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4.0
FLUID SAMPLING
Introduction
The overall quality of the PVT data and subsequent engineering calculation are
depending on the quality of the fluid samples originally collected from the
reservoir. For a proper PVT study, the collection of the reservoir fluid samples
must be conducted at the condition where the reservoir pressure still above the
saturation pressure. Therefore, it is usually essential that the reservoir fluid
samples to be collected immediately after the hydrocarbon discovery. A proper
well conditioning and sampling method for different type of reservoir fluid need to
consider prior to sampling.
In this section, we will discuss about two sampling points/methods i.e.
4.1
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Highly under saturated oil reservoirs where the produced fluids remain in a
single phase under any flowing conditions (including surface conditions) are
relatively easy to sample at the wellhead.
An oil reservoir at or slightly above the bubble point will yield free gas at the
bottom hole flowing pressures and require conditioning prior to sampling.
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If oil and gas samples are taken at the surface, it is vital that the production
rates and gas-oil ratio be accurately determined in order to recombine the
separator liquid and separator gas to a correct ratios to formulate a
representative reservoir fluid sample. If the well is not producing with stable
GORs, or if separation facilities are not adequate for accurate measurements,
a surface recombination sample should not be considered.
Flowing wells are the best candidates for fluid sampling. Production rates are
more easily controlled on flowing wells, and measuring the bottom hole
pressure is impractical on a pumping well. It is obvious that wells on
continuous gas lift are unsuitable for surface sampling procedures. However,
if a gas-lift well will flow at low rates on its own, it may be conditioned and
samples the same as any flowing well.
The wire line subsurface sampling tool is not extremely large, but may be
unsuitable in wells with tubing restrictions (subsurface safety valves, down
hole chokes etc.) or twisted tubing. Any completion equipment that prohibits
the sampler from reaching the producing interval will complicate the
subsurface sampling procedure.
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Wells located on offshore caissons without deck space or wire line equipment
will require special equipment for subsurface sampling work. Wells such as
these often have their production commingled at common separation
facilities, and special care must be taken to ensure that surface separator
samples are representative of the desired well.
4.1.3
Well conditioning
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impractical long time. Replacing the tubing with a smaller diameter string can
sometimes increase the flow velocity enough to eliminate heading at low
rates.
The well also condition by flowing at successively lower flow rate and monitor
the GOR. The GOR should generally decrease as the rate is decrease. This
is because the lower rate results in a lower drawdown, which brings the well
bore pressure back out of the two phase region. The heavier hydrocarbon will
be produced rather than condense in the reservoir, thus increasing the liquid
volume at the surface and decreasing the GOR. When the GOR stabilized,
the well has been conditioned for sampling.
The duration of the conditioning period depends upon the volume of reservoir
fluid that has been altered as a result of producing the well below the bubble
point pressure, and how quickly it can be produced at low rates. Most oil wells
that have not been produced for a long period of time require little
conditioning; however, some wells may require up to a week of conditioning
to achieve stable GORs.
During the conditioning process, the following records should be taken:
a)
b)
c)
d)
e)
f)
g)
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4.2
Sample Collection
Figure 4.5 to 4.8 is the summary of test program for different types of reservoir
fluid.
4.2.1
Procedure
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The specific procedure to follow for bottom hole sampling includes the following
steps.
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samples will be important in optimizing the sampling program if the well would
be drill stem tested. The logs and WFT sample will help the following:
The main problem with the wire line sampling is the limited possibilities to clean
up the formation from mud filtrate, especially if oil based mud (OBM) has been
used. The later generation of wire line formation samplers has a pump out
capability and detection system that can monitor the change in the mud filtrate
contamination of the samples. This has increased the quality of formation fluid
samples taken in open holes.
If the well has been drilled with oil based mud, the samples will be contaminated
with the based oil filtrate. The contamination level will be determined by number
of factors:
Formation permeability
The volume pumped from the formation before the sample is collected.
The seal obtained by the probe against the formation.
The contamination of OBM in the wire line sample can be reduced by pumping
fluid from formation before the sample is closed in. The use of an optical detector
system that can tell the relative changes in the contamination level during the
clean up.
The OBM contamination level will be higher for a low formation reservoir.
It is not feasible to obtain a clean sample from a tight reservoir.
