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Article history:
Received 28 August 2015
Received in revised form 15 May 2016
Accepted 17 May 2016
Available online 26 May 2016
Keywords:
Fractal dimension
Fracture profile
Mortar
Heavy clay
Roughness
Self-affine surface
a b s t r a c t
The fractal modeling of a rugged fracture surface has received different purposes. However
none definitive model for the most of materials has been reached. Therefore, a general selfaffine fractal model is proposed for fracture surfaces and applied to heavy clay and mortar.
An analytical expression for the rugged crack length is obtained for application on fractal
fracture mechanics. Stereoscopic images are obtained for each tested specimens. Image
processing filters are used to extract the rugged profile of the cracks. The box-counting
and sand-box methods are used on the crack profile to obtain the local and the global
roughness exponents. Specimens prepared under different conditions validated the model.
Mortars and heavy clay specimens were characterized by measuring their modulus of rupture and the rugged crack profile under 3-point bending tests. A good agreement between
the model and the experimental results was observed. A strong correlation between the
fractal dimension and the sintering temperature for heavy clay specimens was verified.
The results also showed that the increasing rugged crack length of the profile of the fractured mortar specimens is well correlated with the increase in water/cement ratio. These
results validate the application of the proposed model for estimating the fracture strength
of brittle materials.
2016 Elsevier Ltd. All rights reserved.
1. Introduction
The fracture surface is a record of the information left by the fracture process. Generally, the rugged fracture surface profile has fractal geometry, so it is possible to establish a relationship between its topology and physical quantities of the fracture mechanics using fractal characterization techniques. However, the classical fracture mechanics (CFM) was developed
idealizing a flat, smooth, and regular fracture surface, as the geometry of crack surfaces is usually rugged and cannot be
easily described by the Euclidean geometry [1]. In this sense, the mathematical basis of CFM considers an energetic
equivalent between the rugged and the projected fracture surfaces [2]. Besides the mathematical complexity, part of this
Corresponding author.
E-mail addresses: lucasmaximoalves@gmail.com (L.M. Alves), adilsonchinelatto@gmail.com (A.L. Chinelatto), alkimin@lactec.org.br (L.A. de Lacerda).
http://dx.doi.org/10.1016/j.engfracmech.2016.05.015
0013-7944/ 2016 Elsevier Ltd. All rights reserved.
233
Nomenclature
Latin characters
0
index to denote measurements taken on the projected plane
a
minimal area of fracture surface
DA
area of fracture surface
A1; A2; A3; Ar1; . . . ; Ar30 mortar and ceramic samples
B1; B2; B3; Br1; . . . ; B30 mortar and ceramic samples
C1; C2; C3; Cr1; . . . ; Cr30 mortar and ceramic samples
d
infinitesimal increment
D1; D2; D3; Dr1; . . . ; Dr30 mortar and ceramic samples
DB
fractal box dimension
Df
fractal dimension
divider dimension
DD
DBC
fractal dimension measured by box-counting method
e0
fractal cell size or minimal crack length in transversal direction
E
elastic or Young s modulus
crack length measured in transversal direction
E0
DE0
variation of crack length measured in transversal direction
f
general functions
g
general functions or subscript index for global quantity
G
elastic energy release rate
h0
fractal cell size or minimal crack length in vertical direction
H
Hursts exponent
H0
plane projected crack height
DH0
variation in the plane projected crack height
K
multiplicative factor
Kx
multiplicative factor in x-direction
multiplicative factor in y-direction
Ky
l
subscript index for local quantity
L
rugged crack length
LBC
rugged crack length measured by box-counting method
lx ; ly ; lz rulers length or scale in the x-direction, y-direction, z-direction, respectively
l0
fractal cell size or minimal crack length in propagation direction
L0
plane projected crack length measured in propagation direction
L0S
saturation plane projected crack length measured in propagation direction
Griffiths critical crack length
L0C
DL
rugged crack length
DL0
distance between two points of the crack (the projected length of the crack)
DL0C
critical crack length
NL
number of units of the crack length in longitudinal or propagation direction
NT
number of units of the crack length in transversal direction
NV
number of units of the crack length in vertical or height direction
number of units of the crack length in the growth direction
Nx
Ny
number of units of the crack length in the perpendicular direction
sat
subscript index indicate saturation
Y0
shape function
x; y; z
spatial coordinates
Dx; Dy; Dz, incremental measure length in x-direction, y-direction, z-direction
Dzx ; Dzy fluctuation or roughness mean squares or incremental measure of crack height in x-direction, y-direction,
respectively
w
width of specimen test
Greek letters
exponent
b
d
incremental measure
@
partial derivative
eL ; eT
horizontal and vertical scale of the fractal scaling
ce ; cp
elastic and plastic specific energy surface, respectively
kx
amplification factor scale in x-direction
234
ky
n
fg ; fl
fx ; fy
rf
t
v
background is associated with the difficulties of making an accurate measurement of the real fracture area. Although there
are several methods capable of quantifying the fracture area, the results are dependent on the size of the ruler of measurement [3], which did not contribute for its insertion in the CFM in the past.
With the increasing interest in fractal theory, it became possible to describe and quantify almost any apparently irregular
structure in nature [4]. In fact, many theories based on Euclidean geometry are being reviewed. It has been experimentally
proved that fracture surfaces have fractal scaling, so the fracture mechanics is one of the scientific areas included in this
context.
The work herein deals with the mathematical description of the roughness of cracks in the fracture mechanics, using the
fractal geometry to model its irregular profiles. Considering that the fracture surface is a record of the information left by the
fracture process, it may be possible to establish a relationship between the topology of this surface and the physical quantities of the fracture mechanics using fractal characterization techniques. Mandelbrot et al. [5] developed the Island Slit
method by searching for correlations between fractal dimensions and well-known physical quantities of fracture mechanics.
