APPENDIX 1

MICROFINE CEMENT GROUT TESTING RESULTS

218

Table A1-1 Microfine Cement Grout Mix Designs

Mix

Dispersant
(% BWOC)

Bentonite
(% BWOC)

1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5
1.5

SetRetarder
(% BWOC)
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10

3
3
3
2
1
1
1.5
1.5
0.5
0.5
1
1

Welan
Gum
(% BWOC)
0.01
0.05
0.1
0.1
0.05
0.05
0.05
0.05
0.01
0.05
0.1
0.05
0.1
0.1
0.05

1-1000
2-1000
3-1000
4-1000
5-1000
6-1000
7-1000
8-1000
9-1000
10-1000
11-1000
12-1000
13-1000
14-1000
15-1000
16-1000
17-1000
18-1000
19-1000, 20%
slag cement
20-1000, 80%
slag cement
1-2000
2-2000
3-2000
1-1002-NS
2-1002-NS
2-1002-D25
2-1002-D10
3-1002-NS
Ultrafine cement
4-1002-NS
4-1002-D25
4-1002-D10
5-1002-NS
Ultrafine cement
5-1002-D25
Ultrafine cement
5-1002-D10
Ultrafine cement

1.5

10

0.1

1.5
1.5
1.5
2
2
2
2
2

10
10
10
2.5
10
-

1
1
2
2
2
2

0.05
0.1
0.025
0.025
0.025
-

2
2
2
2

2.5
10
-

1.5
1.5
1.5
1.5

0.025
0.025
0.025
0.025

2.5

1.5

0.025

10

1.5

0.025

219

Silica Fume
(% BWOC)
5
5
5
5
5
-

Mix

Dispersant
(% BWOC)

6-1002-D10
7-1002-D10
8-1002-D10
Ultrafine cement
9-1002-D25
9-1002-D10
10-1002-D25
10-1002-D10
11-1002-D10
Ultrafine cement
1-1002-D25
1-1002-D5
1-1002-D75
1-1002-D10

2
2
2
2
2
2
2
1.5 Disal,
0.5 RB1000
2
2
2
2

SetRetarder
(% BWOC)
10
10
10

Bentonite
(% BWOC)

Silica Fume
(% BWOC)

1.5
1.5
1.5

Welan
Gum
(% BWOC)
0.15
0.1
0.1

2.5
10
2.5
10
10

2
2
2
2
2

0.1
0.1
0.05
0.05
0.05

2.5
5
7.5
10

220

TABLE A1-2 MICROFINE CEMENT GROUT TESTING RESULTS

Mix

1-1000

Date

6/1/99
6/2/99

6/3/99
6/4/99
6/5/99
6/6/99
6/7/99
6/9/99
6/10/99
6/11/99
6/15/99
6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/28/99
7/2/99
7/8/99
7/12/99

2-1000

6/2/99
6/3/99
6/4/99
6/5/99
6/6/99

3-1000

6/2/99
6/3/99
6/4/99
6/5/99
6/6/99

4-1000

6/4/99

6/5/99
6/6/99

Time

Time
(hours)

Bleed
(%)

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

0
18
37
38
40
41
42
42
42
43
43
43
43
43

29

Wet
Lombardi #
Density
(g/cc)

Viscosity
cP

Ingredients

17:00
19:00
10:30
11:40
17:50
9:30
9:30
19:30
9:30
17:00
11:30
20:17
9:00
20:30
10:00
11:45
16:00
15:00
11:00
11:00
2:00
12:00
15:30
13:30
22:30
20:30
10:00
14:00
15:00
14:00
14:00
14:00
16:00

0
2
17.5
18.5
25
40.5
64.5
74.5
88.5
96
114.5
123.25
136
147.5
185
186.75
215
238
330
354
369
379
382.5
404.5
437.5
459.5
473
525
550
645
765
990
1000

43
43
43
43
43
43
43
43
43
43
43

16:00
18:00
9:00
9:00
20:00
10:00
16:00
11:30
20:15

0
2
17
41
52
66
72
91.5
100.25

0
1
3
10
10
12
13
13
14

0.11

17:00
19:00
9:00
20:00
10:00
16:00
11:30
20:15

0
2
16
51
65
71
90.5
99.5

0
1
2
5
7
8
9
9

0.106

57

0.089

60
57

0.764
0.515

3.10E-06
3.10E-06

39 Bentonite - 3%
39 Silica fume - 5%

53

0.5

2.90E-06

36

50

0.563

2.60E-06

32

13:00
15:00
19:45
11:30
20:30
11:30

0
2
6.75
21
27
46.5

0
5
11
18
20
25

0.081

29

0.062

35

0.155

43
43
43
43
43
43

0.14

Cohesion
(mm)

1.27

Base mix:
w/c = 2
Rheobuild 1000 - 1.5%
Delvo - 10%
0 MBT Microfine cement

30
29
28

0.042

4.10E-07

29

0.045

5.50E-07

30

0.054

7.60E-07

0.206

30

0.059

7.50E-07

0.207

29
29
30

0.051
0.061
0.059

5.50E-07
5.40E-07
7.50E-07

7
7
9

30

0.06

7.50E-07

29

0.061

5.40E-07

29
29
29
29
30
28
29

0.065
0.0496
0.055
0.0626
0.063
0.052
0.0598

5.40E-07
5.50E-07
5.40E-07
5.40E-07
7.50E-07
4.10E-07
5.40E-07

7
7
7
7
9
5
7

39

1.27

Base mix plus

44

0.457

2.10E-06

26 Bentonite - 3%

40

0.403

1.70E-06

21

41

0.253

1.90E-06

24

41

0.207

1.95E-06

24

1.27

1.27

Base mix plus

5.60E-07

7 Base mix plus

Silica fume - 5%

221

1.40E-06

17

Mix

5-1000

Date

6/4/99

6/5/99
6/6/99

6-1000

6/4/99
6/5/99
6/6/99
6/7/99
6/9/99

7-1000

6/3/99
6/4/99
6/5/99

6/6/99
6/7/99

8-1000

6/3/99
6/4/99
6/5/99

6/6/99
6/7/99
6/9/99
6/10/99
6/11/99
6/15/99
6/16/99

9-1000

6/4/99
6/5/99
6/6/99
6/7/99

10-1000

6/5/99
6/6/99
6/7/99
6/9/99
6/10/99
6/11/99

Time

Time
(hours)

Bleed
(%)

