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Testing ULPA Filters
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INSTITUTE OF
ENVIRONMENTAL
SCIENCES AND
TECHNOLOGY
Contamination Control Division
Recommended Practice 007.2
IEST-RP-CC007.2
Testing ULPA Filters
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This Recommended Practice is published by the INSTITUTE OF ENVIRONMENTAL SCIENCES AND TECHNOLOGY to
advance the technical and engineering sciences. Its use is entirely voluntary, and determination of its applicability
and suitability for any particular use is solely the responsibility of the user.
This Recommended Practice was prepared by and is under the jurisdiction of Working Group 007 of the IEST Contamination Control Division.
Copyright 2007 by the INSTITUTE OF ENVIRONMENTAL SCIENCES AND TECHNOLOGY
Second printing, February 2009
ISBN 978-0-9787868-4-7
PROPOSAL FOR IMPROVEMENT: The Working Groups of the INSTITUTE OF ENVIRONMENTAL SCIENCES
AND T ECHNOLOGY are continually working on improvements to their Recommended Practices and Reference
Documents. Suggestions from those who use these documents are welcome. If you have a suggestion regarding
this document, please use the online Proposal for Improvement form found on the IEST website at
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FIGURE
1
TABLE
A1
B1
UPPER AND LOWER CONFIDENCE LIMITS FOR UPSTREAM AND DOWNSTREAM COUNTS .... 22
MINIMUM FREQUENCY OF CALIBRATION .............................................................................................. 26
APPENDIX
A
B
C
D
E
F
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1.2
Limitations
Filters tested per IEST-RP-CC007 are typically factory-tested with uniform airflow across the filter. Ducted
filters, fan filter units (FFUs), and poorly designed
inlet housings for in-line filters may result in nonuniform media air velocity that can possibly reduce the
in-situ filter efficiency.
Application of this RP is by mutual agreement between the customer and the supplier. To apply this RP,
the agreement should also include:
a)
IEST-RP-CC007.2
1.3
Application of method
The methodology described in this RP may be applied for particle-counter testing of filters outside the
efficiency and particle size range covered in the document.
REFERENCES
2.1
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2.2
2.3
Institute of Environmental
Sciences and Technology (IEST)
2.5
ASHRAE
American Society of Heating, Refrigerating, and
Air-Conditioning Engineers, Inc.
1791 Tullie Circle, NE
Atlanta, Georgia 30329, USA
Phone: 404-636-8400
Fax: 404-321-5478
www.ashrae.org
ASME International
American Society of Mechanical Engineers
Three Park Avenue
New York, NY 10016-5990, USA
Phone: 800-843-2763
Fax: 973-882-1717
www.asme.org
Institute of Environmental Sciences and Technology
Arlington Place One
2340 S. Arlington Heights Road, Suite 620
Arlington Heights, IL 60005-4510
Phone: 847-981-0100
Fax: 847-981-4130
www.iest.org
TAPPI
Technical Association of the Pulp and Paper Industry
15 Technology Parkway South
Norcross, Georgia 30092
Phone: 770-446-1400
Fax: 770-446-6947
www.tappi.org
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The following terms have special meaning in the context of this RP.
airflow
Airflow refers to volumetric flow rather than mass
flow. Tests are run at the manufacturer-rated airflow
or other airflow as agreed upon by the customer and
supplier.
correlation ratio
The ratio of downstream counts to upstream counts
with no filter in the test system.
For sequential counting systems, the correlation ratio
represents the differences in the upstream and downstream sampling systems, such as:
particle losses in sample lines and test duct
diluter (if used)
sample times
For simultaneous counting systems, the correlation
ratio represents the same factors as for sequential
counting systems, as well as the differences between
the different particle counting instruments used upstream and downstream, such as:
sample flow rate
counting efficiency
DOP
The mineral oil dioctyl phthalate or DEHP (di-2ethylhexyl phthalate) CAS# 117-81-7. With reference
to filter testing, DOP also refers to a polydisperse
aerosol of the above material.
electret filter media
Media made of fibers that carry electrical charge on
their surfaces.
