Delete Weight ............................................................. 513
Insert Weight.............................................................. 514
Print Weights .............................................................. 515
System Controls .......................................................... 516
Definitions and Ranges ............................................ 517
Clean Switch............................................................... 518
With Autocleaner .................................................... 518
Without Autocleaner................................................ 519
Balance Weight ........................................................... 520
Transmit Last.............................................................. 521

Operation

CS-200

547

Select Method ............................................................. 522


Sample Weight Entry ........................................................ 523
Sample Analysis ............................................................... 525
Calibrate Menu................................................................. 527
Calibration Results Format Selection............................... 528
Clear Selection ............................................................ 529
Calculate Calibration .................................................... 530
Edit Calibration ........................................................... 532
Calculate Blank ........................................................... 533
Edit Blank................................................................... 535
Recalculate Results ...................................................... 536
Results Menu ................................................................... 538
Results Format Selection .............................................. 540
Clear Selections .......................................................... 541
Delete Selected Results ................................................ 542
Statistics .................................................................... 543
Definitions ............................................................. 544
Print Selected Results .................................................. 545
Transmit Selected Results............................................. 546
Windows

Operation for Windows .................................................... 547


Windows Software Menus .................................................. 552
File Menu ................................................................... 552
Print ..................................................................... 552
Print Preview ......................................................... 552
Print Setup ............................................................ 552
Import .................................................................. 553
Export................................................................... 553
Exit ...................................................................... 553
Edit Menu ................................................................... 554
Insert ................................................................... 554
Fill........................................................................ 554
Cut....................................................................... 554
Copy..................................................................... 554
Paste .................................................................... 554

548

CS-200

Operation

View Menu.................................................................. 555


Tool Bar ................................................................ 555
Status Bar ............................................................. 555
First Row............................................................... 555
Analysis Row.......................................................... 555
Last Row ............................................................... 555
Samples Menu ............................................................ 556
Login .................................................................... 556
Balance ................................................................. 556
Analyze ................................................................. 556
Reset/Abort ........................................................... 556
Recalculate ............................................................ 557
Transmit ............................................................... 557
Delete................................................................... 557
Configuration Menu...................................................... 558
Calibrations ........................................................... 558
Blank .................................................................... 558
Drift ..................................................................... 558
Linearizations......................................................... 558
Standards.............................................................. 559
Methods ................................................................ 559
Counters ............................................................... 559
Sample Templates .................................................. 559
System ................................................................. 559
Users .................................................................... 559
Transmission Formats ............................................. 560
Select Language ..................................................... 560
Auto Widths ........................................................... 560
Display.................................................................. 560
Hardware Calibrations ............................................. 560
Diagnostics Menu ........................................................ 561
Leak Check ............................................................ 561
Ambients............................................................... 561
Switches ............................................................... 561
Solenoids .............................................................. 561
Comport................................................................ 561
Operation

CS-200

549

Maintenance Menu....................................................... 562


Login .................................................................... 562
View Log File.......................................................... 562
Login a Sample ................................................................ 563
Sample Login Definitions .............................................. 565
Balance Login ............................................................. 566
Login using a Sample Template ..................................... 567
Analyze a Sample ............................................................. 568
Delete a Sample............................................................... 569
Print Sample Results ......................................................... 570
Transmit Results .............................................................. 572
Recalculate Result ............................................................ 573
Calibration....................................................................... 574
Blank Calibration ......................................................... 574
Standard Calibration .................................................... 574
Drift Correction ........................................................... 574
Blank Calibration .............................................................. 575
Standard Calibration ......................................................... 576
Standard Calibration Definitions................................ 578
Drift Correction ................................................................ 579
Drift Correction ........................................................... 580
Data Management ............................................................ 581
Insert Data into the Spreadsheet ................................... 581
Insert a Sample Out-of-Sequence .................................. 582
Fill Selected Cells with the Same Values.......................... 582
Select First Row in the Spreadsheet ............................... 583
Select the Analysis Row in the Spreadsheet..................... 583
Select Last Row in the Spreadsheet................................ 583
Import Sample Data .................................................... 583
Export Sample ............................................................ 584
Export Sample Definitions ........................................ 586
Export Buffer .............................................................. 587
Clipboard Use .................................................................. 588
Cut Data to the Clipboard ............................................. 588
Copy Data to the Clipboard ........................................... 588
Paste Data from the Clipboard ....................................... 588
550

CS-200

Operation

Configure Result Plot......................................................... 589


Display the Menu......................................................... 589
Selection Procedures ............................................... 589

Operation

CS-200

551

Windows Software Menus

Note

The information that follows is a list of all the Menus


available from the CS-200 Windows Software. The menus
appear at the top of the screen and drop down when
clicked.

File Menu
This menu permits the operator to configure and print data on
the system printer, import data from another application
software and export data to a floppy disk.
Click File to display this menu.

Print
Select Print to access the report settings dialog box and print
selected sample results on the system printer. Refer to Print
Sample Results on page 570.
Print Preview
Select Print Preview to access the report settings dialog box
and preview how selected samples would print on the system
printer. Refer to Configure the Analysis Report on page 448.
Print Setup
Select Print Setup to access the printer setup dialog box and
configure the system printer settings.

552

CS-200

Operation

Import
Select Import to transfer sample data from another software
application. Refer to Import Sample Data on page 583.
Export
Select Export to transfer sample data to another storage
location like a floppy disk. Refer to Export Sample on page 5
84.
Exit
Select Exit to stop using the CS-200 application program and
return to the Windows Operating System.

Operation

CS-200

553

Edit Menu
This menu permits the operator to insert a sample out of
sequence into the spreadsheet, fill a group of cells in the
spreadsheet with the same data, cut and move data to other
cells, copy data to other cells and paste data to other cells.
Click Edit to display this menu.

Insert
Select Insert to insert a sample out of sequence, between
unanalyzed samples, into the spreadsheet for analysis. Refer to
Data Management on page 581.
Fill
Select Fill to quickly fill a group of cells in the spreadsheet with
the same data value. Refer to Data Management on page 581.
Cut
Select Cut to move data from an entire row in the spreadsheet
to the clipboard. Refer to Clipboard Use on page 588.
Copy
Select Copy to transfer data from an entire row in the
spreadsheet to the clipboard. Refer to Clipboard Use on page
588.
Paste
Select Paste to insert data from the clipboard to a selected row
in the spreadsheet. Refer to Clipboard Use on page 588.

554

CS-200

Operation

View Menu
This menu permits the operator to turn the tool bar and status
bar ON or OFF and select the first row, last row or analysis row
in the spreadsheet.
Click View to display this menu.

Tool Bar
Select Tool Bar to display or hide the toolbar. Refer to
Configure the Screen on page 450.
Status Bar
Select Status Bar to display or hide the status Bar. Refer to
Configure the Screen on page 450.
First Row
Select the First Row of analysis data in the spreadsheet. Refer
to Data Management on page 581.
Analysis Row
Select the Analysis Row that contains the next sample to be
analyzed in the spreadsheet. Refer to Data Management on
page 581.
Last Row
Select the Last Row of analysis data in the spreadsheet. Refer
to Data Management on page 581.

Operation

CS-200

555

Samples Menu
This menu permits the operator to log sample data into the
spreadsheet, analyze a sample, abort an analysis, recalculate
results, transmit results and delete a sample from the
spreadsheet.
Click Samples to display this menu.

Login
Select Login to enter a sample and sample data into the
spreadsheet. Refer to Login a Sample on page 563.
Balance
Select Balance to enter a mass from the balance into the
sample login screen. Refer to Balance Login on page 566.
Analyze
Select Analyze to login and analyze a sample or analyze a
standard. Refer to Analyze a Sample on page 568.
Reset/Abort
Select Abort to stop an analysis in progress. Refer to Analyze a
Sample on page 568.

556

CS-200

Operation

Recalculate
After an analysis is complete, Recalculate Results can be used
to recalculate the result if the extraction data or calibration has
changed. Refer to Recalculate Result on page 573.
Transmit
Select Transmit to transfer selected sample results to a host
computer. Refer to Transmit on page 572.
Delete
Select Delete to remove a selected sample from the
spreadsheet. Refer to Delete a Sample on page 569.

Operation

CS-200

557

Configuration Menu
This menu is used for instrument calibration, to configure the
instrument hardware, to create a method, to configure the
software and for maintenance configuration.
Click Configuration to display this menu.

Calibrations
Select Calibrations to set the accuracy of the instrument to that
of known calibration standard samples. Refer to Calibration on
page 574.
Blank
Select Blank to calculate the system blank and compensate for
it when calculating the analysis result. Refer to Blank
Calibration on page 575.
Drift
Select Drift to compensate standard calibration and account for
variances or Drift in the instrument hardware that can slightly
change the calibration. Refer to Drift Correction on page 579.
Linearizations
Select Linearizations to enter the IR cell reference and
saturation values. Breaks and slopes are not typically set, they
are provided for those who wish to modify the linearity of the
instrument. Refer to Linearization on page 1032.

558

CS-200

Operation

Standards
Select Standards to create a list of standard calibration
samples. Refer to Standards on page 457.
Methods
Select Method to create a set of analysis parameter values for
analysis. Refer to Method Development on page 453.
Counters
Select Counters to automatically determine when periodic
maintenance is necessary. Maintenance data that was entered
into Login Periodic Maintenance is used by the counters to
determine when maintenance is necessary. Refer to Login
Periodic Maintenance on page 624.
Sample Templates
Sample Templates is a quick way for the operator to login a
sample and enter a method, comment and description. Select
Sample Template to develop a specific sample template. After a
sample template is developed, use Login Using a Sample
Template to login a sample with predetermined sample analysis
data. Refer to Sample Templates on page 456.
System
Select System Configuration to set the overall instrument
operating settings and configure the instrument for a specific
application or set of applications. Refer to System Configuration
on page 459.
Users
Select Users to assign an operator and give them access to use
the instrument. Select Assign User Password to add security to
the system by requiring a password to log on to the instrument.
Select Assign User Functions to grant permissions that a user
can use while operating the instrument. Refer to Users on page
472.

Operation

CS-200

559

Transmission Formats
Before data can be transmitted to a host computer, the
transmitted data format must be configured to match. Use
Transmission Formats to Configure Data Transmission. Refer to
Transmission Formats on page 465.
Select Language
Select Language to determine and change the language of text
display by the software. Refer to Select Language on page 4
71.
Auto Widths
Select Auto Widths to automatically adjust the width of each
cell to fit the text. Refer to Configure the Spreadsheet on page
451.
Display
Select Display to set the desktop characteristics as viewed on
the computer monitor. Refer to Configure the Spreadsheet on
page 451.
Hardware Calibrations
Hardware Calibration permits the operator and service person
to calibrate the Back Pressure Controller, Catalyst Heaters, and
Oxygen Flow Rate. Refer to Hardware Calibrations on page 103.

560

CS-200

Operation

Diagnostics Menu
This menu is used to perform a leak check, monitor the
instrument operating parameters, toggle the solenoid valves,
monitor the electrical switch states and check communications
between the instrument and PC.
Click Diagnostics to display this menu.

Leak Check
Select Leak Check to check and determine if the instrument has
an oxygen or pneumatic gas leak. Refer to Leak Check on page
819.
Ambients
Select Ambients to monitor the system operating parameters
and display the ambient monitor. All parameters can be
displayed. Refer to Ambient Monitor on page 822.
Switches
Select Switches to view the electrical switch states. None of the
states can be changed from this screen. Refer to Switches on
page 826.
Solenoids
Select Solenoids to toggle the solenoid valves to check
operation, diagnose instrument problems and perform periodic
maintenance. Refer to Solenoids on page 827.
Comport
Select Comport to check the transfer of data between the PC
and the instrument. Refer to Comport on page 828.

Operation

CS-200

561

Maintenance Menu
This menu permits the operator to login periodic maintenance
and view the maintenance log file.
Click Maintenance to display this menu.

Login
Select Login to login periodic maintenance after it was
performed. Refer to Login Periodic Maintenance on page 624.
View Log File
The system will automatically keep a record of various
procedures that were performed and error conditions. The
record can be viewed using View Log File. Refer to View Log File
on page 625.

562

CS-200

Operation

Login a Sample
Login a Sample is used by the operator to enter sample
information into the spreadsheet. This procedure is called
Sample Login. Using Sample Login the operator can login a
Blank Sample, Standard Sample, Gas Dose Sample or an
Unknown Sample for analysis.
Before a sample is analyzed, the sample type and information
associated with it must be entered into the spreadsheet. A
sample that has been logged in may be analyzed later.
In addition to Sample Login, a sample can be logged in using
Balance Login, page 566, Login using a Sample Template,
page 567, or directly into the Spreadsheet by clicking on the
next available line and typing in the sample data. The sample
name and method can be inserted using the drop-down menu.
1.

Operation

Click Samples and select Login. The Sample Login screen


will appear.

CS-200

563

564

2.

Enter the information required in the dialog box. Refer to


Sample Login Definitions on page 565. The sample type
should be entered for the sample ID.

3.

To enter the mass, with an interfaced balance, it is only


necessary to click Balance, the mass will be entered
automatically.

4.

After entering all the necessary information, click OK to


login the sample.

CS-200

Operation

Sample Login Definitions


Sample NameThe name or type of sample. Enter the sample
type that is being analyzed so the proper sample type will
appear in the spreadsheet.
MassThe weight of the sample. If blanks or gas doses are
analyzed 1.000 gram is automatically entered as the sample
weight. For standards and unknown samples enter the mass of
the sample.
MethodThe method used for analysis. Click the Down Arrow
to select from the list of methods.
CommentsA statement used to explain an operation or
procedure. This is an optional entry.
DescriptionA statement used to describe the type of operation
or procedure. This is an optional entry.
OperatorThe name of the operator logging the samples. This
is an optional entry.
Add to End of ListLogin the sample and add it to the end of
the list in the spreadsheet.
Add as Next Sample to RunLogin the sample and insert it into
the sample list after the last sample that was analyzed.
Keep logging samples until cancel is pressedCheck this box to
log consecutive samples. The login screen will appear again
after OK is clicked. Click Cancel to exit the login screen.

Operation

CS-200

565

Balance Login
Balance automatically enters a row at the spreadsheet. The
sample ID and method will be entered into the row along with
the mass. The sample ID and method will be the same as those
in the previous row. The mass will be the value read on the
balance.
Before the mass can be automatically transferred to the
spreadsheet, the balance must be interfaced with the
instrument. Refer to Balance on page 33 for instructions.
1.

566

Click the Samples menu and select Balance. A row will be


entered at the bottom of the spreadsheet and the mass
displayed on the balance will be automatically entered into
the row. The function key F4 can also be pressed or
Balance can be selected from the toolbar.

CS-200

Operation

Login using a Sample Template

Operation

1.

Click the Samples menu and select Login. The Login


screen will appear.

2.

Click the drop down arrow to the right of sample name and
enter the desired sample name from the drop down list.
The sample name, mass, method, comments, description,
operator will automatically be entered into the
spreadsheet.

3.

Continue with sample login and enter the other necessary


information. Refer to Sample Login Definitions on page 5
65 for more information.

CS-200

567

Analyze a Sample
After a sample is logged in it can be analyzed. Analyze a
Sample starts an analysis. Analysis will start with the first
unanalyzed sample in the spreadsheet. Analyzing will appear in
the date column as the analysis is in progress.
Abort an Analysis will stop an analysis in progress.
Note

WARNING

Before a Sample can be analyzed it must be logged in. To


log in a sample refer to Login a Sample on page 563.

SERIOUS BURNS
After analysis use crucible tongs to remove the
hot crucibles from the pedestal and place them in
the crucible bucket to cool.

1.

Press the Loader Button to open the furnace. Place the


crucible and sample on the pedestal. Press the Loader
Button again to start analysis.
Alternative: After the crucible is on the pedestal you can
click the Samples menu and select Analyze to start
analysis. The function key F5 can also be pressed or
Analyze can be selected from the toolbar.

Notes

Note

568

If you initiate analysis from the Windows software the


piston will not drop down and open.

If you initiate analysis by pressing the loader button the


piston will drop down and open permitting the operator to
add a sample and insert a new crucible.

2.

If it is necessary to stop an analysis click the Samples


menu and select Abort. The function key F6 can also be
pressed or Abort can be selected from the toolbar. The
analysis in progress will stop and Aborted will appear in
the date column.

If the furnace did not start before abort was selected the
analysis will be reset and can be restarted.

CS-200

Operation

Delete a Sample
A sample that has been logged in or analyzed can be deleted
from the spreadsheet. This may be a sample that was logged in
error or a sample that was improperly analyzed.

Operation

1.

Select the sample or samples in the spreadsheet to delete


by clicking on them. To select more than one sample hold
the control key down and click the samples.

2.

Click Samples and select Delete. The selected samples will


be deleted from the spreadsheet.

CS-200

569

Print Sample Results


Print Sample Results can be used to print sample and analysis
data can be printed on the system printer.
Note

570

To print a report with the fields displayed in the spreadsheet


do not select Define Report Fields.

1.

If necessary, configure the printed report before printing


sample results. Refer to Configure the Analysis Report on
page 448.

2.

From the analysis screen, select the desired samples with


analysis data to print on the system printer.

3.

Click File and select Print. The Report Settings screen will
appear.

CS-200

Operation

4. Click OK. The Print screen will appear.

5. Configure the printer as necessary and click OK. The


selected samples will be printed on the system printer.

Operation

CS-200

571

Transmit
Analysis Results can be transmitted or transferred to a host
computer. This permits another person to analyze data as
samples are being analyzed. It can also be used to save
selected results at another location.

572

1.

Select the sample or samples in the spreadsheet to


transmit by clicking on them. To select more than one
sample hold the control key down and click the samples.

2.

Click Samples and select Transmit. The selected samples


will be transmitted to the host computer.

CS-200

Operation

Recalculate Result
After a sample is analyzed, the result can be recalculated if
sample data has changed. The mass, method or calibration may
have changed, or need to be changed, to obtain the desired
result.

Operation

1.

Select the sample or samples in the spreadsheet to


recalculate by clicking on them. To select more than one
sample hold the control key down and click the samples.

2.

Click Samples and select Recalculate. The selected


samples will be recalculated using the new mass, method
or calibration data. The new result will appear in the
spreadsheet.

CS-200

573

Calibration
Calibration is the process that adjusts the instrument to
produce an analysis result to equal that of a known calibration
standard with the same concentration. First a Blank Calibration
is performed, then Standard Calibration and then as daily
maintenance both a Blank Calibration and Drift Correction.
Single point calibration calibrates the instrument to one
calibration point. Multi-point calibration calibrates the
instrument to a set of calibration points over an expected range
of concentrations.

Blank Calibration
Blank Calibration is used to calculate the system blank or
baseline. Sometimes this is called the blank area. Blank
calibration calculates the system blank and compensates for it
when calculating the analysis result. The system blank should
be determined every day by performing a blank calibration
before analysis. Refer to Blank Calibration on page 575.

Standard Calibration
Standard Calibration is used to calibrate the instrument with
known calibration standards. A single point or multi-point
calibration can be performed and the curve type selected
although, LECO recommends multipoint, linear calibrations that
employ 1/certified weighting. Additionally a blank calibration
should be completed prior to performing a standard calibration.
Since Standard Calibration is saved with each method, each
method must be calibrated after it is created. Refer to Standard
Calibration on page 576.

Drift Correction
Drift Correction is used to compensate standard calibration and
account for variances in the instrument hardware that can
slightly change the calibration. Drift correction should be
performed at the start of every day. This insures accurate
calibration and analysis results. Refer to Drift Correction on
page 579.

574

CS-200

Operation

Blank Calibration
Blank calibration calculates the system blank and compensates
for it when calculating the analysis result. Refer to Calibration
on page 574 for more information.

Note

Note

Operation

1.

Login and perform at least three blank analyses.

2.

Select the results of the blank analyses from the


spreadsheet.

3.

Click Configuration and select Blank. The Element


Selection screen will appear.

In the screen below, the software displays the data in blue


to alert the operator that the data has changed.

Step 4 can only be performed if more than one element is


shown in the dialog box.

4.

Include or exclude an element by clicking a row to select


the element and clicking Include/Exclude. The action box
will indicate if the element is included or excluded. If the
element is included a blank calculation will be calculated
for that element.

5.

Click OK to calculate the system blank based on the


analysis results obtained in step one.

CS-200

575

Standard Calibration
Standard Calibration is used to calibrate the instrument with
known calibration standards. Refer to Calibration on page 574
for more information.
Notes

576

Refer to Standard Calibration Definitions on page 578


when performing this procedure.

The instrument blank should be calibrated before


performing standard calibration.

LECO recommends that multipoint linear calibration that


employs 1/certified weighting be used for standard
calibration.

Gas Dose analysis is very similar to standard calibration.


The gas dose (loop) value, based on 100% CO2 (carbon
only), is entered at the factory into the standards database
on the instrument under the name Gas Dose.

1.

Login and perform at least three standard analyses.

2.

Select the results of the standard analyses from the


spreadsheet.

3.

Click Configuration and select Calibrations.

CS-200

Operation

4.

Click the arrow in the drop down box and Select a Cell
(detector) to calculate a calibration for. A separate
calibration can be calculated for each cell.

5.

Click the arrow in the drop down box and Select a Curve
Type. LECO recommends that multipoint linear calibration
that employs 1/certified weighting be used for standard
calibration.

6.

View the curve displayed on the graph. It should intersect


the black squares, which represent the standards. If youre
using multipoint calibration zoom in on each standard for
the most accurate viewing.

7.

Click the arrow in the drop down box and Select the
desired Weighting. LECO recommends that multipoint
linear calibration that employs 1/certified weighting be
used for standard calibration.

8.

Click OK to select the cell to calibrate. One or more cells


can be selected.

9.

Click Print to print a copy of the calculated calibration on


the system printer.

10. Repeat the process for each cell, carbon high, carbon low,
and sulfur.
11. Click OK to exit the calibration procedure and save the
calibration curve.

Operation

CS-200

577

Standard Calibration Definitions


Cell TypeSelects the measurement cell that will be associated
with the calibration curve. The calculated calibration will be
applied to this cell. A different calibration can be calculated and
applied to each cell.
Curve TypeSelects the type of calibration curve. Select a
curve that intersects each calibration result. LECO recommends
that multipoint linear calibration that employs 1/certified
weighting be used for standard calibration.
WeightingDetermines which calibration results, on the
calibration curve, get priority. LECO recommends that
multipoint linear calibration that employs 1/certified weighting
be used for standard calibration.