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

14:00
16:00
20:00
10:00
16:00
11:30
20:45

0
2
6
20
26
45.5
54.75

0
8
18
20
20
25
27

0.103

18:15
20:15
10:00
16:00
11:30
20:30
9:00
20:30
11:45

0
2
27.5
33.5
53
62
74.5
86
125.25

0
6
16
16
16

0.084

14:00
16:00
19:45
10:00
16:00
17:45
11:45
21:00
9:00

0
2
29.75
44
50
51.75
69.75
79
91

15:00
17:00
19:45
10:00
16:00
17:45
11:00
21:00
9:00
20:30
11:45
17:00
16:00
11:00
11:00

0
2
29
41
47
49
67
77
89
100.5
139.75
168.5
191.5
282.5
306.5

9
10
10
11
12
13
13
13
13

19:00
21:00
10:00
18:00
11:45
21:15
9:00

0
2
15
21
40.75
50.25
62

0
8
30
33
35
37
37

0.124

11:30
13:30
11:45
21:30
9:00
20:30
11:45
16:00
15:00

0
2
24.25
34
45.5
57
96.25
124
147

0
1
2
2
3
3
10
10
10

0.093

1.27

4.10E-07

Viscosity
cP

Ingredients

5 Base mix plus

35

0.173

1.40E-06

17

33

0.104

1.10E-06

14

29

0.06

37

0.154

1.60E-06

Silica fume - 5%
20 Welan gum - 0.05 %

34

0.12

1.20E-06

15

34

0.12

1.20E-06

15

28

1.28

5.60E-07

7 Base mix plus

1.28

Base mix plus

31

36
36
36

0
0
4
5
6

0.062

Wet
Lombardi #
Density
(g/cc)

Silica fume - 5%
Welan gum 0.01%

23
23
23

0
8
30
33
35

28

Cohesion
(mm)

0.082

Welan gum - 0.1%

31

0.069

8.40E-07

11

31

0.078

8.30E-07

10

48

1.27

Base mix plus

58

0.562

3.10E-06

39 Bentonite - 3%
Welan gum - 0.1%

47

0.43

2.20E-06

27

48

0.48

2.25E-06

28

28

0.04

32

0.084

9.60E-07

12

31

0.085

8.40E-07

10

0.074

39

0.368

1.60E-06

20 Base mix plus

0.097

51
42

0.528
0.393

2.80E-06
1.90E-06

Bentonite - 3%
35 Welan gum - 0.05%
24

44
41
39

0.366
0.279
0.259

2.05E-06
1.90E-06
1.70E-06

26
24
21

1.27

4.10E-07

5 Base mix plus

Welan gum - 0.05%

0.115

222

1.27

Mix

Date

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/28/99

11-1000

6/5/99
6/6/99
6/7/99
6/9/99
6/10/99
6/11/99
6/15/99
6/16/99
6/17/99

12-1000

6/5/99
6/6/99
6/7/99
6/9/99
6/10/99
6/11/99
6/15/99
6/16/99

13-1000

6/5/99
6/6/99
6/7/99
6/9/99

14-1000

6/6/99
6/7/99
6/9/99
6/10/99
6/11/99
6/15/99
6/16/99
6/17/99

6/18/99
6/19/99
6/20/99

Time

Time
(hours)

Bleed
(%)

12:00
15:30
13:30
22:30
20:30
10:00
14:00
15:00
14:00

289.5
293
315
348
370
383.5
435.5
460.5
555.5

12:30
14:30
11:45
10:00
9:00
20:30
11:45
15:00
16:00
15:00
11:00
11:00
12:30

0
2
23.5
33.5
44.5
56
95.25
98.5
123.5
146.5
238.5
262.5
288

14:30
16:30
11:45
22:00
9:00
20:30
11:45
15:15
16:00
15:00
11:00
11:00

0
2
21.75
31.5
42.5
54
93.25
96.75
121.5
144.5
164.5
188.5

17
17
18
18

15:00
15:00
11:45
22:00
9:00
20:30
11:45
16:00

0
2
20.75
31
42
58.5
92.75
97

13:00
15:00
9:00
20:30
11:45
16:00
16:00
15:00
11:00
11:00
2:00
12:30
15:30
13:30
22:30
20:30

0
2
20
31.5
71
75
99
123
215
239
254
264.5
267.5
289.5
322.5
344.5

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

11
11
11
11
12
12
12
12

0
1
5
5
6
7
15

Cohesion
(mm)

Wet
Lombardi #
Density
(g/cc)

Viscosity
cP

Ingredients

38

0.154

1.70E-06

21

37

0.15

1.60E-06

20

37
0.137
37
0.133
37
0.121
not enough grout

1.60E-06
1.60E-06
1.60E-06

20
20
20

1.15E-06

14 Base mix plus

0.059

34

0.214

0.111

39
36

0.289
0.179

1.65E-06
1.50E-06

Bentonite - 1%
20 Welan gum - 0.05%
18

37
36
35
34

0.202
0.173
0.164
0.108

1.55E-06
1.50E-06
1.40E-06
1.20E-06

19
18
17
15

34

0.111

1.20E-06

15

0.073

35

0.234

1.30E-06

16 Base mix plus

0.116

40
37

0.356
0.248

1.70E-06
1.50E-06

Bentonite - 1%
21 Welan gum - 0.05%
19 Silica fume - 5%

0.115

37
37
35
34

0.236
0.178
0.16
0.097

1.50E-06
1.55E-06
1.40E-06
1.20E-06

19
19
17
15

0
2
33
33
33
34
35
35

0.148

29

0.056

33

0.084

0
1
3
4
10
11
14
14
15
15
15

0.085

35

0.226

0.1

39

0.122

0.146
16
16
16
16

0
1
7
7
8
10
17

15
15
15
15

0.198

1.25

1.26

1.27

5.70E-07

7 Base mix plus

Welan gum - 0.01%

0.194

1.10E-06

14

1.30E-06

16 Base mix plus

0.259

1.80E-06

22 Bentonite - 1.5%
Welan gum - 0.05%

40
39
36
35

0.302
0.244
0.183
0.118

1.80E-06
1.70E-06
1.50E-06
1.45E-06

22
21
19
18

34

0.086

1.20E-06

15

33

0.11

1.10E-06

14

223

1.26

Mix

15-1000

Date

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

530
650
794
892

15
15
15
15

6/6/99

16:45
18:45
9:00
20:30
11:45
16:00
16:00
15:00
11:00
11:00
2:00
12:30
15:30
13:30
22:30
20:30
10:00
14:00
15:00
14:00
14:00
14:00
16:00