IEST
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IEST-RP-CC007.2
4
4.1
TEST SYSTEM
General
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4.2
Components
(Figure 1, item 1)
4.2.4 Blower
(Figure 1, item 2)
A blower of sufficient capacity to provide steady airflow at the test conditions should be used.
(Figure 1, item 4; sections A3, A16, A17, A18)
All materials for the filter test system that contact the
test airstream, including sampling lines, should be
cleanable, non-particle-shedding, and electrically conductive and grounded. Two preferred materials are
polished stainless steel and aluminum. The test filter
should be mounted in a chucking device that completely encapsulates the filter and frame, so the filter frame
does not become part of the test duct and leaks in the
filter frame are detected.
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The particles of the aerosol used for testing, calibrating, and obtaining correlation ratios should be of
spherical form and have an index of refraction with a
real part between 1.45 and 1.60 and low imaginary
part. The vapor pressure should be low enough to ensure that diameter changes through the test system are
less than 10%. Possible materials include but are not
limited to:
DOP (DEHP)dioctyl phthalate (di-2ethylhexyl phthalate) (CAS# 117-81-7)
PAOpolyalpha olefin (e.g., 4 centistoke,
CAS# 68649-12-7)
DOS (DEHS)dioctyl sebacate (diethyl hexyl
sebacate) (CAS# 122-62-3)
polystyrene microspheres (PSL)
mineral oil
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10
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Many aerosol generators produce highly charged aerosols as a result of mechanical shearing of the liquid in
the process of making drops. These charges should be
neutralized to minimize particle deposition as a result
of electric fields. Commercially available radioactive
or electrostatic neutralizers produce high numbers of
bipolar ions that effectively neutralize the aerosol.
These neutralizers should be used immediately after
the aerosol is generated and before the aerosol is introduced into the filter test duct.
Electrostatic neutralizers may produce large numbers
of ultrafine particles (<0.05 m) that will contribute to
the challenge aerosol. This is not important for particle
counters that are not sensitive to particles smaller than
0.05 m. Radioactive neutralizers do not produce such
ultrafine particles.
Ionizers of the pulse type, if used, require thorough
mixing with the aerosol for effective neutralization.
Otherwise, ionizers can charge rather than neutralize
the particles and thus be detrimental.
a) When testing filters the aerosol challenge upstream of the test filter should be:
1) sufficiently concentrated to complete the test
in a reasonable period of time (see section 6.6);
2) sufficiently concentrated that the background
count rate of the downstream counter does not exceed 5% of the average downstream count;
3) less than 105 particles/cm3 (109 particles/ft3)
to avoid agglomeration.
During calibration of the test system, it is necessary to
have a substantially lower concentration of the same
aerosol to correlate the upstream and downstream
sampling systems and counting system (see section
5.9).
b) The aerosol used for correlation should:
1) be the same material and size distribution as
the test aerosol;
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as short as possible.
Turbulence should be avoided. Use of valves, restrictions, and bends should be minimized.
4.2.15 Diluter
(Figure 1, item 14; section A6)
High upstream concentration can result in particlecounting errors. When the high-count-rate error exceeds 5%, a diluter should be used.
Design and operation of diluters for low flow rates
may present difficulties such as very small capillary
sizes. Hence, for low-flow-rate particle counters, it
may be desirable to sample from the test duct at a
higher flow rate than the particle counter and then subsample for the particle counter, as shown in Figure 1,
item 15.
IEST-RP-CC007.2
SYSTEM QUALIFICATION
AND CALIBRATION
Qualification tests and calibrations should be performed prior to using the filter test system. In addition,
periodic testing and calibration should be performed to
provide continued accurate results. Table B1 summarizes the requirements. Certain tests or calibrations
should precede others. The tests and calibrations described in sections 5.1 through 5.4 may be conducted
in any order; the remaining procedures should be performed in the order in which they are listed.
