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Unanuevaherramientaarqueomtrica:La
datacinporrehidroxilacin
PublicadoporAliciaM.Cantoelmayo21,2009alas10:00pm
Verblog

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Buenanoticiasobreunanuevaherramientaarqueomtrica,la"datacinporrehidroxilacin",
descubiertayperfeccionadaporunequipoconbaseenlaUniversidaddeManchester(ReinoUnido).La
pruebasirveparafecharladrillosycermicasdelosdosltimosmileniosy,porlotanto,tambinpara
detectarfalsosmodernos.Porelmomento,elndicedefiabilidadcontrastadaparecemuyalto(*):

FIREANDWATERREVEALNEWARCHAEOLOGICALDATINGMETHOD
20May2009
ScientistsatTheUniversityofManchesterhavedevelopedanewwayofdatingarchaeologicalobjects
usingfireandwatertounlocktheirinternalclocks.Thesimplemethodpromisestobeassignificanta
techniquefordatingceramicmaterialsasradiocarbondatinghasbecomefororganicmaterialssuchas
boneorwood.
AteamfromTheUniversityofManchesterandTheUniversityofEdinburghhasdiscoveredanew
techniquewhichtheycallrehydroxylationdatingthatcanbeusedonfiredclayceramicslike
bricks,tileandpottery.
WorkingwithTheMuseumofLondon,theteamhasbeenabletodatebricksamplesfromRoman,
medievalandmodernperiodswithremarkableaccuracy.
Theyhaveestablishedthattheirtechniquecanbeusedtodeterminetheageofobjectsupto2,000years
oldbutbelieveithasthepotentialtobeusedtodateobjectsaround10,000yearsold.

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Theexcitingnewfindingshavebeenpublishedonlinetoday(20May2009)bytheProceedingsofthe
RoyalSocietyA.
Themethodreliesonthefactthatfiredclayceramicmaterialwillstarttochemicallyreactwith
atmosphericmoistureassoonasitisremovedfromthekilnafterfiring.Thiscontinuesoveritslifetime
causingittoincreaseinweighttheolderthematerial,thegreatertheweightgain.
In2003theManchesterandEdinburghteamdiscoveredanewlawthatpreciselydefineshowtherateof
reactionbetweenceramicandwatervariesovertime.
Theapplicationofthislawunderpinsthenewdatingmethodbecausetheamountofwaterthatis
chemicallycombinedwithaceramicprovidesaninternalclockthatcanbeaccessedtodetermineits
age.
Thetechniqueinvolvesmeasuringthemassofasampleofceramicandthenheatingittoaround500
degreesCelsiusinafurnace,whichremovesthewater.
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Thesampleisthenmonitoredinasuperaccuratemeasuringdeviceknownasamicrobalance,to
determinethepreciserateatwhichtheceramicwillcombinewithwaterovertime.
Usingthetimelaw,itispossibletoextrapolatetheinformationcollectedtocalculatethetimeitwilltake
toregainthemasslostonheatingrevealingthesamplesage.
TheyhavecalculatedthataRomanbricksamplewithaknownageofaround2,000yearswas2,001
yearsold.Afurthersamplewithaknownageofbetween708and758yearswascalculatedtohavean
ageof748years.
Theresearchersalsotestedamysterybrick,withtherealageonlyrevealedtothemoncetheyhad
completedtheirprocess.Thisknownagewasbetween339and344yearsandthenewtechnique
suggestedthebrickwas340yearsold.
Duringthecourseoftheirresearch,theteamalsofoundthatceramicobjectshavetheirinternaldate
clocksresetiftheyareexposedtotemperaturesof500degreesCelsius.Usedonmedievalbrickfrom
Canterbury,thetechniquerepeatedlydatedasampleasbeing66yearsold.Furtherinvestigationrevealed
thatCanterburywasdevastatedbyincendiarybombsandfiresduringaSecondWorldWarblitzin1942.
Theintenseheatgeneratedbythebombinghadresetthedatingclockbyeffectivelyrefiringthebricks.
TheresultsalsoprovedaccurateenoughtoshowthatabricksamplefromtheKingCharlesbuildingin
Greenwichcamefromreconstructioncarriedoutinthe1690sandnotfromtheoriginalbuildingwhich
wasconstructedbetween1664and1669.
LeadauthorDrMoiraWilson,SeniorLecturerintheSchoolofMechanical,AerospaceandCivil
Engineering(MACE),said:Thesefindingscomeaftermanyyearsofhardwork.Weareextremely
excitedbythepotentialofthisnewtechnique,whichcouldbecomeanestablishedwayofdeterminingthe
ageofceramicartefactsofarchaeologicalinterest.
Themethodcouldalsobeturnedonitsheadandusedtoestablishthemeantemperatureofamaterial
overitslifetime,ifaprecisedateoffiringwereknown".Thiscouldpotentiallybeusefulinclimate
changestudies.
Aswellasthenewdatingmethod,therearealsomorewiderangingapplicationsofthework,suchas
thedetectionofforgedceramic.
Thethreeyear100,000projectwasfundedbytheLeverhulmeTrust,withthemicrobalancewhich
measuresmassto1/10thofamillionthofagramfundedbya66,000grantfromtheEngineeringand
PhysicalScienceResearchCouncil(EPSRC).
Researchersarenowplanningtolookatwhetherthenewdatingtechniquecanbeappliedtoearthenware,
bonechinaandporcelain.
Notesforeditors
FormoreinformationpleasecontactAlexWaddington,MediaRelationsOfficer,theUniversityof
Manchester,01612758387/07717881569.DrWilsonisavailableforcommentbyarrangement.
Thepaper,entitledDatingfiredclayceramicsusinglongtermpowerlawrehydroxylationkinetics
hasbeenpublishedonlineandisduetoappearinafutureeditionofProceedingsoftheRoyalSocietyA.
Acopyofthepaperisavailableonrequest[vermsabajonotadeprensadelapublicacin,ayermismo].