0
2
16
27.5
67
71
95
118
210
234
249
259.5
262.5
281.5
314.5
336.5
350
402
427
522
642
786
884

0
1
2
3
4
7
11
12
12
13
13
13
13
13
13
13
13
13
13
13
13
13

0.194

17:30
19:30
9:00
11:00
20:30
12:00
16:00
16:00
15:00
11:00
11:00

0
2
17.5

0
5
20

29
66.5
70.5
94.5
118.5
210.5
234.5

20
25
26
28
28
28
28

18:15
20:15
9:00
20:30
12:00
16:00
16:00
15:00
11:00

0
2
14.75
26.25
65.5
69.5
93.5
117.5
209.5

10:00
15:00
20:00
11:45
16:00
16:00
15:00
11:00
11:00
2:00
12:30

0
5
10
26
30
54
77
169
193
208
218.5

6/10/99
6/11/99
6/15/99
6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/28/99
7/2/99
7/8/99
7/12/99

6/6/99
6/7/99

6/9/99
6/10/99
6/11/99
6/15/99
6/16/99

6/6/99
6/7/99
6/9/99
6/10/99
6/11/99
6/15/99

18-1000

Bleed
(%)

14:00
14:00
14:00
16:00

6/7/99

17-1000

Time
(hours)

6/28/99
7/2/99
7/8/99
7/12/99

6/9/99

16-1000

Time

6/8/99

6/9/99
6/10/99
6/11/99
6/15/99
6/16/99
6/17/99

Cohesion
(mm)

32
33
33
33

0.113
0.104
0.113
0.101

0.062

37

0.336

0.097

44

0.112

Wet
Lombardi #
Density
(g/cc)

Viscosity
cP

Ingredients

9.50E-07
1.10E-06
1.10E-06
1.10E-06

12
14
14
14

1.65E-06

20 Base mix plus

0.378

2.05E-06

25 Bentonite - 1.5%
Welan gum - 0.1%

42
41
37
36

0.315
0.299
0.178
0.156

1.90E-06
1.90E-06
1.55E-06
1.50E-06

23
23
19
19

35

0.117

1.40E-06

17

34

0.134

1.20E-06

15

33
33
32
32
32
32
32

0.125
0.0913
0.145
0.11
0.112
0.117
0.112

1.10E-06
1.10E-06
9.00E-07
9.50E-07
9.50E-07
9.50E-07
9.50E-07

14
14
11
12
12
12
12

0.083

31

0.09

8.30E-07

10 Base mix plus

0.13

35

0.124

1.45E-06

18 Bentonite - 0.5%
Welan gum - 0.05%

0.155

34

0.142

1.20E-06

15

0
2
12
12
19
20
22
22
22

0.069

31

0.106

8.30E-07

10 Base mix plus

0.13

37

0.101

1.65E-06

20 Bentonite - 0.5%
Welan gum - 0.1%

0.158

35
35
34
33

0.116
0.157
0.106
0.11

1.45E-06
1.40E-06
1.20E-06
1.10E-06

18
17
15
14

0
2
3
6
6
7
13
17
17
17

0.073

33

0.172

1.05E-06

13 Base mix plus

0.112

40
39
36
35

0.215
0.192
0.17
0.172

1.85E-06
1.75E-06
1.50E-06
1.40E-06

23
22
19
17

34

0.15

1.20E-06

15

1.26

1.25

1.26

1.27

Bentonite - 1%
Welan gum - 0.1%

224

Mix

19-1000

Date

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

298.5
312
484
604
748
846

18
18
18
18
18
18

6/8/99

11:00
15:00
20:00
12:00
16:00
16:00
15:00
11:00

0
4
9
25
29
53
76
168

0
34
34
34
34
35
35
35

0.081

20:00
21:30
12:00
16:00
17:00
16:00
15:00
11:00

0
1.5
16
20
21
44
67
159

0
8
22
22

0.059

18:00
20:00
21:30
22:30
12:00
17:30
16:00
15:00
11:00
11:00
2:00
12:45
15:30
9:15
22:30
20:30
10:00
14:00
15:00
14:00
14:00
14:00
16:00

0
2
3.5
5
18
23.25
46
69
161
185
200
210.75
213.5
231.25
268.5
290.5
304
356
381
476
596
740
838

19:00
21:00
12:00
16:00
15:00
11:00
11:00
2:00
12:45
15:30
9:30
22:30
20:30

0
2
17
45
68
160
184
199
209.75
212.5
230.5
267.5
289.5

6/8/99
6/9/99

6/10/99
6/11/99
6/15/99

6/8/99

6/9/99
6/10/99
6/11/99
6/15/99
6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/28/99
7/2/99
7/8/99
7/12/99

2-2000

Bleed
(%)

20:30
10:00
14:00
14:00
14:00
16:00

6/10/99
6/11/99
6/15/99

1-2000

Time
(hours)

6/20/99
6/21/99
6/28/99
7/2/99
7/8/99
7/12/99

6/9/99

20-1000

Time

6/8/99
6/9/99
6/10/99
6/11/99
6/15/99
6/16/99
6/17/99

6/18/99
6/19/99
6/20/99

33
34
34
35
35
35
35
35
35
35
35
35
35
35
35
35

0
1
8
9
12
18
19
19
19
19
19
19

33
31
31
31
32

0.13
0.107
0.107
0.0996
0.109

29

0.062

35

0.164

30

0.045

0.097

40
40
39
39

0.317
0.359
0.226
0.22

0.167

28

0.054

22
22
23

0
17
21
24
32

Cohesion
(mm)

0.189

0.207

0.072

0.174

Wet
Lombardi #
Density
(g/cc)

1.10E-06
8.30E-07
8.30E-07
8.30E-07
9.50E-07

1.27

5.50E-07

1.40E-06

1.27

7.50E-07

1.75E-06
1.70E-06
1.75E-06
1.75E-06

1.26

4.10E-07

Viscosity
cP

Ingredients

14
10
10
10
12

7 Base mix plus

Bentonite - 1%
Welan gum - 0.05%
17 Microfine - 80%
Slag - 20%

9 Base mix plus

Bentonite - 2%
Welan gum - 0.1%
22 Microfine - 80%
21 Slag - 20%
22
22

5 Base mix
w/c = 2
Rheobuild 2000 - 1.5%
Delvo - 10%
12 MBT Microfine cement
10
10
9

32
31
31
30

0.0984
0.104
0.0921
0.0615

9.50E-07
8.30E-07
8.30E-07
7.50E-07

30

0.0579

7.50E-07

30

0.079

7.40E-07

30

0.064

7.50E-07

29
29
28
29
29

0.0746
0.0575
0.05
0.0607
0.0504

5.50E-07
5.60E-07
4.10E-07
5.60E-07
5.60E-07

7
7
0
0
7

32

0.127

42
38
37
37

9.50E-07

12 Base mix plus

0.316
0.286
0.208
0.158

1.95E-06
1.60E-06
1.55E-06
1.60E-06

24 Bentonite - 1%
20 Welan gum - 0.05%
19
20

35

0.158

1.40E-06

18

34

0.125

1.20E-06

15

225

1.28

Mix

3-2000

Date

19
19
19
19

6/8/99

20:30
22:30
12:00
16:00
15:00
11:00
11:00
2:00
15:30
9:30
22:30
20:30
10:00
14:00
15:00
14:00
14:00
14:00
16:00

