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EXPERIMENT JOURNAL

Title of Experiment : Alluminium and Its Compound


Day/Date of Experiment : Thursday, May 23th 2016
Name : Fitrianti
Register Number : 1413440022
Class/ Group : ICP-B of Chemistry/ VI
Members : 1. Harlin Asis
2. Raudina Nuramaliah
Assistant : Ida Mashita
A. OBJECTIVE OF EXPERIMENT
Students are expected to learn about the chemical properties of alluminium
and its compound.
B. APPARATUS AND CHEMICALS
1. Apparatus
a. The test tube (12 pieces)
b. Tube rack (2 pieces )
c. Measuring cylinder 10 ml (1 piece)
d. Beaker glass 100 ml (1 piece)
e. Pipette (6 pieces)
f. Funnel (2 piece)
g. Stirrer (2 pieces)
h. Spiritus burner (1 piece)
i. Wood clamps (1 piece)
j. Spray Botte (1 piece)
k. Analytical balance (1 piece)
l. Spatula (1 piece)
2. Chemicals
a. Solution of aluminum chloride (AlCl3)
b. Anhydrous aluminum chloride (AlCl3)
c. Solution of sodium hydroxide 0,1 M (NaOH)
d. Solution of ammonium hydroxide (NH4OH)
e. Solution of dilute hydrochloric acid (HCl)
f. Magnesium chloride (MgCl2)
g. Magnesium oxide (MgO)
h. Aluminum oxide (Al2O3)
i. Water (H 2O)
j. Universal indicator
k. Solution of methyl violet
l. Filter paper

C. WORK PROCEDURES
1. Aluminium Hydroxide Characteristic

beberapa tetes larutan NH3 NH3 solution more than before

2 mL aluminium salt solution observed

NaOH 0,1 M more than before


some drops NaOH 0,1 M solution HCl solution

precipitate formed devide into 2 part

2 mL aluminium salt (1) (2)

some drops dilute NaOH


methylviolet

washed
filter the precipitate
with
water

2. Compare aluminium chloride with magnesium chloride


AlCl3 anhidrat MgCl2 anhidrat

change with

one by one drop H2O


AlCl3

repeat the treatment by change with MgCl 2

observed and measure the pH

3. Compare the characteristic acid Base of Al 2O3 and MgO

0,1 gram Al2O3 and


MgO in other tube

3 mL aquadest and
then shaked

measure the pH
0,1 gram Al 2O3

dilute 3 mL HCl and


NaOH

4. Compare about the characteristic of Ion Aluminium base and


Magnesium ion

3 mL Al 0,1 M salt and observed the pH


3 mL Mg 0,1 M salt

larutan NaOH 0,1 M


3 mL Al 0,1 M solution and

3 mL Mg 0,1 M solution

Makassar,
Makassar,May 23th 2016
Assistant Practicant

Ida Mashita Fitrianti

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