Following this pioneering work, other authors also made theoretical and geometrical considerations with a similar purpose
[614], as described briefly below.
1.1. Brief review of fractal scaling models of fracture surfaces
Mosolov [15] and Borodich [14] were the pioneers to associate the strain with the surface energies involved in the fracture process with the roughness exponents of the surfaces produced during the breaking process and the splitting of the
crack surfaces. They related these quantities using the singularity exponent of the stress field at the crack tip and the fractionary dependence of the fractal scaling exponent in fracture surfaces, postulating the equivalence between the changes in
the strain and the surface energies. Bouchaud and Bouchaud [16] proposed an alternative model from Mosolov [15] who
showed fracture parameters in terms of the height fluctuations of the rugged fracture surfaces, whose fluctuations are perpendicular to the crack propagation direction. Bouchad proved the relation between the fracture critical parameters as fracture toughness K IC and the relative fluctuations in the height of the rugged surface. The universality of the roughness
exponent for fracture surfaces had been assumed, as it did not depend on the type of material tested [17]. However, this
assumption generated a lot of controversy [18], which led to the discovery of anomalies [19] in the scaling exponents for
the local and the global scales in the fracture surfaces of brittle materials.
Family and Vicsek [20] and Barabsi and Stanley [21] showed a fractal scaling model for rugged surfaces formed in ballistic deposition films. This fractal scaling model was an inspiration for subsequent models of fractal surfaces present in other
phenomenologies. Since then, the modeling of fracture surfaces was done based on the models of Family and Vicsek [22],
receiving different supplements [19,23,24]. Based on this work, Lpez and Schmittbuhl [25] proposed an analogous model
for the fracture surfaces, which accounted for anomalies in the fractal scaling, with critical crossover dimensions for the transition in the roughness behavior of these surfaces in brittle materials. Morel et al. [26] observed experimental anomalies in
the roughness of wood fracture surfaces, and using the fractal model of Lpez et al. [19], they determined the roughness and
the dynamic exponent values. They also showed that the anomalies could only be explained by a dynamic scaling fractal
model involving local and global roughness exponents [25].
From the initial ideas of Lpez and Schmittbuhl [25] and following their fundamental hypothesis, Morel et al. [27] proposed a GR curve model for fracture surfaces in wood. Morel applied this model to describe the relief presented by the
rugged fracture surfaces whose topology is characterized by local and global roughness exponents, relating them with the
behavior of the elastic energy release rate and fracture resistance, called GR curve [28] for a brittle material. He generalized the Lpez and Schmittbuhl model including situations that have size effect [27].
This present work presents a generalization of the previous models, elaborating a fractal scaling in the longitudinal direction similar to that in the transversal direction for the crack propagation direction in a coherent way. The fractal surfaces
always exceeds the Euclidean dimensions of its projection and does not fulfill the immediately superior Euclidean dimensions in which it is immersed. For instance, a fracture profile has a fractal dimension in the interval 1 6 D 6 2, so it exceeds
the dimensions of a smooth line, but it does not fulfill those of a smooth surface. Morel et al. [24] shows that the fractal nature of a fluctuation Dz in a direction must be scaled using lengths and parameters of the same direction, although there can
be other factors related to the perpendicular direction that can be coupled to the model. In this sense, it is adopted the fol
lowing relationship for the roughness mean square Dzx lx ; x and Dzy ly ; y in the transversal and longitudinal directions,
respectively:
235
if lx Dx
if lx Dx
if ly Dy
if ly Dy
where x; y are the coordinates, lx ; ly are the used ruler lengths, Dx; Dy is the interval of measure of roughness, Dzx ; Dzy is the
height variation in the transversal and longitudinal directions on the fracture surface respectively, and fg ; fl ; t are the global,
local and dynamic roughness exponents, respectively.
It is also shown that from a general and analytical definition of a rugged surface, whose height z f x; y is a fluctuation
function of the coordinates of the mean plane of the projected surface, it is possible to establish a general expression that
involves the local and the global self-affine fractal scaling for the rugged fracture surface.
Many researchers have developed fractal models for the fracture surface, by employing the roughness dimension and
introducing it to the CFM [16,2932]. In particular, the work of Alves [32] introduced a self-affine fractal model of a fracture
surface in the mathematical formalism of the CFM through a local roughness derivative term. However, it lacked a more
detailed explanation about the origin of that model. It is shown in the present paper the basic mathematical premises of this
self-affine fractal model derived from Voss [33], who presented a fractal description for the noise in Brownian motions. To
calculate the rugged dimensions and define the model, the box-counting method is used [34]. A general expression for the
rugged crack length as a function of the projected length and fractal dimensions is shown. Also, a roughness expression is
derived, which can be directly introduced into classical fracture mechanics.
Despite the generality of the model presented in the work herein, applications were focused on brittle material and experimental tests were carried out for its validation. Mortar and heavy clay specimens were prepared under different conditions and
characterized by measuring their modulus of rupture and the rugged crack profile after a 3-point bending test. Obtained results
showed that the fractal dimension was capable of representing the roughness of the fracture surface of the different materials. A
strong correlation between the LipfshitHlder exponent for the longitudinal and the vertical directions, and the sintering temperature were verified on the heavy clay material. The results also showed that the increasing rugged crack length of the profile
of the fractured mortar specimens is well correlated with the increasing water/cement ratio. Overall, the application of the proposed self-affine fractal model was validated for estimating the fracture strength of brittle materials.
2. Analytical model for rough surfaces
Consider a rough surface z f x; y, as shown in Fig. 1.