NormalEach point gets equal priority.

ManualA manual weighting can be entered.

1/CertifiedA weighting factor that can be applied to the


calibration data points. This will counteract a bias for higher
concentrations that develops naturally from the curve fitting
routines.

ShowClick Show to show the last calibration. The last


calibration will appear on the graph in blue.
ManualClick Manual to enter a new calibration equation. This
can be done if a calibration was lost and a previous calibration
recorded.
RMS Error
dispersion
determine
RMS error

(Root Mean Square)A method of quantifying the


or spread of data. It is used in the PC software to
which calibration curve is a better fit. The lower the
the better the fit.

Zoom InDraw a box around a calibration point to zoom in.


Zoom OutClick on a calibration point with the right mouse
button. A Zoom Out button will appear. Click the Zoom Out
button to zoom out.

578

CS-200

Operation

Drift Correction
Drift Correction is used to compensate standard calibration and
account for variances in the instrument hardware over a period
of time that can slightly change the calibration. Drift correction
should be performed at the start of each day. This insures
accurate calibration and analysis results.
Perform standard calibration and choose the drift standards
before performing a drift calibration. Refer to Calibration on
page 574 for more information.

Note

Operation

A Blank Calibration should be performed before every Drift


Correction. Refer to Blank Calibration on page 575.

CS-200

579

Drift Correction

Note

Note

580

1.

Login and perform a standard analysis.

2.

Select the result of the standard analysis from the


spreadsheet.

3.

Click Configuration and select Drift the drift correction


screen will appear.

In the screen below, the software displays the data in blue


to alert the operator that the data has changed.

Step 4 can only be performed if more than one element is


shown in the dialog box.

4.

Include or exclude an element by clicking a row to select


the element and clicking Include/Exclude. The action box
will indicate if the element is included or excluded. If the
element is included a drift calculation will be calculated for
that element.

5.

Click OK to calculate the drift based on the analysis result


obtained in step one.

CS-200

Operation

Data Management
Data Management is a group of procedures that permits the
operator to move sample data from one area of the
spreadsheet to another, move data into the spreadsheet and
move data out of the spreadsheet and store it on a floppy disk.
The following procedures are grouped under Data Management.

Insert Data into the Spreadsheet

Insert a Sample out-of-Sequence

Fill Selected Cells with the Same Values

Select First Row in the Spreadsheet

Select the Analysis Row in the Spreadsheet

Import Sample Data

Export Sample Data

Insert Data into the Spreadsheet


A group of cells, in the spreadsheet, can be quickly filled with
the same data. As an example, the method could be changed in
a group of logged in unanalyzed samples.

Operation

1.

Click and drag the mouse pointer to select the cells to fill
with the same data.

2.

Click Edit and select Fill.

3.

Enter the data to fill into each selected cell.

4.

Click OK to insert the data into the selected cells.

CS-200

581

Insert a Sample Out-of-Sequence


To insert a sample into the spreadsheet, out of sequence and
between unanalyzed samples, Insert should be used.

Note

1.

Click and select a row in the spreadsheet after the last


analyzed sample. (Insert will insert a row before the
selected row.)

2.

Click Edit and select Insert. A row will be inserted into the
spreadsheet before the selected row.

You can also insert a sample out-of-sequence from the


Login screen. Click on a row next to the position where you
want to insert the sample and then select Login F3. Click
the insert position button at the bottom of the screen.

Fill Selected Cells with the Same Values

582

1.

Select the spreadsheet cells to fill with the same data


values.

2.

Click Edit and select Fill. The Fill screen will appear.

3.

Enter the desired values in the dialog box on the fill


screen.

4.

Click OK to fill each of the selected cells with the desired


values.

CS-200

Operation

Select First Row in the Spreadsheet


Using this procedure the first row in the spreadsheet can be
quickly selected.
1.

Click View and select First row.

Select the Analysis Row in the Spreadsheet


Using this procedure the analysis row in the spreadsheet can be
quickly selected. The analysis row is the row that contains the
next sample to be analyzed.
1.

Click View and select Analysis row.

Select Last Row in the Spreadsheet


Using this procedure the Last row in the spreadsheet can be
quickly selected.
1.

Click View and select Last row.

Import Sample Data


Sample data can be imported from another application program
using Import. As an example, data can be entered into Excel
and then transferred to the spreadsheet.

Operation

1.

Click the File menu and select Import.

2.

Select the file to import. Data will be entered into the


spreadsheet starting with the last empty row.

CS-200

583

Export Sample
Export Sample permits the operator to select sample data and
data transmission parameters and transfer them to a file for
storage. More than one configuration can be defined and
selected.

584

1.

Select the analysis samples with analysis data to save as a


file.

2.

Click File and select Export. The Export screen will appear.

3.

Click Add to create an export format. A row will be added


to the bottom of the spreadsheet.

4.

If desired, select a row and click Delete to remove the


selected format.

5.

Click a row and enter a format name.

CS-200

Operation

6.

Click Properties. The Export Properties screen will appear.

7.

Select the Fields tab.

8.

For each field to transmit, select the Field from the fields
list box and click Add.

9.

Click the Delimiters tab.

10. Select the Field delimiter and End of Line delimiter.


11. Click the Preview tab to view the selected data transmit
format.
12. Select the Filename tab.
13. Click the edit box and enter a filename to save the sample
analysis data in.
14. Click browse and select a folder to save the sample
analysis data file in.
15. Click Save in the export filename dialog box.
16. Click OK in the export format properties dialog box.
17. Select either append to file, automatically increment
filename or prompt for filename as desired. Refer to
Export Sample Definitions on the next page.
18. Click Export, in the export formats dialog box, to save the
file.

Operation

CS-200

585

Export Sample Definitions


Append to FileWhen selected the highlighted sample analysis
data will be attached to the previously saved file.
Automatically Increment FilenameIf the last characters in the
filename contains numbers they will automatically be
incremented by one when the file is saved.
Prompt for FilenameWhen selected, the export filename
dialog box will appear prompting the operator to enter a
filename.

586

CS-200

Operation

Export Buffer
Export Buffer permits the operator to select a sample and
transfer the plot buffer data contents to a file.

Operation

1.

Select the analysis samples with analysis data to save as a


file.

2.

Click File and select Export. The Export screen will appear.

3.

Click Buffer to display the Save As dialog box.

4.

Select a folder and type as a file name for the buffer


contents you want to save. It is not necessary to add an
extension after the file name.

5.

Click Save to save the buffer contents as a file.

CS-200

587

Clipboard Use
The Clipboard is a temporary storage space for data. Data can
be moved into and out of the clipboard by cutting, copying or
pasting. By using the clipboard cell data can be moved
throughout the spreadsheet.

Cut Data to the Clipboard


Note

Cut is used to remove data from an entire row in the


spreadsheet to the clipboard. Once on the clipboard it can
be pasted into another location.

1.

Select the row of data in the spreadsheet to cut.

2.

Click the Edit menu and select Cut. The data will be
removed from the spreadsheet and moved to the
clipboard.

Copy Data to the Clipboard


Note

Copy is used to duplicate data from an entire row in the


spreadsheet to the clipboard. Once on the clipboard it can
be pasted into another location.

1.

Select the row of data in the spreadsheet to copy.

2.

Click the Edit menu and select Copy. The data will be
copied from the spreadsheet to the clipboard.

Paste Data from the Clipboard


Note

588

Paste is used to paste data from the clipboard to a selected


row in the spreadsheet.

1.

Select an empty row in the spreadsheet to insert analysis


data that has been moved to the clipboard.

2.

Click the Edit menu and select Paste. The data will be
moved from the clipboard to the spreadsheet.

CS-200

Operation

Configure Result Plot


The CS200 Windows Software permits the operator to configure
the result plot to show the desired result information on the
plot as determined by the operator. The Configure Result Plot
menu give the operator the choice of zooming out, zooming out
one level, labeling plotted points, plotting the statistical points,
and selecting an auto independent scale. Plot properties can
also be selected from this menu.

Display the Menu


1.

To display the Configure Result Plot menu, move the


mouse pointer to the result plot and right click on the plot.
The Configure Result Plot menu will appear.

2.

Click on the menu selection to select or deselect it. A


check indicates the item has been selected.

3.

When finished, click on the plot to remove the menu.

Selection Procedures
Zoom In (not a menu selection)Position the pointer (mouse
pointer) over the area to zoom in on. Hold the left mouse
button down and draw a box. The area inside the box will be
magnified. Draw another box to zoom in farther. Zoom In
cannot be used if the sample being analyzed is displayed. Wait
until analysis is complete and then zoom in on the plot.
Zoom OutClick Zoom Out to remove all steps of
magnification.
Zoom Out One LevelClick Zoom Out to remove the last step
of magnification.
Label PointsWhen result points are selected and displayed,
the points can be numbered to show their relationship to the
samples selected. The first sample selected is labeled number 1
and the remaining samples selected are numbered as they
were selected from the spreadsheet. The number displayed on
the plot is not the sample number displayed on the
spreadsheet. Multiple samples and statistics (below) must be
selected before this feature can be used.

Operation

CS-200

589

StatisticsChanges the plotted result curves to plotted result


points. A point is shown for each sample and represents the
peak concentration. Multiple samples must be selected before
result points can be plotted.
Auto Independent ScaleIf multiple plots are displayed they
will be scaled the same. This means if one plot is many times
larger than one of the other plots the smaller plot may be hard
to see or not seen at all. By selecting auto independent scale,
all plots will be made the same height in order to compare one
plot to another.
PropertiesClick Properties to display the Plot Properties
Configuration screen.

From the Properties screen you can select the Reporting Units,
Significant Digits, Plot Pattern and Plot Color. You can also Hide
the Baseline and Plot if desired.

590

CS-200

Operation

Maintenance
6 Maintenance

Illustrations .......................................................................62
Periodic Maintenance Schedule .............................................63
Anhydrone Tube.................................................................64
Removal....................................................................... 64
Packing ........................................................................ 64
Autocleaner .......................................................................66
Autocleaner Assembly .................................................... 67
Autocleaner Mesh Filter .................................................. 69
Autocleaner O-rings ..................................................... 610
Catalyst Heater Tube Packing ............................................. 611
Cellulose Filter ................................................................. 613
Removal..................................................................... 613
Packing ...................................................................... 613
Combustion Tube ............................................................. 615
Combustion Zone O-rings .................................................. 616
Incoming Reagent Tube..................................................... 617
Removal..................................................................... 617
Packing ...................................................................... 617
Lance and Filter Assembly ................................................. 619
Pinch Valve Tubing ........................................................... 621
Reagent Tube Screen Filter ................................................ 623
Login Periodic Maintenance ................................................ 624
View Log File ................................................................... 625
Reset Maintenance Counters .............................................. 626

Maintenance

CS-200

61

Illustrations
Figure 61......... Anhydrone Tube ........................................ 65
Figure 62......... Autocleaner Assembly ................................ 68
Figure 63......... Catalyst Heater Tube Packing ...................... 612
Figure 64......... Cellulose Filter Packing ............................... 614
Figure 65......... Reagent Tube Removal ............................... 618
Figure 66......... Reagent Tube Packing ................................ 618
Figure 67......... Lance and Filter Assembly........................... 620
Figure 68......... Pinch Valve Assembly ................................. 622

62

CS-200

Maintenance

Periodic Maintenance Schedule


Equipment/Material

Replacement/Cleaning
Schedule

Inspection Schedule

Anhydrone Tube

When anhydrone cakes.


Refer to page 64.

Inspect daily.
Replace as needed.

Autocleaner

Daily.
Refer to page 66.

Disassemble
and clean daily.

Autocleaner Mesh Filter

Daily.
Refer to page 69.

Inspect monthly.
Clean if flow is restricted.

Autocleaner O-rings

Daily.
Refer to page 610.

Inspect monthly.
Grease or replace
as necessary.

Catalyst Heater Tube


Packing

Replace packing
every six months.
Refer to page 611.

Replace the silica gel and


quartz wool as directed.

Cellulose Filter

Replace when one inch of


cellulose material turns
black or uniformly brown.
Refer to page 613.

Replace cellulose.
Inspect o-rings.
Clean or grease
as necessary.

Combustion Tube

Brush every
five to ten analysis.
Refer to page 615.

Inspect every eight hours.

Combustion Zone O-rings

Replace if damaged.
Refer to page 616.

Inspect every eight hours.


Grease or replace
as necessary.

Incoming Reagent Tube

When lecosorb turns white


or anhydrone cakes.
Refer to page 617.

Inspect daily and replace


as necessary.

Lance and Filter Assembly

Daily.
Refer to page 619.

Clean when Cleaning Time


message is displayed
or at intervals set
from system options.

Pinch Valve Tubing

Replace every 90 days


or if damaged.
Refer to page 621.

Inspect monthly.
Replace as necessary.

Reagent Tube Screen Filter

Replace if damaged.
Refer to page 623.

Inspect monthly.
Clean or replace
if flow is restricted.

Maintenance

CS-200

63

Anhydrone Tube

Removal
1.

Slide the anhydrone tube upward until the bottom end can
swing free. Refer to Figure 65, page 618.

2.

Tilt out the free anhydrone tube end.

3.

Pull the anhydrone tube downward off the top port.

4.

To reinstall the anhydrone tube, push the top end of the


anhydrone tube over the top port, tilt it inward and pull it
down, pushing it over the bottom port.

Packing

64

1.

Before packing the incoming reagent tube, remove all


material from the inside of the incoming reagent tube;
rinse it with water and let it dry.

2.

Insert a screen filter into the bottom of the anhydrone


tube. Refer to Figure 61, page 65. Position the o-ring
towards the bottom and push the screen filter up onto the
anhydrone tube 1/4 inch.

3.

Pack 2 inches of quartz wool into the bottom of the


anhydrone tube .

4.

Pour 2 inches of anhydrone onto the quartz wool and


gently tap it down. Add anhydrone as necessary to
maintain a level of 2 inches.

5.

Pack 1/2 inch of quartz wool on top of the anhydrone


leaving a 1 inch opening at the top of the anhydrone tube.

6.

Insert the reagent stop into the top of the anhydrone


reagent tube. Push is firmly on top of the quartz wool to
hold the packing material in place.

7.

Reinstall the packed anhydrone tube into the lower left


reagent tube port blocks on the front panel.

CS-200

Maintenance

789-095
REAGENT STOP
765-976
O-RING
(2 REQ'D)
502-177
1/2" QUARTZ WOOL

501-171
2" ANHYDRONE

601-390
QUICK
DISCONNECT
TUBE

502-177
2" QUARTZ WOOL

775-306
SCREEN FILTER

Figure 61
Anhydrone Tube

Maintenance

CS-200

65

Autocleaner

Notes

Keypad

The Autocleaner Kit is an optional accessory. Refer to


Options, page 134, for ordering information.

If the autocleaner is not installed, refer to Lance and Filter


Assembly, page 619, for the combustion area cleaning
procedure.

The autocleaner should be disassembled daily and the lance


cleaned.

Refer to the following steps for operation with the DSP


instrument.

Refer to System Options on page 419 and enable the


autocleaner and door option. The Autocleaner will not function
until these system options have been selected.

Windows

The autocleaner cleans the combustion tube according


to the clean interval programmed in the System Controls
procedure, page 516. It is not recommended to set the
clean counter at 0, as the Dust Filter Alarm will appear
on the screen. Change the setting to 1 to 50.

If cleaning is desired before the interval is reached, or if


the configuration is set to clean the combustion tube at
the operator's discretion, initiate a cleaning cycle from
the analyze menu.

Refer to the following steps for operation with the Windows


instrument.

Refer to System Configuration on page 459 and enable the


autocleaner and door option. The Autocleaner will not function
until these system options have been selected.

66

The autocleaner cleans the combustion tube according


to the clean interval programmed in the Configure
Maintenance Counters procedure, page 446.

If cleaning is desired before the clean interval is


reached, or if the configuration is set to clean the
combustion tube at the operator's discretion, initiate a
cleaning cycle from the tool bar above the spreadsheet
by clicking F10.

CS-200

Maintenance

Autocleaner Assembly

Maintenance

1.

Unlock the autocleaner cap by pulling down on the


plunger, rotate the autocleaner cap clockwise and lift the
autocleaner cap. Refer to Figure 62, page 68.

2.

Remove the autocleaner cap and lance assembly from the


body assembly. Clean the end of the lance using the wire
brush.

3.

Clean the inside of the lance using the lance cleaning rod.

4.

Inspect the brushes for wear. Remove the o-rings from the
filter and replace them.

5.

Reassemble the autocleaner cap and lance assembly to the


autocleaner body.

CS-200

67

604-291
AIR CYLINDER
806-214
FITTING
(2) REQD

604-519
EXTENSION

807-261
FITTING
(2) REQD
193-143
LOCKWASHER
610-735
SLOTTED
BRUSH

807-196
TUBING
(2) REQD

604-517
RETAINER
604-516
FITTING

773-320
O-RING
(2 REQD)

789-115
LANCE TUBE

604-268
BODY
ASSEMBLY

193-164
LOCKWASHER
(2 REQD)

604-172
O-RING
604-274
SHAFT
604-163
BRUSH
762-058
O-RING

190-228
SCREW
(2 REQD)
604-159
PLUNGER

604-273
BUSHING
ADAPTOR

604-272
CAP
190-757
SCREW
(4) REQD

604-168
LOCK
MOUNT

771-991
O-RING

778-703
SPACER
(4) REQD

778-596
FILTER

190-090
THUMBSCREW
(2 REQD)

762-058
O-RING

773-926
PLATE
190-431
SCREW
(2) REQD

762-058
O-RING

773-577
PISTON RING

Figure 62
Autocleaner Assembly

68

CS-200

Maintenance

Autocleaner Mesh Filter

Note

Note

The mesh filters, located in both the automatic cleaning


mechanism and the lance and filter assembly, must be
inspected monthly and cleaned or replaced when flow is
restricted.

1.

Turn off the oxygen gas flow.

2.

Disconnect the gas lines to the autocleaner assembly (or


lance and filter assembly).

3.

Remove and disassemble the cleaning assembly.

4.

Reach into the body assembly and pull the metal filter out.

5.

Remove the o-rings from the filter using the o-ring


removal tool.

6.

Use one liter (or quart) of ultrasonic cleaner and 3.5 ml of


Leconal wetting agent in 700 ml of room temperature
water to clean the metal mesh filter.

7.

Suspend the filter in the solution so it is completely


immersed but does not touch the sides or bottom of the
cleaner tank.

8.

Switch the ultrasonic cleaner on and clean the filter for a


minimum of 10 minutes.

9.

Higher frequency cleaners, which are generally more


efficient, need less cleaning time than lower frequency
cleaners.
While the filter is being cleaned, inspect the brush
assembly.
A.

Put a light coat of silicone grease on the brush shaft


and plate assembly.

B.

Insert the lance cleaning rod into the lance extension


tube and clean out the lance extension tube.

10. After the filter has been cleaned, remove it from the tank
and rinse it for two minutes under clean running water,
then dry with warm air.
11. Wipe clean and lubricate the o-rings with silicone grease.
Reinstall the o-rings.
12. Install the filter in the body assembly and reassemble the
cleaning brush assembly if necessary.
13. Reconnect the gas lines.

Maintenance

CS-200

69

Autocleaner O-rings

Note

1.

Disconnect the pneumatic lines and the lance and measure


flow lines.

2.

Unlock the autocleaner cap by pulling down on the


plunger, rotate the autocleaner cap clockwise and lift the
autocleaner cap. Refer to Figure 62, page 68.

3.

Unscrew the shaft from the air cylinder rod.

4.

Unscrew the four screws from the air cylinder and remove
the cylinder from the autocleaner cap.

5.

Reach into the cap and remove both o-rings.

6.

Wipe the o-rings and apply a small amount of fresh


silicone grease to each. Replace the o-rings in the
autocleaner cap.

7.

For proper alignment when reassembling the auto cleaner:

8.

610

Every month, inspect the o-rings located in the autocleaner


assembly and grease when needed.

A.

Extend the air cylinder rod about two inches.

B.

Slide the autocleaner cap over the rod and screw the
shaft into the rod.

C.

Set the screws and spacers in place.

D.

Grasp the extension and push the shaft up into the


bore of the autocleaner cap.

E.

When the shaft is in the cap bore, the screws can be


tightened down in radial fashion.

Replace the autocleaner cap on the body assembly and


twist it counterclockwise.

CS-200

Maintenance

Catalyst Heater Tube Packing

WARNING

HIGH TEMPERATURE HAZARD


The catalyst heater tube is extremely hot. Wear
heat-resistant gloves when removing the tube.

1.

Set the gas flow to OFF.

2.

Locate the catalyst heater on the front panel.

3.

Remove the movable block, from the top of the catalyst


heater, by unscrewing the moveable block knob. Refer to
Figure 63, page 612.

4.

Lift the catalyst heater tube straight up to remove it and


set it aside to cool.

5.

Remove the packing material from the catalyst heater


tube. Discard the packing material and clean the empty
catalyst heater tube.

6.

Insert 3/4 inch of quartz wool into the catalyst heater tube
and position it at the bottom of the bubble in the catalyst
heater tube.

7.

Pour 1 inch of platinized silica gel into the catalyst heater


tube filling the bubble above the quartz wool.

8.

Insert 3/4 inch of quartz wool into the catalyst heater tube
and position it on top of the platinized silica gel.

9.

Carefully check the packed catalyst heater tube to ensure


no strands of quartz wool are left in the neck of the
catalyst heater tube.

10. Reinstall the catalyst heater tube using the procedure in


steps 3 and 4.
11. Set the gas flow to ON.

Maintenance

CS-200

611

772-694
MOVABLE
BLOCK
KNOB

614-316
MOVABLE
BLOCK

772-520
O-RING
772-739
TUBE

502-177
/4" QUARTZ
WOOL

501-587
1" PLATINUM
SILICA CATALYST

502-177
/4" QUARTZ
WOOL

Figure 63
Catalyst Heater Tube Packing

612

CS-200

Maintenance

Cellulose Filter

Notes

When 1 inch of cellulose turns black or when the cellulose


uniformly turns brown, replace the cellulose filter tube.

Cellulose filter tube is located under the catalyst heater.

Removal
1.

Slide the cellulose filter tube upward until the bottom end
can swing free.

2.

Tilt out the free cellulose filter tube end.