0
2
15.5
43.5
66.5
158.5
182.5
197.5
211
229
266
288
301.5
353.5
378.5
473.5
593.5
737.5
835.5

0
0
3
4
5
16
17
17
17
17
17
17
17
17
18
18
18
18
18

0.058

18:30
20:30
11:00
2:00
10:00
14:45

0
2
16.5
31.5
39.5
68.25

0
4
12
13

0.073

19:30
21:30
11:00
2:00
10:00
14:45

0
2
16.5
31.5
39.5
68.25

0
2
9
13

19:30
21:30
8:30
13:00
14:45

0
2
13
41.5
67.25

0
2

20:00
22:00
11:00
2:00
10:00
14:45

0
2
15
30
38
61.25

0
3
9
10

0
2
12
37.5
66.25

0
1

6/16/99
6/17/99
6/18/99

20:30
22:30
8:30
10:00
14:45

6/16/99

13:45

6/15/99

6/18/99

6/15/99
6/16/99
6/17/99
6/18/99

6/15/99
6/16/99
6/17/99
6/18/99

4-1002-NS

6/15/99
6/16/99
6/17/99
6/18/99

5-1002-NS

4-1002-D2.5

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

475
595
739
837

6/16/99
6/17/99

3-1002-NS

Bleed
(%)

14:00
14:00
14:00
16:00

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/28/99
7/2/99
7/8/99
7/12/99

2-1002-NS

Time
(hours)

6/28/99
7/2/99
7/8/99
7/12/99

6/9/99
6/10/99
6/11/99
6/15/99
6/16/99
6/17/99

1-1002-NS

Time

6/15/99

0.19

Cohesion
(mm)

33
32
32
32

0.0898
0.106
0.121
0.12

34

0.194

48
45
40
42

Wet
Lombardi #
Density
(g/cc)

Viscosity
cP

1.17E-06
9.50E-07
9.40E-07
9.40E-07

15
12
12
12

1.22E-06

15 Base mix plus

0.389
0.333
0.242
0.32

2.40E-06
2.20E-06
1.80E-06
1.95E-06

30 Bentonite - 1%
27 Welan gum - 0.1%
22
24

38
37

0.22
0.204

1.60E-06
1.65E-06

20
21

35

0.201

1.35E-06

17

34
34
33
34
33

0.156
0.176
0.144
0.149
0.154

1.20E-06
1.18E-06
1.05E-06
1.20E-06
1.05E-06

15
15
13
15
13

27

0.047

1.27

1.26

2.90E-07

4 Base mix with no Delvo

gelled
4.5+ tsf

0.077

Ingredients

29

0.059

1.27

5.60E-07

w/c = 2
Rheobuild 1000 - 2.0%
MBT Microfine cement

7 Base mix with no Delvo, plus

Bentonite - 2%
Welan gum - 0.025%
gelled
4.5+ tsf

0.153

31

0.135

1.27

8.10E-07

10 Base mix with no Delvo, plus

set <13 hrs Bentonite - 2%
1 tsf
Welan gum - 0.025%
4.5 bottom, U.S. Grout premium ultrafine
instead of MBT cement

0.077

29

0.06

1.3

5.60E-07

7 Base mix with no Delvo, plus

Bentonite - 1.5%
Welan gum - 0.025%
gelled
4.5+ tsf

0.133

32

0.156

1.26

9.30E-07

11 Base mix with no Delvo, plus

set <12 hrs Bentonite - 1.5%
1 tsf
Welan gum - 0.025%
4.5 bottom, U.S. Grout premium ultrafine
instead of MBT cement

0.0798

30

0.1

226

1.27

7.10E-07

9 Base mix plus

Mix

6-1002-D10

Date

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

481
547
644

6/16/99

16:15
18:15
2:00
14:00
15:30
10:30
22:30
20:30
10:30
14:00
15:00
11:30
16:00
10:00
14:00

0
2
11.75
23.75
25.25
44.25
80.25
102.25
116.25
164.75
193.75
215.25
289.75
331.75
383.75

16:30
18:30
2:00
14:15
15:30
10:30
22:30
20:30
10:30
14:00
15:00
11:30
16:00
16:00
10:00
14:00
16:00
10:00
11:00

0
2
10
22.25
23.5
42.5
78.5
100.5
114.5
163
192
213.5
288
312
330
382
480
546
643

17:00
19:00
2:00
14:15
15:30
10:30
22:30
20:30
10:30
14:00
15:00
11:30
16:00
16:00
10:00
14:00
16:00
10:00
11:00

0
2
9
21.25
22.5
41.5
77.5
99.5
113.5
162
191
212.5
287
311
329
381
479
545
642

10

19:30
21:30

0
2

0
1

6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/25/99
6/28/99
6/29/99
6/30/99
7/2/99
7/6/99
7/9/99
7/13/99

6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/25/99
6/28/99
6/29/99
6/30/99
7/2/99
7/6/99
7/9/99
7/13/99

2-1002-D2.5

Bleed
(%)

16:00
10:00
11:00

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/25/99
6/28/99
6/30/99
7/2/99

8-1002-D10

Time
(hours)