The area DA of the surface can be parameterized and calculated from Greenberg [35],
DA
DE0 dE0
DE0
DL0 dL0
D L0
s
2 2
@f
@f
1
dxdy:
@x
@y
If this rough surface is discretized with a mesh lx by ly elements with l0 6 lx 6 dL0 and e0 6 ly 6 dE0 , a box-counting method
can be used to define a relationship between the surface height fluctuations and the area within the limits dL0 and dE0 . Thus,
for a non-differentiable rough surface the rough area can be approximately calculated from the following:
DA
since
@f
@x
DE0 dE0
DE0
DDzxx and
DL0 dL0
D L0
@f
@y
s
Dzx x; y 2
Dzy x; y 2
1
dxdy
lx
ly
D zy
.
Dy
s
2
Dz x
Dzy 2
da lx ly 1
lx ly n
lx
ly
It is observed that the term n da=lx ly represents the local roughness of the rugged surface and the whole area DA is given by,
Ny X
Nx
X
DA
daij dL0 dE0
j1 i1
"
y X
Nx
1 X
n
Nx Ny j1 i1 ij
DL
"
#
Nx
Nx
X
1 X
dli dL0
ni
Nx i1
i1
236
Fig. 1. (a) Generic rough surface z = f(x, y); (b) close view of the rough surface limited by dL0 and dE0 .
where fx is the roughness exponent of the surface in direction x and fy is the rough exponent of the surface in direction y. The
self-affinity property allows formulation of Eq. (7) in an uncoupled form and in each perpendicular direction, one has the
following:
zx kx x; y kfxx zx; y
zy x; ky y kyy zx; y
3.1. Computing the area of the rugged fracture surface
The height fluctuations Dzx; y of the fracture surface can be correlated with their fractal behavior in a window of observation in directions x and y in the following manner,
To calculate the area effectively, it is useful to uncouple the mutual dependence of the transversal and the longitudinal
fractal properties of the height fluctuations. The following general scaling relationships for the height fluctuations are proposed, dividing Eq. (9) by the unit scale sizes lx and ly , respectively, one obtains
Dzx lx ;x
lx
Dz
Dzy ly ;y
ly
kxx
lx
Dz
kyy
ly
Dlxz
fx
Dlyz
Dx
lx
fy
Dy
ly
10
237
8
fx
>
< Dlxx
Dzx lx ; x K y
f
>
: Dx gx
if x xsat
8
fy
>
< Dlyy
Dz y l y ; y K x
f
>
: Dy gy
if y ysat
lx
ly
11
if x xsat
if y ysat
12
where K x ; K y are functions that relates the interaction of the roughness of one direction to another direction. Note the cross
terms in this equation where the roughness in one direction affects the roughness in the other direction. Although the model
separates contributions from every direction, the fracture occurs at the same time in both directions. Thus the fibers or particles in the microstructure to break up, suffer local strains that have normal and tangential components affecting perpendicular directions. fgx and fgy are the global rough fractal exponents in directions x and y, respectively.
3.3. Relationship between transversal and longitudinal roughness exponents
As the self-affine crack presents rough exponents with local and global aspects, the following expressions can be used to
account for the roughness transition from local to global scales in x and y directions [24,26,27].
fx fgx flx
13
fy fgy fly
14
Considering, for example, that the crack propagates in y direction, the rough exponent fy differs from fx by a dynamic factor
1=t [22],
238
fy fx =t b
15
8
fgx flx
>
>
< Dl x
x
Dzx lx ; x K y
f
> Dx gx
>
:
if x xsat
8
fgy fly
>
>
< Dl y
y
Dzy ly ; y K x
f
> Dy gy
>
:
if y ysat
16
if x xsat
lx
17
if y ysat
ly
@f
@f
$
@x
@y
18
fgx flx
Dx
lx
fgx
Dx
lx
Kx
ly
$ Klyx
fgx tflx
Dy
ly
fgxt
Dy
ly
if DA0 DA0sat
19
if DA0 DA0sat
1t
Dx
Dy
lx
ly
20
Based on Eq. (19), it is possible to express K x and K y as functions of the same scaling factors and roughness exponents such
as,
Kx K
Ky K
fgx flx
Dx
lx
21
fgx f
lx
t
Dy
ly
Dz x l x ; x K
Dy
ly
8
> Dx
fgx flx
lx >
fgx f
<
t
lx
if x xsat
lx
if x xsat
fgx
>
>
: Dx
22
and
8
fgx flx
t
>
fgx flx >
< Dl y
Dx
y
Dz y l y ; y K
fgy
>
lx
>
: Dy t
ly
if y ysat
if y ysat
23
239
Fig. 3. Scheme of a window lx ; ly on a rough fracture surface showing the minimal crack lengths e0 ; l0 for the transversal and the longitudinal directions.
Height fluctuations also depend on the scaling of vertical direction, suggesting that K depends on scaling between directions z and x and directions z and y of the crack. In this way, to calculate K f h0 ; DH0 as a power law function of parameters
in directions x; y, and z, one must analyze the crack profile on the planes xz or yz, as illustrated in Fig. 4.
Considering square units with sizes l0 h0 , covering the crack length DL0 within the area DL0 DH0 , and e0 h0 , covering
the crack thickness DE0 within the area DE0 DH0 , the number of necessary units to cover the self-affine profile in each
direction is obtained from,
fly
longitudinal
24
flx
transv ersal
25
NL N V
eL
NT NV
eT
where N V is the number of minimal boxes on the z-perpendicular direction to the plane of the crack. flx ; fly is the local roughness exponent, related to the called divider dimension as fl D1D [42], DE0 is the transversal projection of the crack, DH0 is its
vertical projection,
eT and eL are the transversal and the longitudinal scale factors, and e0 6 lx 6 DE0 and l0 6 ly 6 DL0 .