3.

Pull the tube downward off the top port.

4.

Using tweezers, remove the cellulose material and discard.

5.

To reinstall the cellulose filter tube, push the top end of


the cellulose filter tube over the top port, tilt it inward and
pull it down, pushing it over the bottom port.

Packing
1.

Notes

Maintenance

Fill the cellulose filter tube with 21/2 inches of cellulose


material, packing the cellulose to a uniform density.

The cellulose fibers should not be twisted.

Leave 1/2 inch of the cellulose filter tube open at both ends
for reinstallation onto the unit. Refer to Figure 64, page 6
14.

2.

Reinstall the packed cellulose filter tube into the cellulose


filter tube port blocks on the front panel.

CS-200

613

764-098
CELLULOSE

771-030
QUICK
DISCONNECT
TUBE

Figure 64
Cellulose Filter Packing

614

CS-200

Maintenance

Combustion Tube

Notes

Keypad

If the autocleaner is installed the clean interval can be set


to automatically clean the combustion tube. There are two
procedures available, one for the DSP version and one for
the Windows version.

Refer to the following steps for operation with the DSP


instrument.

A. Refer to System Options, page 419, to enable the


autocleaner and door option. Autocleaner will not function
until the system option has been set.
B. The autocleaner cleans the combustion tube according to
the clean interval programmed in the System Controls
procedure, page 516. It is not recommended to set the
clean counter at 0, as the Dust Filter Alarm will appear on
the screen. Change the setting to 1 to 50.
C. If cleaning is desired before the interval is reached, or if the
configuration is set to clean the combustion tube at the
operator's discretion, initiate a cleaning cycle from the
analyze menu.
Windows

Refer to the following steps for operation with the Windows


instrument.

A. Refer to System Configuration, page 459, to enable the


autocleaner and door option. Autocleaner will not function
until the system option has been set.
B. The autocleaner cleans the combustion tube according to
the clean interval programmed in the Configure
Maintenance Counters procedure, page 446.
C. If cleaning is desired before the clean interval is reached, or
if the configuration is set to clean the combustion tube at
the operator's discretion, initiate a cleaning cycle from the
tool bar above the spreadsheet by clicking F10.

Note

Maintenance

If the lance and filter assembly is installed, perform the


following procedure.

1.

Brush the combustion tube every five to ten analyses to


remove dust from the screen filter and combustion area.

2.

Inspect the combustion tube every eight hours for severe


pitting and slag build-up. Remove and clean the
combustion tube if necessary.

CS-200

615

Combustion Zone O-rings


Inspect both combustion zone o-rings every 8 hours of
operation. Check for contamination or damage. One o-ring is
located at the top of the combustion tube. The other o-ring is a
red silicone o-ring located at the bottom of the combustion
tube. Refer to Figure 2-9, page 219.

616

CS-200

Maintenance

Incoming Reagent Tube

Removal
1.

Slide each reagent tube upward until the bottom end can
swing free. Refer to Figure 65, page 618.

2.

Tilt out the free reagent tube end.

3.

Pull the tube downward off the top port.

4.

To reinstall the reagent tube, push the top end of the


reagent tube over the top port, tilt it inward and pull it
down, pushing it over the bottom port.

Packing

Maintenance

1.

Before packing the reagent tube, remove all material from


the inside of the reagent tube; rinse it with water and let it
dry.

2.

Insert a screen filter into the bottom of each reagent tube.


Position the o-ring towards the bottom and push the
screen filter up into the reagent tube 1/4 inch. Refer to
Figure 66, page 618.

3.

Insert a screen filter into the bottom of the reagent tube,


see Figure 66, page 618. Position the o-ring towards the
bottom and push the screen filter up onto the reagent tube
1
/4 inch.

4.

Pack 1/2 inch of quartz wool into the bottom of the reagent
tube.

5.

Pour 1 inch of anhydrone onto the quartz wool and gently


tap it down. Add anhydrone as necessary to maintain a
level of 1 inch.

6.

Pour Lecosorb onto the anhydrone until all but the top 1/2
inch of the reagent tube is filled, gently tapping it down.

7.

Firmly pack 1/2 inch of quartz wool on top of the Lecosorb


filling the bubble in the reagent tube.

8.

Reinstall the packed reagent tube into the lower left


reagent tube port blocks on the front panel.

CS-200

617

771-373
REAGENT
TUBE

Figure 65
Reagent Tube Removal

502-177
/2" QUARTZ WOOL

502-174
2" LECOSORB

771-373
QUICK DISCONNECT
TUBE
501-171
1" ANHYDRONE

502-177
/2" QUARTZ WOOL
775-306
SCREEN FILTER

Figure 66
Reagent Tube Packing

618

CS-200

Maintenance

Lance and Filter Assembly

Notes

Note

Maintenance

The lance and filter assembly should be cleaned when the


cleaning counter reaches the preset limit.

If the optional vacuum cleaner was installed, it may be used


to remove dirt, soot, or debris from the lance, combustion
area, and furnace shelf.

If the autocleaner is installed, refer to Autocleaner, page


66, for mesh filter cleaning.

1.

Loosen the connection on the lance flow inlet 1/4 turn and
disconnect the line.

2.

Unscrew the filter cap. Scrape and remove the dust and
soot from inside the filter cap. Refer to Figure 67, page
620.

If the vacuum cleaner is installed, it may be turned on to


draw dust from the filter housing.

3.

Thoroughly brush the entire lance guard using the cleaning


brush.

4.

Insert the cleaning brush into the combustion tube


chamber and brush the inside of the chamber several
times.

5.

Inspect the tip of the lance to verify that it is open. If it is


clogged, open it using the lance cleaning rod. Refer to
Figure 67, page 620.

6.

Replace the filter cap and reconnect the lance flow line.

7.

Turn the vacuum cleaner off if it was used during the


cleaning process.

CS-200

619

773-311
FILTER

781-422
FILTER CAP
781-424
O-RING

762-058
O-RING

*772-704
FITTING

781-421
FILTER
HOUSING
*773-136
FITTING

781-663
LANCE
GUARD
789-118
LANCE TUBE
ASSEMBLY

771-991
O-RING
781-423
ADAPTOR TUBE
BUSHING

772-381
LANCE
CLEANING
ROD

762-058
O-RING
773-577
PISTON
RING
190-431
SCREW
(4) REQD

781-425
FILTER END
PLATE
190-258
SCREW
(2) REQD

LANCE
TUBE

762-068
O-RING

*781-401
ADAPTER
RING
NOTE: * NOT PART OF ASSEMBLY

Figure 67
Lance and Filter Assembly

620

CS-200

Maintenance

Pinch Valve Tubing

Note

Replace the pinch valve tubing, which passes through the


pinch valve assembly that controls dust ejection, every 90
days. Only use silicone tubing for replacement.

1.

Remove the dust box and vacuum hose from the right side
of the furnace and remove the right side furnace panel.

2.

Turn off the pneumatic gas supply and relieve the


pressure.

3.

Remove the two screws holding the furnace interlock


relay and pinch valve assembly in place. Refer to
Figure 11-3 on page 11-5.

4.

Set the furnace interlock relay and screws aside.

5.

Remove the two screws retaining the pinch valve cap.


Refer to Figure 68, page 622.

6.

Slide the tubing off the cup assembly.

7.

Replace the silicone tube and reassemble pinch valve


assembly.

8.

Position the pinch valve assembly and furnace interlock


relay in place. Fasten using the two screws removed in
step #4.

9.

Replace the side panel, sliding the silicone tube through


the hole provided at the bottom of the side panel.

10. Replace the dust box and vacuum hose then restore
pneumatic pressure.

Maintenance

CS-200

621

616-892
BRACKET

190-246
SCREW
(2 REQ'D)

589-182
FITTING

774-612
HOUSING
774-613
O-RING
769-973
ROLL PIN
(2 REQ'D)
774-610
PISTON

772-909
PINCH VALVE
ASSEMBLY

776-093
CAP
190-246
SCREW
(2 REQ'D)
501-110-019
SILICONE
TUBE

Figure 68
Pinch Valve Assembly

622

CS-200

Maintenance

Reagent Tube Screen Filter

Note

Maintenance

Clean the screen filter in the reagent tube whenever the


reagents are replaced.

1.

Tap the filter lightly to remove any dust.

2.

If necessary, clean the filter in an ultrasonic cleaner.

CS-200

623

Login Periodic Maintenance


After periodic maintenance is performed it should be recorded.
To electronically record maintenance the procedures under
maintenance should be used. Login permits the service
technician or operator to enter maintenance that was
performed. View log file automatically enters past events and
maintenance performed.
Logging in periodic maintenance creates a periodic maintenance
history file, sets the analysis counter back to zero, increments
the reset counter, enters the reset data and enters any
comments.

624

1.

Click Maintenance and select Login. The Maintenance


screen will appear.

2.

Click the Maintenance Item Check Box that periodic


maintenance was performed on. Items that need
maintenance will have already been checked.

3.

Click the Comment Box and enter any maintenance


comments.

4.

Click OK.

CS-200

Maintenance

View Log File


The Log File is a history of past events. Every time one of the
following procedures is performed it will be recorded in the Log
File.

Maintenance

Change of Mass by Operator

Data Out of Range (Ambient Monitor parameter values)

Date of last calibration, drift or blank

Date scheduled maintenance is performed

Dust Clog in System

Equivalency Test Results (the variation between the two


CO2 cells)

Network Errors

Network Sign-on Errors

Sample Aborted

Sample Deleted

Standard check out-of-range

1.

Click Maintenance and select View Log File the Log File
screen will appear.

2.

Click Print to receive a printout of the log file on the


system printer.

3.

Click OK when finished.

CS-200

625

Reset Maintenance Counters

Note

626

After maintenance is performed a history log of


maintenance is generated. Refer to View Log File on page
625. This information can be used to verify that
maintenance was performed and help troubleshoot
problems that may occur during operation.

1.

Select the Maintenance and click Login. The Maintenance


dialog box will appear.

2.

Select the item(s) that maintenance has been performed


on.

3.

Click OK.

CS-200

Maintenance

4.

5.

6.

Maintenance

The Confirm dialog box for the first maintenance item will
appear.
A.

Click Yes if maintenance was performed.

B.

Click No if maintenance was not performed.

C.

Click Cancel to exit procedure.

The Confirm dialog box for the second maintenance item


will appear.
A.

Click Yes if maintenance was performed.

B.

Click No if maintenance was not performed.

C.

Click Cancel to exit procedure.

Continue until all maintenance items were displayed in the


Confirm dialog boxes and answer Yes, No or Cancel to the
procedure.

CS-200

627

Theory of Operation
7 Theory of Operation

Illustrations .......................................................................72
General Information............................................................73
Infrared Radiation, Absorption, and Detection.........................74
Comparator Level ...............................................................78

Theory of Operation

CS-200

71

Illustrations
Figure 71 Gas Flow Diagram............................................... 76
Figure 72 Gas Flow with Autocleaner Diagram....................... 77

72

CS-200

Theory of Operation

General Information
The CS-200 Carbon/Sulfur Determinator is a microprocessor
based, software driven instrument for measurement of carbon
and sulfur content in metals, ores, ceramics, and other
inorganic materials. The CS-200 uses an induction furnace and
measures carbon and sulfur by infrared absorption.
Analysis begins by weighing out a sample (1 g nominal) into a
ceramic crucible on a balance. Accelerator material is added,
the crucible is placed on the loading pedestal, and the analyze
key is pressed. Furnace closure is performed automatically,
then the combustion chamber is purged with oxygen to drive
off residual atmospheric gases. After purging, oxygen flow
through the system is restored and the induction furnace is
turned on. The inductive elements of the sample and
accelerator couple with the high frequency field of the furnace.
The pure oxygen environment and the heat generated by this
coupling cause the sample to combust. During combustion,
carbon bearing elements are reduced, releasing the carbon,
which immediately binds with the oxygen to form CO and CO2,
the majority being CO2. Also, sulfur-bearing elements are
reduced, releasing sulfur, which binds with oxygen to form SO2.
Sample gases are swept into the carrier stream. Sulfur is
measured as sulfur dioxide in the first IR cell. A small amount
of carbon monoxide is converted to carbon dioxide in the
catalytic heater assembly; SO2 is converted to SO3, while sulfur
trioxide is removed from the system in a cellulose filter. Carbon
is measured as carbon dioxide in the IR cell as gases flow
through the IR cells.
The optional automatic autocleaner is ideal for high volume
applications and reduces operator time. The autocleaner
brushes the filter screen and combustion tube at intervals
specified in System Configuration.

Theory of Operation

CS-200

73

Infrared Radiation, Absorption, and Detection


The infrared (IR) source consists of nichrome wire that is
resistance-heated to 850oC. The IR source radiates visible
energy as well as all wavelengths in the infrared spectrum.
The description below uses carbon dioxide although, the same
principle applies to sulfur detection.
Carbon dioxide absorbs IR energy at a precise wavelength
within the IR spectrum. Energy from the IR source is absorbed
as the gas passes through the cell, preventing it from reaching
the IR detector. All other IR energy is prevented from reaching
the IR detector by a narrow bandpass filter. Because of the
filter, the absorption of IR energy can be attributed only to
carbon dioxide (CO2). The concentration of CO2 is detected as a
reduction in the level of energy at the detector.
One IR cell is used as both a reference and for measurement.
The total carbon, as carbon dioxide, is detected on a continuous
and simultaneous basis. The cell consists of an IR source,
chopper motor, a narrow bandpass filter, a condensing cone, an
IR energy detector and the cell body. Radiated energy is
chopped at a rate of 87.5 Hz. before it enters the cell body. The
chopped energy enters the cell body through a window, travels
through the cell body, then exits through a second window and
a precise bandpass filter. The selective filter passes only the
CO2 absorption wavelength into a condensing cone that
concentrates the energy on the detector. The solid state
detector is AC coupled to a preamplifier. As the gas
concentration increases, the voltage to the preamplifier
decreases.
The starting reference level, or baseline, for the detector is
established by running 100% oxygen through the cell. The pure
oxygen environment permits the maximum amount of energy
to reach the detector. This maximum energy level is AC coupled
to the preamp where it is amplified, rectified, and filtered. It is
then sent to an A/D converter where the analog signal is
converted to a digital signal. The nominal voltage read at the
cell output, via the Ambient Monitor, is 8.500 VDC.
During every analysis, the computer reads the baseline. This
level is then adjusted digitally until a nominal level is achieved.
For example, if the cell output is 8.400 VDC, then this level is
change digitally until the level reads 8.500 VDC. This level
change is done in the computer and used for a reference, if the
cell output voltage were actually measured, no change would
be observed.

74

CS-200

Theory of Operation

As analysis begins, the cell output decreases with the amount


of carbon (as CO2) present in the cell. The computer reads the
cell output 20 times per second and produces data points that
are stored in memory. The computer then processes the curve
or graph formed by these data points. The curve or graph is
then used by the computer to calculate the element weight
percent of an unknown sample.

Theory of Operation

CS-200

75

BAROM
PRESSURE
TRANSDUCER

BAROM
CTRL
VALVE

PT

OVEN

FM

EXHAUST

FLOW
CONTROLLER

TRANSDUCER &
REGULATOR
ASSEMBLY
MEASURE
FLOW
ROTAMETER

SO3
TRAP
CELLULOSE
FILTER

SV3

CATALYST
HEATER

UPSTREAM
PRESSURE
GUAGE

PS

RESTRICTOR

PRESSURE
SWITCH

WIRE MESH
FILTER

PS
O2 IN
40 PSI

LECOSORB/ANH
PARTICLE
FILTER

SO2
IR
CELL

CO 2
IR CELL

SV1

SV2
QUARTZ
WOOL

C
NO

ANH

PRESSURE
REGULATOR

NC
SV9

INCOMING
PRESSURE
GUAGE
RESTRICTOR

EXH

SV5
PS

PRESSURE
SWITCH

SV11
NC

DOOR SOL. (OPTIONAL)

NO
4 PSI
PRESSURE
SWITCH

PS

SV12
NC

AUTO CLEANER (OPTIONAL)

NO

PS
25 PSI

PS
SV7

PNEUMATIC
PRESSURE
40 PSI

4 PSI

DOWN
SV10
NC

PARTICLE
FILTER

UP

NO

SAFETY
PRESSURE
REGULATOR

Figure 71
Gas Flow Diagram

76

CS-200

Theory of Operation

BAROM
PRESSURE
TRANSDUCER

BAROM
CTRL
VALVE

PT

OVEN

FM

EXHAUST

FLOW
CONTROLLER

TRANSDUCER &
REGULATOR
ASSEMBLY

SO2
IR
CELL

CO 2
IR CELL

MEASURE
FLOW
ROTAMETER

SO3
TRAP
CELLULOSE
FILTER

CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE

PS

SV3

MEASURE FLOW

QUARTZ
WOOL

PRESSURE
SWITCH

RESTRICTOR
ANH

PS
O2 IN
40 PSI

LECOSORB/ANH
PARTICLE
FILTER

PRESSURE
REGULATOR

SV1

SV9

PS

PRESSURE
SWITCH

SV5

DOWN

RESTRICTOR

SV10
NC
NO

UP

NO
FURNACE NC
BYPASS FLOW

SV11
NC
NO

DOOR SOL.
(OPTIONAL)
4 PSI

PRESSURE
SWITCH

PS

SV12
NC

AUTO CLEANER
(OPTIONAL)

NO

PS
25 PSI

PS
4 PSI

SV7

PNEUMATIC
PRESSURE
40 PSI

DUST
EJECT

PINCH VALVE
PARTICLE
FILTER

SAFETY
PRESSURE
REGULATOR

NC

SV6
NO

Figure 72
Gas Flow with Autocleaner Diagram

Theory of Operation

CS-200

77

SV2

Comparator Level

Note

One comparator level is associated with each analysis


method. Selecting a different method also selects a new
comparator level.

An analysis that lasts excessively long causes unnecessarily


long delays, while an analysis that isnt long enough can cause
loss of significant analyte data collection. Since not all samples
combust in the same manner, analyses should not be
performed based on time alone.
The length of each analysis is determined on an individual basis
by the minimum analysis time and the comparator level.
Analysis ends when the minimum time limit is reached and the
analyte rate drops below the comparator level after passing its
peak. This comparator level is a preset constant (k) plus a
percent of the peak:
COMPARATOR LEVEL = k + (X)(P)
P

Detector output peak

Selected comparator level percentage

During an analysis, the output of the detector is collected in the


form of digital data and summed to arrive at the analysis result.
If this data were plotted, it would reflect the curve of the
detector output.

78

CS-200

Theory of Operation

Shown below are two examples of the same detector output


curve (buffer plot). The first example shows the amount of
detector output collected during an analysis with a comparator
level setting at 6% while the second example illustrates
at 25%.

End of Analysis where "X" equals 6%


DETECTOR
OUTPUT

START OF
ANALYSIS

COMPARATOR
LEVELEND OF ANALYSIS

DETECTOR OUTPUT
COLLECTED

End of Analysis where "X" equals 25.0%


DETECTOR
OUTPUT

START OF
ANALYSIS

COMPARATOR
LEVELEND OF ANALYSIS

DETECTOR OUTPUT
COLLECTED

The following conclusions can be drawn from the examples:


1.

A high comparator level shortens analysis time.

2.

A low comparator level includes more sample gas, and


therefore more sulfur, into result calculations.

3.

A comparator level that is too low, however, results in the


inclusion of very low concentrations that dont significantly
effect the result (noise), but lengthen the analysis.

A comparator level of 1.0% usually provides optimum


performance by allowing the collection of all significant output
within a reasonable time.

Theory of Operation

CS-200

79

Extremely low output peaks may need a larger comparator


level to exclude insignificant output levels produced toward the
end of analysis and cut down on drift. The minimum time
should be extended to match what would be considered a
reasonable time length for the analysis of such samples. The
combination of a high comparator level and an extended
minimum analysis time insures that all significant output is
collected and analysis time lengths are consistent without being
extensive.
Whenever the comparator level changes check the system
calibration since interaction can occur.
COMPARATOR LEVEL
(SET TOO HIGH)

DETECTOR
OUTPUT
COLLECTED

SIGNIFICANT
DETECTOR
OUTPUT
EXCLUDED

COMPARATOR LEVEL
(SET TOO LOW)

INSIGNIFICANT
DETECTOR
OUTPUT

DETECTOR
OUTPUT
COLLECTED

710

CS-200

Theory of Operation

Diagnostics

Windows

Keypad

Keypad

8 Diagnostics

For instruments using Windows software refer to the


instructions listed in the Windows Software Diagnostics on
page 817.

For instruments using DSP software refer to the instructions


listed below.

Diagnostics........................................................................84
Ambient Monitor.................................................................85
Ambient Monitor Definitions ............................................ 87
Switch States.....................................................................88
Valve States ......................................................................89
Leak Check...................................................................... 810
Definitions .................................................................. 811
Print Buffer...................................................................... 812
Plot Buffer ....................................................................... 813
System Print.................................................................... 815
Reset Memory.................................................................. 816

Windows

Diagnostics for Windows .................................................. 817


Leak Check...................................................................... 819
Leak Check................................................................. 820
Leak Check Definitions ................................................. 821

Diagnostics

CS-200

81

Ambient Monitor............................................................... 822


Ambients.................................................................... 823
Ambient Monitor Definitions ..................................... 824
Ambient Monitor Ranges .......................................... 825
Switches ......................................................................... 826
Solenoids ........................................................................ 827
Comport.......................................................................... 828

82

CS-200

Electronic Adjustments

This page intentionally left blank.

Diagnostics

CS-200

83

Diagnostics
This procedure permits the operator to view and print the
ambient monitor, view the digital input switch states, view and
change the solenoid valve states, and perform system leak
checks.

Note

Access the diagnostics menu by pressing [5] Diagnostics


from the main menu.
Diagnostic
[1]
[2]
[3]
[4]
[5]
[6]

84

Ambient Monitor
Switches
Valves
Leak Check
Print Buffer
Plot Buffer

CS-200

Electronic Adjustments

Ambient Monitor

Notes

The ambient monitor is used to display system parameters


during servicing of the unit.

If the determinator has just been turned on, wait one to two
hours for the system to stabilize.

The ambient monitor will continuously update as the


operator views it.

1.

From the main menu, press [5] Diagnostics then press [1]
Ambient Monitor to display the ambient monitor.
Ambient Monitor

Carbon IR Cell
Sulfur IR Cell
Oven Temp
Catalyst Heater
System Pressure
Plate Current
Grid Current

2.

