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Metallography
Applications
Ashraf Ali
NED University of Engineering and Technology, Karachi
1
Macro Examination
Macro-etching is the procedure
in which a specimen is etched
and evaluated macro
structurally at low
magnifications. It is a frequently
used technique for evaluating
products such as billets, bars,
blooms, and forgings.
Macro Examination
Macro-etching is the procedure
in which a specimen is etched
and evaluated macro
structurally at low
magnifications. It is a frequently
used technique for evaluating
products such as billets, bars,
blooms, and forgings.
Macro Examination
Macro-etching of Steel Ingot
Macro Examination
Macro-Examinations are also performed on a
polished and etched cross-section of a welded
material.
During the examination, a number of features
can be determined including weld run
sequence, important for weld procedure
qualifications tests.
Slag, porosity, lack of weld penetration, lack of
sidewall fusion and poor weld profile are
among the features observed in such
examinations.
It is normal to look for such defects either by
standard visual examination or at magnifications
of up to 50X.
It is also routine to photograph the section to
provide a permanent record. This is known as a
photomacrograph.
Micro Examination
This is performed on samples either cut to
size or mounted in a resin mold.
The samples are polished to a fine finish,
normally one micron diamond paste, and
usually etched in an appropriate chemical
solution prior to examination on a
metallurgical microscope.
Micro-examination is performed for a
number of purposes, the most obvious of
which is to assess the structure of the
material.
Weld Microstructure
Weld
Heatd
Affected
Zone
(HAZ)
Base Metal
Fig. 30 Microstructure of 7-Mo PLUS duplex stainless steel (Fe-<0.03%C-<2%Mn-27.5%Cr4.85%Ni-1.75%Mo-0.25%N) welded with Nitronic 50, etched with Beraha's BI reagent, and
viewed with brightfield illumination. Ferrite is colored, and austenite is unaffected. The
magnification bar is 200 m long.
Micro Examination
It is also common to examine for metallurgical anomalies such as third
phase precipitates, excessive grain growth, etc.
Many routine tests such as phase counting or grain size determinations
are performed in conjunction with micro-examinations.
Micro Examination
Revealing -ferrite in
Martensitic Stainless Steel
Nodular
Cast Iron
Nodular
Cast Iron
Weld Examination
Metallographic weld evaluations can
take many forms.
In its most simple form, a weld deposit
can be visually examined for large scale
defects such as porosity or lack of
fusion defects.
On a micro scale, the examination can
take the form of phase balance
assessments from weld cap to weld root
or a check for non-metallic or third
phase precipitates.
Examination of weld growth patterns is
also used to determine reasons for poor
mechanical test results.
For example, an extensive central
columnar grain pattern can cause a
plane of weakness giving poor charpy
results.
Case Depth
Case hardening may be defined as a process for
hardening a ferrous materials in such a manner
that the surface layer (known as the case), is
substantially harder than the remaining materials
(known as the core).
This process is controlled through carburizing,
nitriding, carbonitriding, cyaniding, induction and
flame hardening.
The chemical composition, mechanical properties,
or both, are effected by these practices.
Methods for determining case depth are either
chemical, mechanical or visual and should be
selected on the basis of specific requirements.
Decarburisation Measurement
This method is designed to detect
changes in the microstructure,
hardness, or carbon content at the
surface of the steel sections due to
carburization.
The depth is determined as the depth
where a uniform microstructure,
hardness, or carbon content, typical of
the interior of the specimen is
observed.
This method will detect surface losses
in carbon content due to heating at
elevated temperatures, as in hot
working or heat treatment.
Coating /
Plating Evaluation
A coating or plating application is used primarily for
protection of the substrate.
The thickness is an important factor in the
performance of the coating or plating.
A portion of the specimen is cut, mounted
transversely, a prepared in accordance with
acceptable or suitable techniques.
The thickness of the cross section is measured with
an optical microscope.
When the coating or plating is thinner than .00020",
the measurement should be taken with the aid of
the scanning electron microscope.
Cross-sectioned metallographic examinations of
substrates with platings, surface evaluations,
thickness measurements, weight per volume
Surface Evaluation
Surface inspection includes the
detection of surface flaws and he
measurement of surface defects
and roughness. One method
includes the use of a laser light.
When the scattered light is reflected
off the surface of a sample, it can
be analyzed and measure. Another
method is the use of a motorized
stylus (profilometer). The stylus is
placed on the surface and the
texture of the material is measured
in micro-inches or millimeters
Quantitative
Metallography
NED University of Engineering and Technology, Karachi
Quantitative Metallography
The properties of materials
depends upon size, spacing
and amount of phases in
the sample.
Quantitative metallography
is a group of material
characterisation techniques
in which amount and size of
microconstitunts in the
sample measured.
Phase Proportions
Phase Proportions
One of the most common measurements,
determination of the amount of phases present,
can be done using three different methods:
(a) Areal analysis, developed by Delesse in 1848, says that the
area percent of a phase on a 2-D plane is equal to its volumetric
percent, that is, AA = VV. However, measuring the area of second
phases is very tedious unless they are quite coarse.
(b) Lineal analysis, developed by Rosiwal in 1898,
says that the lineal fraction of test lines in a phase on the 2-D plane
is equal to its volumetric percentage, that is, LL = VV. This is easier
to determine but still rather tedious.
(c) Point Count Analysis developed by several metallographers
state that the percentage of points on a test grid lying in the phase of
interest was equal to the volumetric percentage, that is, PP = VV.
Phase Proportions
Point Count Analysis, of
the three methods, is the
most efficient technique;
that is, it produces the
best precision for the
least effort when done
manually.
AA=
LL=
PP=
No. of Particles
required to
be counted
1.0
48000
2.0
12000
4.0
3000
5.0
1920
10.0
480
Fe-0.18C-0.43Mn steel
ASTM
E112
n = 2G-1
where n is the number of grains per square inch at 100X.
NA = f (Ninside + Nintercepted)
where f is Jefries multiplier =0.0002M2 to
obtain grains/mm2 (M is magnification).
This method is slow when done manually
because the grains must be marked when
counted to obtain an accurate count.
l = 1/NL = 1/PL
m.l.i. l is a measure of grain size that can be converted
to ASTM no. G according to the formula given in
ASTM112:
LT
No. of grains=N=5
No. of grain boundaries=P=5
The intercept method is more efficient than the planimetric method yielding acceptable
measurement precision (<10% relative accuracy) in much less time.
ASTM E 112 contains a complete description of these methods.
Inter-Lamellar Spacing
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