Qualification tests and calibrations should be performed prior to initial startup and prior to startup after
any system modifications.
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5.1
Flow
a) Calibration of the measurement equipment required to obtain the volume flow rate should be traceable to a national metrology institute (NMI), primary
standards, or recognized equivalent. If a nozzle as described in ASHRAE-52 is used, the following devices
should be calibrated:
1) linear measuring devices for nozzle and duct
diameter,
2) the differential pressure measuring device,
3) absolute pressure measuring devices (such as
a barometer and a differential pressure measuring
device),
4) the temperature measuring device.
b) The standard for duct lengths, pressure tap location, and so forth should also be followed.
Possible standards to follow include, but are not limited to:
1) Fluid Meters: Their Theory and Application
(ASME)
2) ASHRAE 52.2-2007, Section 4.5 Device
Flow Measurement
3) Orifices calibrated with secondary standard
orifice plates that are themselves calibrated as described by Fain and Selby (see Appendix F).
The flow measurement device should be calibrated prior
to system use and a minimum of once a year thereafter.
The calibration should be accurate within 3%.
5.2
5.3
Temperature
5.4
Relative humidity
12
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5.5
Particle counters
5.6
Particle counter
high-count-rate error
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5.7
Aerosol neutralization
Aerosol neutralization systems should be used according to manufacturer instructions. Operation should be
verified as directed in manufacturer instructions at system startup and a minimum of once a year thereafter.
Radioactive aerosol neutralizers should be replaced after
one half-life has passed since the time of manufacture.
5.8
Aerosol source
The aerosol source characteristics that should be verified on startup include the particle size distribution,
output rate, or concentration and stability.
When polydisperse aerosols are used with particlesize-detecting counters, the statistical mode of the
count distribution should be in the size range of 0.1 to
0.2 m. When monodisperse aerosols are used, it
should be shown that other potentially interfering particles do not interfere with the system operation.
The aerosol generator output rate should be compared
to the particle-counter saturation limits, as described in
section 5.6, for the following two conditions:
a) When determining the correlation ratio (with no
test filter in place) with the aerosol source adjusted for
low output, it should be determined that the downstream count rate is sufficiently low to keep the highcount-rate error less than 5%.
b) When testing a filter with the aerosol source in its
high output, it should be determined that the upstream
count rate including the diluter, if necessary, is low
enough to keep the high-count-rate error less than 5%.
These tests should be conducted at the minimum test
flow rate to be used.
The aerosol source stability should be demonstrated.
This is particularly important for a sequential counting
system where the challenge aerosol concentration
should not vary by more than 5% between subsequent
upstream-downstream cycles.
The aerosol source characteristics should be verified at
least yearly, or each time a new aerosol is used.
IEST-RP-CC007.2
5.9
Dilution
Dilution systems, if employed, should have demonstrated stability and accuracy. As a minimum, the dilution ratio at the size range used for penetration
measurement should be measured at the sampling
flows to be used during testing and with the challenge
aerosol to be used. The aerosol concentration should
allow measurement upstream and downstream of the
diluter with the same instrument. The diluter should be
capable of reducing the upstream challenge concentration to an error rate (resulting from high concentration)
below 5% for the particle counter being used.
Several measurements of diluter ratio should be made.
Averages and standard deviations of these measured
values should be calculated to determine the confidence level in the final penetration calculation.
The actual dilution ratio should be measured by comparing particle concentrations upstream and downstream of the diluter, measured with the same sampling
system and particle counter. By using the correlation
ratio described in section 5.17, the measured dilution
ratio is automatically included as part of the correlation
ratio.
Dilution system measurements as described in this
section should be performed at startup, after modification, and yearly thereafter.
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accumulated and correlation ratios determined for other size ranges also.
IEST-RP-CC007.2
TEST PROCEDURE
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6.1
6.2
Airflow
6.3
Pressure drop
6.4
Temperature
6.5
Challenge aerosol
6.6
6.7
Acceptance or rejection
of the filter
DATA REDUCTION
(Section A5)
Symbols
Sequential counting should be performed by measuring upstream and downstream particle counts, making
appropriate allowance for system response times (see
section 5.16).
