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Article history:
Received 29 May 2015
Received in revised form 29 July 2015
Accepted 13 August 2015
Available online 15 August 2015
Keywords:
Shot peening
Quenched and tempered steels
Roughness
Residual stress proles
Full width at half maximum
a b s t r a c t
Shot peening induces important effects on the surface of materials, both positive and negative, the correct
balance between them being the key to success.
Roughness, impact mark size, compressive residual stress and work hardening of six steel grades
obtained from an AISI 4340 steel were studied to explain their evolution according to the Almen intensity
and their mechanical properties. A linear relationship between the impact diameter, the kinetic energy
of the balls and the Almen intensity was found. Moreover, under full coverage, the surface and the maximum compressive stresses only depend on the mechanical properties of the steels, whereas the depth
subjected to high compressive residual stresses and the total depth subjected to compressive residual
stresses depend on the mechanical properties of the steel and the Almen intensity. Furthermore, several
mathematic expressions were formulated to predict the residual stress proles using the Almen intensity
and the mechanical properties of the steels.
2015 Elsevier B.V. All rights reserved.
1. Introduction
Conventional shot peening (SP) is a cheap surface treatment that
consists in projecting very hard, tiny, spherical ceramic or metallic balls (0.3 < < 1.6 mm) at high speed onto the surface of the
component to treat. These impacts produce local surface plastic
deformation, the expansion of which is constrained by the adjacent
deeper material, giving rise to a uniform surface compressive residual stress eld (Fig. 1), along with other important effects. These
include modication of the roughness and appearance of the surface in addition to work hardening, which, if properly controlled,
can signicantly improve the nal properties of metallic components [14]. The aforementioned effects provided by shot peening
treatments cannot be called merely positive or negative, as this role
depends on the purpose of each treatment.
Shot peening has many applications: for instance, it can be used
to improve the fatigue life of industrial components [58], obtain
a specic surface nishing [9], enhance the wear resistance [10] or
prevent stress corrosion cracking [11,12]. Consequently, it is necessary to control the shot peening parameters, mainly the Almen
476
nish modication, surface work hardening and compressive residual stress elds), in different quenched and tempered steel grades
presenting a relatively broad range of mechanical properties submitted to different shot peening intensities. The main objective of
the experimental study was to understand the role played by the
mechanical properties of the treated steel and the applied Almen
intensity on the main effects induced by shot peening treatments.
Furthermore, several simple, practical expressions are proposed to
predict the impact diameter and some characteristic values of the
residual stress proles. These expressions may be used in a practical way to predict the effects induced by shot peening treatments
on industrial components, being an effective tool to select the correct parameters to satisfy the requirements xed by the nal client
in an easy and fast way.
Fig. 1. Schematic illustration of the shot peening process.
Table 1
Chemical composition of AISI 4340 alloy steel.
Element
Mn
Si
Cr
Ni
Fe
wt%
Element
wt%
0.410
Mo
0.235
0.710
V
0.005
0.260
Cu
0.210
0.013
Al
0.016
0.024
Sn
0.011
0.870
Ti
0.004
1.920
Nb
0.003
Balance
Table 2
Hardness and tensile properties of quenched and tempered AISI4340 steel (Vickers hardness, HV, yield strength, ys , ultimate tensile strength, uts , and elongation, E).
Steel
Tempering temperaturea ( C)
HV (31,25 kg)
ys (MPa)
uts (MPa)
E (%)
Q + T200
Q + T425
Q + T540
Q + T590
Q + T650
Q + T680
200
425
540
590
650
680
552
424
350
325
255
226
1604
1364
1123
983
863
626
2057
1426
1201
1123
897
764
10.5
10.6
13.7
14.6
19.3
24.7
477
Table 3
Work parameters for the different shot peening treatments.
Almen intensity (deection of
the Almen strip (A), in mm)
Shot size
(mm)
Pressure
(bar)
Shot Speed
(m/s)
Impact
angle ( )
Stand-off
distance (mm)
nozzle
(mm)
8A (0.2 mm)
10A (0.25 mm)
12A (0.3 mm)
14A (0.35 mm)
16A (0.4 mm)
19A (0.475 mm)
21A (0.52 mm)
CW-0.3
CW-0.4
CW-0.5
CW-0.5
CW-0.7
CW-0.7
CW-0.7
2
2
2
3
1.5
3
4
52.2
53.4
55.1
43.9
49.9
90
240
All the tests were carried out on small slices cut transversely from the bars, with an approximate thickness of 10 mm.
These samples were ground in SiC papers of progressively
lower grit sizes and carefully polished with diamond paste
(6 m and, nally, 1 m) to ensure a soft and homogeneous
initial state (Ra 0.1 m,Rmax 0.2 m, residual stress in the
near-surface region below 200 MPa, and depth affected by the
so-mentioned residual stresses lower than 20 m), thus guaranteeing that all the evaluated effects were only induced by shot
peening.