Fig. 4. Self-affine fractal of WeierstrassMandelbrot, where eek 1=4, Dx = 1.5, and H 0:5, is used to represent a fracture profile. Source: Modified from
FAMILY and VICSEK [20, p. 7].
240
Taking a cut plane of the fracture surface in the longitudinal direction the profile of Fig. 4 is obtained. In the profile shown
in Fig. 4, the basic measuring units l0 , and h0 are different in the longitudinal y, and the vertical z directions, respectively.
If h0 is the minimum scaling factor in vertical direction, one has,
NV
DH 0
v ertical
h0
Choosing
26
eL eT and NL NT for counting the number of cells in the profile at the xz and the yz planes, one has
DH 0
DH 0
f
f
eL ly
eT lx
h0
h0
27
fly
flx
DH 0
l0
DH 0
e0
h0
DL 0
h0
DE 0
28
or
Thus,
l0
DL0
e0
DE 0
fflx
ly
29
For each xz and yz plane across the crack surface, there is a projected crack profile. The number of cells covered by the
fractal scaling in each of these planes in the horizontal and the vertical directions is given by,
Nxz
L
Nxz
V
and
Nyz
T
Nyz
V
fy 9
>
=DL fy DH
0
0
>
h0
DH 0
; l0
D L0
l0
30
h0
fx 9
>
=DE fx DH
0
0
;
> e0
h0
DH 0
;
D E0
e0
31
h0
9
DL0
=DL 1=t DE
DhH00 >
l0
0
0
fx
> l
e0
0
DE0
DH 0 ;
h0
e0
fy
32
which is equivalent to Eq. (20). Therefore, from Eq. (31) for K h0 , one has
K DH 0
e0
DE0
flx
33
Substituting Eq. (33) in Eqs. (22) and (23), one can now drop the x subscript of all equations. Therefore the height fluctuations are as follows:
8
fl
fg fl
fg tfl
>
>
@f
Dy
Dx
>
< @x
Dlzx x DlHx 0 DeE00
lx
ly
fl
fg
>
>
>
Dy
Dx
: @f Dzx DH0 e0
lx
lx
lx
D E0
@x
ly
fg fl
t
if x xsat
34
if x xsat
and
8
fl
fg fl
fg tfl
>
Dz
@f
Dy
>
Dx
< @y
lyy DlHy 0 DeE00
ly
lx
if y ysat
fg
>
>
: @f Dzy DH0 e0 fl Dx fg fl Dy t
lx
ly
ly
DE0
@y
ly
if y ysat
35
Substituting Eqs. (34) and (35) in Eq. (3) for lx e0 and ly l0 , the area DA is given by:
8
s
>
2
2fl
2fg fl
2fgtfl
2
>
> R DE0 dE0 R DL0 dL0
DH 0
DH0
e0
Dy
Dx
>
>
2
2fl
2fg fl
2ftg
>
2
R
R
>
e0
Dy
>
Dx
> DDEE0 dE0 DDLL0 dL0 1 DlH0 DeH0
dxdy
if DA0 DA0sat
:
e0
DE0
l0
0
0
0
0
36
241
This equation is in agreement with the model presented by Morel et al. [24] and can be seen as a
generalization.
Alternatively, Eq. (36) for the rugged area can be rewritten like,
8
s
>
2
2fl
2fg fl
2fgtfl
2
>
>
DH 0
DH 0
e0
D E0
D L0
>
D
A
if DA0 DA0sat
>
l0
e0
DE0
e0
l0
< 0
DA
s
>
2fg
>
>
> DA 1 DH0 2 DH0 2 e0 2fl DE0 2fg fl DL0 t
>
if DA0 DA0sat
: 0
l0
e0
DE0
e0
l0
37
8
s
>
2
2fgtfl
2
>
>
DH 0
DH 0
DL0
>
D
L
if DL0 DL0s
>
< 0
l0
e0
l0
DL
s
>
2fg
>
>
> DL 1 DH0 2 DH0 2 DL0 t
>
if DL0 DL0s
: 0
l0
e0
l0
38
Observe that the lengths DL0 and DH0 are not necessarily equal and correspond to the projected lengths of the crack, in the
horizontal and the vertical directions, respectively.
To describe a growing crack, one can define a fixed origin coincident with the crack onset at the left (or right) side of the
counting box. The size of the counting box can be adjusted to cover the growing crack. This is the basis of the sand-box
method [41] for crack length measurement. Mathematically, this is defined with DL L; DL0 L0 and the rugged length
is given by,
8 s
>
2
2fgtfl
2
>
>
DH0
L0
>
DeH00
if L0 L0s
>
< L0 1
l0
l0
L
s
>
2
2ftg
>
2
>
L0
>
> L0 1 DlH0 DeH0
if L0 L0s
:
l0
0
0
39
Applying the logarithm on the both sides of Eq. (39) one obtains an expression that relates the fractal dimension to the projected crack length:
Df
8
>
>
>
>
>
>
>
<1 1
ln L=l0
ln L0 =l0 >
>
>
>
>
>
>
:
(
ln
(
ln
1 12
DH0
l0
DH 0
e0
ln L0
DH0
l0
DH 0
e0
ln L0
2
2fgtfl
L0
l0
2
2ftg
if L0 L0s
40
L0
l0
if L0 L0s
It is important to point out that DL0 denotes the projected distance between two points of the crack (the projected crack
length) and l0 is the minimum possible length of a microcrack, which defines the scale l0 =L0 under which the crack profile is
scrutinized.