7/6/99
7/9/99
7/13/99

6/17/99

7-1002-D10

Time

6/16/99

16

41
43
43

0.425
0.584
0.518

0.047

39

0.346

0.196

59
50
46

16

0
0
1
1
2
3
6
8
12
12
12
13
13

0
1
1
2
3
7
10
12
13
13
13
13

0.06

Viscosity
cP

Ingredients

1.75E-06
1.80E-06
1.85E-06

21
22
23

1.60E-06

20 Base mix plus

0.612
0.454
0.323

3.20E-06
2.70E-06
2.30E-06

Bentonite - 1.5%
Welan gum - 0.15%
40 Delvo - 10%
33
28

41
39
37
38
38
36
35

0.223
0.272
0.186
0.143
0.223
0.153
0.15

1.95E-06
1.70E-06
1.60E-06
1.70E-06
1.60E-06
1.50E-06
1.40E-06

24
21
20
21
20
19
17

35

0.299

1.20E-06

15 Base mix plus

1.26

1.26

55
47
41

0.592
0.414
0.309

2.90E-06
2.30E-06
1.90E-06

0.198

40
39
36
35
33
34
34
33
33
32
33

0.339
0.247
0.222
0.158
0.115
0.142
0.1
0.116
0.114
0.109
0.106

1.75E-06
1.70E-06
1.40E-06
1.40E-06
1.10E-06
1.20E-06
1.25E-06
1.10E-06
1.10E-06
9.50E-07
1.10E-06

22
21
17
17
14
15
15
14
14
12
14

0.0458

32

0.125

9.50E-07

12 Base mix plus

0.19

14
14

2
3
3
3
4
5
6
7
8

Wet
Lombardi #
Density
(g/cc)

Bentonite - 1.5%
Welan gum - 0.1%
36 Delvo - 10%
28
23

13

0
0
1

Cohesion
(mm)

1.25

39
42
43

0.117
0.252
0.269

1.85E-06
2.00E-06
2.05E-06

Bentonite - 1.5%
Welan gum - 0.1%
23 Delvo - 10%
25 U.S. Grout premium ultrafine
25 instead of MBT cement

0.108

42
43
43
43
44
43
46
50
48
51
51

0.108
0.281
0.18
0.228
0.31
0.366
0.436
0.577
0.518
0.604
0.582

2.10E-06
2.05E-06
2.10E-06
2.05E-06
2.05E-06
2.00E-06
2.15E-06
2.40E-06
2.30E-06
2.50E-06
2.50E-06

26
25
26
25
25
25
26
29
28
31
31

0.0956

33

0.173

1.05E-06

13 Base mix plus

0.103

9
10

227

1.28

Mix

Date

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/25/99
6/28/99
6/30/99
7/2/99
7/6/99
7/9/99
7/13/99

2-1002-D10

6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/25/99
6/28/99
6/30/99
7/2/99
7/6/99
7/9/99
7/13/99

9-1002-D2.5

6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/25/99
6/28/99
6/30/99
7/2/99
7/6/99
7/9/99
7/13/99

9-1002-D10

6/16/99
6/17/99
6/18/99
6/19/99
6/20/99

Time

Time
(hours)

11:00
12:00
22:30
20:30
21:00
14:00
15:00
11:30
16:00
10:00
14:00
16:00
10:00
11:00

39.5
40.5
74
96
120.5
165.5
190.5
211
287.5
329.5
381.5
479.5
545.5
642.5

20:00
22:15
2:00
15:00
15:30
11:00
12:15
22:30
20:30
21:00
14:00
15:00
11:30
16:00
10:00
14:00
16:00
10:00
11:00

0
2.25
6
19
19.5
39
40.25
74.5
96.5
121
166
191
211.5
288
330
382
480
546
643

20:15
22:15
2:00
15:00
15:30
11:00
12:15
22:30
20:30
21:00
14:00
15:00
11:30
16:00
10:00
14:00
16:00
10:00
11:00

0
2
5.75
18.75
19.25
38.75
40
74.25
96.25
120.75
160.75
190.75
211.25
287.75
329.75
381.75
479.75
545.75
642.75

20:45
22:45
2:00
15:30
11:00
12:30
22:30
20:30

0
2
5.25
18.75
38.25
39.75
73.75
95.75

Bleed
(%)

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

Cohesion
(mm)

Wet
Lombardi #
Density
(g/cc)

Viscosity
cP

Ingredients

10
0.196
18
20
21
23
23
23
23
23

0.22

23
23

0
1
1

0.0893

40
38

0.391
0.375

1.70E-06
1.55E-06

21
19

37
36
35
37
36
37
37
38
38
40

0.284
0.211
0.16
0.163
0.204
0.221
0.27
0.348
0.3
0.397

1.45E-06
1.40E-06
1.40E-06
1.60E-06
1.55E-06
1.50E-06
1.50E-06
1.55E-06
1.60E-06
1.70E-06

18
18
18
20
19
19
19
19
20
21

36

0.173

1.50E-06

19 Base mix plus

45

0.431

2.05E-06

Bentonite - 2%
25 Welan gum - 0.025%
Delvo - 10%

47
41

0.584
0.431

2.10E-06
1.70E-06

26
21

43
40
37
38
37
35
35
34
34
34

0.468
0.348
0.237
0.247
0.186
0.146
0.181
0.165
0.136
0.152

1.90E-06
1.70E-06
1.50E-06
1.60E-06
1.60E-06
1.50E-06
1.50E-06
1.20E-06
1.20E-06
1.20E-06

23
21
19
20
20
19
19
15
15
15

37

0.251

1.50E-06

19 Base mix plus

49

0.447

2.40E-06

Bentonite - 2%
30 Welan gum - 0.1%
Delvo - 2.5%

48
45

0.55
0.467

42
39
38
38
39
38
39
41
41
42

0.374
0.302
0.256
0.181
0.22
0.19
0.272
0.29
0.33
0.435

2.20E-06
2.05E-06
1.90E-06
1.65E-06
1.60E-06
1.65E-06
1.75E-06
1.75E-06
1.65E-06
1.70E-06
1.90E-06
1.85E-06
1.85E-06

21
20
21
22
22
21
21
24
23
23

40

0.432

1.65E-06

20 Base mix plus

65

0.644

4.00E-06

48
45

0.569
0.417

2.20E-06
2.10E-06

1.26

3
4
0.118
10
12
13
14
14
15
15
15

0.22

15
15

0
0
1

0.0569

1.27

2
4
0.134
10
13
15
17
17
17
17
17

0.221

17
17

0
1
1
2
2

0.0593

0.16
3
7

228

1.26

27
26

Bentonite - 2%
49 Welan gum - 0.1%
Delvo - 10%
27
26

Mix

10-1002-D2.5

Date

Bleed
(%)

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

11:30
16:00
10:00
14:00
16:00
10:00
11:00

210.75
287.25
329.25
381.25
479.25
545.25
642.25

11
12
12

6/16/99

21:00
23:00
2:00
15:30
11:00
12:45
22:30
20:30
21:00
14:00
15:00
11:30
16:00
16:00
10:00
14:00
16:00
10:00
11:00

