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1. Scope
1.1 This test method covers the determination of the degree
of solubility in trichloroethylene of asphalt materials having
little or no mineral matter.
NOTE 1This method is not applicable to tars and their distillation
residues or highly cracked petroleum products. For methods covering tars,
pitches, and other highly cracked petroleum products, and the use of other
solvents, see Test Methods D4, D2318, and D2764.
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
and Paving Materials and is the direct responsibility of Subcommittee D04.47 on
Miscellaneous Asphalt Tests.
Current edition approved June 1, 2009. Published June 2009. Originally
approved in 1966. Last previous edition approved in 2001 as D2042 01. DOI:
10.1520/D2042-09.
2
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contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standards Document Summary page on
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D2042 09
% Soluble 5
C2A
3 100
B
B 2 ~C 2 A!
3 100
B
(1)
(2)
where:
A = mass of crucible and filter,
B = mass of sample, and
C = mass of crucible, filter and insoluble material.
11.2 For percentages of insoluble less than 1.0, report to the
nearest 0.01 %. For percentages of insoluble 1.0 or more,
report to the nearest 0.1 %.
12. Precision
12.1 AASHTO Materials Reference Laboratory (AMRL)
data for Test Method D2042 (and its AASHTO equivalent
standard, T44) were analyzed in 2001 as prescribed in Practice
C670. These data represent approximately 13 200 repetitions
of the test, conducted on 132 samples having solubility values
between 99.5 % and 100.0 %. For samples within this range,
the analysis suggests the following precision values are appropriate:
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D2042 09
Multilab Standard Deviation (1S)
Single-Operator Standard Deviation (1S)
13. Keywords
13.1 asphalt; Gooch crucible; solubility; trichloroethylene
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