Escolar Documentos
Profissional Documentos
Cultura Documentos
Weldability of a Low-Carbon
Mo-Nb X-70 Pipeline Steel
Better SMAW and GMAW techniques and consumables
offering higher toughness at lower temperatures than
those presently used for pipeline construction in North
America appear to be needed to meet weld zone
requirements at 20C (4F)
BY A. J. BRYHAN A N D W. TROYER
W E L D I N G RESEARCH S U P P L E M E N T I 37-s
g r a d e w h i c h w a s f i n i s h r o l l e d at a l o w passes of a w e l d are e s p e c i a l l y s u s c e p - parts t h a t are of a c r i t i c a l n a t u r e s u c h
temperature. The l o w temperature t i b l e t o H A C w h i c h is d u e t o t h e as valves a n d f i t t i n g s . S o m e of t h e
rolling p r o d u c e d some d e f o r m e d fer- c o m b i n a t i o n of s m a l l w e l d b e a d size, reasons w h y t h i s e l e c t r o d e is n o t u s e d
rite. T h e h i g h d e n s i t y o f m o b i l e d i s l o - high joint constraint, and the low pipe f o r r o u t i n e w e l d i n g are t h a t t h e s e e l e c -
c a t i o n s in t h i s f e r r i t e p r o m o t e s a c o n - t e m p e r a t u r e w h i c h r e d u c e s t h e rate o f t r o d e s are m o r e e x p e n s i v e , t h e d e p o s i -
t i n u o u s stress-strain b e h a v i o r with h y d r o g e n d i f f u s i o n . T o r e d u c e t h e sus- t i o n rate is n o t as h i g h a n d t h e y are n o t
increased w o r k hardening w h i c h m o r e ceptibility to HAC, the three above- as c o n v e n i e n t t o use as c e l l u l o s i c e l e c -
t h a n o f f s e t s t h e loss of s t r e n g t h c o m - mentioned low-hydrogen electrodes/ trodes.
m o n l y associated w i t h t h e Bauschin- techniques w e r e i n c o r p o r a t e d into this Because o f t h e d i f f i c u l t i e s w i t h t h e
ger e f f e c t . 1 study. vertical-up type electrodes, vertical-
Four w e l d i n g c o n s u m a b l e s a n d / o r T h e gas m e t a l arc w e l d i n g ( G M A W ) d o w n l o w - h y d r o g e n e l e c t r o d e s are
process v a r i a t i o n s o f p o t e n t i a l i n t e r e s t p r o c e s s is a n i n h e r e n t l y l o w - h y d r o g e n being d e v e l o p e d . These electrodes
w e r e selected for this study. These process as v i r t u a l l y n o h y d r o g e n is seek t o c o m b i n e t h e ease o f w e l d i n g
included cellulosic electrodes, v e r t i j i n t r o d u c e d i n t o t h e w e l d by t h e c o n - and productivity of the cellulosic elec-
cal-up and v e r t i c a l - d o w n l o w - h y d r o - sumables. A l t h o u g h the G M A W pro- trodes w i t h a l o w diffusible hydrogen
g e n e l e c t r o d e s f o r s h i e l d e d m e t a l arc cess p o t e n t i a l l y o f f e r s a d v a n t a g e s , it c o n t e n t . T h e i n t e n t is t o d e s i g n e l e c -
w e l d i n g ( S M A W ) , plus a solid wire has n o t g a i n e d w i d e a c c e p t a n c e f o r trodes w h i c h may be used w i t h essen-
e l e c t r o d e f o r s e m i a u t o m a t i c gas m e t - field welding of pipe. Hydrogen t i a l l y t h e s a m e t e c h n i q u e as a c e l l u l o s -
al arc w e l d i n g ( G M A W ) . T h e c o n s u m - assisted c r a c k i n g m a y also b e c o n - ic t y p e e l e c t r o d e , t h u s r e q u i r i n g less
ables w e r e s e l e c t e d t o be c o m p a t i b l e trolled by using low-hydrogen welder training.
w i t h t h e usual or d e s i r e d m e t h o d s s h i e l d e d m e t a l arc w e l d i n g ( S M A W ) The proposed Alaskan Highway
currently e m p l o y e d for pipeline c o n - electrodes. The flux coating o n these Pipeline Project, w h i c h w i l l transport
struction. The w e l d i n g procedures electrodes is n o t cellulosic; thus n a t u r a l gas f r o m t h e N o r t h S l o p e in
w e r e t o b e t y p i c a l o f t h o s e p r a c t i c e d in h y d r o g e n is n o t g e n e r a t e d by d i s s o c i a - Alaska t o m a r k e t s in t h e n o r t h w e s t e r n
North America. t i o n o f t h e f l u x in t h e w e l d i n g arc. a n d e a s t e r n parts o f t h e U n i t e d States,
T h e use o f c e l l u l o s i c electrodes T w o t y p e s of l o w - h y d r o g e n e l e c - w i l l be a large c o n s u m e r o f X-70 g r a d e
c o m b i n e s relatively high p r o d u c t i o n t r o d e s are availablea t y p e t h a t is u s e d p i p e . O n e s e c t i o n o f t h i s p r o j e c t is t h e
rates w i t h w e l d e r a c c e p t a n c e and in a v e r t i c a l - u p d i r e c t i o n , a n d a t y p e F o o t h i l l s p i p e l i n e w h i c h crosses t h e
results in h i g h q u a l i t y w e l d s if c e r t a i n t h a t is u s e d in a v e r t i c a l - d o w n d i r e c - Y u k o n , British C o l u m b i a and Alberta.