8.500 V
8.500 V
48oC
350oC
725 mm
480 mA
100 mA

Check that all system parameters, temperatures, and


voltages fall within the range limits shown below.

Parameter

Nominal Value

Range

Units

Carbon IR Cell

8.5

7.5 to 9.2

Sulfur IR Cell

8.5

7.5 to 9.2

Oven Temp

48

46 to 50

Catalyst Heater

350

325 to 375

System Pressure

750

Elevation Dependent

Plate Current*

460

420 to 500

mA

Grid Current*

100

80 to 120

mA

V
C
C

mmHg

*Nominal values during analysis only. When furnace power is off, the
plate and grid current should be zero.

Diagnostics

CS-200

85

3.

Press Select to toggle the displayed parameters between


voltages and units.

4.

Press Menu to display the ambient monitor menu.


Diagnostics
Ambient Monitor
[1] Display Units
[2] Display Voltages
[3] Print

86

5.

Press [1] Display Units to display the system parameters


in voltages, temperatures, and pressure.

6.

Press [2] Display Voltages to display the A/D output


voltages.

7.

Press Exit to remove the ambient monitor menu and


return to the ambient monitor screen.

CS-200

Electronic Adjustments

Ambient Monitor Definitions


CO2 DetectorThe IR Cell output voltage in volts. A properly
operating cell should have an output of approximately 8.5 volts.
SO2 DetectorThe IR Cell output voltage in volts. A properly
operating cell should have an output of approximately 8.5 volts.
Oven TemperatureThe temperature of the IR cell oven. The
value is in degrees centigrade. The oven temperature should be
approximately 48 oC.
Catalyst Heater TemperatureThe temperature of the Measure
Flow Catalyst Heater in degrees centigrade. The temperature of
the catalyst heater should be set at 350 oC.
SystemThe System Barometric Pressure in mmHg measured
by the barometric pressure transducer on the back-pressure
controller board. Typically the barometric pressure should be 20
mmHg above current local barometric pressure.
Plate CurrentThe electrical DC current flowing from the
cathode to the plate of the oscillator vacuum tube V1. As RF
power increases during analysis the plate current rises.
Grid CurrentThe electrical DC current flowing from the
cathode to the grid of the oscillator vacuum tube V1. As RF
power increases during analysis the grid current rises.

Diagnostics

CS-200

87

Switch States

Notes

Switch states permits the operator or service technician to


monitor the digital input switch states.

This is a status screen, none of the switch states can be


changed from this screen.

1.

Press [2] Switches to display the digital input switch


states.
Switches
Description
Pneumatic Pressure
Lance Pressure
Piston Up Limit
Oxygen Pressure
Piston Control
Brush Down LSW
Brush Up LSW
Door Open LSW
Piston Down Limit

2.

88

State
Closed
Open
Closed
Closed
Open
Open
Closed
Closed
Open

Press Exit to return to the diagnostics menu.

CS-200

Electronic Adjustments

Valve States

Notes

This procedure permits the operator or service technician to


change the state of each solenoid valve listed.

Each solenoid valve has a quick access number. To quickly


access a solenoid valve, press the corresponding number on
the keypad.

1.

Press [3] Valves to display the solenoid valve status


screen.
Valves
## Description
1 Oxygen Carrier
2 Furnace Bypass
3 Lance Solenoid
4 Furnace Gas
5 Safety Solenoid
6 Purge Solenoid
7 Piston Solenoid
8 Door Solenoid
9 Brush Solenoid
more

Diagnostics

State
> Off
Off
Off
Off
Off
Off
Off
Off
Off

2.

Press Next to move the cursor down the list of solenoid


valves.

3.

Press Previous to move the cursor up the list of solenoid


valves.

4.

Press Yes to turn each solenoid valve on

5.

Press No to turn each solenoid valve off.

6.

Press Select to toggle the state of each solenoid valve


between on and off.

7.

Press Exit to return to the diagnostics menu.

CS-200

89

Leak Check

Note

1.

The leak check procedure determines if leaks are present in


the combustion and measure systems and checks for leaks
both into and out of the system.
From the diagnostics menu, press [4] Leak Check to
display the leak check menu.
Leak Check

[1] Entire System


[2] By-Pass Furnace

Note

810

After the system pressurizes, it will wait 60 seconds before


the OK message will appear. If a leak is detected, the Leak
In System message can occur before the 60 second time
period is complete.

2.

From the leak check menu, select one of the two choices:
A.

Choose [1] Entire System to perform an entire


system leak check. The entire system leak check
screen will appear.

B.

Press [2] By-Pass Furnace to perform a leak check


with the furnace/combustion area by-passed. The
screen that appears will be identical to entire system
leak check.

CS-200

Electronic Adjustments

Notes

A negative number, under change in pressure, indicates a


leak into the system (an increase in pressure). A positive
number, under change in pressure, indicates a leak out of
the system (a decrease in pressure).

If a leak is indicated, refer to the Leak Check Flow Diagrams


Figure 107 and Figure 108, pages 1019 and1020).

3.

Press Exit to return to the leak check menu.

Definitions
System PressureThe operating pressure of the system before
it is pressurized. The system pressure will not change as the
system is being pressurized.
Initial PressureThe system pressure at the start of system
pressurization. Normally, initial pressure is the same value as
system pressure.
Current PressureThe system pressure at the current time.
The current pressure changes rapidly as the system is being
pressurized.
Change PressureThe difference between the initial pressure
and the current pressure. A negative number indicates an
increase in system pressure. A positive number indicates a
decrease in system pressure.
TimeThe length of time, in seconds, that the test has been
running. Normally, after 60 seconds the test is complete.

Diagnostics

CS-200

811

Print Buffer
From the diagnostics menu, choose [5] Print Buffer to receive a
printout from the system printer of the buffer contents from the
last carbon analysis and then return to the diagnostics menu.

812

CS-200

Electronic Adjustments

Plot Buffer

Notes

Plot buffer prints a graph of the sample rate of change in


concentration, as measured by the IR cell, over a period of
time.

The area between the base line and plotted curve is the
integrated concentration of sample gas as it passes through
the IR cell.

1.

From the diagnostics menu, choose [6] Plot Buffer to


display the plot buffer screen.
Carbon

Diagnostics

X-axis
Start
End

0
48

Y-axis
Start
End

0
6000

2.

Press Next/Previous to move the highlight and select the


parameter values to edit.

3.

Press Select to move the highlight down and select the


parameters to edit.

4.

Press the number keys to enter the parameter value.

5.

Press the arrow keys to move the cursor to a digit position


and enter the digit value, with the number keys on the
keypad.

CS-200

813

6.

Press Menu to display the print plot menu or Exit to return


to the diagnostic menu.
Carbon

[1] Print

7.

814

Press [1] Print to receive a printed plot of sample


concentration verses time on the system printer. After the
plot is printed, the diagnostics menu will be displayed.

CS-200

Electronic Adjustments

System Print

Notes

Diagnostics

System print prints out the system operating parameters on


the system printer.

The system operating parameters include the following:


System Options, Analysis Method, Transmit Options,
Balance Options, System Controls, Combustion Furnace,
Reduction Furnace (Catalyst Heater), and Ambient Monitor.

1.

Press [7] System Print from diagnostics menu to receive a


printout of the system operating parameters on the
system printer. After the system parameters are printed,
the diagnostics menu will be displayed.

2.

Press Exit to return to the main menu.

CS-200

815

Reset Memory

Notes

816

Reset memory resets the system operating parameters to


their default values.

Before the memory is reset, print the system operating


parameters using system print to obtain a record of the
parameter values if replacement is necessary.

1.

Press Yes to reset values back to their default values.

2.

Press [8] Reset Memory from the diagnostics menu to


reset the system operating parameters back to their
default values. The diagnostics menu will be displayed.

3.

Press Exit to return to the main menu.

CS-200

Electronic Adjustments

Diagnostics for Windows

Keypad

Windows

Keypad

For instruments using DSP software refer to the instructions


listed in the DSP Software Diagnostics on page 84

For instruments using Windows software refer to the


instructions listed below.

Diagnostics........................................................................84
Ambient Monitor.................................................................85
Ambient Monitor Definitions ............................................ 87
Switch States.....................................................................88
Valve States ......................................................................89
Leak Check...................................................................... 810
Definitions .................................................................. 811
Print Buffer...................................................................... 812
Plot Buffer ....................................................................... 813
System Print.................................................................... 815
Reset Memory.................................................................. 816

Windows

Diagnostics for Windows .................................................. 817


Leak Check...................................................................... 819
Leak Check................................................................. 820
Leak Check Definitions ................................................. 821
Ambient Monitor............................................................... 822
Ambients.................................................................... 823
Ambient Monitor Definitions ..................................... 824
Ambient Monitor Ranges .......................................... 825

Diagnostics

CS-200

817

Switches ......................................................................... 826


Solenoids ........................................................................ 827
Comport.......................................................................... 828

818

CS-200

Electronic Adjustments

Leak Check
This procedure automatically check the measurement system of
the instrument for a gas leak. The entire system can be
checked or the operator can by-pass the furnace to isolate the
leak.
During a system leak check the system is pressured to 500 mm
Hg above current system pressure and sealed. It is then
permitted to equilibrate. For the next 60 seconds the system
pressure is measured. If the pressure remains within 5 mm Hg
of the pressurized value the system passes the leak check (for
system check only). If the pressure changes more than 5 mm
Hg of the pressurized value the leak check fails.
In the Leak Check Progress box the status of the leak check is
displayed. If a leak check fails it may be caused by gas leaking
into or out of the system.
If Change in Pressure has increased the incoming valve SV6
may be malfunctioning or the catalyst heater tubes are not at a
steady temperature. If Change in Pressure has decreased gas
is leaking out of the system.
If a leak is present, "Leak Check Failed" appears next to Leak
Check Status. If there isn't a leak " Leak Check Passed"
appears. If the system fails a leak check and a leak is detected,
perform a by-pass the furnace leak check to isolate the leak.
Before a leak check is performed the instrument should warm
up for at least for 30 minutes and the catalyst heater tubes
must be at a steady temperature. It is recommended that a
leak check be performed after autocleaner maintenance,
furnace maintenance or anytime a reagent tube is removed or
replaced.

Diagnostics

CS-200

819

Leak Check

820

1.

Click Diagnostics and select Leak Check. The Leak Check


screen will appear.

2.

Click System Leak Check to perform a leak check on the


entire measurement system or click By-pass Furnace Leak
Check to perform a leak check of the measurement with
the furnace bypassed. The result of the leak check will
appear in the Results box.

3.

Click Stop Leak Check to stop a leak check in progress.

4.

Click Print to print the results of the leak check on the


system printer.

5.

Click View to look at various areas inside the instrument


where a leak may be found.

CS-200

Electronic Adjustments

Leak Check Definitions


Starting System PressureThe operating pressure of the
system before it is pressurized. The system pressure will not
change as the system is being pressurized.
Initial PressureThe system pressure at the start of system
pressurization. Normally, initial pressure is the same value as
system pressure.
Current PressureThe system pressure at the current time.
The current pressure changes rapidly as the system is being
pressurized.
Change PressureThe difference between the initial pressure
and the current pressure. A negative number indicates an
increase in system pressure. A positive number indicates a
decrease in system pressure.
Elapsed TimeThe length of time, in seconds, that the test has
been running. Normally, after 60 seconds the test is complete.

Diagnostics

CS-200

821

Ambient Monitor
This procedure permits the operator to view and print the
ambient monitor parameter values.
Refer to Ambient Monitor Definitions, on page 824, for
Ambient Monitor Definitions.

822

CS-200

Electronic Adjustments

Ambients

Diagnostics

1.

Click Diagnostics and select Ambients to display the


Ambient Monitor screen.

2.

Click the Check Box, to the left of the desired parameter,


to plot the parameter value in the graph above the chart.
More than one parameter can be plotted on the graph.
Hold down the Control Key and click the Parameter Check
Box for each parameter to be plotted. A yellow circle with
an exclamation point to the left of the check box indicates
the parameter value is outside the desired range of values.

3.

Click the right mouse button, with the mouse pointer


inside the graph, to reset, restore, zoom in, zoom out, and
set the graph range. The parameter value is displayed on
the vertical axis and the time is displayed on the
horizontal axis. The box in the lower left corner of the
graph displays the hours since the instrument was turned
on or the graph reset. The hours reset to 0 after 24.

4.

Right-click the Parameter Name to reset the parameter


values and time on the chart and graph.

5.

Click Print to print the parameter values on the system


printer.

CS-200

823

Ambient Monitor Definitions


Oven TemperatureThe temperature of the IR cell oven. The
value is in degrees centigrade. The oven temperature should be
approximately 48 oC.
SystemThe System Barometric Pressure in mmHg measured
by the barometric pressure transducer on the back-pressure
controller board. Typically the barometric pressure should be 20
mmHg above current local barometric pressure.
Catalyst Heater TemperatureThe temperature of the Measure
Flow Catalyst Heater in degrees centigrade. The temperature of
the catalyst heater should be set at 350 oC.
Plate CurrentThe electrical DC current flowing from the
cathode to the plate of the oscillator vacuum tube V1. As RF
power increases during analysis the plate current rises.
Grid CurrentThe electrical DC current flowing from the
cathode to the grid of the oscillator vacuum tube V1. As RF
power increases during analysis the grid current rises.
CO2 DetectorThe IR Cell output voltage in volts. A properly
operating cell should have an output of approximately 8.5 volts.
SO2 DetectorThe IR Cell output voltage in volts. A properly
operating cell should have an output of approximately 8.5 volts.

824

CS-200

Electronic Adjustments

Ambient Monitor Ranges

Note

This symbol
will appear next to the parameter name, on
the ambient monitor screen, if the parameter value is out of
minimum or maximum range.
Parameter

Nominal Value

Range

Units

Oven Temp

48

46 to 50

System Pressure

750

Elevation Dependent

Catalyst Heater

350

325 to 375

Plate Current*

460

420 to 500

mA

Grid Current*

100

80 to 120

mA

Carbon IR Cell

8.5

7.5 to 9.2

Sulfur IR Cell

8.5

7.5 to 9.2

mmHg
o

* The values shown for these parameters are typical values during an analysis.

Diagnostics

CS-200

825

Switches
Switches are used throughout the instrument as sensors to
determine the status of a condition. Theyre not only used to
control the instrument, they're used for safety to prevent the
instrument from damage and the operator from harm.
The Switch screen is a diagnostic status screen. None of the
switch states can be changed from this screen. View the screen
to determine the switch status. Refer to Switch Conditions to
determine the meaning of each condition.

826

1.

Click Diagnostics and select Switches. The Switches screen


will appear.

2.

Click Close to exit the switches screen.

CS-200

Electronic Adjustments

Solenoids
The Solenoids screen permits the service technician or operator
to toggle the solenoid valves either on or off. It is also used to
test operation of the Batch Loader (autoloader).
By using the valve state drop down box the service technician
or operator can determine which valves should be turned per
valve state. To determine what each valve may affect refer to
the Flow Diagram Figure 105, on page 1017.
After this procedure is closed the solenoid valve states will
automatically be set to their default states.

Diagnostics

1.

Click Diagnostics and select Solenoids. The Solenoid


screen will appear.

2.

Click the check box to the left of the solenoid valve to


activate it. Observe operation of the instrument and
solenoid valve.

3.

Click Close to exit the solenoids screen.

CS-200

827

Comport
Comport is a diagnostic utility that can be used by the service
technician, operator and software engineer to troubleshoot the
instrument. In some cases it may be of advantage to the
service person and LECO to analyze the data collected by this
utility for diagnostic and trouble shooting purposes. Comport
must be used with direction from a LECO engineer.

Note

828

1.

Click Diagnostics and select Communications. The


Communications screen will appear.

2.

Click the Pause Check Box to stop the data scrolling in the
communications data window.

3.

Click the Hide Status Messages check box to stop the


analysis status messages from being displayed.

4.

Click Copy to Clipboard to copy comport data to the


clipboard. From the clipboard, data can be copied to a file.

If Hide Status Messages is checked only error messages will


be displayed.

CS-200

Electronic Adjustments

Electronic Adjustments
9 Electronic Adjustments

Illustrations .......................................................................92
Barometric (PID) Pressure Regulator Adjustment ....................93
Catalyst Heater Control Card................................................96
Induction Power Control Card ...............................................98
Oven Heater Control Card.................................................. 911
IR Cell ............................................................................ 912

Electronic Adjustments

CS-200

91

Illustrations
Figure 91......... Barometric (PID) Pressure Regulator Card ..... 95
Figure 92......... Catalyst Heater Control Card ....................... 97
Figure 93......... Induction Power Control Card ...................... 910
Figure 94......... Oven Heater Control Card ........................... 911
Figure 95......... IR Cell Adjustment Location ........................ 913

92

CS-200

Electronic Adjustments

Barometric (PID) Pressure Regulator Adjustment


This adjustment has been factory set to a highest anticipated
barometric pressure of 762 mm. If the highest anticipated
pressure in the operational environment varies more than 5
mm from 762 mm, this adjustment must be performed to
eliminate calibration shifts that may occur as a result of
barometric pressure changes.
The present (operation environment) barometric pressure must
be determined. If an accurate method of measurement is not
available, the nearest weather bureau or airport can provide
this information. The pressure must be referenced to the
operational site altitude, not sea level. The highest anticipated
pressure for the area must also be determined.

Notes

The determinator power must be on for a minimum of 30


minutes prior to performing this adjustment.

The furnace piston must be in the up position and the


furnace power switch must be in the on position.

This adjustment should be performed if the barometric


pressure transducer or PID pressure regulator card is
replaced.

1.

2.

Insure that the jumpers on the circuit board are installed


as follows, see Figure 91, page 95:
A.

J1The two pins nearest transistor Q2 should be


jumpered.

B.

J2, J3 and J4Both pins on each connector should be


jumpered.

Insure that the controls on the circuit board are positioned


as follows, see Figure 91, page 95:
A.

R27Set to 9.

B.

R28Set to 2.

C.

R29Set to 5.

3.

Remove the left side panel of the determinator.

4.

Turn the AC power on to both the determinator and


furnace.

5.

From the main menu, press [4] Setup and then [6] Set
Barometer. Set the barometric pressure to the current
value at the location of the determinator.

Electronic Adjustments

CS-200

93

6.

94

From the main menu, press [1] Analyze and then Menu to
display the analysis menu.

CS-200

Electronic Adjustments

7.

Press [4] System Controls. Set carrier gas to on.

8.

From the main menu, press [5] Diagnostics and then [1]
Ambient Monitor. Monitor the system pressure.

9.

While monitoring the system pressure, adjust control R30,


on the PID pressure regulator card, for a system pressure
value of 20 mmHg above the highest expected barometric
pressure value. Refer to Figure 91, page 95.
A.

Turn the adjustment clockwise to decrease pressure.

B.

Turn the adjustment counterclockwise to increase


pressure.

10. Reinstall the left side panel of the determinator.

R1
R2

J038A

CR3
CR4
C11

C17

R26

J038B

C14
TP4
R27
5
J3
1

R30

C13

C12

J2
1
TP5
D

J2

R30

R27

10

C15

C18
R29

R28
J4
1

10

J038C
C16

U4
J1

U3

10

C20

C19

TP3

R25

C5

C21

R12
R14
R13
R15
R16

C8

R11

TP2

R7

C6

R23
C10

J1
C9

C7

C3
R6
R10

Q4

R8
R9

U1

C4

C2

Q2 Q3 TP1

R17
R18
R19
R20
R21
R22

Q1

R3
R4
R5

C1

COPYRIGHT C 1993
ALL RIGHTS RESERVED
LECO CORPORATION
ST, JOSEPH, MI U.S.A.

LED1 J038

CR1

R24

Q2

J3
R28

R29

Figure 91
Barometric (PID) Pressure Regulator Card

Electronic Adjustments

CS-200

95

Catalyst Heater Control Card

WARNING

Notes

Note

96

HIGH VOLTAGE HAZARD


After the side panels are removed, high voltage
is present. Use caution when making these
adjustments. Contact with voltages inside the
instrument can be lethal or cause serious injury.

This procedure adjusts the catalyst heater control card to


ensure proper temperature tracking of the catalyst heater
and to provide an accurate temperature read-out on the
ambient monitor.

This adjustment is only necessary when the catalyst heater


card or heating element is replaced.

To properly perform this adjustment, a digital voltmeter


capable of measuring 7 volts is needed. Also, a calibrated
thermocouple is necessary to externally measure the
operating temperature of the catalyst heater.

1.

Turn the analysis gas OFF.

2.

Remove the left side panel of the unit to access the


catalyst heater controller card. Refer to Figure 11-1, page
11-3.

3.

Attach the negative terminal of the digital voltmeter to the


metal chassis of the determinator where there is no paint.
Be sure a good connection is made.

4.

Attach the positive lead to pin 4 of connector J078A or pin


7 of U4. Refer to Figure 92, page 97.

5.

Adjust control R16 until 3.5 volts is read on the digital


voltmeter. At pin 4 of J078A, one volt equals 100oC.

6.

Remove the digital voltmeter leads from the determinator.

7.

Using protective gloves, remove the catalyst heater tube


from the catalyst heater and set it on a heat-resistant
surface.

To remove the catalyst heater tube refer to page 611,


steps 3 and 4.

CS-200

Electronic Adjustments

8.

Install an empty catalyst heater tube into the catalyst


heater, and allow ten minutes for the catalyst heater tube
to heat. The top of the catalyst heater tube should be
left open.

9.

Insert a digital thermometer thermocouple into the


catalyst heater tube approximately seven inches.

10. Access the ambient monitor and observe the catalyst


heater temperature.
11. Adjust control R13 until the temperature displayed on the
ambient monitor equals the temperature read on the
digital thermometer.
12. Remove the thermocouple and empty catalyst heater tube.
Place on a heat-resistant surface.
13. Reinstall the packed catalyst heater tube, and reinstall the
top block on the tube.
14. Further adjust R16 as needed until the temperature is
350oC 10oC.

C3

C2

U1
CR1

C4

C9

C7

R11

R10

R8
R7

R6

C5

R5

U2

C10

R9

R4

R3

C8

R2
C6

J078A

+ C1

R1

J078A

COPYRIGHT C 1993
ALL RIGHTS RESERVED
LEC O CORPORATION
ST. JOSEPH, MI U.S.A.