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ThefullresearchteamcomprisedDrMoiraWilson,DrMargaretCarter,ProfWilliamHoff,
CerenInce,ShaunSavageandBernardMcKayfromTheUniversityofManchester,ProfessorChrisHall
fromtheSchoolofEngineeringandCentreforMaterialsScienceandEngineeringatTheUniversityof
EdinburghandIanBettsfromTheMuseumofLondon.TheCanterburyArchaeologicalTrustprovided
additionalsamplesandinformationforthestudywhileIbstockBrickLtdprovidedkilnfreshbricks.
............

Msinfo:Seminariohabidoel12demarzopasadoenlaSchoolofEngineeringandCentreforMaterials
ScienceandEngineeringdelaUniversidaddeEdimburgo:
Prof.ChrisHall
InstituteforMaterialsandProcesses,UniversityofEdinburgh
Oldbricks:datingfiredclayceramicsusinglongtermpowerlawr...
Firedclaymaterialslikebrick,tileandceramicartefactsarefoundwidelyinarchaeologicaldeposits.The
slowprogressivechemicalrecombinationofceramicswithenvironmentalmoisture(rehydroxylation)
providesthebasisforamethodofarchaeologicaldating.Rehydroxylationratesaredescribedbya
(time)1/4powerlaw.Aceramicsamplemaybedatedbyexposingittowatervapourtomeasureitsmass
gainrateandhenceitsindividualrehydroxylationkineticconstant.Thekineticconstantdependson
temperature.Meanlifetimetemperaturesareestimatedfromhistoricalmeteorologicaldata.Calculated
agesofsamplesofestablishedprovenancefromRomantomoderndatesagreeexcellentlywithassigned
(known)ages.Thisagreementsuggeststhatthepowerlawholdspreciselyonmillenialtimescales.The
powerlawexponentisaccurately,consistentwiththetheoryoffractional(anomalous)'singlefile'
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diffusion.
.....................
Elartculo,enefecto,hasidopublicadoconfechadeayerenlacitadarevista,aqulanotadeprensadela
misma:
"FIREANDWATERREVEALTRUEAGEOFANCIENTRELICS"
20May2009
Fireandwaterareallthatisneededtounlocktheinternalclocks'ofarchaeologicalremainsand
accuratelyrevealtheirage,sayscientists.Theresearch,publishedonlinetodayinProceedingsofthe
RoyalSocietyA,willhelparchaeologistsdateremainsthatarethousandsofyearsold,andalsoreveal
whereothertechniquesgowrong.
Datingmethodsareofparamountimportanceintheearthandenvironmentalsciences,palaeontology,
archaeology,andarthistory.Firedclaymaterialsuchasbricks,tileandceramicsrepresentan
importantsampleoftheremainsunearthedatarchaeologicaldigs,buttheyarenotoriouslyhardto
dateaccurately(**).Carbon14dating,whichcanbeusedonbone,doesnotworkwithceramics,and
thosetechniquesthatdoexistareextremelycomplex.
NowateamofscientistsfromtheUniversitiesofManchesterandEdinburghhavefoundasurprisingly
simplewaytogetaroundthisissue.
Fromthemomenttheyarefired,ceramicsbegintoabsorbmoisturefromtheenvironmentwhichcauses
themtogainmass.Usingatechniquetheycallrehydroxilationdating'researchersledbyDrMoira
WilsonfromtheUniversityofManchesterfoundthatheatingasampleoftherelictoextreme
temperaturescausesthisprocesstobereversedallthemoistureithasgainedsinceitwasfiredislost
again.
Themoreweightasamplelosesduringheating,themoremoisturetherewastostartwith,andsothe