Fig. 5 shows the influence of the height DH0 of the box on the rugged crack length measure, as a function of the projected
length L0 , for L0 L0S and characteristic values for the parameters fl 0:8; fg 1:2; t 4:0, and l0 0:1. Considering a
fixed roughness exponent fl 0:8, a linear relationship between L and L0 is seen in lower boxes DH0 ! 0, while in higher
boxes DH0 ! 1 a nonlinear one is observed.
Fig. 6 shows the influence of the roughness dimension of the rugged crack length, as a function of the projected length L0 .
Observe that for fl ! 1, which corresponds to a flatter profile, the relationship between the rugged and the projected lengths
is more linear. Whereas for fl ! 0, corresponding to a more rugged profile, the relationship between the rugged and the projected lengths is increasingly nonlinear.
In near-flat cracks, the box height can be chosen as DH0 l0 e0 , and Eq. (39) simplifies to,
8 s
>
2fgtfl
>
>
L
>
>
if L0 L0s
< L0 1 2 l00
L
s
>
>
2ftg
>
>
>
if L0 L0s
: L0 1 2 Ll00
41
242
Fig. 5. Rugged length, L as a function of the projected length, L0 and the varying the box height, DH0 , width l0 0:1, representing the box height (rectangular
box DL0 DH0 with local roughness dimension, fl 0:8, global roughness dimension fg 1:2, and dynamic exponent, t 4:0.
Fig. 6. Rugged length L as a function of the projected length L0 and the varying the local roughness dimension, fl representing the box height for flat cracks
with rectangular boxes DH0 1:0; l0 0:1, global roughness dimension, fg 1:2, and dynamic exponent, t 4:0.
In analogous way to the case of Eq. (39), i.e., applying the logaritm on the both sides of Eq. (41) one obtains an expression
that relates the fractal dimension to the projected crack length,
Df
8
>
>
>
>
>
>
>
>
<1 1
2
ln L=l0
ln L0 =l0 >
>
>
>
>
>
>
>
:1 1
2
"
ln
2fgtfl
12
ln L0
"
ln
2fg
12
L0
l0
if L0 L0s
42
L0
l0
ln L0
if L0 L0s
In the study of a self-affine fractal, two limits can be verified. The first is called local limit, when the height of the boxes
is increased compared to its length DH0 ! L0 . The second is the global limit, when the height of the boxes is small compared to its length DH0 ! h0 . These limits are presented as follows.
243
3.7. Case 1: The initial apparent self-similar limit of the local fractality
The local self-similar limit of the crack fractal measure can be obtained from Eq. (39), considering DH0 L0 l0 ,
L L0
1fg tfl
l0
L0
43
It is a self-similar relationship between the projected crack length Lo and the height ho of the unit box. This expression shows
that all self-affine crack fractals can represent a local self-similarity when the square areas L0 L0 are considered instead of
the rectangular ones L0 DH0 . This is commonly observed in the onset of cracks [12,13,43], where one can extract the following result,
fg fl
L
fg fl
L0
l0
1
cte
44
L L0
45
Ductile materials presenting a higher fractality possess a crack profile that can be better adjusted by Eq. (43), while brittle
materials presenting a lower fractality are better adjusted by Eq. (45), which is closer to the classical fracture mechanics
model with a flat fracture profile.
3.9. The roughness of a fracture profile
The classical definition of roughness in the fracture mechanics is given by n L=L0 [2,3]. Alternatively, a local roughness is
defined in this work considering a limiting approach for the counting box dimensions,
n lim
DL0 !l0
46
In practice, Eq. (46) can be seen as the derivative of the rugged length L f L0 with respect to its projected length Lo , written
as
dL
dL0
47
This definition provides a full characterization of fractal profiles and can be useful to describe the crack growth phenomena.
Eq. (47) can be used to calculate the local roughness of the profile, if an expression that relates the rugged length L to the
projected length L0 is known. For instance, for the monofractal case with a square counting box, the measure of the rugged
crack length is given by Eq. (39). Therefore, the expression for the local roughness is given by,
v
2
2fgtfl
u
DH 0
L0
2 2fgtfl
u
fg fl
l0
l0
DH 0
L0
t
s
n 1
P1
l0
l0
t
2
2fgtfl
DH 0
L0
1 l0
l0
48
or simply
1
n
fg fl
2fg fl
2
t
DH 0
L0
1
t
l0
l0
s
P1
2
2fgtfl
DH0
L0
1 l0
l0
49
244
Table 1
Weight proportions of cement, sand and water used for molding the mortar
specimens.
Mortar type
Number of specimens
A1, A2, A3
B1, B2, B3
C1, C2, C3
D1, D2, D3
1:1:0.30
1:2:0.45
1:3:0.60
1:4:0.75
3
3
3
3
Table 2
Average modulus of rupture of mortar specimens obtained after seven days
curing.
Modulus of rupture (MPa)
Mortar type
Number of specimens
Average stress
Error
A1, A2, A3
B1, B2, B3
C1, C2, C3
D1, D2, D3
3
3
3
3
9.6
7.8
6.3
4.6
0.7
0.9
0.2
0.5
Table 3
Heavy clay specimens prepared with different sintering temperatures.
Specimen type
Number of specimens
800
900
1000
30
30
30
Table 4
Average modulus of rupture of heavy clay specimen types.
Modulus of rupture (MPa)
Specimen type
Number of specimens
Average stress
Error
30
30
30
2.0
4.2
9.0
0.2
1.3
1.0
245
5. Experimental results
The proposed fractal model was used to describe the roughness of ruptured mortar and heavy clay specimens.