J078

U4

R13
U4
Figure 92
Catalyst Heater Control Card

Electronic Adjustments

CS-200

R16

C13

R15

R14
C12

TB1

U3
R13

R12

C11

R16

97

Induction Power Control Card

Note

1.

Verify correct installation of vacuum capacitor and


oscillator tube in furnace.

2.

Turn on the furnace service switch and verify that plate


current is approximately 150 mA and grid current is
approximately 100 mA on the analyze screen.

3.

Turn off the service switch and verify that the plate and
grid currents go to zero.

4.

Turn the power level control clockwise to the max position.

5.

Put a calibration load on the furnace pedestal.

If the calibration load recommended and calibrated by LECO


is not used during adjustment, the performance of this
instrument cannot be guaranteed.

6.

Press the piston switch on the furnace. The pedestal


should rise.

7.

Perform either step 7A or step 7B.


A.

Note

Be sure to reset the minimum time-out to the original


setting after the electronic adjustments have been
performed.
B.

98

Enter a weight in the stack. When using this method,


the minimum time-out parameter under the analysis
method option in the setup screen should be
extended to 120 seconds or more to allow ample time
to perform the adjustments.

Move jumper J1 on the card from pins 1 and 2 to


pins 2 and 3. This will cause the furnace to turn
on until the jumper is replaced on pins 1 and 2. Refer
to Figure 93, page 910.

CS-200

Electronic Adjustments

8.

Note

9.

Verify that turning power level control up and down


(located on the front panel) causes the plate current to
increase and decrease respectively. Return the power level
control to the max position.

If the power level control adjustments do not seem to affect


the power level read-out, adjust R29 down and try adjusting
the power level control again.
Adjust the overload control (R32) up (approximately 10
turns) to prevent the furnace from going into overload.

10. Adjust the offset control (R29) as follows:

Note

A.

If the oscillator current is below 500 mA, adjust R29


counterclockwise until 500 mA of plate current is
obtained and then proceed to step 11.

B.

If the oscillator is not oscillating, and the plate


current is low, turn R29 clockwise until 500 mA of
plate current is obtained.

C.

With the power control at maximum, adjust R32


counterclockwise until the current overloads. Then
gradually adjust R32 clockwise and R29
counterclockwise until the oscillator tube oscillates
at 500 mA.

Sometimes it requires a couple of attempts at this step if


the oscillator gets into this mode of oscillation. Once the
oscillator is set, it should function normally for the life of
the oscillator tube.

11. Adjust the overload control, R32, down until the furnace
power trips. Be sure the power has actually tripped and
that the power has not merely turned off because the
analysis has ended. Verification can be accomplished by
observing that LED1 is lighted.
12. Turn the overload control back approximately 11/2 turns to
ensure that the furnace will go into overload just above
the full-scale current setting of 500mA.
13. Reset the overload by turning the power level control to
reset and then back to max. Now the furnace should not
go into overload when the power level control is returned
to max.

Electronic Adjustments

CS-200

99

TP1 TP2

TP3

TP4
C1

J112A
C11

C10

R12

R18

R1 6

R17

R28

Q10

R25
R27

R29

LED1
R32
R33
SCR1

R39
R40
COPYRIGHT C 1995
ALL RIGHTS RESERVED
LECO CORPORATION
ST. JOSEPH, MI U.S.A

C22

C23

J112B

R32

R26

C16

R20

R2 2

R21

C19
C21

J1

LED1

U3

C18

Q8

R38

C20

R35

R34

R37

R36

C17

R29

Q6

Q9

CR 3

Q11

R31

R30

C14

U2

R24

C15

R23

R19

Q7

R13

C13
R15

C12
Q5

J1

Q3

CR2

Q2

R14

R11

J112

R10

C9

Q4

C6

C7

C8
Q1

C4 C5

U1

R6
R7
R8

R9

BR1

R1

R4

R3
R5

CR1

R2

C2

C3

J112C

Figure 93
Induction Power Control Card

910

CS-200

Electronic Adjustments

Oven Heater Control Card

This procedure should be completed if the oven temperature


falls out of range (48oC 2oC) as displayed on the ambient
monitor, or when replacing the oven heater control card.

This adjustment requires a digital voltmeter.


Remove the left side panel and oven compartment side
panel.

2.

Locate the oven heater control card. On the card locate


control R14, TP1, and TP2. Refer to Figure 94 below.

3.

Connect the digital voltmeters positive lead to TP1, and


the negative lead to TP2. The voltage measured will be
100 mV/oC.

4.

When readings have stabilized, adjust control R14 for a


reading of 4.8 volts.

5.

Disconnect the digital voltmeter.

6.

Reinstall the side panels.

7.

Permit the temperature to stabilize then recheck the


temperature reading on the ambient monitor. It should be
48oC 2oC.

U5

CS-200

C5

J224

C7

C6

C4

R12

TEMP
TP3

R4

R5

R9

U3
U1

U2
R1

C2

C3

U4
R3

Figure 94
Oven Heater Control Card
Electronic Adjustments

C1R8

R7
R6
J224C

J224B

J224A

R2

R14

COPYRIGHT C 1997
ALL RIGHTS RESERVED
LECO CORPORATION
ST, JOSEPH, MI U.S.A.

K1

R14

TEST

TP1

TP1

TP2

CR1

TP2
GND

1.

R10
R11

Notes

TP3

911

IR Cell

Notes

The IR cell output range is 7.500 to 9.200 volts. An alarm


occurs if the cell exceeds this range, indicating that the
following adjustment should be performed.

J152 is the chopper motor connector for the CO2 IR cell.


J152A is the chopper motor connector for the SO2 IR cell.
Refer to Figure 95, page 913.

This procedure should be repeated for both IR cells.

1.

Note

Notes

The instrument should be at operating temperature, and the


gas supply should be on before performing this adjustment.

2.

Remove the right side panel of the determinator to access


the IR cell oven.

3.

Remove the IR cell oven side panel.

4.

Locate the zero adjustment control (R24), the gain


adjustment control (R3), and the chopper motor connector
(J152/J152A).

The gain adjustment can be made without adjusting the


zero adjustment.

For locations, refer to Figure 95, page 913.

5.

Note

912

Access the ambient monitor by pressing [5] Diagnostics


and then [1] Ambient Monitor. The ambient monitor
screen will be displayed.

Disconnect the chopper motor connector and observe the


display. The reading should drop to zero. If not, adjust the
zero control (R24) until the display indicates 0.001 volts.

Do not adjust to zero.

CS-200

Electronic Adjustments

6.

Note

7.

Reconnect the chopper motor connector, and observe the


display. The reading should indicate 8.500 0.200 volts. If
not, adjust the gain adjustment control (R3) until the
display indicates 8.500 0.200 volts.

After adjustments are made, permit the oven temperature


to stabilize before analyzing samples.
Reinstall the side panels.

CO2 IR CELL
R3
GAIN

J-152
CONNECTOR

R24
ZERO
ADJUST

R3
GAIN

R24
ZERO
ADJUST
OVEN HEATER
CONTROL CARD

J-152A
CONNECTOR

SO 2 IR CELL

Figure 95
IR Cell Adjustment Location

Electronic Adjustments

CS-200

913

10

Service
10 Service

Illustrations ..................................................................... 102


Combustion Pressure Adjustment ....................................... 103
Flow Controller Adjustment ................................................ 105
Safety Pressure Adjustments.............................................. 106
Vertical Crucible Alignment ................................................ 108
Gas Flows...................................................................... 1012
Analysis ................................................................... 1012
Autocleaner .............................................................. 1015
Valve Control States ....................................................... 1016
Notices, Errors, and Warnings .......................................... 1022
Software Upgrade........................................................... 1026
DSP Software Upgrade Procedure ................................ 1026
Software Upgrade with Windows ................................ 1029
Linearization with DSP..................................................... 1030
Linearization with Windows ............................................ 1032

Service

CS-200

101

Illustrations
Figure 101 ....... Combustion Pressure Adjustment Knob ......... 104
Figure 102 ....... Flow Controller Location.............................. 105
Figure 103 ....... Piston Pressure Regulator ........................... 107
Figure 104 ....... Crucible Alignment..................................... 1011
Figure 105 ....... Gas Flow Diagram...................................... 1017
Figure 106 ....... Gas Flow with Autocleaner Diagram.............. 1018
Figure 107 ....... Leak Check Flow Diagram ........................... 1019
Figure 108 ....... Leak Check Flow with Autocleaner Diagram ... 1020
Figure 109 ....... Analyze Sequence Diagram ......................... 1021
Figure 10-10...... EPROM Location......................................... 1028

102

CS-200

Service

Combustion Pressure Adjustment

Note

1.
Keypad

The Set Barometer procedure, page 427, should be


completed before this adjustment is made.
Remove the left side panel.
Use the following procedure for a DSP instrument to turn
the gas ON.

A. From the main menu, press [1] Analyze then Menu to


display the analysis menu.
B. Press [4] System Controls and set carrier gas to on.

Windows

Use the following procedure for a Windows instrument to


turn the gas ON.

A. Click F10 on the toolbar to turn the gas ON.

Service

2.

Using the adjustment knob, adjust the pressure regulator


for 12 psi as shown on the pressure gauge. Refer to
Figure 101, on page 104.

3.

Replace the left side panel.

CS-200

103

ADJUSTMENT
KNOB

PRESSURE
REGULATOR

Figure 101
Combustion Pressure Adjustment Knob

104

CS-200

Service

Flow Controller Adjustment


1.

Remove the left side panel to access the IR cell oven.


Refer to Figure 11-1, page 11-3.

2.

Using a screwdriver, adjust the flow controller assembly


through the access hole in the oven directly above the flow
controller assembly. Refer to Figure 102, below.

3.

From the main menu, press [1] Analyze to turn the gas on
and then [4] System Controls.

4.

Adjust the oxygen flow controller for 3 liters per minute


indicated on the determinator's front panel oxygen flow
rotameter.

5.

Reinstall the IR cell oven side panel and the determinators


left side panel.

FLOW CONTROL
ASSEMBLY
ACCESS HOLE

602-454
REGULATOR
FLOW CONTROL
ASSEMBLY

666-224-110
OVEN HEATER
CARD

782-067-110
SO2 IR-CELL

778-574-120
CO2 IR CELL

Figure 102
Flow Controller Location

Service

CS-200

105

Safety Pressure Adjustments

WARNING

Notes

HIGH VOLTAGE HAZARD


After the left side panel of the unit is removed,
high voltage is present. Do not touch any
component inside the cabinet when performing
this adjustment unless instructed to do so.

Piston safety pressure (6 psi) is applied to the pneumatic


piston except when the piston is fully extended.

The pneumatic piston closing speed increases as pressure


increases.

1.

Access the analyze menu and select Manual Operation.

2.

Remove the left side panel and locate the piston pressure
regulator. Refer to Figure 11-1, page 11-3.

3.

Press the up/down switch and open the furnace. Observe


the speed of the piston while the piston is in transit. If the
piston does not travel from top to bottom and bottom to
top in approximately two seconds locate the safety
pressure adjustment knob, Figure 103, page 107 and
adjust as follows:
A.

106

If the piston travel is too slow:


1)

Cycle the furnace piston by pressing the up/down


switch and rotate the safety pressure adjustment
knob clockwise while observing the speed of the
piston.

2)

The time for piston travel should be


approximately two seconds.

3)

Cycle the furnace piston by pressing the up/down


switch twice.

4)

The time for piston travel should still be


approximately two seconds.

5)

Press the up/down switch to close the furnace


and complete this procedure.

CS-200

Service

B.

If the piston travel is too fast:


1)

Cycle the furnace piston by pressing the up/down


switch and rotate the safety pressure adjustment
knob counter-clockwise while observing the
speed of the piston.

2)

The time for piston travel should be


approximately two seconds.

3)

Cycle the furnace piston by pressing the up/down


switch twice.

4)

The time for piston travel should still be


approximately two seconds.

5)

Press the up/down switch to close the furnace


and complete this procedure.

!
CAUTION

FIRE HAZARD
Oxygen increases the flammability of materials.
Always use caution when adjusting or operating
units using oxygen supplies. LECO recommends
routine leak check procedures to reduce the
possibility of fire hazards.

620-611 W/AC
620-120 WO/AC
MANIFOLD
ASSEMBLY

SAFETY
PRESSURE
REGULATOR
KNOB

Figure 103
Piston Pressure Regulator

Service

CS-200

107

Vertical Crucible Alignment

Note

To assure efficient lance flow to the sample, and optimal


sample coupling, with the high-energy field around the coil,
the crucible must be properly positioned on the pedestal.

WARNING

ELECTRICAL SHOCK HAZARD


The capacitors on the oscillator chassis store a
lethal amount of energy and must be discharged
to avoid electric shock . Contact the LECO service
department for more information before
servicing the oscillator chassis.

WARNING

HIGH VOLTAGE HAZARD


After the power has been turned on, both the
oscillator and the furnace power supply produce
lethal voltages. Contact the LECO service
department for more information before
servicing the oscillator chassis.

1.

Place an empty crucible on the furnace pedestal and close


the furnace.

2.

Observe the crucible position through the furnace screen.


The bottom of the crucible should be located just below or
even with the lower portion of the third coil turn from the
top. Refer to Figure 104, page 1011.

3.

If the crucible is not in the proper position, it will be


necessary to adjust the induction coil.
A.

WARNING

108

Place the furnaces power on/off switch to the off


position and unplug the furnace power cord from
facility power.

ELECTRICAL SHOCK HAZARD


Disconnect from facility power before continuing
with this procedure.

CS-200

Service

B.

Remove the crucible from the pedestal and the


pedestal from the adapter. Set the crucible and
pedestal aside. Refer to Figure 104, page 1011.

C.

Open the lance access door and remove the lance


assembly.

D.

Remove the combustion tube and set it aside.

E.

Remove the front cover and metal screen to access


the induction coil.

WARNING

ELECTRICAL SHOCK HAZARD


The capacitors on the oscillator chassis store a
lethal amount of energy and must be discharged
to avoid electric shock . Contact the LECO service
department for more information before
servicing the oscillator chassis or touching the
induction coil.

WARNING

HIGH VOLTAGE HAZARD


After the power has been turned on, the
oscillator produces lethal voltages. Contact the
LECO service department for more information
before servicing the oscillator chassis or touching
the induction coil.

F.

Adjust the induction coil.

!
CAUTION

Service

POSSIBLE MACHINE ERROR


Make sure the spacing between the coil turns
remains the same.

CS-200

109

1)

For very minor adjustments: Carefully grasp the


induction coil and bend it into the proper
position.

2)

For average adjustments:

3)

1010

a)

Loosen the two coil collets, Figure 2-5,


page 213.

b)

Move the induction coil until the induction


coil is in the proper position.

c)

Tighten the coil collets being careful not to


over-tighten.

For large adjustment:


a)

Remove the right side panel.

b)

Remove the RF shield.

c)

Loosen the four screws holding the oscillator


chassis in place.

d)

Move the oscillator until the induction coil is


in the proper position.

e)

Tighten the oscillator chassis screws.

f)

Reinstall the RF shield and the right side


panel.

G.

Replace the combustion tube, lance assembly, metal


screen, and front cover.

H.

Close the lance access door.

I.

Plug the furnace into facility power and place the


furnaces power on/off switch in the on position.

4.

When the adjustment is completed, reinstall the pedestal,


place an empty crucible on the furnace pedestal, and close
the furnace.

5.

Observe the crucible position. If the crucible still needs


adjustment, repeat step 3 until the crucible is properly
aligned.

CS-200

Service

528-018
CRUCIBLE

605-814
PEDESTAL
ADAPTER
ASSEMBLY

INDUCTION
COIL
EMPTY
CRUCIBLE

605-816
PEDESTAL

LOWER SEAL
ASSEMBLY
METAL
SCREEN

FRONT
COVER

Figure 104
Crucible Alignment

Service

CS-200

1011

Gas Flows

Analysis
Analyze Valve StateIn this valve state, oxygen flows through
both the furnace and the determinator system.
When the gas is turned on, oxygen, regulated at 35 psi at its
source, enters the determinator through the O2 inlet port on the
cabinet back panel. Oxygen flow is then filtered through a 6
inch bubble tube (located on the front of the furnace)
containing Lecosorb and anhydrone. Carbon dioxide is removed
from the oxygen flow using Lecosorb reagent and moisture is
removed in the anhydrone reagent. Oxygen, with all impurities
removed, serves as the carrier gas in the system.
After all impurities have been removed from the carrier gas, the
flow is divided into two paths; one path, the lance flow, is
directed through solenoid valve 3 and into the top of the
combustion tube. During an analysis, lance flow is held
constant and is directed into the sample to assist carbonbearing components to convert into CO or CO2. The second
path is directed through solenoid valve 5 into the bottom of the
combustion tube; this flow rate varies (2 to 3 lpm) in
accordance with each valve state.
The carrier gas flows from the combustion tube sweeping
released gases from the combustion tube through a screen
filter, then through a 4 inch filter tube containing anhydrone to
remove water. The carrier gas, regulated by a flow controller in
the oven, flows through the catalyst heater. A small percentage
of the carbon is present as carbon monoxide, which is
converted to carbon dioxide as the gas flows through the
platinized silica gel in the heater. Sulfur trioxide is removed in a
cellulose trap. Gas then flows through the cellulose trap, CO2 IR
cell and solenoid valve 15. It is then exhausted out the back of
the unit.
Furnace Open 1 Valve StateIn this valve state, the
combustion tube is depressurized so that residual dust can be
ejected.
Lance flow remains the same as in the analyze valve state, but
the measure flow is bypassed through both solenoid valve 9
and solenoid valve 2. Flow through solenoid valve 9 is briefly
purged through the combustion chamber while flow from
solenoid valve 2 passes through the cellulose trap and IR cell as
previously described for the measure flow. Pneumatic gas flows
through the safety pressure regulator. With solenoid valve 9
open, the lance and purge flow (through solenoid valve 9)
ejects residual dust from the combustion tube.

1012

CS-200

Service

Furnace Open 2 Valve StateIn this valve state, the piston


moves down and, if selected, the vacuum turns on.
Lance flow is on while measure flow bypasses the furnace
altogether and flows directly through solenoid valve 2 and is
directed to the IR cell. Pneumatic gas is switched through the
safety pressure regulator and solenoid valve 10 causing the
piston to be lowered. In addition, the vacuum solid-state relay
switches on if it has been selected.
Furnace Open 3 Valve StateIn this valve state, the vacuum, if
selected, shuts off and the furnace remains open to load the
next crucible on the pedestal.
Flow is identical to Furnace Open 2 Valve State, but the vacuum
solid state relay switches the vacuum cleaner off.
Furnace Closed 1 Valve StateThis valve state is triggered
when a loaded crucible is placed on the piston and the piston
up/down key is pressed. The piston moves up under low
pressure until the up piston limit switch closes.
Oxygen flow completely bypasses the furnace through solenoid
valve 2 and is directed through the cellulose trap and IR cell.
Pneumatic gas flows through the safety pressure regulator and
closes solenoid valve 10 to move the piston up.
Furnace Closed 2 Valve StateIn this valve state, the lower
seal changes to high pressure and is sealed against the
combustion tube o-ring. Atmospheric gases are quickly purged
out of the combustion tube.
Lance flow is on and measure flow is on through the IR cell as
well as purged through the top of the combustion tube.
Pneumatic gas allows atmospheric gases to be purged from the
combustion tube.
Furnace Closed 3 Valve StateAfter a pre-analyze purge delay,
the combustion tube is pressurized in this valve state.
Oxygen flow is identical to that in Furnace Closed 2 Valve State,
but pneumatic flow goes through solenoid valve 9 only.
Analysis Valve StateFollowing Furnace Closed 3 Valve State,
there is a 2 second delay, after which the CPU checks that the
lance pressure switch is closed and a weight has been entered
in the weight stack. If both conditions are affirmative, the
system goes into Analyze Valve State, (previously discussed).
During a preanalyze delay, a stable IR baseline is obtained,
after which IR zeros are taken. Integration begins just before
the furnace is heated. As the sample is combusted in the
furnace, sample gases are mixed with the carrier gas (oxygen)
and CO2 is collected and released by the trap. Then the gas is
directed to the IR cell. Percent carbon is displayed on screen,
the furnace shuts off, and the answers are saved in memory
and then printed.

Service

CS-200

1013

Post-Analyze Valve StateIn this valve state, lance flow is shut


off while measure flow remains on to maintain a constant flow
through the IR detection system.
Lance flow is off, while measure flow is directed into the bottom
of the furnace and subsequently through the IR cell. The piston
remains raised under pneumatic pressure.

1014

CS-200

Service

Autocleaner
After a programmed number of analyses, the furnace must be
cleaned, either manually or automatically, to prevent excessive
residue buildup. The following procedure generally describes
both manual and automatic cleaning cycle flows; however, in
system controls, several autoclean options can be selected.
Refer to the System Controls procedure on page 516 and
System Configuration on page 459, for details.
In each of the three clean valve states, oxygen flow is bypassed
through the IR cell, the piston is down, and the door is closed.
Differences in these valve states include vacuum cleaner on or
off and brush up or down.
A clean cycle is begun by pressing [5] Clean from the analyze
menu. If the cup is up, the combustion tube is depressurized
(Furnace Open 1 Valve State) and the lance pressure switch
opens. If the piston switch is down, Clean 1 Valve State is
signaled and the furnace door closes.
If an autocleaner has been installed, the vacuum turns on, the
brush moves down (Clean 2 Valve State) and up (Clean 1 Valve
State), and then the cycle repeats 2 times. If manually
cleaning, the vacuum switch shuts off automatically (Clean 3
Valve State) and the vacuum switch is pressed manually to
begin cleaning. After cleaning the filter and combustion tube,
the vacuum switch is shut off manually. Then [5] Clean is
pressed and the furnace door opens (Furnace Open 3 Valve
State).
The cycle is completed when atmospheric gases are purged
from the system (gas flows for each valve state have been
previously discussed). After cleaning, the vacuum is shut off
(Furnace Open 3 Valve State), the clean switch is pressed, and
the cup moves up under low pressure (Furnace Closed 1 Valve
State). The cup then goes to high pressure, sealing the piston
against the o-ring. Atmospheric gases are purged from the
combustion tube (Furnace Closed 2 Valve State) and after a
purge delay, the combustion tube is pressurized. Finally, after a
two second delay, oxygen flows through both the furnace and
determinator (Post Analyze Valve State).