oldertherelic.Afterheating,Wilsonandherteamusedanextremelyaccuratemeasuringdeviceto
monitorthesampleasitbegantorecombinewithmoistureintheatmosphere.Theythenusedalawto
predicthowlongitwouldtakeforallthewaterlostinheatingtobereabsorbed,andsorevealthetrue
ageofthesample.
TotesttheirnewtechniquethescientiststeamedupwiththeMuseumofLondonandtrieditouton
samplesofknowage.TheysuccessfullydatedbricksamplesfromtheRoman,medievalandmodern
periods,andthemethodwassoaccuratethatitlookstobecomethewayinwhichsuchartefactsaredated
inthefuture,accordingtoWilson.
Sofar,thetechniquehasbeenusedwithspecimensthatareasmuchas2000yearsold,buthasthe
potentialtobeusedonmucholderartefacts,saysWilson,eventhosedatingback10,000years.
What'smore,thetechniquehasrevealedaflawinpreviousdatingverdicts.Whenclayobjectsare
submittedtoextremetemperatures,andmoistureremoved,thisinternalclock'isreset.Thatmeansthat
objectsthathavebeensubjectedtoextremeheat,suchasthosedatingbacktotheWWIIBlitzareoften,
intruth,mucholder.

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Thetechniquehasfarreachingimplications."Aswellasthenewdatingmethod,therearealsomore
widerangingapplicationsofthework,suchasthedetectionofforgedceramic,"saysWilson."The
methodcouldalsobeturnedonitsheadandusedtoestablishthemeantemperatureofamaterialover
itslifetime,ifaprecisedateoffiringwereknown,"sheadds,whichcouldmakethemethodausefultool
forclimatechangestudies.
...............

(*)Porelmomentonoheencontradonadaenespaolsobreestanoticia(noesdeltipoqueseprestea
llamarmucholaatencindelaprensa,oatitularesllamativos).Paralectoresquetenganalguna
dificultadconlalengua,dosmuyaceptablestraductoresdetextoseningls(yotraslenguas),por
ejemplo,enElMundoyYa.com.ParatrminosconcretoselsitiodeWordReference,conotrosrecursos.
(**)Serefierenamaterialesdefechasmsproblemticasonobiendatadosporestratigrafahabraque
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exceptuar,pues,algunostipos,comolascermicasticasdefigurasnegrasyrojas,lamayoradelas
sigillatasromanaso,enelcasodelosladrillos,losbienfechadosatravsde"bollilaterizi",porejemplo,
enlosquelapruebaserasuperflua.

.............
Complemento:Excelentesitioparaladrilloslegionarios,selladosoinscritos,enInglaterrayotras
zonaseuropeasconacuartelamientosromanosaqu,enRomanCoins.

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.............
Fotosinsertadas:RomanCoinsyWikipedia.
Fuentedelanoticia:N.Thorpe,enlalistaBritarch,atravsdeJ.Valdez,enArchport.
Visitas:547
Etiquetas:Arqueologa,arqueometra,cermicas,datacin,ladrillos,rehidroxilacin
Tegusta?
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ComentarioporYrgelmayo22,2009alas1:59pm
Esunamuybuenanoticiaperonoexplicansitieneencuentaladiferenteexposicinalahumedad
quetienenlosladrillosocermicasenterradasbajotierraporsiglos,osidebenaplicarsediferentes
patronesparahallazgosconhumedadmenoralainglesa(Carthago,Ur...).
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ComentarioporKoenraadVandenDriesscheelmayo24,2009alas3:56pm
Interesanteartculo,Alicia.

