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  • Sample Name Pulse Sequence Temperature Study Owner Date Collected Solvent Spectrometer Operator

    Enviado por

    Collin Sanderson
    25 visualizações2 páginas
    This document summarizes an NMR spectroscopy experiment on a sample called xCS_2_05_mesylatedprdct. The 1H NMR spectrum was collected on October 8, 2017 in CDCl3 solvent using a Hahn-Inova300 spectrometer. Key experimental parameters are provided, including temperature, solvent, pulse sequence used, transmitter frequencies, acquisition parameters, and processing details.

    Descrição original:

    benzyl mesyl carbamate

    Título original

    cs_05

    Direitos autorais

    © © All Rights Reserved

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    PDF, TXT ou leia online no Scribd

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    This document summarizes an NMR spectroscopy experiment on a sample called xCS_2_05_mesylatedprdct. The 1H NMR spectrum was collected on October 8, 2017 in CDCl3 solvent using a Hahn-Inova300 spectrometer. Key experimental parameters are provided, including temperature, solvent, pulse sequence used, transmitter frequencies, acquisition parameters, and processing details.

    Direitos autorais:

    © All Rights Reserved
    Baixe no formato PDF, TXT ou leia online no Scribd
    Sinalizar o conteúdo como inadequado
    25 visualizações2 páginas

    Sample Name Pulse Sequence Temperature Study Owner Date Collected Solvent Spectrometer Operator

    Enviado por

    Collin Sanderson
    This document summarizes an NMR spectroscopy experiment on a sample called xCS_2_05_mesylatedprdct. The 1H NMR spectrum was collected on October 8, 2017 in CDCl3 solvent using a Hahn-Inova300 spectrometer. Key experimental parameters are provided, including temperature, solvent, pulse sequence used, transmitter frequencies, acquisition parameters, and processing details.

    Direitos autorais:

    © All Rights Reserved
    Baixe no formato PDF, TXT ou leia online no Scribd
    Sinalizar o conteúdo como inadequado
    de 2

    xCS_2_05_mesylatedprdct

    Sample Name xCS_2_05_mesylatedprdct Pulse sequence PROTON Temperature 25 Study owner sbohman2
    Date collected 2017-10-08 Solvent cdcl3 Spectrometer hahn-inova300 Operator sbohman2

    7.416
    7.293

    5.292

    3.193

    1.639

    0.914
    8.104

    1.298
    8 7 6 5 4 3 2 ppm
    1.00

    5.53
    3.30

    2.70

    4.33

    4.69

    0.72
    1.64

    1.62
    Data file /groups/research/nmr/working/userdata/sbohman2/xCS_2_05_mesylatedprdct_20171008_01/PROTON_01.fid Plot date 2017-10-09
    xCS_2_05_mesylatedprdct

    Sample Name xCS_2_05_mesylatedprdct Pulse sequence PROTON Temperature 25 Study owner sbohman2
    Date collected 2017-10-08 Solvent cdcl3 Spectrometer hahn-inova300 Operator sbohman2

    xCS_2_05_mesylatedprdct

    SAMPLE PRESATURATION

    date Oct 8 2017 satmode n


    solvent cdcl3 wet n
    file /groups/research/n
    mr/working/userdata/sboh SPECIAL
    man2/xCS_2_05_mesylatedp
    rdct_20171008_01/PROTON_ temp not used
    01.fid gain 60
    spin 0
    hst 0.008
    ACQUISITION pw90 9.500
    alfa 10.000
    sw 4799.6
    at 1.707 FLAGS
    np 16384
    fb 3000 il n
    bs 32 in nw
    ss 4 dp y
    d1 1.000 hs nn
    nt 8
    ct 8 PROCESSING

    TRANSMITTER lb 0.50
    fn 131072
    tn H1
    sfrq 299.971 DISPLAY
    tof 300.0
    tpwr 58 sp 188.5
    pw 4.750 wp 2319.7
    rfl 599.9
    DECOUPLER rfp 0
    rp -27.4
    dn C13 lp -25.7
    dof 0
    dm nnn PLOT
    decwave W40_pfgAuSW
    dpwr 29 wc 234
    dmf 26316 sc 8
    vs 194
    th 8
    ai cdc ph

    Data file /groups/research/nmr/working/userdata/sbohman2/xCS_2_05_mesylatedprdct_20171008_01/PROTON_01.fid Plot date 2017-10-09

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