A single upstream-downstream sampling cycle is sufficient for generated aerosol sources producing upstream counts that vary by less than 5% from one
sample period to the next in the particle size range
from 0.1 to 0.2 m or appropriate range. For aerosols
that vary by more than 5% from one sample period to
the next in the particle size range from 0.1 to 0.2 m or
appropriate range, the upstream-downstream sampling
cycle should be repeated twice more for a total of three
upstream and three downstream samples.
The upstream and downstream counts and sampling
periods should be recorded, if the number and duration
of the sampling periods are not equal.
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Particle counting
16
6.6.3 Calculation
U
D
R
P
T
upstream counts
downstream counts
correlation ratio
penetration
sampling time
Subscripts
o
ucl
lcl
spec
c
t
uc
dc
ut
dt
observed
upper confidence limit
lower confidence limit
specified performance
correlation (i.e., no filter installed)
testing a filter
upstream during correlation
downstream during correlation
upstream during test
downstream during test
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7.1
Correlation ratio
Ro =
Do,c
U o,c
Rlcl =
7.2
7.3
Retest
(Section 6.7)
7.4
If
Tuc Tut
=
Tdc Tdt
then no adjustments for sampling time need to be
made.
If this condition is not met, then the equation for the
observed penetration is:
Do,t
T ut
Po =
D T T dt
U o,t o,c uc
U o,c T dc
Dlcl ,c
U ucl ,c
Penetration
The equations for the UCL and LCL values of the penetration are:
Ducl,t
T ut T dc
Pucl =
D
T uc T dt
lcl,c
U lcl,t
U ucl,c
Dlcl,t
T ut T dc
Plcl =
D
T uc T dt
U ucl,t ucl,c
U lcl,c
Pucl =
Plcl =
IEST-RP-CC007.2
Ducl ,t
U lcl ,t Rlcl
Dlcl ,t
U ucl ,t Rucl
7.5
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for repeated tests on reference filters provides estimates of the precision of the penetration measurement.
7.6
Pm
C1 + [(C 2 )(TT )]
where:
Pc = filter resistance in Pa (in. w.c.), corrected to 21
C (70 F)
Pm = filter resistance in Pa (in. w.c.), measured
C1 = 1st constant, 0.9468 for C (0.902 for F)
C2 = 2nd constant, 0.00252 for C (0.0014 for F)
TT = test air temperature, C (F)
Resistance
Pc =
18
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IEST-RP-CC007.2
A2 MIXING OF AEROSOLS
In testing for the efficiency of a filter, the challenge
aerosol should be homogeneous over the entire upstream area, and the downstream sample should represent filtered air from all points equally.
The measured penetration of a filter may vary by as
much as several orders of magnitude when the filter is
rotated about its axis between tests in a test duct that
does not mix upstream and downstream aerosol. To
ensure uniformity of the challenge aerosol, the aerosol
should pass through static or motionless mixers between the aerosol generator and the upstream sampling
probe. Downstream air should pass through similar
mixers between the test filter and the downstream
sampling probe.
A3 AIRFLOW MEASUREMENT
The pressure drop across a filter medium as a function
of airflow is a primary measure of filter performance.
Particle collection efficiency is the only other key
measurable property of the filter. Both measurements
depend on how airflow is controlled within the test
duct.
Increasing airflow, inadvertently or deliberately, will
lead to the following:
a) The pressure drop will increase, and the observer
may incorrectly ascribe this increase to a change in the
filter.
b) Particle capture efficiency by impaction (if any)
will be enhanced.
c) However, particle capture efficiency by diffusion
will be reduced. Because particle capture by interception is unchanged, the MPPS (where the sum of both
interception and diffusion is at a minimum) will become smaller, and the efficiency at the new size will
be lower than it was at the old size.
d) If the output of the generator remains constant,
even the challenge aerosol concentration will change.