2.2. Shot peening treatments
Shot peening treatments were carried out by means of a direct
compressed air machine (Guyson Euroblast 4 PF) using conditioned
cut wire shots with rounded off edges (CW, 670-730 HV). Seven
shot peening treatments were designed with Almen intensities ranging between 8A and 21A (0.20.52 mm) following SAE J442 and
SAE J443 specications [29,30] employing A type Almen strips.
In order to achieve this range of Almen intensities, it was necessary to use shots with diameters ranging between 0.3 and 0.7 mm.
The combination of parameters selected in each treatment, including the impact angle, the diameter of the nozzle and the distance
between sample and nozzle, is shown in Table 3. It is important
to remark that both nozzle and samples remained xed during the
whole treatment.
The last step in dening and performing the treatments is the
selection of the exposure time to achieve the required degree of
coverage. Residual stress proles and surface work hardening were
always evaluated in samples with full coverage (100%), but roughness was also studied using different degrees of coverage (25%, 50%,
75%, 100% and 200%). The lower coverage degrees were used to
measure the impact marks.
2.3.2. Roughness
The surface roughness after shot peening was characterized on
a Diavite DH-6 roughness tester by means of the average roughness
Ra and Rmax parameters. The latter parameter is the largest of the
ve Rimax within the assessment length of 4.8 mm, where Rimax is
the maximum peak-to-valley height of the prole in each of the
ve aforementioned measurements [31]. Six different roughness
proles were performed on each sample (three in the longitudinal
direction and another three in the transversal direction) and the
average results were reported.
Table 4
Experimental parameters employed in the X-ray diffraction analysis.
Wavelength K (Cr)
0.2291 nm
Filter
Vanadium
20
9 points between 45/+45
Parabolic
-modied
(2 1 1)
collimator (mm)
Rotation angle, ( )
Fit
Diffraction angle
Elastic constant, E (1 + )1 (GPa)
2
45, 0 y 45
Pseudo-Voigt
156.0
168.9 2.8
478
Table 5
Expressions to predict the compressive residual stress at the surface, src .
(2)
(3)
Mechanical property
Expression
Error
ys
uts
HV
9.9%
6.6%
7.1%
src (MPa)
(1)
Fig. 5. Kinetic energy versus Almen intensity (AI). 14A intensity was provided using
CW0.5 and CW0.6 shots.
479
Fig. 6. Roughness. (a) Evolution of roughness versus the degree of coverage; (b) evolution of Ra and Rmax versus Almen intensity (full coverage).
steel initial hardness was used instead of the surface hardness after
shot peening, but as hardness increases were always below 10%,
results would not change signicantly). The effect of steel hardness on impact size was indirectly shown in Fig. 4, as tempering
temperature is inversely related to the hardness of the steel.
3.2. Residual stresses
Every compressive residual stress prole can be well characterized using four parameters [39,41,42]: the compressive residual
stress at the surface, src ; the maximum value of the compressive
Fig. 7. Evolution of the roughness parameters, Ra and Rmax , versus steel hardness. SP14A and full coverage.
480
Mechanical property
Expression
Error
ys
uts
HV
rc
max
= 0.67 ys [Eq. (7)]
rc
max
= 0.58 uts [Eq. (8)]
rc
max
= 2 HV [Eq. (9)]
9.7%
4.5%
6.1%
Table 7
Expressions to predict the total depth of the compressive residual stresses, Z0 .
Z0 (mm)
rc
residual stress, max
(usually located at a certain depth under
the surface); the total depth submitted to compressive residual
stresses, Z0 ; and the depth subjected to high compressive residual stresses, Zhc . This last parameter was dened in this study as
the depth at which the compressive residual stress is at least half
the yield strength of the steel. These parameters are represented in
Fig. 8 over a typical residual stress prole induced by shot peening.
Fig. 9 shows the residual stress proles produced by two
given shot peening treatments (10A and 16A) on the different
steel grades: surface and maximum compressive residual stresses
decrease with decreasing strength of the steel (higher tempering temperature) [22,39,40]. However, the total depth of the
compressive residual stresses and the depth subjected to high compressive residual stresses increase with decreasing strength of the
steel.
In addition, all the residual stress proles obtained in our experimental measurements onto the Q + T steels under the different
Almen intensities (full coverage) are shown in Fig. 10. According
to this last gure, compressive residual stresses (surface and maximum) barely depend on the applied Almen intensity. However,
the affected depths (total depth submitted to compressive stresses
and depth subjected to high compressive residual stresses) increase
with increasing Almen intensity, as previously reported by other
authors [22,43,44].
As well as other authors [4548], we have formulated different simple and practical expressions to predict these parameters
making use only of the applied Almen intensity (mmA) and one of
the main mechanical properties of the treated steel (yield strength,
ultimate tensile strength or hardness). The expressions shown in
Tables 58, Eqs. (4)(15), were obtained along with their average error through lineal regressions and statistical analysis and
Mechanical property
Expression
Error
ys
uts
HV
6.6%
6.7%
5.8%
Table 8
Expressions to predict the depth subjected to high compressive residual stresses,
Zhc . ( c > ys /2).
Zhc (mm)
Mechanical property
Expression
Error
ys
uts
HV
7.8%
10.9%
5.6%
combine precision (error < 10%; in the best cases around 5%) with
simplicity.
