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Experiment No. 5
Date & Time Started:
Group No.: 7
Supervisor/Instructor: Engr. Juvyneil E. Cartel
2. of
After
say 1 hourof
of0.1
mixing,
takein10
sample
and place
in the filtration
standardized 0.1 M NaOH and 250 mL
standardized
M EtOAc
1 mL
L flask
and secure
stopper.
c
way
from and
naked
lights.soda
For a
similaris0.1
M solution
the amount
of EtOAc
needed
is (molecular
weight
x 10up
liters
s of solid
caustic
needed
(molecular
weight
x 0.1 x10)
= 40 g
in 10 liters
. Make this
solution
wea
c
Activity Flow:
2
cribe the commissioning
Switch on bothsection
pumps.ofAdjust
this manual
flow rates
andto
allow
0.10the
liters/min
temperature
for each
of the
feedreactor
and check
to reach
that 30C
the product
with the
d
inlet20-30
tank minutes
and analyze
forthe
caustic
soda
Repeat
sampling
analyze
to ensure
steady
state
con
fter
when
reactor
hasconcentration.
reached a steady
state
note theand
following
readings.
Flow
rates
of NaOH
Plot Xa vs t
and Ca vs t
NOMENCLATURE:
t
ra
= reaction rate
Na
Na0
X
SCHEDULING OF TASKS:
o Morbos conducts reaction in a flask
o Ymas conducts reaction in a tubular reactor
o Gepiga conducts reaction in a tubular reactor
o Orevillo - conducts reaction in a flask
Experimental Raw Data
Trial 1
sampl
e
1
2
3
4
Trial 2
sampl
e
1
2
3
4
Trial 3
30 NaOH; 30 EtOAC
t
5
10
15
20
Vi
49
45.8
42.6
39.5
Vf
45.8
42.6
39.5
36.8
V
3.2
3.2
3.1
2.7
50 NaOH; 30 EtOAC
t
5
10
15
20
Vi
36.8
34.3
31.8
29.8
Vf
34.3
31.8
29.8
27.9
V
2.5
2.5
2
1.9
30 NaOH; 30 EtOAC
4
sampl
e
1
2
3
4
t
5
10
15
20
Vi
27.9
25.3
22.7
20
Vf
25.3
22.7
20
17.4
V
2.6
2.6
2.7
2.6
Processed Data