p r e c a u t i o n s are u s e d t o r e d u c e h y - t i o n . T h e v e r t i c a l - u p e l e c t r o d e has T h e p i p e for t h i s s e c t i o n w i l l h a v e
d r o g e n assisted c r a c k i n g ( H A C ) in t h e b e e n a v a i l a b l e f o r m a n y years. It has d i a m e t e r s w h i c h vary f r o m 914 m m (36
r o o t area o f a p i p e w e l d . T h e r o o t been used most f r e q u e n t l y for w e l d i n g in.) t o 1422 m m (56 in.) a n d w a l l
t h i c k n e s s r a n g i n g f r o m 10 m m (0.40
in.) t o 18 m m (0.72 in.). T h e t o t a l
l e n g t h f o r this s e c t i o n w i l l be 2848 k m
Table 1Mechanical Properties and Composition of USINOR X-70 Pipe Steel (1780 m i l e s ) . T h e d e s i g n t e m p e r a t u r e is
t o b e - 4 C ( + 25F) f o r t h e m a j o r i t y of
0.2% yield Ultimate t h e l i n e w i t h a m i n i m u m service t e m -
stress, tensile stress, Elongation, Reduction Yield tensile
p e r a t u r e of 20C (4F) f o r a p p r o x i -
MPa (ksi) MPa (ksi) % in area, % ratio
m a t e l y 2% of t h e t o t a l l e n g t h . T h i s
488 (70.8) 644 (93.5) 19.1 33.9 0.76 l o w e r d e s i g n t e m p e r a t u r e is also l i k e l y
to be a p p l i e d for the Alaskan section
Foothills Pipe Line (Yukon) Ltd. Specification: of t h e p r o j e c t .
Yield stress: m i n i m u m 482 MPa (70 ksi); maximum less than 586 MPa (85 ksi)
Yield to Ultimate Tensile Strength Ratio less than 0.90 It w a s d e c i d e d t o use t h e s p e c i f i c a -
tions for the Foothills section to evalu-
ate t h e success o f t h e w e l d i n g in this
Chemical Composition % s t u d y . In a d d i t i o n t o t h e t e s t i n g s p e c i -
f i e d by F o o t h i l l s w h i c h is d i s c u s s e d
C Mn Si P S Nb Mo
later, a c o m p l e t e c h a r a c t e r i z a t i o n of
0.093 1.53 0.024 0.004 0.057 0.22 the girth w e l d and associated heat-
0.18
affected zones ( H A Z ) was made using
Electrodes'" C Mn Si P S Ni Mo Cu Cr Ti Nb
Weldments
1 0.15 0.52 0.22 0.016 0.009 1.24 0.20 0.021 0.062 0.008 0.015 0.01
E 8010/8010
2 0.15 0.44 0.21 0.012 0.011 1.39 0.19 0.018 0.025 0.010 0.020 <01
E70S-1B/8010
3 0.062 0.92 0.30 0.013 0.013 2.21 0.048 0.019 0.045 0.014 0.010 <.01
E70S-1B/8010-C1
4 0.051 0.96 0.37 0.014 0.006 1.37 0.46 0.014 0.025 0.007 0.009 0.01
E70S-1B/LB-86VU
,a
'Analysis s u p p l i e d by manufacturer.
T h e s h i e l d e d m e t a l arc welding
( S M A W ) was p e r f o r m e d by welders
the crack opening displacement deg angle w i t h a root face a p p r o x i - s u p p l i e d by a N o r t h A m e r i c a n p i p e l i n e
( C O D ) test. U p u n t i l t h i s t i m e , f r a c t u r e m a t e l y 1.6 m m (Vi6 in.) w i d e . company. The G M A W root welds
t o u g h n e s s tests, s u c h as t h e C O D This p i p e w a s w e l d e d u s i n g f o u r w e r e m a d e by a t e c h n i c i a n f r o m an
m e t h o d , have o n l y been used by p i p e - c o n s u m a b l e s E 8010 c e l l u l o s i c e l e c - electrode manufacturing company.