There are two possible measurements of flow: mass
flow and volume flow. Volume flow is expressed in
units of volume per time, for example, cubic feet per
minute. Mass flow is expressed as mass per time, for
example, pounds (mass) per hour. Mass flow is im-
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the standard air temperature of 21 C (70 F). A correction factor formula is:
where:
A4 VISCOSITY AND
PRESSURE DROP
The pressure drop required to force air through a filter
medium is a function of the viscosity of the air. In fact,
in contrast to ducts and valves, filter media usually
owe nearly all their resistance to viscosity and almost
none to inertial effects. Therefore, if the viscosity of
the test air changes, the pressure drop across the filter
medium changes proportionally.
A4.2 Practice
The viscosity of air varies by 5% between 10 C and
29.4 C (50 F and 85 F). Thus, an uncompensated
tester operating in this range will wrongly indicate a
5% variation in inherent media resistanceprobably
the largest non-reproducibility that can be suffered in
an otherwise functional, volumetric flow system.
A4.3 Recommendation
The best approach is to regulate test temperature, but
this method can be very expensive.
When it is not possible to test filters at 21 C (70 F),
the resistance of the filter should be corrected for air
viscosity due to variations in test air temperature from
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Pm
+ c(TT ST
A5 POISSON STATISTICS
AND COUNTING
A5.1 Theory
A4.1 Theory
20
Pc =
A5.2 Practice
When top-performance, noise-free particle counters
are used in a good duct according to this RP, count
statistics become the largest error on highly efficient
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A5.3 Recommendation
A5.3.1 Determination of confidence limits
on a count
This procedure uses particle count data to establish the
confidence limits on penetration. Section A5.3.5 gives
the 95% confidence limits on a single observed particle count from 0 to 50. For a single observed particle
count n, there is a 95% confidence that the true mean
count is between the upper and lower limits given in
the table below. The true mean count is the average
count that would be obtained if the tests were repeated
indefinitely.
For larger values of counts (n), the Poisson distribution
tends toward normality with mean n and variance n. In
this case, the 95% confidence levels for a count of n
can be expressed
n2 n
Once the confidence limits on a particle count are established, it is necessary to establish the confidence
limits on the correlation ratio and penetration.
In most cases, one number in the ratio is substantially
smaller than the other, and it is the uncertainty in the
smaller value that dominates the uncertainty in the
ratio. In this case, it is reasonable to calculate the confidence limits of the ratio by calculating the ratio with
the limits of the smaller value and the observed level
of the larger value.
IEST-RP-CC007.2
Example:
Observed Value
10,000 counts upstream
1,000,000 counts
downstream
A5.3.3 Penetration
This correlation example is used to calculate the penetration of a filter test:
Observed Value
10,000 counts upstream
10 counts downstream
Other error sources may contribute to the uncertainty of the penetration measurement.
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Upper
3.7
5.6
7.2
8.8
10.2
11.7
13.1
14.4
Observed
Count (n)
Lower
8
3.4
9
4.0
10
4.7
11
5.4
12
6.2
13
6.9
14
7.7
15
8.4
16
9.2
17
9.9
18
10.7
19
11.5
20
12.2
21
13.0
22
13.8
23
14.6
24
15.4
25
16.2
26
17.0
27
17.8
28
18.6
29
19.4
30
20.2
31
21.0
32
21.8
33
22.7
34
23.5
35
24.3
36
25.1
37
26.0
38
26.8
39
27.7
40
28.6
41
29.4
42
30.3
43
31.1
44
32.0
45
32.8
46
33.6
47
34.5
48
35.3
49
36.1
50
37.0
Upper
15.8
17.1
18.4
19.7
21.0
22.3
23.5
24.8
26.0
27.2
28.4
29.6
30.8
32.0
33.2
34.4
35.6
36.8
38.0
39.2
40.4
41.6
42.8
44.0
45.1
46.3
47.5
48.7
49.8
51.0
52.2
53.3
54.5
55.6
56.8
57.9
59.0
60.2
61.3
62.5
63.6
64.8
65.9
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A6 PARTICLE COUNTER
SATURATION AND
COINCIDENCE
Particle counters produce erroneous data when sampling high-concentration aerosols. Particle counters
exhibit coincidence error when two or more particles
occupy the sensing zone at the same time because overly rapid pulses cause the electronics to saturate. Reported counts are erroneously low in these situations.