Oil systems are less affected by OBM contamination than condensate and higher
contamination level can be accepted without dramatically changing the main fluid
properties. There will be effect on bubble point pressure, oil formation volume
factor, density and viscosity.
The effect of OBM on gas condensates depend on the relative difference in the
molecular weight distribution of the C7 plus fraction of the OBM and the pure
condensate. If the OBM contamination has higher carbon number components
than in the reservoir fluid, the effect on the dew point pressure of the samples
can be very significant even for a very small contamination.
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The quality of the wire line sample should be assessed at surface and decision
made to whether the objective regarding samples has been reached or if further
sampling is needed by more WFT or by DST testing. If no information is available
from comparable wells the decision has to be based on the following:
1. The samples give consistent bubble point pressure.
2. The reservoir fluid density consistent with the measured pressure gradient
3. Acceptable contamination level of OBM
For oil close to or at saturation pressure it has been shown that surface sampling
techniques are more likely to give representative samples than the use of bottom
hole technique.
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The quality of the bottom hole sample will be evaluated from the measured
saturation pressure at reservoir temperature. The saturation pressure has to be
below the reservoir pressure. Duplicate samples should always be taken in the
sampling run. The samples should give consistent saturation pressure in order to
define as a good sample. The sample is considered suspect when the measured
saturation pressure is equal or above the flowing pressure at the sampling point.
In the case of a sample for asphaltene studies, the bubble point pressure
measurement will be conducted on the small portion of the fluid.
Note: The test separator GOR measured during the bottom hole sampling flow
will usually not be accurate due to the low flow rate.
4.2.2
Surface sampling
A large volume of both oil and gas are required for analysis
The fluid at the bottom of the well is not representative of the reservoir
fluid (i.e. gas condensate reservoirs and oil reservoirs producing large
quantities of water)
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Method 1.
Method 2.
c)
Method 3.
a)
Method 1
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with
with
This method requires the connecting line between the separator and sample
container be purged with gas, and then the gas be allowed to flow into the
container until the desired pressure is reached. Although this method requires an
evacuated container, it is recommended method for gas sampling.
Pressure on the container should be checked prior to sampling to ensure that a
vacuum exists.
b)
Method 2
This method requires the container be filled and emptied with separator gas
several times in order to purge air in the container. The number of recommended
successive purge cycles is inversely proportional to the separator's maximum
gas pressure.
c)
c)
Method 3
Method 3
This method requires that a two-valve sample container be filled with a liquid,
preferably mercury or salt water (glycol or water may also be used).The container
is kept vertical while the upper valve is connected to the separator and the lower
valve is opened to withdraw the liquid. When all the liquid is displaced, the valves
are closed and the container is removed for shipment.
Several problems may be encountered during gas sampling, including:
a)
Corrosive gases such as H2S or CO2 are easily absorbed by water and will react
with steel containers. If such gases are present, the liquid displacement method
should not utilize water, brine or glycol. Additionally, the gas should be dried by
passing it over a suitable drying agent (such as anhydrous calcium sulphate).
Non-metal cylinders should be used if gas is suspected to contain H2S or CO2.
c)
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Requires that a sample container with a capacity of about 700 cm3, be filled with
a liquid (brine, glycol or water) and connected to the separator as per Figure 2.
After purging the sampling line, top cylinder valve is opened to allow the
container to come to separator pressure. Then bottom cylinder valve is slowly
opened to allow the oil to flow into the container and displace the resident liquid
with minimum pressure reduction. When the desired sample volume is collected,
bottom valve is closed, followed by top valve. A vapor space is left in the
container by withdrawing an additional 10% of the displacement fluid. The
container is disconnected, checked for leaks and tagged for shipment.
The method has the objective of obtaining a sample of separator oil with no loss
of dissolved gas and with no contamination by extraneous gases or liquids. All
connections used to conduct fluid from the separator to the sample container
must be purged with separator oil to avoid contamination.
Several problems can occur during oil sampling, including these possibilities:
H2S and CO2 can react with water and attack the container walls.
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Dry gas wells and oil wells that flow under saturated liquid at the surface
may be sampled at the wellhead using these surface sampling techniques,
provided the pressure rating of the sample containers is sufficient to
permit such a procedure.
4.3
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4.4
Summary
a)
b)
c)
4.5
References
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