Service

CS-200

1015

Oxygen Solenoid

Bypass Solenoid

Lance Solenoid

Furnace Gas Solenoid

Pinch Valve Solenoid

Safety Solenoid

Doser Solenoid

Purge Solenoid

Piston Solenoid

Door Solenoid

Brush Solenoid

Furnace Control Solid State Relay*

Vacuum Cleaner Solid State Relay*

Barometric Control Valve Closed

Barometric Control Valve Open

Valve Control States

SV
1

SV
2

SV
3

SV
4

SV
5

SV
6

SV
7

SV
8

SV
9

SV
10

SV
11

SV
12

SV
13

SV
14

SV
15

SV
16

Gas Off

00

Standby

Analyze

Furnace Open 1

Furnace Open 2

Furnace Open 3

Furnace Closed 1

Furnace Closed 2

Furnace Closed 3

Post Analyze

Leak Check 1

Leak Check 2

Leak Check 3

Leak Check 4

Barometric

Clean 1

Clean 2

Clean 3

CS-200

Valve State

Notes

1 (One): Indicates the solenoid valve is open.

0 (Zero): Indicates the solenoid valve is closed.

* Independent of valve states

1016

CS-200

Service

BAROM
PRESSURE
TRANSDUCER

BAROM
CTRL
VALVE

PT

OVEN

FM

EXHAUST

FLOW
CONTROLLER

TRANSDUCER &
REGULATOR
ASSEMBLY
MEASURE
FLOW
ROTAMETER

SO3
TRAP
CELLULOSE
FILTER

SV3

CATALYST
HEATER

UPSTREAM
PRESSURE
GUAGE

PS

RESTRICTOR

PRESSURE
SWITCH

WIRE MESH
FILTER

PS
O2 IN
40 PSI

LECOSORB/ANH
PARTICLE
FILTER

SO2
IR
CELL

CO 2
IR CELL

SV1

SV2
QUARTZ
WOOL

C
NO

ANH

PRESSURE
REGULATOR

NC
SV9

INCOMING
PRESSURE
GUAGE
RESTRICTOR

EXH

SV5
PS

PRESSURE
SWITCH

SV11
NC

DOOR SOL. (OPTIONAL)

NO
4 PSI
PRESSURE
SWITCH

PS

SV12
NC

AUTO CLEANER (OPTIONAL)

NO

PS
25 PSI

PS
SV7

PNEUMATIC
PRESSURE
40 PSI

4 PSI

DOWN
SV10
NC

PARTICLE
FILTER

UP

NO

SAFETY
PRESSURE
REGULATOR

Figure 105
Gas Flow Diagram
Service

CS-200

1017

BAROM
PRESSURE
TRANSDUCER

BAROM
CTRL
VALVE

PT

OVEN

FM

EXHAUST

FLOW
CONTROLLER

TRANSDUCER &
REGULATOR
ASSEMBLY

SO2
IR
CELL

CO 2
IR CELL

MEASURE
FLOW
ROTAMETER

SO3
TRAP
CELLULOSE
FILTER

CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE

PS

SV3

MEASURE FLOW

QUARTZ
WOOL

PRESSURE
SWITCH

RESTRICTOR
ANH

PS
O2 IN
40 PSI

LECOSORB/ANH
PARTICLE
FILTER

PRESSURE
REGULATOR

SV1

SV9

PS

PRESSURE
SWITCH

SV5

DOWN

RESTRICTOR

SV10
NC
NO

UP

NO
FURNACE NC
BYPASS FLOW

SV11
NC
NO

DOOR SOL.
(OPTIONAL)
4 PSI

PRESSURE
SWITCH

PS

SV12
NC

AUTO CLEANER
(OPTIONAL)

NO

PS
25 PSI

PS
4 PSI

SV7

PNEUMATIC
PRESSURE
40 PSI

DUST
EJECT

PINCH VALVE
PARTICLE
FILTER

SAFETY
PRESSURE
REGULATOR

NC

SV6
NO

Figure 106
Gas Flow with Autocleaner Diagram

1018

CS-200

Service

SV2

LEAK CHECK WITH FURNACE BY-PASSSED


LEAK CHECK ENTIRE SYSTEM

BAROM
PRESSURE
TRANSDUCER

BAROM
CTRL
VALVE

PT

OVEN

FM

EXHAUST

FLOW
CONTROLLER

TRANSDUCER &
REGULATOR
ASSEMBLY
MEASURE
FLOW
ROTAMETER

SO3
TRAP
CELLULOSE
FILTER

SV3

PRESSURE
SWITCH

CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE

PS

RESTRICTOR
WIRE MESH
FILTER

PS
O2 IN
40 PSI

LECOSORB/ANH
PARTICLE
FILTER

SO2
IR
CELL

CO2
IR CELL

SV1

SV2

QUARTZ
WOOL

C
NO

ANH

PRESSURE
REGULATOR

NC

SV9

INCOMING
PRESSURE
GUAGE
RESTRICTOR

EXH

SV5
PS

PRESSURE
SWITCH

SV11
NC

DOOR SOL. (OPTIONAL)

NO
4 PSI
PRESSURE
SWITCH

PS

SV12
NC

AUTO CLEANER (OPTIONAL)

NO

PS
25 PSI

PS
SV7

PNEUMATIC
PRESSURE
40 PSI

4 PSI

DOWN
SV10
NC

PARTICLE
FILTER

UP

NO

SAFETY
PRESSURE
REGULATOR

Figure 107
Leak Check Flow Diagram

Service

CS-200

1019

LEAK CHECK WITH FURNACE BY-PASSED


LEAK CHECK ENTIRE SYSTEM

BAROM
PRESSURE
TRANSDUCER

BAROM
CTRL
VALVE

PT

OVEN

FM

EXHAUST

FLOW
CONTROLLER

TRANSDUCER &
REGULATOR
ASSEMBLY

SO2
IR
CELL

CO 2
IR CELL

MEASURE
FLOW
ROTAMETER

SO3
TRAP
CELLULOSE
FILTER

CATALYST
HEATER
UPSTREAM
PRESSURE
GUAGE

PS

SV3

MEASURE FLOW

QUARTZ
WOOL

PRESSURE
SWITCH

RESTRICTOR
ANH

PS
O2 IN
40 PSI

LECOSORB/ANH
PARTICLE
FILTER

PRESSURE
REGULATOR

SV1

SV9

PS

PRESSURE
SWITCH

SV5

RESTRICTOR

DOWN
SV10
NC
NO

UP
FURNACE

NC

NO
SV2

BYPASS FLOW
SV11
NC
NO

DOOR SOL.
(OPTIONAL)
4 PSI

PRESSURE
SWITCH

PS

SV12
NC

AUTO CLEANER
(OPTIONAL)

NO

PS
25 PSI

DUST
EJECT

PS
4 PSI

SV7

PNEUMATIC
PRESSURE
40 PSI

PINCH VALVE
PARTICLE
FILTER

SAFETY
PRESSURE
REGULATOR

NC

SV6
NO

Figure 108
Leak Check Flow with Autocleaner Diagram

1020

CS-200

Service

Figure 109
Analyze Sequence Diagram

Service

CS-200

1021

YES

FURNACE OPEN
3 VALVE STATE

YES

DELAY
1 SECOND

YES

LANCE
PRESSURE
SWITCH
OPEN
?

YES

FURNACE OPEN
1 VALVE STATE

YES

PISTON
CONTROL

YES

ANALYZE
V5

YES

PNEUMATIC
PRESSURE
+ 25 PSI

YES

O2
PRESSURE
+ 25 PSI

TURN
GAS ON

NO PNEUMATIC
PRESSURE

DUST CLOG IN
FLOW SYSTEM

YES

HAVE
2 SECONDS
ELAPSED
?

CUP MOVES DOWN

NO

NO

MEASURED FLOW
BY-PASSES FURNACE.
TUBE DEPRESSURIZED.
SOME DUST PURGED
THRU PINCH VALVE.

O2 FLOW THRU
FURNACE AND
ANALYTICAL SYSTEM

NO

YES

PRE-ANALYZE
PURGE DELAY

FURNACE
CLOSED 2
VALVE STATE
YES

YES

YES

PISTON
UP LIMIT
SWITCH

FURNACE
CLOSED 1
VALVE STATE
YES

YES

PISTON
CONTROL

YES

LOAD CRUCIBLE
AND SAMPLE

YES

NO

PISTON
NO
DOWN LIMIT
SWITCH

EDITABLE THRU
ANALYSIS METHOD

CUP CHANGES TO
HIGH PRESSURE.
PURGE ATMOSPHERIC
GASES OUT OF
COMBUSTION TUBE.

NO PISTON
UP LIMIT SWITCH

YES

HAVE
5 SECONDS
ELAPSED
?

NO

CUP MOVES UP
UNDER LOW PRESSURE

NO PISTON
DOWN LIMIT SWITCH

YES

HAVE
3 SECONDS
ELAPSED
?

NO

YES

TAKE
IR ZEROS

YES

750mV
< IR <
9500mV
RANGE

CHECK
COMBUSTION
PRESSURE
575L=PRESS
=625
YES

YES

PRE-ANALYZE
DELAY

LANCE
PRESSURE
SWITCH
CLOSED
?
YES

YES

ANALYZE
VALVE STATE

HAS SAMPLE
WEIGHT BEEN
ENTERED
?
YES

YES

DELAY
2 SECONDS

FURNACE
CLOSED 3
VALVE STATE
YES

ENTER
WEIGHT

O2 FLOW
THRU FURNACE
AND ANALYTICAL
SYSTEM

NO COMBUSTION
TUBE PRESSURE

NO

IR CELL
OUT OF RANGE

WARNING
COMBUSTION
PRESSURE

NO

EDITABLE THRU
ANALYSIS METHOD
ALL ATMOSPHERIC GASES
PURGED FROM SYSTEM.
WAITING FOR GOOD
STABLE IR BASELINE.

NO

NO

COMBUSTION TUBE
IS PURGED AND
PRESSURIZED

NO

DISPLAY
CARBON
ANSWER
YES

YES

SAVE AND
PRINT
ANSWERS

MINIMUM
SULFUR
TIME
?
YES

POST ANALYZE
VALVE STATE

NO

NO

LANCE FLOW
IS OFF

LOW PLATE
CURRENT
OR
LOW GRID
CURRENT

DISPLAY
SULFUR
ANSWER
YES

SULFUR
COMPARATOR
LEVEL
?
YES

YES

FURNACE
OFF

NO

MONITOR
GRID & PLATE
CURRENT

CARBON
COMPARATOR
LEVEL
?
YES

MINIMUM
CARBON
TIME
?
YES

MONITOR GRID
AND
PLATE CURRENT

YES

LIVE ANSWER
DISPLAY

YES

FURNACE
ON

YES

START
INTEGRATION

Notices, Errors, and Warnings


Notices
Message

Cause

Probable Solution

Data Transmit Port


Disabled

Data transmit
option is disabled.

Select transmit options


from the setup menu
and enable data transmit.

No Results Available

No results are
stored in result list.

Run analysis
to obtain results.

No Results Selected

No results selected
from the result list.

Select results before


performing procedure.

No Weights Entered

No weights have
been entered into
the weight stack.

Enter weights into


the weight stack.

Password Mismatch

The incorrect
password was entered.

Enter the
correct password.

Printer Not Ready

Printer is not turned on,


on-line, or connected.

Make sure the printer


is turned on, on-line,
and connected.

Reset Memory

Appears when memory


reset is selected from a
menu or when a software
update is performed.

Either reset memory


by pressing Yes or
abort and do not reset
memory by pressing No.

Sample Weight
Out Of Range

Sample weight exceeded


limits of reasonable value.

Enter correct
sample weight.

1022

CS-200

Service

Warnings
Message

Cause

Probable Solution

Clean Dust Filter

Clean counter limit


reached.

Clean the dust filter,


either manually or
automatically.

Combustion Pressure

Pressure outside of
575mm to 625mm range.

Perform a combustion
pressure adjustment.

Low Plate Current


Or Low Grid Current

Plate current drops


below 200mA causing
poor coupling or
grid current drops
below 50mA causing
weak oscillator tube.

Add accelerator or iron


chip depending on
sample.
Replace oscillator tube.
Replace lance flow
restrictor.

Service

CS-200

1023

Errors
Message

Cause

Probable Solution

Balance Port Open Failure

Balance port
will not initialize.

Hardware problem.
Contact the LECO
service department.

Blank Out Of Range


[Element Name]

Blank result range of ~


1% exceeded. Incorrect
blank results selected.

Select correct blank


results from results list.

Calibration Out Of Range


[Element Name]

Calibration results out


of range, .01 to 10.
Incorrect calibration
results selected.

Select correct calibration


results from results list.

Data Transmit
[Port Disabled,
Buffer Is Full,
Buffer Is Empty,
String Is Too Long,
Not Enough Room]

Data transmit port


inoperative.

Hardware problem.
Contact the LECO
service department.

Dust Clog In Flow System

Dust filter is dirty.

Clean dust filter.

IR cell voltage
exceeds range limits.

Access the ambient


monitor to determine the
IR cell voltage output.
Refer to the IR Cell
procedure (page 9-11)
to adjust IR cell
output voltage.

Cleaning brush did not


reach the fully extended
position during cleaning.

Check the lance flow


path in the center of
the brush for clogging.
Turn pneumatic pressure
on and off and check for
possible jam-up.

Cleaning brush did


not reach fully retracted
position during cleaning.

Check the lance flow


path in the center of
the brush for clogging.
Turn pneumatic pressure
on and off and check for
possible jam-up.

Combustion system
cannot pressurize.

Gross leak in
combustion system.
Check furnace o-rings
and outer combustion
tube for possible cracks.

IR Cell Out Of Range

No Brush Down Limit


Switch

No Brush Up Limit Switch

No Combustion
Tube Pressure

1024

CS-200

Service

Message

Cause

Probable Solution

No Door Open Limit


Switch

Door did not retract


after cleaning cycle.

Turn pneumatic pressure


off and then on.
Check for door jam.

No Oxygen Pressure

Pressure loss from oxygen


supply or pressure is less
than 25 psi.

Check oxygen supply


and supply lines.
Check oxygen regulator.

No Piston Up Limit Switch

Piston did not raise


crucible to the up position.

Check pneumatic
pressure. Check to see if
crucible is jammed.

No Pneumatic Pressure

Pneumatic pressure is
turned off or gas bottle is
empty.

Check and determine if


gas supply is turned off.
Replace gas bottle.

Transmit Port Open


Failure

Transmit port will not


initialize.

Hardware problem.
Contact the LECO
service department.

Pneumatic supply
is turned off.
Possible gross
leak in system.

Determine that pneumatic


supply is turned on.
Perform a leak check and
check for leaks.
Bypass furnace.
Check o-rings.
Look for a cracked
combustion tube.

Unable To Pressurize

Service

CS-200

1025

Software Upgrade
A major portion of the determinator's functions are defined and
controlled by a software program that may be updated. Most
updates do not affect the physical design of the determinator,
but can improve performance and make operation easier.
Therefore, an identification system for program changes called
'Program Version' is used in the CS-200 Carbon and Sulfur
Determinator and other LECO instruments.
A three-digit number identifies program version levels. The first
generation of a program is version '1.00'. Each time a program
is changed, the version number is increased.

Keypad

The following procedure is for DSP instruments. For


Windows instruments refer to Software Upgrade with
Windows on page 1029.

DSP Software Upgrade Procedure

Note

1.

WARNING

1026

When installing new EPROMs, be careful not to bend any of


the EPROM pins out of the socket or under the EPROM.
Place the determinator's power on/off switch in the off
position and disconnect from facility power.

ELECTRICAL SHOCK HAZARD


The CS-200 operates from 230V~. Contact with
this voltage can be lethal. Disconnect the
determinator from the facility power source
before removing the side panels.

CS-200

Service

2.

WARNING

Note

Service

Remove the left side panel of the determinator to expose


the CPU circuit board. Refer to Figure 10-10, page 1028.

ELECTRICAL SHOCK HAZARD


After the side panel is removed high voltage is
present. Use caution when making these
adjustments. Contact with voltages inside the
instrument can be lethal or cause serious injury.

3.

Locate the program EPROMs IC3 and IC4. With a small flat
tip screwdriver, pry the old EPROMs from their sockets.
Discard the EPROMs.

4.

Install the new program EPROMs in sockets IC3 and IC4.


Install the low EPROM in socket IC4 and the high EPROM in
socket IC3.

Make sure the notch at the end of the EPROM is located


over the half circle screened on the CPU circuit board.

5.

Reinstall the left side panel of the determinator.

6.

Turn the AC power on. The Copyright screen should be


displayed.

7.

After approximately 10 seconds the Reset Confirmation


screen will be displayed. Answer Yes to all questions. All
system parameters will be set to their factory default
values.

8.

If desired, enter the old system parameter values printed


from System Parameters. The barometric pressure should
be set.

9.

Proceed with setup and operation of the determinator.

CS-200

1027

IC3

IC4

C1
C2

R7

U1

U9

C123

U10

C46

PD1A

PD2A

C54

IC4

PD2

IC3

J1

U30

C6

PD4

PD1 C5

R42

U14

U13

CR3

C49
CR1
+

C110

C109

C122
CR2 + U31

C121

U29

C50 R17 R18

C25 C26

C72

C108

C73

C71

C48

R13

R28

U12

U11
C44

C45

C47
U27

C68
R29
C69
U28
C107
R33

C111

C114

C7
U3

C9

PD5

C10
RN1

C30

PD8

C11

Y1

C31

U17

C58

C87

U36

COPYRIGHT C 1994-95
ALL RIGHTS RESERVED
LECO CORPORATION
ST. JOSEPH, MI U. S. A.

C56

C8

C57

U34

C85 C86

U35

R8
R9
R10
CR4 R11
R12

U33

C55

PD6

U15

U2

J859A

C27

U16

C80

U32

C113

J859K

PD9

C59

C88

C12

U4

C32

U18

U39

C60

IC39

C115

C90

C89

U19

TP1
TP2
TP3

C66

U37

U38

J859I

+
C4

C20
C21

C3

C23
C24
+
J859H
1

C67

19

C106

C13

J859B

13
U5

U45

U41

C92

U22

J859C

C16

U23

C93

R3
R2 R4

RN2

C95
C96
C97
C98

C63

C17

R1

U46

R34

U42

C117

U7

Y2 C62

C34
C35
J859H

C116

C61

C33

U6

U20

U44

U40

C91

U21

C15

19

C14

A1
B1
C1
A32
B32
C32

C118

C18

J859D

U8

R24
R25
R26
R27

U24

L1

U43

Y3

PD3

IC9

J859F
1
1

Q1

C19

R6

C103

C65

+ C43

C42

R5

U26

C101

TP5
TP6
TP7

U48
C120

SW1

+
C104
+
C105

+ C102

U25

C124

1
J859E

C64

C41

+
C99

C100

C94
PD7

U47

J859N

C119

1
1
1

R19
R20
R21
R22
R23

CPU BOARD
C28
R43
C29

J859G

J859J

J859L

Service

CS-200

1028

C76

C36
C37
C38
C39
C40
R35
R36
R37
R38
R39
R40
R41

C78
C79
C82
C83
C84

C74
C75

C51
C52
C53
C77
C81
C112

R14
R15
R32 R30

R16
C70
R31

C22

Figure 10-10
EPROM Location

Software Upgrade with Windows

Windows

Service

The following information is for Windows instruments. For


DSP instruments refer to DSP Software Upgrade Procedure
on page 1026.

1.

With the computer on, place the software update disk in


the CDROM drive.

2.

Click on the Start button in the lower left-hand corner of


the desktop.

3.

Click Run. The Run dialog box is displayed.

4.

Enter D:\Setup.exe and click OK.

5.

Follow the instructions displayed on the screen to


complete the installation.

6.

If desired, enter the old system parameters. The time and


barometric pressure should be set.

7.

Proceed with setup and operation of the determinator.

CS-200

1029

Linearization with DSP

Keypad

Notes

The following procedure is for DSP instruments. For


Windows instruments refer to Linearization on page 1032.

To optimize linearity of the detection system, break and


slope values are employed.

The break and slope values to enter are found on the


linearization tag attached to the IR cell.

The break and slope values were entered during the


manufacturing process, new values should be entered only
if the IR cell is replaced, the version of software is updated
or the system has been reset.

1.

Access linearization by choosing [9] More then [2]


Linearization from the setup menu.
Carbon
#
Break
0
0
0
565
1
1101
2
2258
3
3785
4
6424
5
9261
6
12414
7
16063
8
18503
9
20584
Range:

Note

1030

Adj Bk
1.0000
565
1125
2326
3898
6677
9612
12873
16821
19493
21776

Slope
1.0466
1.0381
1.0299
1.0534
1.0348
1.0344
1.0822
1.0921
1.1001
0 - 52000

Linearization permits the operator to enter the break and


slope values that were determined during the
manufacturing process.

CS-200

Service

Service

2.

Press Select or Next to move the cursor to the next line.

3.

Press Previous to move the cursor back one line.

4.

Press the left or right arrow keys to move the cursor and
edit a digit using the keypad.

5.

Press Menu to access the print command. If a copy of the


linearization is desired, press [1] Print from the menu.

6.

After all break and slope values have been entered, press
Exit to return to the setup menu. The determinator will
calculate the adjusted break value.

CS-200

1031

Linearization with Windows

Windows

The following information is for Windows instruments. For


DSP instruments refer to Linearization on page 1030.

The output signal (voltage) from the IR cell detector is not


linear with respect to element concentration. To make the
output of the IR cell appear linear, each cell is linearized by
LECO during the manufacturing process.
Notes

It is only necessary to perform this procedure if an IR cell is


replaced. The reference and saturation values to enter
during this procedure can be found on a tag attached to the
replacement IR cell.

The Break and Slope values are not used by LECO but can
be used by the operator to customize their instrument. Click
on the table to enter a break and slope value.

1.

1032

Click Configuration and select Linearizations. The


linearization dialog box will appear.

CS-200

Service

Service

2.

Click the arrow in the Select Cell drop down box and select
the IR cell to linearize. Selections are Carbon Low Range,
Carbon High Range or Sulfur.

3.

Click on the table and enter the break and slope values. The
determinator will calculate the adjusted break value.

4.

Click OK to save the adjusted break value and exit this


procedure.