The following specimens had their two sides modeled: mortars A2; B2; C1; D2 and heavy clay Ar8; Br3; Cr25. For each profile, the roughness dimensions were obtained applying the box-counting and sand-box methods and fitting the proposed
monofractal model given by Eq. (39). These results are listed in Table 5, represented by DBC ; LBC ; L0 ; L0s and Table 6 repre-
Fig. 7. Fracture profile of mortar specimen D2 side 1: digital images side by side and crack profile from processed image with a comparative total ruler
length equal to 1.0 mm.
Fig. 8. Fracture profile of mortar specimen D2 side 2: digital images side by side and crack profile from processed image with a comparative total ruler
length equal to 1.0 mm.
246
Fig. 9. Fracture profile of heavy clay specimen Ar8: digital images side by side and crack profile from the processed image with a comparative total ruler
length equal to 1.0 mm.
sented by DH0 ; l0 ; fl ; fg ; b and t. The fitting parameters L0 40 mm for mortar and L0 4 mm for heavy clay ceramic, l0 and fl
in Eq. (39) are also shown in Table 6.
Despite the different roles in the morphological description of the fracture surface in x and y directions, experimental
measurements showed that the roughness in these two directions has similar scaling properties for very different materials
[48]. A unique roughness exponent is then generally considered and it has been claimed that it has a universal value of
fl 0:8 [17]. This behavior has been confirmed for a large variety of experimental situations [23,49]. However, other studies
have also shown that a different value for fl 0:5 may be applicable [5052]. These two values of the roughness exponent
are connected to the length scale at which the crack is examined. In particular, at small length scales, one observes a roughness exponent fl 0:5, whereas at large length scales, the larger value fl 0:8 is found. Results presented in Table 6 show
rough exponent values between 0.59 and 0.99.
The value of l0 for mortar D2 specimen is very small because its roughness global dimension is very next of unity. This
means that the crack profile is almost a straight line. In this case a straight line can be scrutinized by any l0 value that is
infinitely small.
Fig. 11 shows the asymptotic behavior of the fractal dimension with the growing crack length L0 , measured with sand-box
method. The local L0 L0S and global L0 L0S ranges are depicted in the figure.
In Figs. 12 and 13, a good agreement is observed in the curve fitting of Eq. (40) to the fractal analyses of the mortar specimen A2 side1 and the heavy clay specimen A8, respectively.
In Figs. 14 and 15, a good agreement is observed in the curve fitting of Eq. (39) to the fractal analyses of the mortar specimen A2 side1 and the heavy clay specimen Ar8, respectively.
In Figs. 16 and 17, a comparison of the rugged length L projected length L0 of each crack profile is made for mortars and
heavy clay, respectively.
The general behavior is consistent within each group of results. This trend is observed in the LBC =L0 ratios in Table 5.
In Fig. 18, the local roughness dL=dL0 was plotted versus the square value of the modulus of rupture r2f , for the mortar
specimens. A linear trend can be observed where the values plotted are correlated for a R-square correlation coefficient of
0.7012.
247
Fig. 10. Fracture profile of heavy clay specimen Br3: digital images side by side and crack profile from the processed image with a comparative total ruler
length equal to 1.0 mm.
Table 5
Results from fractal analysis using box-counting method of brittle specimens.
Specimen
DBC
LBC (mm)
L0 (mm)
LBC =L0
L0s (mm)
Mortar A2 side 1
Mortar A2 side 2
Mortar B2 side 1
Mortar B2 side 2
Mortar C1 side 1
Mortar C1 side 2
Mortar D2 side 1
Mortar D2 side 2
Heavy clay Ar8
Heavy clay Br3
Heavy clay Cr25
1.0500 0.0001
1.0534 0.0001
1.0431 0.0005
1.0380 0.0001
1.0607 0.0003
1.0504 0.0001
1.0240 0.0002
1.0514 0.0001
1.1511 0.0004
1.2292 0.0001
1.1627 0.0001
59.2064 0.0001
61.0022 0.0002
65.8381 0.0003
58.5383 0.0002
67.1098 0.0008
72.9876 0.0004
69.3074 0.0003
73.6647 0.0005
11.4017 0.0003
12.7726 0.0002
13.7940 0.0008
37.2288 0.0001
39.1765 0.0006
38.2453 0.0001
37.8984 0.0001
35.3309 0.0008
40.0000 0.0003
40.0000 0.0003
38.3006 0.0005
3.5490 0.0004
3.950 0.001
3.7148 0.0004
1.59034
1.55711
1.72147
1.54461
1.89947
1.82469
1.73269
1.92333
3.21282
3.23357
3.71326
3.616 0.001
3.0123 0.0003
8.5710 0.0003
8.7261 0.0003
9.9510 0.0006
13.700 0.001
12.1460 0.0004
8.2860 0.0002
0.5400 0.0004
0.0728 0.0001
0.7232 0.0003
In Fig. 19 it is shown the increasing water/cement ratio in the mortar specimens in function of the decreasing modulus of
rupture. Comparing this result with Fig. 18 it is observed that the water/cement ratio affects directly the roughness of the
fracture profile. The nonlinear fitting of this curve shown a result given by the following equation:
50
r2f 237:59 GPa2 , a 3:1205 and x = water/cement ratio for a R-square correlation coefficient value of 0.9515.
248
Table 6
Results from fitting the model for brittle specimens.