0
2
5
18.5
38
39.75
73.5
95.5
120
165
190
210.5
287
311
329
381
477
545
642

0
1
2
4
8

22:45
0:45
2:00
15:30
11:00
13:00
22:30
20:30
21:00
14:00
15:00
11:30
16:00
16:00
10:00
14:00
16:00
10:00
11:00

0
2
3.25
16.75
36.25
38.25
71.75
93.75
118.25
163.25
188.25
208.75
285.25
309.25
327.25
379.25
475.25
543.25
640.25

23:15
1:15
2:00
15:30
11:00
13:15
22:30
20:30
21:00
14:00
15:00
11:30
16:00
16:00
10:00
14:00

0
2
2.75
16.25
35.75
38
71.25
93.25
117.75
162.75
187.75
208.25
284.75
308.75
326.75
378.75

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/25/99
6/28/99
6/29/99
6/30/99
7/2/99
7/6/99
7/9/99
7/13/99

6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/25/99
6/28/99
6/29/99
6/30/99
7/2/99
7/6/99
7/9/99
7/13/99
11-1002-D10

Time
(hours)

6/25/99
6/28/99
6/30/99
7/2/99
7/6/99
7/9/99
7/13/99

6/17/99

10-1002-D10

Time

6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/25/99
6/28/99
6/29/99
6/30/99
7/2/99

0.229

42

0.417

1.85E-06

0.158

42
40

0.365
0.366

1.90E-06
1.70E-06

Bentonite - 2%
23 Welan gum - 0.05%
Delvo - 2.5%
24
21

0.21

39
35
35
33
40
38
38
38
39
38
39

0.287
0.194
0.188
0.117
0.294
0.256
0.245
0.281
0.388
0.291
0.358

1.70E-06
1.30E-06
1.35E-06
1.10E-06
1.80E-06
1.60E-06
1.60E-06
1.55E-06
1.60E-06
1.55E-06
1.60E-06

21
16
17
14
22
20
20
19
20
19
20

0.087

38

0.393

1.50E-06

19 Base mix plus

45

0.514

2.05E-06

0.193

44
39

0.544
0.38

1.90E-06
1.60E-06

Bentonite - 2%
25 Welan gum - 0.05%
Delvo - 10%
23
20

0.198

41
39
38
36
35
35
34
35
33
33
33

0.348
0.316
0.204
0.184
0.155
0.163
0.127
0.128
0.102
0.121
0.109

1.80E-06
1.65E-06
1.65E-06
1.55E-06
1.50E-06
1.40E-06
1.20E-06
1.40E-06
1.10E-06
1.10E-06
1.10E-06

22
20
20
19
19
17
15
17
14
14
14

0.0664

31

0.098

36

0.24

1.50E-06

0.111

38
39

0.289
0.258

1.60E-06
1.60E-06

Bentonite - 2%
19 Welan gum - 0.05%
Delvo - 10%
20 U.S. Grout premium ultrafine
20 instead of MBT cement

0.142

38
39
40
40
41
41
42
43

0.262
0.28
0.235
0.206
0.316
0.324
0.367
0.408

1.60E-06
1.70E-06
1.85E-06
1.90E-06
1.90E-06
1.85E-06
1.90E-06
1.95E-06

20
21
23
23
23
23
23
24

20
20

17
17

17
0
1
1
2
4
7
8
8
9
9
10
10
10

Ingredients

35

0.0814

20

10
13
13
15
15
17
17

Viscosity
cP

0.243
0.232
0.2
0.176
0.152
0.121
0.127

12

0
1
2
3
6

Wet
Lombardi #
Density
(g/cc)

38
38
37
36
35
34
34

0.218

12

17
19
20
20
20
20
20

Cohesion
(mm)

229

1.27

1.26

1.26

1.60E-06
1.60E-06
1.55E-06
1.50E-06
1.50E-06
1.20E-06
1.20E-06

20
20
19
19
19
15
15

1.30E-06

16 Base mix plus

8.30E-06

103 Base mix plus

Mix

1-1002-D2.5

Date

6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/28/99

1-1002-D5

6/16/99
6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/28/99
6/29/99
6/30/99
7/2/99
7/6/99
7/8/99
7/12/99

1-1002-D7.5

6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/28/99
6/29/99
6/30/99
7/2/99
7/6/99
7/8/99
7/12/99
1-1002-D10

6/17/99

6/18/99
6/19/99
6/20/99
6/21/99
6/23/99
6/24/99
6/28/99
6/29/99
6/30/99
7/2/99
7/6/99

Time

23:30
1:30
2:00
15:30
13:30
22:30
20:30
12:00
14:00
16:00
14:00

Time
(hours)

Bleed
(%)

0
1.5
2
15.5
37.5
70.5
92.5
108
160
186
280 SET

23:45
1:45
2:00
15:30
13:30
14:00
22:30
20:30
21:00
14:00
16:00
14:00
16:00
16:00
14:00
16:00
14:00
16:00

0
2
2.25
15.75
37.75
38.25
70.75
92.75
108.25
160.25
186.25
280.25
306.25
330.25
376.25
474.25
520.25
618.25

0:00
2:00
15:30
13:30
14:00
22:30
20:30
12:00
14:00
16:00
14:00
16:00
16:00
14:00
16:00
14:00
16:00

0
2
15.5
37.5
38
70.5
92.5
108
160
186
280
306
330
376
474
520
618

0:15
2:00
15:30
13:30
22:30
23:15
20:30
12:00
14:00
16:00
14:00
16:00
16:00
14:00
16:00

0
1.75
15.25
37.25
70.25
71
92.25
107.25
159.25
185.25
279.25
305.25
329.25
375.25
473.25

Pressure Marsh
Filtration Viscosity
(min^-1/2)
(sec)

Cohesion
(mm)