ComentarioporAliciaM.Cantoelmayo24,2009alas4:59pm
Gracias.

Comentarioporandreaelmayo25,2009alas1:03am
Dra.Canto:Haceunosdashiceuncomentarioaestanoticia,queborr,posteriormente,porque
pensqueseprestaraaunmontndecomentarios"paradoxos"ynoquisequeseemborronaraeste
artculo.Cuandoquiseexplicarestacuestin,setermindeestropeartodomi"aparataje"
informtico,peroahoraque"noshemosrecuperado",yanariesgodequesuceda,meparece
importantequesepresteatencinalasfotografasdematerialesconstructivosconepgrafes
impresoseincisosantecoctionemquehaincluidoenesteartculo.

ComentarioporAliciaM.Cantoelmayo25,2009alas1:07am
Andrea:Mealegrodesu"recuperacin",ydequealmenosalguiensedieracuentademis
intencionesalrespectodelasfotos,aunquenuncalosquenecesitarandeverdaddrsela,queson
comounfrontn!)

ComentarioporAliciaM.Cantoeljunio12,2009alas1:09am
Bueno,yavahabiendoalgomsenespaolsobreestanuevatcnica,aunquepoco:
ArtculoenWikipedia(2752009):Rehidroxilacin
(buenasreferenciaseninglsnobiencategorizado,en"Tecnologaprehistrica")
Noticiaenhttp://www.amazings.com(1062009):
Arqueologa
NuevoMtododeDatacinArqueolgicaParaObjetosdeCermica
10deJuniode2009
Unequipodecientficoshadesarrolladounanuevaformadedatarobjetosarqueolgicos
valindosedelfuegoyelaguaparaaccederasus"relojesinternos".Estemtodosimplepromete
serunatcnicadedatacintanimportanteparaobjetosdecermicacomoloesladatacinpor
radiocarbonoparamaterialesorgnicoscomoelhuesoolamadera.
Lanuevatcnica,descubiertaporexpertosdelaUniversidaddeManchesterydelaUniversidadde
Edimburgo,puedeserutilizadaenarcillahorneada,ascomoenladrillos,baldosasyobjetosde
alfarera.

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TrabajandoconelMuseodeLondres,elequipofuecapazdedatarmuestrasdeladrillosdelos
periodosRomano,MedievalyModernoconnotableprecisin.

Losinvestigadoreshanestablecidoquesutcnicapuedeserutilizadaparadeterminarlaedadde
objetosdehasta2.000aos,peroconsideranquetieneelpotencialparafecharobjetosconcercade
10.000aosdeantigedad.
Elmtodosebasaenelhechodequeunmaterialcermicodearcillahorneadacomienzaa
reaccionarqumicamenteconlahumedadatmosfricatanprontocomoselesacadelhorno.Este
procesoqumicocontinadurantetodasuvidacausandoqueganepeso:Cuantomsantiguoseael
material,mspesohabrganado.
Enelao2003,elequipodelasuniversidadesdeManchesteryEdimburgodescubriunanueva
leyquedefinedeformaprecisacmovaraconeltiempolavelocidaddelareaccinentrela
cermicayelagua.
Laaplicacindeestaleyeslabasedelnuevomtododedatacin,debidoaquelacantidaddeagua
quesecombinaqumicamenteconlacermicaproporcionaun"relojinterno"alcualsepuede
accederparaaveriguarsuedad.
Elusodelatcnicaimplicamedirlamasadeunamuestradelacermicayluegocalentarlahasta
cercade500gradoscentgradosenunhorno,locualeliminaelagua.
Lamuestraesluegoexaminadaconundispositivodemedicindemuyaltaprecisinconocido
comomicrobalanza,paradeterminarlavelocidadexactaalaquelacermicase
combinaconelaguasegntranscurreeltiempo.
Valindosedeestemismofactortiempo,esposibleextrapolarlainformacinobtenidapara
calculareltiempoqueelmaterialtardarenrecuperarlamasaperdidaporelcalentamiento,
revelndoseaslaedaddelamuestra.
LaautoraprincipaldeestainvestigacinesMoiraWilson.
Informacinadicionalen:
*U.Manchester
Comentar
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