Specimen
DH0 (mm)
l0 (mm)
fl 1=DD
fg
b
Mortar A2 side 1
Mortar A2 side 2
Mortar B2 side 1
Mortar B2 side 2
Mortar C1 side 1
Mortar C1 side 2
Mortar D2 side 1
Mortar D2 side 2
Heavy clay Ar8
Heavy clay Br3
Heavy clay Cr25
0.3740 0.0003
0.3635 0.0001
0.7071 0.0001
0.3040 0.0003
0.84250 0.0003
0.83470 0.0004
1.4160 0.0001
1.4618 0.0003
4.1542 0.0003
1.6998 0.0001
3.2733 0.0001
1.3249 0.0004
2.2526 0.0003
0.0800 0.0003
0.7610 0.0001
0.8261 0.0001
0.0623 0.0004
(1.6040 0.0001)E6
(3.75 0.0001)E10
0.1376 0.0003
0.3641 0.0001
0.1555 0.0001
0.800 0.001
0.800 0.001
0.5954 0.0001
0.6148 0.0001
0.8613 0.0001
0.8705 0.0001
0.9927 0.0001
0.9854 0.0001
0.7062 0.0001
0.7322 0.0001
0.6579 0.0001
1.0652
1.0652
1.109095
1.051606
1.0000
1.0000
1.0016
1.0031
1.179023
1.171628
1.197972
0.86097
0.92510
0.402303
0.96519
2.233964
2.294475
1.321737
1.257799
0.287048
0.091712
0.227454
0.0991 0.0001
0.0997 0.0001
0.1945 0.0001
0.3555 0.0001
0.0621 0.0001
0.0564 0.0001
0.0067 0.0001
0.0141 0.0001
0.1531 0.0001
0.1554 0.0001
0.1829 0.0001
Fig. 11. Determination of crack length saturation by fractal analysis of mortar specimen A2 side 1 fractal dimension projected length, L0 .
Fig. 12. Fractal analysis of mortar specimen A2 side 1 fractal dimension, D versus projected length, L0 . Source: 2012 Alves LM. Published in [short
citation] under CC BY 3.0 license. Available from: http://dx.doi.org/10.5772/51813 [52, p. 61].
249
Fig. 13. Fractal analysis of heavy clay specimen Ar8 side 1 fractal dimension, D versus projected length, L0 . Source: 2012 Alves LM. Published in [short
citation] under CC BY 3.0 license. Available from: http://dx.doi.org/10.5772/51813 [52, p. 61].
Fig. 14. Fractal analysis of mortar specimen A2 side 1 rugged length, L versus projected length, L0 . Source: 2012 Alves LM. Published in [short citation]
under CC BY 3.0 license. Available from: http://dx.doi.org/10.5772/51813 [52, p. 61].
6. Discussion
6.1. The relation with the LopezMorel fractal model of fracture surface
Morel et al. [24,2628] describe the variations of roughness with the distance x measured from the notch in the transversal direction to the crack propagation. In fact, observing the microstructural aspects of rugged fracture surfaces of woods
used in their work [53], it appears as a wave beach or as a brazilian roof, where in the direction of crack propagation
there are almost no fluctuations in the height of the rugged surface. In spite of this fact, to adapt his scaling to the experimental reality, prefactors A and B were presented whose nature depends on the material and are obtained by fitting of experimental curves. This means that if the material to be modeled presents fluctuations of height in the growth direction, these
prefactors must be explained mathematically in terms of the relations of fractal scaling for the distances of rugged length in
250
Fig. 15. Fractal analysis of heavy clay specimen Ar8 rugged length, L versus projected length, L0 . Source: 2012 Alves LM. Published in [short citation]
under CC BY 3.0 license. Available from: http://dx.doi.org/10.5772/51813 [52, p. 61].
Fig. 16. Comparative plot of the rugged crack length, L projected crack length, L0 for the sides A and B among main mortars specimen profiles.
the direction parallel to the crack growth. The model represents the dependencies in the transversal x and the longitudinal y
directions in a unique mathematical term.
However, for materials such as glass, alumina and mortar, that present fluctuations in the transversal and the longitudinal
directions, the model cannot portray authentically the fluctuations in the height observed in the fracture surface of these
materials in both directions.
The work herein, it has been shown that the dependence of the fluctuations in the height Dzxt ; yt can be decoupled
and written in a simple way as,
Dzxt; yt f xt
g yt
51
without changes in the final result and obtaining the Morels model [24,2628] as a particular case.
From Eq. (36), it is possible to reduce dimensionally the model of a fracture surface proposed by Morel et al. [24,2628] to
a fracture profile model, neglecting the fluctuations of the roughness in the transversal crack propagation direction, as in the
case of wood fracture surfaces considering a fracture propagation in the transversal direction to the fibers. In that case the
fracture surface is given by:
251
Fig. 17. Comparative plot of the rugged crack length, L projected crack length, L0 among main heavy clay specimen profiles.
Fig. 18. Plot of square of modulus of rupture versus the derivative of the rugged crack length, dL=dL0 .
8
s
>
2
2fl
2fg fl
2fgtfl
>
R
R
>
D
E
dE
D
L
dL
e0
Dy
0
0
0
0
>
Dx
>
1 DeH00
dxdy if DA0 DA0sat
< DE0
DL0
lx
DE0
ly
DA
s
>
>
2
2fl
2fg fl
2ftg
>
> R DE0 dE0 R DL0 dL0
e0
Dy
Dx
>
1 DeH00
dxdy
if DA0 DA0sat
: DE0
DL0
lx
DE0
ly
52
where DA0 dL0 dE0 and DA0sat L0s E0 . For minimal subdivisions of the profile in the transversal and the longitudinal directions, i.e., lx e0 and ly l0 , Eqs. (34) and (35) are rewritten as,
Dz
f f
fl
fg fl Dy
g t l
>
>
Dx
< DeH0 DeE0
e
l
0
fg
>
>
: DH0 e0 fl Dx fg fl Dy t
e0
DE0
e0
l0
53
252
Fig. 19. Plot of modulus of rupture versus the water/cement ratio for a mortar cured by seven days.
