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Lab 6
Abstract
SCN +2
( aq ) Fe( SCN ) ( aq )
Fe+3(aq) +
3. Method
Part 1
Part 2
3 mL of 0.1M K2CrO4 (aq) has been placed into a test tube. An equal
3mL of 6M HNO3 has been added to solution. The change of color
has been observed due to change of concentration. The reverse
process has been achieved by adding 10% NaOH solution
dropwise. Basic solution reacts with hydrogen ions to recover
original mixture.
Part 3
Part 4
Third test tube has been used for analysis of equilibrium during
variation in temperature. Solid NH4Cl has been added in small
amount to the tube and heated using heating mantle. Changes in
color has been recorded
Part 5
To the third test tube 1mL of 0.1M KSCN have been added and
color change have been recorded.
To the final test tube with solution 0.1M AgNO3 has been added
dropwise until original color disappeared and some precipitate
formed. Amount of silver nitrate added has been recorded.
4. Materials
Chemicals used:
Solid NH4Cl (s), saturated NaCl (aq), concentrated 12M HCl (aq),
0.1M FeCl3 (aq), 0.1M KSCN (aq), 0.1M AgNO3 (aq), 0.1M CoCl2
(aq), concentrated 15M NH3 (aq), phenolphthalein, 0.1M K2CrO4
(aq), 6M HNO3 (aq), and 10% NaOH (aq).
Part 1
Part 2
2 H + 2
( aq ) Cr 2 O 7 ( aq ) + H 2 O ( l )
2 Cr O42(aq) +
Part 4
4 Cl 2
( aq ) CoCl 4 ( aq ) +6 H 2 O ( l )
Co( H 2 O)6+2(aq) +
Part 5
SCN +2
( aq ) Fe( SCN ) ( aq )
Fe+3(aq) +
6. Conclusion