Recalculation 21/08/2015 15:14 Page 1 /7

AAS 5 Flame
Report file: C:\ARQUIV~1\WinAAS\tmp\Pro_006
Program version: 3.22.0 Printed on: 21/08/2015 15:14
Recording started on 21/08/2015 14:50 GMT-3.0
Operator: Erika
Laboratory: Diqui
Code:
Technique: Flame
Remarks:

Method parameters Cu
Method Cu-teste
Created on 20/08/2015 Time 10:08
Program ---
Spectrometer
Line 324.8 nm Slit 1.2 nm
Lamp type HCL Lamp current 4.0 mA
Integr. mode Rep. mean Integr. time 3.0 s
PMT 332.0 V D2-HCL curr. ---
AZ time 3.0 s Peak smoothing 2/25
Delay 2.0 s
BC ampl.level: --- HC ampl.level: ---
Flame
Flame C2H2/air
Fuel flow 45 l/h
Burner type 100 mm
Burner height 5 mm Burner angle 0
Nebulizer rate 5.0 mL/min
Injection switch off

QC parameters
QC type Conc. check
QC check samp. 1 QC check samp. 2
Conc. 1.0000 mg/L Conc. 1.0000 mg/L
Error limit 10.00% Error limit 50.00%
Rep. measurement off Reaction flag + continue
QC std.1 no. 4(0.30 mg/L) QC std.2 no. 2(3.00 mg/L)
QC std.1 limit 10.00% QC std.2 limit 10.00%
QC std. act. flag + continue
Expect. blank abs. 0.0100 0.0100 Reaction flag + continue
QC precision off
Reaction off
QC Recal.factor Off

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Sample statistics
Stat. mode Mean Meas. cycles 10
Confid. level 95.4 % Blind cycles 1
Grubbs stat. off

Sample table: Means of abs./emis. values Rep. mean Cu

Mean value Peak height

No Name Pos
Abs SD RSD/% Abs SD RSD/%

1 Sample ## -0.0032 0.00016 5.040

2 Sample ## 0.399 0.00505 1.265
3 Sample ## 0.423 0.00842 1.988
4 Sample ## 0.641 0.00606 0.945
5 Sample ## 0.408 0.00548 1.343
6 Sample ## 0 0 $$$$
7 Sample ## 0 0 $$$$
8 Sample ## 0 0 $$$$
9 Sample ## 0 0 $$$$
10 Sample ## 0.646 0.00440 0.681
11 Sample ## 0 0 $$$$
12 Sample ## 0 0 $$$$
13 Sample ## 0 0 $$$$
14 Sample ## 0 0 $$$$
15 Sample ## 0 0 $$$$
16 Sample ## 0 0 $$$$
17 Sample ## 0 0 $$$$
18 Sample ## 0 0 $$$$
19 Sample ## 0 0 $$$$
20 Sample ## 0 0 $$$$
21 Sample ## 0 0 $$$$
22 Sample ## 0 0 $$$$
23 Sample ## 0 0 $$$$
24 Sample ## 0 0 $$$$
25 Sample ## 0 0 $$$$
26 Sample ## 0 0 $$$$
27 Sample ## 0 0 $$$$
28 Sample ## 0 0 $$$$
29 Sample ## 0 0 $$$$
30 Sample ## 0 0 $$$$
31 Sample ## 0 0 $$$$
32 Sample ## 0 0 $$$$
33 Sample ## 0 0 $$$$
34 Sample ## 0 0 $$$$
35 Sample ## 0 0 $$$$

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36 Sample ## 0 0 $$$$
37 Sample ## 0 0 $$$$
38 Sample ## 0 0 $$$$
39 Sample ## 0 0 $$$$
40 Sample ## 0 0 $$$$
41 Sample ## 0 0 $$$$
42 Sample ## 0 0 $$$$
43 Sample ## 0 0 $$$$
44 Sample ## 0 0 $$$$
45 Sample ## 0 0 $$$$
46 Sample ## 0 0 $$$$
47 Sample ## 0 0 $$$$
48 Sample ## 0 0 $$$$
49 Sample ## 0 0 $$$$
50 Sample ## 0 0 $$$$
51 Sample ## 0 0 $$$$
52 Sample ## 0 0 $$$$
53 Sample ## 0 0 $$$$
54 Sample ## 0 0 $$$$
55 Sample ## 0 0 $$$$
56 Sample ## 0 0 $$$$
57 Sample ## 0 0 $$$$
58 Sample ## 0 0 $$$$
59 Sample ## 0 0 $$$$
60 Sample ## 0 0 $$$$
61 Sample ## 0 0 $$$$
62 Sample ## 0 0 $$$$
63 Sample ## 0 0 $$$$
64 Sample ## 0 0 $$$$
65 Sample ## 0 0 $$$$
66 Sample ## 0 0 $$$$
67 Sample ## 0 0 $$$$
68 Sample ## 0 0 $$$$
69 Sample ## 0 0 $$$$
70 Sample ## 0 0 $$$$
71 Sample ## 0 0 $$$$
72 Sample ## 0 0 $$$$

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Sample table: Concentration/content Cu

A: analysed sample O: original sample

No Name weight/g ASDF A: mg/L
Conc. CI SD RSD/% Rem
Rec. date Pos SV/mL Pre-DF O: mg/L
1 Sample --- A: 0.101 0.00120
21/08/2015 14:50 ## 1.000 O: 0.101 0.00120
2 Sample --- A: 2.89 0.0630 0.0368 1.276
21/08/2015 14:50 ## 1.000 O: 2.89 0.0630 0.0368 1.276
3 Sample --- A: 3.06 0.0655 0.0613 2.004
21/08/2015 14:50 ## 1.000 O: 3.06 0.0655 0.0613 2.004
4 Sample --- A: 4.65 0.104 0.0441 0.950
21/08/2015 14:50 ## 1.000 O: 4.65 0.104 0.0441 0.950
5 Sample --- A: 2.95 0.0639 0.0399 1.354
21/08/2015 14:50 ## 1.000 O: 2.95 0.0639 0.0399 1.354
6 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
7 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
8 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
9 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
10 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
11 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
12 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
13 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
14 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
15 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
16 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
17 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
18 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
19 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
20 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
21 Sample --- A:
21/08/2015 14:50 ## 1.000 O:

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22 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
23 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
24 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
25 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
26 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
27 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
28 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
29 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
30 Sample --- A:
21/08/2015 14:50 ## 1.000 O:
31 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
32 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
33 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
34 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
35 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
36 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
37 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
38 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
39 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
40 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
41 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
42 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
43 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
44 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
45 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
46 Sample --- A:
21/08/2015 14:51 ## 1.000 O:

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47 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
48 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
49 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
50 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
51 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
52 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
53 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
54 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
55 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
56 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
57 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
58 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
59 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
60 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
61 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
62 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
63 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
64 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
65 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
66 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
67 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
68 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
69 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
70 Sample --- A:
21/08/2015 14:51 ## 1.000 O:
71 Sample --- A:
21/08/2015 14:51 ## 1.000 O:

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72 Sample --- A:
21/08/2015 14:51 ## 1.000 O:

AAS 5