0
21
30
46
47
47
47
47
47
47

0.146

27

0.0327

0.213

28
29
30

0.213

0
20
30
39
40
41
41
41
42
42
42

0.0496
0.0512
0.11

4.10E-07
5.60E-07
7.20E-07

5
7
9

31

0.117

8.30E-07

10

0.164

27

0.0346

0.18

30
29

Delvo - 2.5%

2.90E-07

4 Base mix plus

0.0937
0.0634

7.20E-07
5.60E-07

9
7

29

0.0555

5.60E-07

0.221

28
31
28
29
28
28
28
28
28
29

0.0492
0.089
0.0409
0.0342
0.0528
0.0563
0.0468
0.0547
0.0468
0.106

4.05E-07
8.40E-07
4.05E-07
5.70E-07
4.05E-07
4.05E-07
4.05E-07
4.05E-07
4.05E-07
5.40E-07

5
10
5
7
5
5
5
5
5
7

0.124

28

0.0488

31

0.111

8.30E-07

0.207

30
30

0.0776
0.0567

7.30E-07
7.40E-07

9
9

0.212

30
29
29
29
29
29
28
28
28
28

0.0657
0.059
0.0547
0.0461
0.0464
0.0433
0.0445
0.0449
0.0516
0.048

7.40E-06
5.60E-06
5.60E-06
5.70E-07
5.70E-07
5.70E-07
4.10E-07
4.10E-07
4.05E-07
4.05E-07

92
70
70
7
7
7
5
5
5
5

0.1

28

0.0409

0.206

31
31

0.104
0.107

0.231

38
38
38

35
35
35
35
35
35
35

1.27

Delvo - 5%

38

0
22
33
34
34

Ingredients

4 Base mix plus

42
42
42

37
38
38
38
38
38

1.27

Viscosity
cP

2.90E-07

42

0
22
35
37

Wet
Lombardi #
Density
(g/cc)

0.201

1.27

1.27

4.10E-07

4.10E-07
8.30E-07
8.30E-07

5 Base mix plus

10 Delvo - 7.5%

5 Base mix plus

10 Delvo - 10%
10

30

0.0697

7.30E-07

30
29
29
29
30
29
29
28

0.0665
0.0618
0.0551
0.0311
0.0504
0.0488
0.0488
0.0524

7.30E-07
5.50E-07
5.60E-07
5.70E-07
7.40E-07
5.70E-07
5.70E-07
4.05E-07

9
7
7
7
9
7
7
5

230

APPENDIX 2
COLLOIDAL SILICA VISCOSITY TESTING RESULTS

231

Table A2-1 Colloidal Silica Viscosity Testing Results

Sample
HSS10-10-8-1
HSS10-10-7.5-2
HSS10-05-7.5-1
HSS10-05-7-2
HSS10-05-6.5-3
HSS15-10-7.8-1
HSS15-05-7.8-1
HSS15-05-7.5-2
HSS15-05-7-3
TMS15-10-7.5-1
TMS15-10-7.25-2
TMS15-10-6.85-3
TMS15-05-6.85-1
TMS15-05-6.5-2
TMS15-05-6-3
TMS15-03-6.5-1
TMS15-03-6-2
TMS15-03-5.5-3

2/4
1.5
1.75
1.25
1.5
1.5
1.75
2
1.5
1.5
1.5
1.75
1.75
1.5
1.75
1.75
1.75
1.75
1.75

2/7
1.5
1.75
1.5
1.75
5.25
1.75
1.5
1.5
1.75
1.75
1.75
3
1.75
1.75
1.75
1.75
1.75
1.75

2/9
1.5
1.5
1.5
1.75
gel
1.75
1.75
1.75
3.75
1.5
18

1.75

2/10

7.5

49.5

2/13
1.75
2.25
1.25
2.25

2/15

2.5
1.75
1.75
gel
1.5
2
gel
1.5
1.75
2
1.75
1.75
1.75

2.25
1.5

1.5

2.25

2/18
1.5
5.25
1.5
1.75

2/22
1.75
100
1.75
2

2/25
1.75
gel
1.75
2

12.3
1.5
2.5

gel
2
3.25

1.5
1.5

2
1.5

1.5
1.5
2.75
1.25
1.5
1.5

1.5
1.5
3.5
1.75
1.75

Viscosity (cP)
3/1
3/2
3/6
1.75
2.75

3/8
1.75

3/22
5.25

4/4
300

4/10
gel

4/23

5/10

5/19

5/30

370

1.75
2

2.75
3

1.5
3

2.25
19.8

1.75
gel

3.5

11.7

1.75
6

1.5
57.5

2.25
gel

2.75

5.5

435

gel

2
2.5

3
2.75

2.5
2.75

8
5.5

250
20.5

gel
69

520

gel

1.75
1.75
13.8
2
1.75
2.25

1.75
1.75
17.3
1.75
1.75
2.25

1.75
2
47.5
2
2.5
2

1.75
3

2
3

1.5
1.75

2
2

2
3.25

2
3

1.5
1.75
3

2
1
12

2
1.75
93

3.25
2.5
gel

1.75
2

3
2.25

4.75

232

1.5
1.5
7.5
1.75
1.5
1.75

2
1.75
10.2

APPENDIX 3
STABILIZED SAND SAMPLE DETAILS AND CYCLIC TESTING RESULTS

233

Table A3-1 Details of Stabilized Sand Samples

Sample
SM20-6A
SM20-6B
SM20-6C
SM10-7A
SM10-7B
SM10-7C
SM5-8A
SM5-8B
SM5-8C
SM20-9A
SM20-9B
SM20-9C
SM20-9D
SM20-9E
SM20-9F
SM10-10A
SM10-10B
SM10-10C
SM10-10D
SM10-10E
SM10-10F
SM10-11A
SM10-11B
SM10-11C
SM10-11D
SM10-11E
SM10-11F

Type and
Percent
Ludox
SM, 20
SM, 20
SM, 20
SM, 10
SM, 10
SM, 10
SM, 5
SM, 5
SM, 5
SM, 20
SM, 20
SM, 20
SM, 20
SM, 20
SM, 20
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10

Date Made

Gel Time

Date
Tested

Age at
Testing

6/18/00
6/18/00
6/19/00
6/18/00
6/18/00
6/18/00
6/18/00
6/18/00
6/18/00
6/19/00
6/19/00
6/19/00
6/19/00
6/19/00
6/19/00
7/17/00
7/17/00
7/17/00
7/17/00
7/17/00
7/17/00
7/17/00
7/17/00
7/17/00
7/17/00
7/17/00
7/17/00

4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours

7/6/00
7/6/00
7/6/00
7/6/00
7/6/00
broke
7/10/00
7/10/00
7/10/00
6/26/00
6/28/00
6/29/00
6/28/00
6/28/00
6/30/00
7/23/00
7/23/00
7/23/00
7/19/00
7/19/00
broke
7/24/00
7/24/00
7/24/00
7/21/00
broke
7/23/00

18 days
18 days
18 days
18 days
18 days
-22 days
22 days
22 days
7 days
9 days
10 days
9 days
9 days
11 days
6 days
6 days
6 days
40 hours
40 hours
-7 days
7 days
7 days
4 days
7 days