Low counts due to coincidence errors are not obvious.
If the errors are not caught, the result is usually a filter
efficiency curve that has an apparent low efficiency for
small particle sizes because the challenge count was
saturated in these sizes.
For routine work, the test system should be known
always to operate below saturation levels by design
and subsequent measurement, as recommended in section 5.6.
A9 ANISOKINETIC SAMPLING
A7 PARTICLE COUNTER
BACKGROUND COUNT
RATES
IEST-RP-CC007.2
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The same quantity of liquid causes a significantly larger fractional increase in the diameter
of a small fiber than in a larger fiber.
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IEST-RP-CC007.2
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Calibration Procedure
Flow
Pressure drop
Temperature
Relative humidity
Particle counters
Zero count
Sizing
High-count-rate error
Neutrality of aerosol
Aerosol source
Size distribution
Stability
Dilution
Duct integrity (leaks)
Cleanliness of test air
Airflow distribution
Upstream uniformity
Downstream leak
System particle losses
System response time
Correlation
Pressure drop tare
Reference filter test
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Daily
Per Filter
Model
Yearly
X
X
X
X
Initial system
startup and
after system
changes
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
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C2 ELECTROSTATICALLY
CHARGED MEDIA
IEST-RP-CC007.2
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IEST-RP-CC007.2
E2 PRACTICE
In practice, particle size distributions are assumed to
follow a lognormal relationship. Lognormal distributions are a normal probability function with logarithm
of the particle size. The properties of the size distribution are the geometric mean and the geometric standard deviation. This is usually a valid assumption if the
aerosol is generated by one mechanism, such as nebulization. In lognormal size distributions, the geometric
standard deviation does not depend on the property of
the size distribution measured, e.g. number, surface or
mass. The various means can be related mathematically. For example (Hinds, 1982, Appendix F):
E3 RECOMMENDATIONS
If the challenge aerosol particle size distribution characteristics need to be reported, the geometric number
mean and geometric standard deviation should be used.
If means based on surface or mass are used, this should
be explicitly identified. If test data from two test facilities are compared, care should be taken that the statistics
used to report the size distribution are identical and instrumentation differences are understood.
The method of measurement and the specific instrument including manufacturer and model number
should be explicitly reported.
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APPENDIX FBIBLIOGRAPHY
Abramowitz, M. and I.A. Stegun. 1972. Handbook of
Mathematical Functions. National Bureau of Standards (available from National Institute of Standards
and Technology (NIST), 100 Bureau Drive, Stop 1070,
Gaithersburg, MD 20899-1070, USA; 301-975-6478;
www.nist.gov).
ASHRAE-51: Laboratory Methods of Testing Fans for
Rating.
ASTM F1471-93: Standard Test Method For Air
Cleaning Performance Of A High-Efficiency Particulate Air Filter System.
Box, G.E.P., W.G. Hunter, and J.S. Hunter. 1978. Statistics for Experimenters. John Wiley & Sons.
Fain, D.E. and T.W. Selby. 1984. Calibration and Use
of Filter Test Facility Orifice Plates. Oak Ridge Gaseous Diffusion Plant, Martin Marietta Energy Systems
Corp., reported page 1168, 18th Department of Energy
Nuclear Airborne Waste Management Air Cleaning
Conference, Baltimore, Maryland.
Hinds, W.C. 1982. Aerosol technology, properties,
behavior, and measurement of airborne particles. New
York: John Wiley and Sons.
IEST-RD-CC011: A Glossary of Terms and Definitions Relating to Contamination Control.
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