8
s
>
2
2fl
2fg fl
2fgtfl
>
R
>
D
L
dL
e0
DE0
Dy
0
0
>
>
1 DeH00
dy if DA0 DA0sat
< dE0 DL0
D E0
e0
l0
DA
s
>
>
2
2fl
2fg fl
2ftg
>
R DL dL
>
e0
DE0
Dy
>
dy
if DA0 DA0sat
: dE0 DL00 0 1 DeH00
D E0
e0
l0
54
Eq. (52) is analogous to the approximations presented by Morel et al. [24] considering the crack propagation direction as
being the y direction and the constants A; B, and ny in their equation given by,
A DeH00
B
e0
D E0
fl
fg fl
1
e0
E0
55
1=t
ly
ny E0
1=t
Dy
ly
The saturation length of the fracture surface in the transversal crack propagation is given by,
nysat E0
Dy
L0S
1=t
E0
56
253
The local and the global roughness dimensions determined in this work, for the mortar and the heavy clay specimens, are
compatible with results in the literature [24,2628,30,31,52,53]. However, for some specimens, the values seem to exceed
the expected number, as in the case of mortar C1 (13.699 for the sides 1 and 2) and D2 (12.1456 for the sides 1 and 2).
The fractal box-dimension, DB shown in Table 5 compared to the rugged global dimension, fg in Table 6 presents compatibles results one with other. The mortar fractal dimensions are in the interval between 1.0 and 1.1 and the heavy clay has its
fractal dimension in the interval between 1.15 and 1.23. This results is in agreement with the more rugged aspect of the
crack in the heavy clay as shown in Figs. 9 and 10. Therefore, it is possible to distinguish mathematically a crack in this
two materials using its geometrical characteristics which can be portraited by different values of the exponents in the relations (39) and (41).
A linear relation is observed between the square of modulus of rupture r2f and the values of the local roughness of the
crack given by n dL=dL0 , for the mortar specimens, as shown in Fig. 18. A linear fitting is shown in that figure. Observe that
the data more below of the linear fitting presented a constant displacement compared to data closer to the straight line. Thus
it was due to systematic deviation of the points in the roughness values.
Some authors [20,22,42,50,53] suggest a relation between the local, global, and Hurst exponents, for the tridimensional
case, such as:
1H
3b
;
2
57
3 fg fl =t
1H
2
58
and one finds an approximate relation for the dynamic exponent t given by:
t
fg fl
1 2H
59
If the local roughness dimension fl is equal to Hurst exponent H 2 DB 1=DD where DB is the box-dimension and DD is
the divider dimension. Then one has the following relation between the obtained exponents,
fg fl
1 2fl
60
fg fl 1 H
61
t
where
and
t
1H
1 2H
62
Values presented in Table 6 were derived from this expression. Values of t are lower than those in the literature. This was
expected as the tests were conducted to a fast rupture instead of crack growth.
6.3. Mechanical results
The increasing water/cement ratio in the mortar specimens resulted in a decreasing modulus of rupture as shown in
Fig. 19. Comparing this result with Fig. 18 it is observed that these results are also well correlated with the roughness of
the crack profile.
In Tables 3 and 4 for heavy clay, the increasing sintering temperature resulted in higher modulus of rupture. However, the
roughness cannot be associated due to the small number of temperatures values of tested specimens.
From the digitalized images of mortar and heavy clay, it can be observed that the fracture surface of the heavy clay presented bigger tortuosity compared to the mortar material. This is also evident in the fitting results where the rugged length is
near 3.5 times the projected length for heavy clay, and only 1.7 for mortar.
It can also be seen in Figs. 14 and 15 that for each type of material the slopes of the asymptotic curves are in very close
agreement with the model proposed.
This work presents several future perspectives in terms of correlating the rugged profiles with the material granulometry,
chemical composition, and cement curing time. The mathematical model can still be explored for understanding the minimal
crack length and the fractal dimension according to the mechanical testing parameters and material properties.
254
7. Conclusions
A general self-affine fractal model was presented and applied to brittle fracture surfaces. From the proposed equation, an
analytical expression for the rugged profile length was derived. Also, an analytical expression for the local roughness was
derived, which can be directly introduced into the classical fracture mechanics.
Comparing the fractal box-dimension, DB shown in Table 5 and the rugged global dimension, fg shown in Table 6 for the
mortar and heavy clay it was possible to distinguish mathematically a more rugged crack in this two materials using its geometrical characteristics which can be portraited by different values of those exponents in the relations (39) and (41).
The small ratio between roughness dimension for transversal and longitudinal directions, t, presented in Table 6 and
given by Eqs. (15), (60) and (62) shown that these two directions are weakly coupled for the analyzed materials, mortar
and heavy clay.
The rugged crack length is a response to the interaction of the crack tip with the microstructure of the material. By the
model presented in work herein it is possible mathematically to portray the peculiar rough behavior of a crack in Portland
cement mortar and red ceramics using fractal geometry.
The experimental technique of obtain crack profiles, proved very able to present satisfactory results that are very close to
reality.
A good agreement between the fractal model and the experimental results was observed. A strong correlation between
the fractal dimension and the sintering temperature was verified. The results also showed that the increasing rugged crack
length of the profile of the fractured mortar specimens is well correlated with the rising water/cement ratio.
Acknowledgments
The authors acknowledge contributions of Interdisciplinary Laboratory of Ceramic Materials LIMAC-CIPE-UEPG, Prof.
Dr. Vicente Campitelli (Civil Engineering Laboratory) and PIBIC/CNPq/UEPG.
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