CS-200

1033

11

Illustrations

Figure 11-1 ....... CS-200 Left Side View ................................ 11-3


Figure 11-2 ....... CS-200 Right Side View .............................. 11-4
Figure 11-3 ....... CS-200 with Autocleaner Right Side View ...... 11-5
Figure 11-4 ....... 609-626 Autocleaner Assembly.................... 11-6
Figure 11-5 ....... 616-771 Catalyst Heater Panel .................... 11-7
Figure 11-6 ....... 614-492 Display ........................................ 11-8
Figure 11-7 ....... 617-248 Barometric Flow Controller ............. 11-9
Figure 11-8 ....... 616-896 Gas Panel Assembly ...................... 11-10
Figure 11-9 ....... 604-080-110 CO2 IR Cell............................. 11-11
Figure 11-10...... 778-574-120 CO2 IR Cell ............................ 11-12
Figure 11-11...... 782-723-110 CO2 IR Cell ............................ 11-13
Figure 11-12...... 616-706 SO2 IR Cell ................................... 11-14
Figure 11-13...... 782-067-110 SO2 IR Cell ............................ 11-15
Figure 11-14...... 781-420 Lance and Filter Assembly .............. 11-16
Figure 11-15...... 620-612 Manifold Assembly......................... 11-17
Figure 11-16...... 604-001 Oscillator ..................................... 11-18
Figure 11-17...... 616-893 Pinch Valve Assembly .................... 11-19
Figure 11-18...... 616-715 Power Supply ............................... 11-20
Figure 11-19...... 616-705 Power Supply Chassis .................... 11-21
Figure 11-20...... 773-383 Pressure Regulator ........................ 11-22
Figure 11-21...... 782-839 Pressure Regulator ........................ 11-22
Figure 11-22...... 602-491 Pressure Switch and Restrictor ........ 11-23
Figure 11-23...... 604-059 Solenoid Valve .............................. 11-24
Figure 11-24...... 606-649 Solenoid Valve .............................. 11-24
Figure 11-25...... 606-651 Solenoid Valve .............................. 11-25
Figure 11-26...... 606-652 Solenoid Valve .............................. 11-25
Figure 11-27...... 616-764 Twin Rod Cylinder ......................... 11-26
Figure 11-28...... CS200 and CS200CH Series Oven Tubing Diagram
....................... 11-27
Figure 11-29...... CS200CL Series Oven Tubing Diagram .......... 11-28
Figure 11-30...... CS200CSH Series Oven Tubing Diagram ....... 11-29
Figure 11-31...... CS200SH Series Oven Tubing Diagram ......... 11-30

11-1

CS-200

Illustrations

This page intentionally left blank.

Illustrations

CS-200

11-2

620-611 W/AC
620-612 WO/AC
MANIFOLD
ASSEMBLY
666-147
CELL POWER
SUPPLY CARD

614-833
FAN
ASSEMBLY

606-466
FILTER

666-339-xxx
CPU CARD

666-004*
BRIGHT / CONTRAST
ADJUSTMENT CARD
773-383
REGULATOR
777-836*
POWER SUPPLY
LCD

777-759
OVEN
INTERFACE
CARD

604-727*
LCD DISPLAY
666-112
INDUCTION
POWER CARD

777-504
CHOPPER
MOTOR
CARD
777-899-101
16 POSITION
SOLENOID
INTERFACE
CARD

608-399
SPEAKER
ASSEMBLY

666-038
PID PRESSURE
REGULATOR
CARD

666-042
DUAL SWITCH
INTERFACE
CARD

666-078-101
CATALYST
HEATER
CONTROL
CARD
777-923
POWER
DISTRIBUTION
CARD

666-034
FILTERED
D-SHELL
775-296
ISOLATION
CARD A

608-497
RELAY

781-165
RELAY

769-370
RELAY

603-818
FAN & PLATE
ASSEMBLY

602-454
REGULATOR
FLOW CONTROL
ASSEMBLY

666-224-110
OVEN HEATER
CARD

782-067-110
SO2 IR-CELL

778-574-120
CO2 IR CELL

* THESE ITEMS ARE ONLY FOUND ON UNITS WITH NO PC.


-xxx CPU CARD VARIES BY PACKAGE.

CONSULT THE PACKING SLIP.

Figure 11-1
CS-200 Left Side View

11-3

CS-200

Illustrations

776-008
VACUUM CAPACITOR

604-001
OSCILLATOR
ASSEMBLY
781-420
LANCE AND FILTER
ASSEMBLY
( NOT ON UNITS
WITH AUTOCLEANER)

771-354
OSCILLATOR
TUBE

550-048
GRID CHOKE

775-298
ISOLATION
CARD B

616-718
FILAMENT
TRANSFORMER

616-705
POWER
SUPPLY
CHASSIS

762-066
RECTIFIER
(4) REQD

789-410
BRACKET &
RECTIFIER
ASSEMBLY
604-155
LIMIT SWITCH
(2 REQ'D)

614-465
HIGH VOLTAGE
TRANSFORMER

607-157
RELAY FURNACE
INTERLOCK

771-986
AC FILTER
779-270
SAFETY
INTERLOCK
SWITCH

770-990
VOLTAGE
SELECTION
TERMINAL
STRIP

781-165
RELAY

Figure 11-2
CS-200 Right Side View

Illustrations

CS-200

11-4

776-008
VACUUM CAPACITOR

604-001
OSCILLATOR
ASSEMBLY

609-626
AUTOCLEANER
ASSEMBLY

771-354
OSCILLATOR
TUBE

550-048
GRID CHOKE

775-298
ISOLATION
CARD B

616-718
FILAMENT
TRANSFORMER

616-705
POWER
SUPPLY
CHASSIS

762-066
RECTIFIER
(4 REQD)

789-410
BRACKET &
RECTIFIER
ASSEMBLY
604-155
LIMIT SWITCH
(2 REQ'D)

614-465
HIGH VOLTAGE
TRANSFORMER

616-893
PINCH VALVE
ASSEMBLY

607-157
RELAY FURNACE
INTERLOCK

771-986
AC FILTER
779-270
SAFETY
INTERLOCK
SWITCH

770-990
VOLTAGE
SELECTION
TERMINAL
STRIP

781-165
RELAY

Figure 11-3
CS-200 with Autocleaner Right Side View

11-5

CS-200

Illustrations

604-291
AIR CYLINDER
806-214
FITTING
(2) REQD

604-519
EXTENSION

807-261
FITTING
(2) REQD
193-143
LOCKWASHER
610-735
SLOTTED
BRUSH

807-196
TUBING
(2) REQD

604-517
RETAINER
604-516
FITTING

773-320
O-RING
(2 REQD)

789-115
LANCE TUBE

604-268
BODY
ASSEMBLY

193-164
LOCKWASHER
(2 REQD)

604-172
O-RING
604-274
SHAFT
604-163
BRUSH
762-058
O-RING

190-228
SCREW
(2 REQD)
604-159
PLUNGER

604-273
BUSHING
ADAPTOR

604-272
CAP
190-757
SCREW
(4) REQD

604-168
LOCK
MOUNT

771-991
O-RING

778-703
SPACER
(4) REQD

778-596
FILTER

190-090
THUMBSCREW
(2 REQD)

762-058
O-RING

773-926
PLATE
190-431
SCREW
(2) REQD

762-058
O-RING

773-577
PISTON RING

Figure 11-4
609-626 Autocleaner Assembly

Illustrations

CS-200

11-6

CATALYST HEATER
TUBE

781-364
CATALYST HEATER
ASSEMBLY

772-725
ENCLOSURE
772-694
KNOB

772-738
O-RING

614-316
MOVABLE
BLOCK

614-319
STATIONARY
BLOCK
190-229
SCREW
(3 REQ'D)

192-004
SCREW
(4 REQ'D)

772-737
INSULATOR
768-798
PLUG

193-008
WASHER
(6 REQ'D)

782-042
TOP
INSULATOR

772-729
CORE
INSULATOR

614-411
BLOCK
772-520
O-RING
(4 REQ'D)

190-278
SCREW
(6 REQ'D)

614-412
LOWER BLOCK

781-365
CATALYST HEATER
ELEMENT
781-366
THERMOCOUPLE
TYPE K

616-767
PANEL

762-664
CHROMAL
WIRE

772-730
BOTTOM
INSULATOR

772-736
CATALYST
HEATER
CAP

Figure 11-5
616-771 Catalyst Heater Panel
11-7

CS-200

Illustrations

610-754
SWITCH
MEMBRANE

783-741
BRACKET
614-290
CONDUCTIVE
SHIELD

783-757
SLEEVE
(4 REQUIRED)

194-105
NUT
(4 REQUIRED)
777-836
LCD POWER
CARD

614-294
GASKET

J836C
604-727
DISPLAY
J836G

PLUG INTO J836G

604-744
STUD EXTENSION
(4 REQUIRED)

CONDUCTIVE SIDE OF
614-290 HAS TO BE
PLACED AGAINST THE
BRACKET 783-741

Figure 11-6
614-492 Display

Illustrations

CS-200

11-8

783-791
VALVE
ASSEMBLY
617-246
PRESSURE
SENSOR

537-165
ELBOW
FITTING

604-316
FITTING
761-784
FITTING

193-054
WASHER
(2-REQ'D)
190-227
SCREW
(2-REQ'D)

783-792
BRACKET

602-581
STANDOFF
(4-REQ'D)

666-038
PID PRESSURE
REGULATOR CARD ASSEMBLY

Figure 11-7
617-248 Barometric Flow Controller

11-9

CS-200

Illustrations

616-771
CATALYST
ASSEMBLY

772-458
FITTING
(2 REQ'D)

194-056
NUT
(6 REQ'D)
193-055
WASHER
(6 REQ'D)

614-414
UPPER
BLOCK

190-698
SCREW
(2 REQ'D)
783-689
BRACKET
194-056
NUT
(2 REQ'D)

789-349
BLOCK
765-976
O-RING
773-383
REGULATOR

772-520
O-RING
(3 REQ'D)

803-431
FITTING
(2 REQ'D)

614-413
LOWER
BLOCK
(2 REQ'D)
190-277
SCREW
(4 REQ'D)
193-008
WASHER
(4 REQ'D)

193-008
WASHER
(8 REQ'D)

616-891
BRACKET
194-056
NUT
(2 REQUIRED)
606-650
3 WAY
SOLENOID
VALVE

190-278
SCREW
(8 REQ'D)
772-702
FITTING TEE
(2 REQ'D)
616-768
PANEL

772-458
FITTING
(4 REQ'D)

NOTE:
616-896 ASSEMBLY IS AS SHOWN;
FOR 616-897 ASSEMBLY USE 614-931
PANEL INSTEAD OF 616-771 CATALYST
ASSEMBLY.

606-649
2 WAY
SOLENOID
VALVE

Figure 11-8
616-896 Gas Panel Assembly

Illustrations

CS-200

11-10

Figure 11-9
604-080-110 CO2 IR Cell

11-11

CS-200

Illustrations

783-040
PREAMP
COVER

193-006
WASHER
(4 REQ'D)

190-227
SCREW
(4 REQ'D)

777-818
PREAMP
CARD
783-038
HEX SPACER
(4 REQ'D)

770-838
THERMAL
RESISTOR

193-104
WASHER

190-227
SCREW
(4 REQ'D)

783-127
EXTENSION
(2 REQ'D)

781-637
FOAM PAD

783-124
COVER SEAL

783-037
MOUNT

190-866
SET SCREW

768-944
O-RING

190-766
SCREW

781-941
SOURCE
END CAP

190-295
SCREW
(4 REQ'D)

781-949
GUARD
FEEDTHRU

190-247
SCREW
(2 REQ'D)

772-560
CHOPPER MOTOR

781-943
SOURCE
PLATE

190-174
SCREW
(2 REQ'D)

781-945
LECOSORB
CYLINDER

772-561
IR SOURCE AND
REFLECTOR PLATE

190-766
SCREW

772-563
IR SOURCE
ASSEMBLY

782-063
CONE IR DETECTOR 768-974
ASSEMBLY
CHOPPER
BLADE

604-096
END DETECTOR BODY
ASSEMBLY

782-697
INNER
GASKET

193-054
WASHER
(4 REQ'D)

Figure 11-10
778-574-120 CO2 IR Cell

Illustrations

CS-200

11-12

783-040
PREAMP
COVER

193-006
WASHER
(4 REQ'D)

190-227
SCREW
(4 REQ'D)

777-818
PREAMP
CARD
783-038
SPACER
(4 REQ'D)

770-838
THERMAL
RESISTOR

193-104
WASHER

190-227
SCREW
(4 REQ'D)

783-127
EXTENSION
(2 REQD)

781-637
FOAM PAD

783-124
COVER SEAL

783-037
MOUNT

190-766
SCREW

772-563
IR SOURCE
ASSEMBLY

190-866
SET SCREW

782-063
768-974
CONE IR DETECTOR CHOPPER
ASSEMBLY
BLADE

772-809
BLOCK & WINDOWS
ASSEMBLY

782-697
INNER
GASKET

193-054
WASHER
(4 REQ'D)

190-766
SCREW

772-561
IR SOURCE AND
REFLECTOR PLATE

768-944
O-RING

781-941
SOURCE
END CAP

190-247
SCREW
(2 REQ'D)

190-295
SCREW
(4 REQ'D)

781-949
GUARD
FEEDTHRU

772-560
CHOPPER MOTOR

781-943
SOURCE
PLATE

190-174
SCREW
(2 REQ'D)

781-945
LECOSORB
CYLINDER

Figure 11-11
782-723-110 CO2 IR Cell

11-13

CS-200

Illustrations

190-247
SCREW
(2-REQ'D)

772-560
MOTOR

768-944
O-RING

190-295
SCREW
(4-REQ'D)

190-766
SCREW

190-174
SCREW
(2-REQ'D)

781-945
ASSY CYLINDER
ASCARITE

781-987
SOURCE
CAP ASSEMBLY

190-866
SCREW

190-601
SCREW
(4 REQ'D)

772-806
PLATE
(2 REQ'D)

768-974
CHOPPER MOTOR
BLADE
190-820
SCREW
(6-REQ'D)

190-766
SCREW

781-942
IR SOURCE
AND
772-561
REFLECTOR

783-038
STANDOFF
(4 REQ'D)

190-227
SCREW
(4 REQ'D)

193-104
WASHER

770-838
THERMAL
RESISTER

782-697
GASKET

781-992
CELL
BODY
ASSEMBLY

190-227
SCREW
(4 REQ'D)

781-637
FOAM PAD

777-818
PREAMP CARD
ASSEMBLY

783-040
193-006
COVER
WASHER
(4 REQ'D) ASSEMBLY

783-037
MOUNT

782-063
CONE DETECTOR
ASSEMBLY

Figure 11-12
616-706 SO2 IR Cell

Illustrations

CS-200

11-14

783-040
PREAMP
COVER

193-006
WASHER
(4 REQ'D)

190-227
SCREW
(4 REQ'D)

777-818
PREAMP
CARD
783-038
HEX SPACER
(4 REQUIRED)

770-838
THERMAL
RESISTOR

193-104
WASHER

190-227
SCREW
(4 REQ'D)

783-127
EXTENSION
(2 REQD)

781-637
FOAM PAD

783-124
COVER SEAL

783-037
MOUNT

782-065
CONE IR
DETECTOR
ASSEMBLY

190-866
SET SCREW

768-944
O-RING

190-766
SCREW

781-941
SOURCE
END CAP

190-295
SCREW
(4 REQ'D)

781-949
GUARD
FEEDTHRU

190-247
SCREW
(2 REQ'D)

772-560
CHOPPER MOTOR

781-943
SOURCE
PLATE

190-174
SCREW
(2 REQ'D)

781-945
LECOSORB
CYLINDER

772-561
IR SOURCE AND
REFLECTOR PLATE

190-766
SCREW

772-563
IR SOURCE
ASSEMBLY

768-974
CHOPPER
BLADE

781-992
END DETECTOR BODY
ASSEMBLY

782-697
INNER
GASKET

193-054
WASHER
(4 REQ'D)

Figure 11-13
782-067-110 SO2 IR Cell

11-15

CS-200

Illustrations

783-040
PREAMP
COVER

193-006
LOCKWASHER
(4 REQUIRED)

770-838
THERMAL
RESISTOR

783-038
HEX SPACER
(4 REQUIRED)

777-817
PREAMP
CARD

193-104
WASHER

190-227
SCREW
(4 REQUIRED)

783-127
EXTENSION
(2 REQUIRED)
190-227
SCREW
(4 REQUIRED)

781-637
FOAM PAD

783-124
COVER SEAL

783-037
MOUNT

782-697
INNER
GASKET

190-820
SCREW
(3 REQUIRED)

193-054
WASHER
(4 REQUIRED)

781-849-010
DETECTOR
BLOCK

12

782-056
TUBE CELL BODY
ASSEMBLY

109-601
SCREW
(4 REQUIRED)

190-866
SET SCREW

768-974
CHOPPER BLADE

190-766
SCREW

772-563
IR SOURCE
ASSEMBLY

772-806
PLATE
(2 REQUIRED)

781-990
0-RING
(3 REQUIRED)

190-820
SCREW
(3 REQUIRED)

781-991-010
SOURCE
BLOCK

777-066
TUBE BODY

772-520
0-RING
(2 REQUIRED)

775-795
SPACER
(2 REQUIRED)

772-804
GOLD PLATED
GLASS TUBE

772-557
TUBE
(2 REQUIRED)

190-766
SCREW

772-561
IR SOURCE
REFLECTOR
PLATE

768-944
O-RING

190-295
SCREW
(4 REQUIRED)

781-941
SOURCE
END CAP

781-949
GUARD
FEEDTHRU

190-247
SCREW
(2 REQUIRED)

772-560
CHOPPER MOTOR

781-943
SOURCE
PLATE

190-174
SCREW
(2 REQUIRED)

781-945
LECOSORB CYLINDER

773-311
FILTER

781-422
FILTER CAP
781-424
O-RING

762-058
O-RING

*772-704
FITTING

781-663
LANCE
GUARD

781-421
FILTER
HOUSING
*773-136
FITTING

789-118
LANCE TUBE
ASSEMBLY

771-991
O-RING
772-381
LANCE
CLEANING
ROD

781-423
ADAPTOR TUBE
BUSHING
762-058
O-RING

LANCE
TUBE

773-577
PISTON
RING
190-431
SCREW
(4) REQD

781-425
FILTER END
PLATE
190-258
SCREW
(2) REQD

762-058
O-RING

*781-401
ADAPTER
RING
NOTE: * NOT PART OF ASSEMBLY

Figure 11-14
781-420 Lance and Filter Assembly

Illustrations

CS-200

11-16

Figure 11-15
620-612 Manifold Assembly

11-17

CS-200

Illustrations

S2

SV1 616-567-106 2-way valve


SV2 616-567-106 2-way valve
SV3 616-567-106 2-way valve
SV5 616-567-106 2-way valve
SV7 616-567-106 2-way valve

SV10A 616-567-108 3-way valve


SV10B 616-567-108 3-way valve

SV12A 616-567-107 3-way valve with speed control


SV12B 616-567-107 3-way valve with speed control
SV11A 616-567-107 3-way valve with speed control
SV11B 616-567-107 3-way valve with speed control

Safety Pressure
Regulator

S5

Oxygen

SV1

S14

S14

Bypass

SV2

Furnace

SV6

783-772 Pressure Switch

Lance

SV3

No Hole indicates
2-way valve.

609-113 Pressure Switch

S2 and S5

Autocleaner

Door

Safety
Cylinder

SV10A SV10B SV11A SV11B SV12A SV12B

Hole in lower position


indicates 3-way valve
normally closed.

SV7

Hole in upper position


indicates 3-way valve
normally open.