The best mechanical parameter for predicting residual compressive stresses is seen to be tensile strength, though hardness
is the best for predicting affected depths. Fig. 11 compares the predicted surface and maximum compressive stresses produced by
shot peening with the experimental results, while Fig. 12 compares
the predicted depths with their experimentally measured values.
Good correlations have been found with the four parameters.
3.3. Work hardening. FWHM proles
As previously stated, the shot peening work hardening study
was carried out employing the FWHM parameter, the proles of
which were obtained by XRD at the same time as those corresponding to the residual stress. Moreover, this parameter was shown to be
a useful and practical tool to evaluate the surface work hardening
induced by shot peening treatments.
Fig. 13 shows that the steel surface layer affected by shot peening becomes deeper as the applied Almen intensity increases, and
covers a similar depth to that subjected to the compressive residual
Fig. 9. Residual stress proles following different SP treatments on diverse steels. Two applied Almen intensities, 10A and 16A, full coverage.
Fig. 10. Residual stress proles obtained by applying different SP treatments to the different Q + T steels (full coverage).
Fig. 11. Predicted compressive residual stress vs experimental results (full coverage) a) at the surface; b) maximum value.
481
482
Fig. 12. Predicted depths vs experimental results (full coverage) (a) total depth subjected to compressive residual stresses; (b) depth subjected to high compressive residual
stresses.
Fig. 13. FWHM proles following different SP treatments applied to the studied steel grades (full coverage).
483
Table 9
Predicted results from an average impact diameter of 179 m (Q + T540 4340 steel).
Z0 = 0.26 mm
rc
max
= 697 MPa
ys
2
= 562 MPa
Fig. 14. FWHM proles obtained on different steel grades using a 14A SP (full coverage). *Q corresponds to the quenched and non-tempered 4340 steel.
Fig. 16. Experimentally measured residual stress prole and predicted values
(Q + T540 4340 steel, SP12A and full coverage).
Fig. 15. Evolution of the FWHM. The greatest hardness represented in the graphs (662 HV) corresponds to the quenched and non-tempered 4340 steel. (a) The base FWHM
parameter; (b) the surface FWHM minus the base FWHM versus steel hardness (full coverage).
484
4. Conclusions
It is well-known that shot peening is a complex technology
which produces different effects on the surface of the treated components, the most important being the modication of surface
appearance, work hardening and residual stresses. The most relevant results obtained using an AISI 4340 steel submitted to different
quenched and tempered heat treatments in order to obtain a wide
range of mechanical properties are reported below.
Impact marks: as impact diameter is a direct measure of the
intensity of any shot peening treatment, there is a linear relationship between the diameter of the surface impact marks and the
applied Almen intensity. A simple, accurate expression is proposed
to predict the impact diameter, which increases with increasing
Almen intensity and with decreasing steel hardness.
Kinetic energy: the kinetic energy of the projected balls is partially transferred to the specimen surface and, consequently, Almen
intensity and the kinetic energy of the shots are also linearly related.
Roughness: the analysis of surface roughness through Ra and
Rmax conrmed that both parameters evolve in the same way. For
the same material, roughness increases with increasing applied
Almen intensity (larger impact marks). However, the size of the
shots also plays an important role: roughness decreases with
increasing shot size, even when a higher Almen intensity is produced. Moreover, roughness depends on the degree of coverage,
increasing until full coverage and subsequently remaining constant, due to the saturation of surface work hardening.
Residual stress proles: any compressive residual stress prole
is well dened using four parameters: the compressive residual
stress at the surface, src ; the maximum compressive residual stress,
rc ; the depth subjected to high compressive residual stresses,
max
Zhc ; and the total depth subjected to compressive residual stresses,
rc
Z0 . It was conrmed that, under full coverage, src and max
only
depend on the mechanical properties of the treated steel (they do
not depend on the applied Almen intensity, as surface hardening
saturates after attaining full coverage), whereas, Z0 and Zhc depend
on both the mechanical properties of the steel and the applied
Almen intensity. Several simple, accurate, practical expressions
were formulated to predict these four parameters in quenched and
tempered 4340 steel grades which only require the applied Almen
intensity (mmA) and one of the main mechanical properties of the
treated steel as input.
Work hardening: shot peening also induces an increase of the
hardness of the surface region which can be easily quantied by
means of the FWHM parameter. It was seen that the base FWHM
of the steel, being a hardening parameter, is linearly related to its
hardness. On the other hand, from the study of the surface evolution
of this parameter, it can be stated that softer steels have a greater
work-hardening capacity, although some kind of softening was also
observed in the harder steels unduly associated with dislocation
re-arrangement.
Acknowledgements
The authors are grateful for the nancial support for this study
provided by the European Union (FEDER funds) and Principado
de Asturias, through the Plan de Ciencia, Tecnologa e Innovacion,
20132017 (FC-15-GRUPIN14-001 Project). Vctor Llaneza grateful
acknowledges funding from the Principado de Asturias Government, through the Severo Ochoa Programme (contract BP10-021).
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