234

Curing
Period (times
gel time)
108
108
108
108
108
-132
132
132
42
54
60
54
54
66
36
36
36
10
10
42
42
42
24
42

Method of
Preparation

Type of
Test

P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P

Conc. UC
Conc. UC
Conc. UC
Conc. UC
Conc. UC
Conc. UC
UC
UC
UC
C, UC
C, UC
C, UC
C, UC
C, UC
C, UC
C, UU
C, UC
C, UC
C, UC
UC
UU
UU
UU
C, UU
C, UU
C, UU

Cyclic Data
Files

S9AC45
S9BC45
S9CC45
S9DC45
S9EC45
S9FC45
S10AC35, 45
S10BC45
S10CC45
S10DC30

S11DC30, 45
S11FC35

Sample
SM15-12A
SM15-12B
SM15-12C
SM10-13A
SM10-13B
SM10-13C
SM10-14A
SM10-14B
SM10-15A
SM10-15B
SM10-15C
SM10-16A
SM10-16B
SM10-16C
SM10-17A
SM10-17B
SM10-17C
SM10-18A
SM10-18B
SM10-18C
SM10-19A
SM10-19B
SM10-19C
SM15-20A
SM15-20B
SM15-20C
HS20-12A
HS20-12B
HS20-12C

Type and
Percent
Ludox
SM, 15
SM, 15
SM, 15
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 10
SM, 15
SM, 15
SM, 15
HS, 20
HS, 20
HS, 20

Date Made

Gel Time

Date
Tested

Age at
Testing

7/18/00
7/18/00
7/18/00
7/19/00
7/19/00
7/19/00
7/20/00
7/20/00
7/27/00
7/27/00
7/27/00
7/27/00
7/27/00
7/27/00
7/27/00
7/27/00
7/27/00
7/27/00
7/27/00
7/27/00
8/25/00
8/25/00
8/25/00
8/25/00
8/25/00
8/25/00
6/28/00
6/28/00
6/28/00

4 hours
4 hours
4 hours
6 hours
6 hours
6 hours
6 hours
6 hours
1 day
1 day
1 day
1 day
1 day
1 day
1 day
1 day
1 day
1 day
1 day
1 day
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours
4 hours

7/25/00
7/25/00
7/25/00
7/26/00
7/26/00
broke
8/7/00
broke
8/7/00
8/7/00

7 days
7 days
7 days
7 days
7 days

Curing
Period (times
gel time)
42
42
42
28
28

18 days

108

11 days
11 days

11
11

21 days
21 days
21 days
32 days
32 days
32 days
53 days
55 days
56 days
7 days
7 days
7 days
10 days
10 days
10 days
12 days
16 days
14 days

21
21
21
32
32
32
53
55
56
42
42
42
60
60
60
72
96
84

8/17/00
8/17/00
8/17/00
8/28/00
8/28/00
8/28/00
9/8/00
9/10/00
9/11/00
9/1/00
9/1/00
9/1/00
9/4/00
9/4/00
9/4/00
7/10/00
7/14/00
7/12/00

235

Method of
Preparation

Type of
Test

Cyclic Data
Files

P
P
P
MT, PG
MT, PG
MT, PG
MT, PG
MT, PG
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P
P

C, UC
C, UC
C
C, UC
C, UC

S12AC45
S12BC45
S12CC45
S13AC40
S13BC40

UC
C, UU
C, UU

S15AC35
S15BC30

C, UC
C, UC
C, UC
C, UC
C, UC
C, UC
C, UC
C, UC
C, UC
UC
UC
UC
UC
UC
UC
C, UU
C, UU
C, UU

S16AC35
S16BC40
S16CC45
S17AC45
S17BD40
S17CC35
S18AC35
S18BC45
S18CC40

H12AC45
H12BC45
H12CC45

Sample
TM20-7A
TM20-7B
TM20-7C
TM20-7D

Type and
Percent
Ludox
TM, 20
TM, 20
TM, 20
TM, 20

Date Made

Gel Time

Date
Tested

Age at
Testing

7/13/00
7/13/00
7/13/00
7/13/00

4 hours
4 hours
4 hours
4 hours

7/20/00
7/20/00
broke
broke

7 days
7 days

236

Curing
Period (times
gel time)
42
42

Method of
Preparation

Type of
Test

Cyclic Data
Files

P
P
P
P

C
C

T7AC45
T7BC45

Table A3-2 Cyclic Testing Results

Sample

Cyclic Stress
Ratio

Number of
Cycles

M35B1C22
M35B1C25A
M35B1C25B
M35B1C30
SM20-9A
SM20-9B
SM20-9C
SM20-9D
SM20-9E
SM20-9F
SM10-10A

0.19
0.21
0.23
0.27
0.44
0.44
0.44
0.44
0.44
0.44
0.30
0.40
0.40
0.23
0.25
0.27
0.40
0.27
0.43
0.43
0.41
0.30
0.37
0.29
0.25
0.30
.035
0.39
0.41
0.37
0.30
0.32
0.41
0.37
0.43
0.42
0.41
0.41
0.41

31
20
21
13
1000
1000
1000
1000
1000
1000
1000
200
500
300
400
1000
200
400
1000
1000
1000
1000
400
300
400
200
300
200
100
100
100
100
100
100
1000
1000
1000
100
200

SM10-10B
SM10-10C
SM10-10D
SM10-11D
SM10-11F
SM15-12A
SM15-12B
SM15-12C
SM10-13A
SM10-13B
SM10-15A
SM10-15B
SM10-16A
SM10-16B
SM10-16C
SM10-17A
SM10-17B
SM10-17C
SM10-18A
SM10-18B
SM10-18C
HS20-12A
HS20-12B
HS20-12C
TM20-7A
TM20-7B

237

Cycles to
1% DA
Strain
28
18
18
11
NA
NA
NA
NA
NA
NA
36
3
10
101
NA
4
35
NA
NA
10
992
NA
1
2
1
1
1
1
1
NA
3
1
3
NA
NA
NA
2
102

Cycles to
2% DA
Strain
28
19
19
11
NA
NA
NA
NA
NA
NA
NA
49
10
46
101
NA
14
159
NA
NA
901
NA
NA
220
NA
24
3
2
2
3
NA
NA
2
NA
NA
NA
NA
8
NA

Cycles to 5%
DA Strain
29
20
20
12
NA
NA
NA
NA
NA
NA
NA
NA
NA
261
NA
NA
NA
276
NA
NA
NA
NA
NA
NA
NA
NA
NA
106
NA
NA
NA
NA
NA
NA
NA
NA
NA
52
NA