604-009
COIL STRAP

604-010
HIGH VOLTAGE
STRAP

764-640
CAPACITOR
(2-REQ'D)

776-008
VACUUM
CAPACITOR

771-356
PLATE
CONNECTOR

550-047
CHOKE
ASSEMBLY

776-129
COIL
ASSEMBLY

771-354
OSCILLATOR
TUBE
566-002
COIL COLLET
(2-REQ'D)

550-187
CAPACITOR
500
100

200
200

771-487
STANDOFF
(4 REQ'D)

200

764-641
CAPACITORS
(4-REQ'D)
604-008
SUPPRESSOR
773-066
CERAMIC
STANDOFF
(5 REQ'D BUT
NOT SHOWN)

521-037
TERMINAL BLOCK

773-572
GROMMET

776-175
5K RESISTOR
(UNDER SHELF)

550-048
RF CHOKE

Figure 11-16
604-001 Oscillator

Illustrations

CS-200

11-18

616-892
BRACKET

190-246
SCREW
(2 REQ'D)

589-182
FITTING

774-612
HOUSING
774-613
O-RING
769-973
ROLL PIN
(2 REQ'D)
774-610
PISTON

772-909
PINCH VALVE
ASSEMBLY

776-093
CAP
190-246
SCREW
(2 REQ'D)
501-110
SILICONE
TUBE

Figure 11-17
616-893 Pinch Valve Assembly

11-19

CS-200

Illustrations

190-227
SCREW
(4 REQD)

777-923
ASSY CARD
900-537
STANDOFF
(4 REQD)

190-231
SCREW
(8 REQD)
190-277
SCREW
(3 REQD)

193-006
WASHER
(4 REQD)

602-407
COVER

193-008
WASHER
(11 REQD)

190-277
SCREW
(11 REQD)

193-008
WASHER
(3 REQD)

194-055
NUT
(4 REQD)

193-006
WASHER
(6 REQD)

615-728
ASSY HARNESS
190-277
SCREW
(7 REQD)

190-004
SCREW
(4 REQD)

194-055
NUT
(8 REQD)

602-439
PLATE

193-008
WASHER
(7 REQD)

609-081
ASSY HARNESS
602-410
PANEL

782-746
FILTER

604-709
GUARD

194-055
NUT
(2 REQD)

194-105
NUT
(4 REQD)

608-386
FAN

194-055
NUT
(4 REQD)

193-006
WASHER
(4 REQD)
190-239
SCREW
(4 REQD)

TB101

608-604
POWER SUPPLY

190-232
SCREW
(2 REQD)

190-424
SCREW
(2 REQD)
615-574
RECEPTACLE

190-229
SCREW
(4 REQD)

194-059
NUTS
(4 REQD)

194-105
NUT
(2 REQD)

190-277
SCREW
(22 REQD)
193-008
WASHER
(22 REQD)

194-056
NUT
(2 REQD)
193-008
WASHER
(2 REQ'D)

750-155-106
TERMINAL
BLOCK

616-707
TRANSFORMER
ASSEMBLY

750-155-100
JUMPER

616-714
BOX
778-951
CIRCUIT
BREAKER

190-381
SCREW
(4 REQD)

602-410
PLATE

602-409
BRACKET

Figure 11-18
616-715 Power Supply

Illustrations

CS-200

11-20

190-752
SCREW
(4 REQ'D)

193-108
WASHER
(4 REQ'D)

616-718
TRANSFORMER

193-008
WASHER
(3 REQ'D)
190-277
SCREW
(3 REQ'D)
802-340
INSULATOR
589-275
TERMINAL
BLOCK
190-231
SCREW
(2 REQ'D)

190-277
SCREW
(2 REQ'D)
773-666
SNUBBER
190-279
SCREW
(2 REQ'D)
190-227
SCREW
(2 REQ'D)

616-701
BRACKET

770-991
INSULATOR

190-279
SCREW
(2 REQ'D)

770-990
TERMINAL
BLOCK

193-008
WASHER
(2 REQ'D)

190-282
SCREW
(2 REQ'D)
190-479
SCREW
(2 REQ'D)

616-702
CHASSIS

781-165
RELAY
572-037
GROMMET

193-108
WASHER
(4 REQ'D)
194-059
NUT
(4 REQ'D)
771-986
FILTER

194-056
NUT
(2 REQ'D)

Figure 11-19
616-705 Power Supply Chassis
11-21

CS-200

Illustrations

SCREW
(2-REQ'D)
RETAINER
PLATE
RETAINER
CAP

O-RING
SEAT RING
INNER VALVE
ASSEMBLY PLUG

DIAPHRAGM

REGULATOR
BODY

ADJUSTMENT
NUT

METAL
BAND

SPACER

SCREW
(4-REQ'D)

(2-REQ'D)

SPRING
SPRING
SEAT
SPRING
HOUSING

SCREW
(4-REQ'D)

KNOB

Figure 11-20
773-383 Pressure Regulator

STEM

REGULATOR
BODY

SPRING

VALVE

Figure 11-21
782-839 Pressure Regulator

Illustrations

CS-200

11-22

783-772
PRESSURE
SWITCH

778-523
FITTING

767-866
FITTING
767-866
FITTING

778-246
RESTRICTOR
604-154
FITTING
805-063
TEE BLOCK

Figure 11-22
602-491 Pressure Switch and Restrictor

11-23

CS-200

Illustrations

SCREW
(2-REQ'D)

SCREW
(2-REQ'D)

CAP

WASHER
(2-REQ'D)

ARMATURE

SPRING

HOUSING

SEAL

O-RING
(3-REQ'D)

O-RING
(3-REQ'D)

PIN

SCREW
(2-REQ'D)

Figure 11-23
604-059 Solenoid Valve

VALVE
BODY

O-RING
ARMATURE

SPRING ARMATURE
HOUSING

SPACER

HOUSING
&
COIL

NUT

Figure 11-24
606-649 Solenoid Valve

Illustrations

CS-200

11-24

O-RING

O-RING

STEM

SPACER

HOUSING &
COIL

NUT

Figure 11-25
606-651 Solenoid Valve

NUT

HOUSING
&
COIL

SPACER

STEM
O-RING

O-RING

Figure 11-26
606-652 Solenoid Valve

11-25

CS-200

Illustrations

616-732
VACUUM DOOR
MOUNT
190-174
SCREW
(2-REQ'D)
194-105
NUT
(3-REQ'D)
616-731
BRACKET

789-366
TWIN ROD
CYLINDER

190-174
SCREW
(2-REQ'D)

602-427
TWIN ROD
MOUNT

190-008
SCREW
(3-REQ'D)

773-661
BARB FITTING
(2-REQ'D)

789-367
SENSOR
ASSEMBLY

J203
CONNECTOR

Figure 11-27
616-764 Twin Rod Cylinder

Illustrations

CS-200

11-26

TO
CATALYST HEATER
TOP
TO
CATALYST HEATER
BOTTOM

TO
SV2 FRONT

GAIN

J-152
CONNECTOR

TO
ROTAMETER
BOTTOM

ZERO
ADJUST
GAIN

ZERO
ADJUST

OVEN HEATER CONTROL CARD

J-152A
CONNECTOR

782-067-110
SO2 IR-CELL

NOTE - FOR CS200 AND CS200CH SERIES UNITS

Figure 11-28
CS-200 and CS-200CH Series Oven Tubing Diagram

11-27

CS-200

Illustrations

TO
CATALYST HEATER
TOP

TO
CATALYST HEATER
BOTTOM

782-723-110
CO2 IR CELL

SV2 FRONT

GAIN

ZERO
ADJUST

GAIN

OVEN CARD BRACKET


ZERO
ADJUST

782-067-110
SO2 IR CELL

NOTE - FOR CS200CL SERIES UNITS

Figure 11-29
CS-200CL Series Oven Tubing Diagram

Illustrations

CS-200

11-28

TO
ROTAMETER
BOTTOM

TO SV2

604-080-110
CO2 IR CELL

GAIN

ZERO
ADJUST

OVEN CARD BRACKET


GAIN

NOTE - FOR CS200CSH SERIES UNITS

ZERO
ADJUST

616-706
SO2 IR CELL

Figure 11-30
CS-200CSH Series Oven Tubing Diagram

11-29

CS-200

Illustrations

TO
ROTAMETER
BOTTOM

TO
CATALYST HEATER
TOP
TO
SV2 BOTTOM

GAIN

778-574-120
CO2IR CELL

TO
CATALYST HEATER
BOTTOM

ZERO
ADJUST

OVEN HEATER CONTROL CARD

GAIN

ZERO
ADJUST
616-706
SO2 IR CELL

NOTE - FOR CS200SH SERIES UNITS

Figure 11-31
CS-200SH Series Oven Tubing Diagram

Illustrations

CS-200

11-30

12

Index
12 Index

A
Abort ......................................................................... 556
About the Examples ..................................................... 410
Add a User ................................................................. 472
Add Password ............................................................. 473
After Use, what to do ..................................................... 58
Ambient Monitor.......................................................... 416
Ambient Monitor Definitions ................................... 87, 824
Ambient Monitor Ranges............................................... 825
Ambient Monitor, DSP .................................................... 85
Ambient Monitor, Windows............................................ 822
Ambients.................................................................... 561
Analysis Gas Flow States ............................................ 1012
Analysis Menu Definitions and Ranges ............................ 517
Analysis Method Menu .................................................. 432
Analysis Row .............................................................. 555
Analysis Valve State, Gas Flow Analysis ........................ 1013
Analyze...................................................................... 556
Analyze a Sample ............................................... 525, 568
Analyze Menu ............................................................. 511
Analyze Sequence Diagram ......................................... 1021
Analyze Valve State, Gas Flow Analysis......................... 1012
Anhydrone.............................................................63, 64
Anhydrone Tube ............................................23, 214, 64
ASCII Character Definition Table.................................... 436
Assign User Functions .................................................. 474
Auto Widths................................................................ 560
Autocleaner ......................................................... 312, 66
Autocleaner Assembly .................................................... 67

Index

CS-200

121

Autocleaner Gas Flow States ....................................... 1015


Autocleaner Mesh Filter .................................................. 69
Autocleaner O-rings ..................................................... 610
Automatically Transmit Analysis Results.......................... 444
Average, Statistics....................................................... 544

B
Balance............................................................... 33, 556
Balance Configuration Definitions ................................... 463
Balance Definitions ...................................................... 463
Balance Installation ....................................................... 33
Balance Interfacing ........................................................ 34
Balance Login ............................................................. 566
Balance Options .......................................................... 423
Balance Tab................................................................ 462
Balance Weight ........................................................... 520
Balance Weight, Analyze Menu ...................................... 520
Balance, Resetting the ................................................... 35
Balance, Setting the Data Output Parameter ..................... 35
Barometric (PID) Pressure Regulator Adjustment ............... 93
Barometric Pressure..................................................... 464
Blank ......................................................................... 558
Blank Calibration ......................................................... 575
Blank Samples ............................................................ 510
Blank Samples defined ................................................. 510
Buffer ........................................................................ 587
Buffer, Plot ................................................................. 813
Buffer, Print................................................................ 812

C
Calculate Blank ........................................................... 533
Calculate Calibration .................................................... 530
Calibrate Menu ............................................................ 527
Calibration.................................................................. 574
Calibration Format ....................................................... 528
Calibration Results Format Selection............................... 528
Calibrations ................................................................ 558

122

CS-200

Index

Catalyst Heater Control Card ........................................... 96


Catalyst Heater Tube Packing ........................................ 611
Caution, Operator........................................................ 111
Cellulose Filter ............................................................ 613
Change Password ........................................................ 431
Clean Switch............................................................... 518
Clean Switch without Autocleaner .................................. 519
Clean Switch, Analyze Menu.......................................... 518
Clean Swith with Autocleaner ........................................ 518
Clear Selection ............................................................ 529
Clear Selection, Calibration Menu................................... 529
Clear Selections .......................................................... 541
Clear Selections, Results Menu ...................................... 541
Clipboard Use ............................................................. 588
Combustion Pressure ................................................... 428
Combustion Pressure Adjustment................................... 103
Combustion Pressure Adjustment Knob, Illustration.......... 428
Combustion Tube ........................................................ 615
Combustion Tube Cleaning............................................ 615
Combustion Tube Installation ........................................ 218
Combustion Zone O-Rings ............................................ 616
Comparator ................................................ 434, 455, 78
Comparator Level .......................................................... 78
Components and Accessories List................................... 127
Comport............................................................ 561, 828
Computer Installation................................................... 222
Configuration Menu...................................................... 558
Configure Maintenance Counters.................................... 446
Configure Plot Definitions.............................................. 452
Configure Result Plot.................................................... 589
Configure the Analysis Report........................................ 448
Configure the Screen ................................................... 450
Configure the Spreadsheet............................................ 451
Confirmation............................................................... 414
Controls and Indicators ......................................... 46, 442
Copy................................................................. 554, 588
Index

CS-200

123

Copyright Screen......................................................... 414


Counters .................................................................... 559
Crucible Alignment....................................................... 108
Crucibles ...................................................................... 59
Cut................................................................... 554, 588

D
Data Management ....................................................... 581
Data Transmit ............................................................. 435
Data Transmit Format .................................................. 437
Declaration of Conformity ............................................. 115
Define Delimiters......................................................... 467
Define Fields ............................................................... 465
Defining, Quick Access Menu ......................................... 430
Definitions and Ranges, Analyze Menu ............................ 517
Definitions and Selections, Balance Options ..................... 425
Definitions, Leak Check ................................................ 811
Definitions, Linearization ............................................ 1033
Definitions, Ranges, and Defaults, Analysis Method Menu .. 434
Definitions, Ranges, and Defaults, System Options ........... 420
Definitions, Ranges, and Defaults, Transmit Options ......... 422
Definitions, Statistics ................................................... 544
Delete........................................................................ 557
Delete a Sample .......................................................... 569
Delete Selected Results ................................................ 542
Delete Weight ............................................................. 513
Delete Weight, Analyze Menu ........................................ 513
Delimiters .................................................................. 467
Deskjet (Inkjet) Printer ................................................ 311
Diagnostics for DSP ....................................................... 81
Diagnostics for Windows ............................................... 817
Diagnostics Menu ........................................................ 561
Diagnostics Procedure, DSP ............................................ 84
Diagnostics, Comport ................................................... 828
Diagnostics, Solenoid Valves ......................................... 827
Display ...................................................................... 560

124

CS-200

Index

Dot Matrix Printer .......................................................... 37


Drift .......................................................................... 558
Drift Correction ........................................................... 579
DSP Analyze Menu ....................................................... 511
DSP Diagnostics ............................................................ 81
DSP Operation .............................................................. 51
DSP Screen Description ................................................ 511
DSP Software Upgrade Procedure ................................ 1026
DSP System Setup......................................................... 41
Dust Removal Kit......................................................... 312

E
Edit Blank, Calibration Menu ......................................... 535
Edit Calibration ........................................................... 532
Edit Menu ................................................................... 554
Enter Sample Weight .......................................... 425, 523
Enter Standards .......................................................... 457
Error Messages ......................................................... 1024
Errors ...................................................................... 1024
Exit ........................................................................... 553
Export ....................................................................... 553
Export Buffer .............................................................. 587
Export Sample ............................................................ 584
Export Sample Definitions............................................. 586

F
Facility Requirements ..................................................... 26
Facility Voltage Selection .............................................. 210
Fields......................................................................... 465
File Menu ................................................................... 552
Fill............................................................................. 554
Fill Selected Cells with the Same Values.......................... 582
Filter, Cellulose ........................................................... 613
Filter, Lance Assembly....................................63, 66, 619
First Row.................................................................... 555
Flow Controller Adjustment ........................................... 105
Format Results............................................................ 540

Index

CS-200

125

Furnace Closed 1 Valve State, Gas Flow Analysis............ 1013


Furnace Closed 2 Valve State, Gas Flow Analysis............ 1013
Furnace Closed 3 Valve State, Gas Flow Analysis............ 1013
Furnace Open 1 Valve State, Gas Flow Analysis ............. 1012
Furnace Open 2 Valve State, Gas Flow Analysis ............. 1013
Furnace Open 3 Valve State, Gas Flow Analysis ............. 1013

G
Gas Connections.......................................................... 221
Gas Flow Diagram .............................................. 76, 1017
Gas Flow States ........................................................ 1012
Gas Flow with Autocleaner Diagram ...................... 77, 1018
General Information, Theory of Operation ......................... 73
Gudelines Before an Analysis........................................... 57
Guidelines After an Analysis ............................................ 58
Guidelines for Operation ................................................. 56

H
Hardware Calibration ................................................... 464
Hardware Calibrations .................................................. 560
High Sulfur Samples .................................................... 510

I
Illustrations List ............................................................ 18
Import ....................................................................... 553
Import Sample Data .................................................... 583
Incoming Reagent Tube....................................... 216, 617
Induction Power Control Card Adjustment ......................... 98
Infrared Radiation, Absorption, and Detection.................... 74
Insert ........................................................................ 554
Insert a Sample Out-of-Sequence .................................. 582
Insert Data into the Spreadsheet ................................... 581
Insert Weight.............................................................. 514
Insert Weight, Analyze Menu......................................... 514
Installation of Optional Kits for the Autocleaner................ 312
Instrument Installation................................................... 23
Interference to Other Devices........................................ 114
International Installation ................................................ 27

126

CS-200

Index

IR Cell Adjustment....................................................... 912

K
Keypad ...................................................................... 411

L
Lance and Filter Assembly............................................. 619
Language .......................................................... 471, 560
Last Row .................................................................... 555
Leak Check................................................................. 561
Leak Check Definitions ........................................ 811, 821
Leak Check Gas Flow Diagram..................................... 1019
Leak Check Gas Flow with Autocleaner Diagram............. 1020
Leak Check Procedure, DSP .......................................... 810
Leak Check Procedure, Windows .................................... 819
Linearization with DSP................................................ 1030
Linearization with Windows ......................................... 1032
Linearizations.............................................................. 558
Log File ...................................................................... 562
Log File, View ............................................................. 625
Login ................................................................ 556, 562
Login a Sample ........................................................... 563
Login Periodic Maintenance ........................................... 624
Login using a Sample Template ..................................... 567
Login, Balance ............................................................ 566

M
Main Menu Overview .................................................... 415
Maintenance ................................................................. 63
Maintenance Counters, Reset ........................................ 626
Maintenance Menu....................................................... 562
Maintenance Schedule.................................................... 63
Major Equipment ......................................................... 118
Memory, Reset............................................................ 816
Menu Organization Chart ................................................ 48
Menu,Calibrate DSP ..................................................... 527
Menus............................................................... 410, 552
Mesh Filter, Autocleaner ................................................. 69

Index

CS-200

127

Method ...................................................... 453, 57, 559


Method Development ................................................... 453
Method Parameter Definitions........................................ 455
Methods ..................................................................... 559

N
Notice, Operator.......................................................... 111
Notices .................................................................... 1022
Notices and Errors ....................................................... 413
Notices, Errors, and Warnings ..................................... 1022

O
Operation for DSP.......................................................... 51
Operation for Windows ................................................. 547
Operation Guidelines...................................................... 56
Operation, Quick Access Menu....................................... 429
Optional Equipment ..................................................... 134
Options ...................................................................... 134
O-rings, Autocleaner .................................................... 610
O-rings, Combustion .................................................... 616
Oscillator Tube ............................................................ 212
Oven Heater Control Card Adjustment ............................ 911

P
Packing, Anhydrone Tube ...................................... 214, 64
Packing, Cellulose Filter ................................................ 613
Packing, Incoming Reagent Tube .......................... 216, 617
Paste ................................................................ 554, 588
Pedestal Installation..................................................... 223
Periodic Maintenance Schedule ........................................ 63
Periodic Maintenance, Login .......................................... 624
Pinch Valve Assembly, Illustration .................................. 622
Pinch Valve Tubing ...................................................... 621
Plot Buffer .................................................................. 813
Plot Configuration ........................................................ 589
Points, Statistics.......................................................... 544
Post-Analyze Valve State, Gas Flow Analysis.................. 1014
Power Adjustment, Induction .......................................... 98

128

CS-200

Index

Power-Up ................................................................... 410


Prepare the Sample for Analysis .................................... 510
Preview Transmitted Data ............................................. 469
Print .......................................................................... 552
Print Buffer................................................................. 812
Print Preview .............................................................. 552
Print Sample Results .................................................... 570
Print Selected Results .................................................. 545
Print Setup ................................................................. 552
Print System Parameters .............................................. 815
Print Weights .............................................................. 515
Print Weights, Analyze Menu ......................................... 515
Printer ......................................................................... 37
Printer, Settings .......................................................... 310

Q
Quick Access Menu ...................................................... 429

R
Reagent Tube Screen Filter ........................................... 623
Reagent Tube, Incoming............................................... 617
Recalculate ................................................................. 557
Recalculate Result ....................................................... 573
Recalculate Results, Calibration Menu ............................. 536
Relative Standard Deviation, Statistics............................ 544
Removal, Anhydrone Tube ..................................... 214, 64
Removal, Cellulose Filter .............................................. 613
Removal, Incoming Reagent Tube ......................... 216, 617
Reset......................................................................... 556
Reset Maintenance Counters ......................................... 626
Reset Memory............................................................. 816
Resetting the Balance .................................................... 35
Result Plot Menu ......................................................... 589
Result, Recalculate ...................................................... 573
Results Format Selection .............................................. 540
Results Menu .............................................................. 538
Results, Transmit ........................................................ 572

Index

CS-200

129

S
Safety Pressure Adjustments......................................... 106
Sample ...................................................................... 568
Sample Analysis ................................................. 525, 568
Sample Login .............................................................. 563
Sample Login Definitions .............................................. 565
Sample Preparation ..................................................... 510
Sample Results, Print ................................................... 570
Sample Size................................................................ 510
Sample Template, Login ............................................... 567
Sample Templates .............................................. 456, 559
Sample Weight Entry ................................................... 523
Samples Menu ............................................................ 556
Screen Description, Analyze Menu.................................. 511
Screen Filter ............................................................... 623
Select First Row in the Spreadsheet ............................... 583
Select Language................................................. 471, 560
Select Last Row in the Spreadsheet................................ 583
Select Method ............................................................. 522
Select Method, Analyze Menu ........................................ 522
Select the Analysis Row in the Spreadsheet..................... 583
Serial Port Tab ............................................................ 461
Set Barometer ............................................................ 427
Setting the Data Output Parameter, Balance ..................... 35
Shutdown After Use ....................................................... 58
Software Upgrade Procedure ....................................... 1026
Solenoid Valve Control States...................................... 1016
Solenoid Valve States..................................................... 89
Solenoid Valves, ................................................. 561, 827
Solenoids ................................................................... 561
Specifications.............................................................. 135
Standard Calibration .................................................... 576
Standard Calibration Definitions..................................... 578
Standard Deviation, Statistics........................................ 544
Standards ......................................................... 457, 559

1210

CS-200

Index

Standards Definitions ................................................... 458


Statistics .................................................................... 543
Statistics Definitions .................................................... 544
Statistics, Results Menu................................................ 543
Status Bar ......................................................... 450, 555
Sulfur Samples............................................................ 510
Switch States................................................................ 88
Switches ........................................................... 561, 826
Symbols..................................................................... 112
System ...................................................................... 559
System Check ............................................................. 416
System Clock .............................................................. 426
System Configuration................................................... 459
System Configuration Definitions ................................... 460
System Controls .......................................................... 516
System Controls, Analyze Menu ..................................... 516
System Options........................................................... 419
System Overview ........................................................ 415
System Print ............................................................... 815
System Setup ............................................................. 418
System Setup for DSP .................................................... 41
System Setup for Windows ........................................... 438
System Tab ................................................................ 460

T
Theory of Operation ....................................................... 73
Tool Bar ............................................................ 450, 555
Transmission Formats ......................................... 465, 560
Transmit .................................................................... 557
Transmit Last.............................................................. 521
Transmit Last, Analyze Menu......................................... 521
Transmit Options ......................................................... 421
Transmit Results ......................................................... 572
Transmit Selected Results............................................. 546
Transmitted Data ........................................................ 469
Tubing, Pinch Valve ..................................................... 621

Index

CS-200

1211

U
User Functions ............................................................ 474
User Password ............................................................ 473
Users................................................................ 472, 559
Using the Keypad ........................................................ 412

V
Vacuum Cleaner Kit ..................................................... 312
Valve Control States .................................................. 1016
Valve States ................................................................. 89
Vertical Crucible Alignment ........................................... 108
View Log File ..................................................... 562, 625
View Menu.................................................................. 555

W
Warnings.................................................................. 1023
Warranty.................................................................... 110
Windows Diagnostics.................................................... 817
Windows Operation...................................................... 547
Windows Sample Analysis ............................................. 568
Windows Software Menus ............................................. 552
Windows System Configuration...................................... 459
Windows System Configuration Definitions ...................... 460
Windows System Setup ................................................ 438
Windows Software Upgrade Procedure ........................ 1029
With Autocleaner, Pedestal Installation ........................... 224
Without Autocleaner, Pedestal Installation....................... 223

1212

CS-200

Index

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