line c o m p a n i e s for i n f o r m a t i o n a l pur- t r o d e s , E 70S-1B e l e c t r o d e s w i t h t h e W e l d i n g conditions and electrode de-
poses. G M A process u s i n g c a r b o n d i o x i d e f o r tails are d e s c r i b e d in T a b l e 3. W e l d s
s h i e l d i n g gas, E 8018-C1 v e r t i c a l - u p were made w i t h o u t preheating the
Experimental Procedures low-hydrogen electrodes, and a devel- p i p e . T h i s is c o n s i d e r a b l y m o r e severe
opmental vertical-down low-hydro- than a typical field w e l d i n g procedure,
Materials s i n c e v i r t u a l l y all c o m m e r c i a l f i e l d
gen electrode m a n u f a c t u r e d by Kobe
The c o m p o s i t i o n and mechanical Steel a n d d e s i g n a t e d L B - 8 6 V U . T h e w e l d i n g o f large d i a m e t e r p i p e w o u l d
p r o p e r t i e s o f t h e p i p e steel u s e d f o r c o m p o s i t i o n s of t h e e l e c t r o d e s a n d be p e r f o r m e d o n p i p e p r e h e a t e d t o
this i n v e s t i g a t i o n are p r e s e n t e d in r e s u l t i n g w e l d m e n t d e p o s i t s are listed 100-150C (212-300F). W e l d i n g w i t h -
T a b l e 1 . T h i s p i p e m a t e r i a l is an X-70 in T a b l e 2. o u t p r e h e a t w a s d o n e t o d e t e r m i n e if
g r a d e , p e a r l i t e - r e d u c e d M o - N b steel. h y d r o g e n assisted c r a c k i n g w o u l d o c -
These f o u r c o n s u m a b l e s w e r e c o m -
The material was s u p p l i e d by Vallour- cur. T h e a m b i e n t t e m p e r a t u r e w a s in
b i n e d to p r o d u c e w e l d m e n t s t y p i c a l o f
ec o f France f r o m t h r e e heats of n o m i - t h e range o f 1 5 - 2 1 C ( 6 0 - 7 0 F ) .
t h o s e u s e d in a c t u a l p i p e l i n e c o n s t r u c -
nally i d e n t i c a l steel a n d w a s u s e d in t i o n . Four w e l d s w e r e m a d e : The girth w e l d made using the E
this p r o j e c t w i t h o u t r e g a r d t o a n y p o s - 1 . E 8010 used f o r r o o t , h o t , a n d fill 8010 c e l l u l o s i c e l e c t r o d e f o r all passes
sible effects of h e a t - t o - h e a t variations. passes. s i m u l a t e s t h e t e c h n i q u e w h i c h is m o s t
T h e p i p e w a s 1219 m m (48 in.) in 2. E70S-1 B u s e d f o r t h e r o o t a n d h o t f r e q u e n t l y u s e d in t h e f i e l d . This p r o -
d i a m e t e r w i t h a 16 m m (0.661 in.) w a l l passes a n d E 8010 used f o r f i l l . c e d u r e w a s t o b e used as a c o m p a r i s o n
thickness. The three pipe sections 3. E 70S-1 B u s e d for t h e r o o t a n d h o t base f o r e v a l u a t i n g t h e o t h e r e l e c t r o d e
u s e d f o r t h i s s t u d y w e r e 1 m (39 in.) passes a n d E 8018-C1 u s e d f o r f i l l . p r o c e d u r e s . It w a s t h o u g h t t h a t t h e
l o n g . T h e e n d s w e r e b e v e l l e d t o a 30 4. E 70S-1B u s e d f o r t h e r o o t a n d h o t welders s h o u l d have been t h o r o u g h l y
in.H
fl- "X,
(9 in.
2W + 5 mm min. 2W + 5 mm min.
WELD REINFORCEMENT
SHOULD NOT BE REMOVED ON WALL = Critical COD value
EITHER SIDE OF SPECIMEN THICKNESS [3(a+z)/(W-a)] + l
Fig. 2Nick-break test specimen = Value of clip gauge displacement
WELDING R E S E A R C H S U P P L E M E N T I 39-s
familiar and have no difficulties with
this electrode. Table 4Typical Welding Parameters for the Implant Test
When using the G M A W process for
the remaining welds, however, diffi- Process: shielded metal arc welding (SMAW)
culties were encountered in trying to Voltage: 28-32 V
obtain adequate penetration. Limited Current: 150-155 A
on-site experimentation indicated that Travel speed: 4.7 mm/s (11 ipm)
a wider root gap was required for the Average heat input: 0.98 M|/m (25 kj/in.)
GMA weld as compared to the SMA Preheat: none
weld because arc penetration was less Ambient temperature: 23C (73F)
for the G M A W process. An opening of Electrode: Lincoln Shield Arc X-70, E-8010-G, 4 mm (3/ in.) diameter
at least 3 mm (% in.) seemed neces- Implant test schedule:
Relative time,
sary. Keeping a uniform gap was diffi-
minutes Action
cult w i t h the experimental set-up and, 0 Weld deposited
as a consequence, root penetration 2 Weld surface cooled in water
proved to be a continuing problem. 6 Specimen removed from water
The GMA welding technique was 10 Specimen loaded in test fixture, test-
acceptable in all other respects. ing commences
Actual welding performance of the 1000 Test ends for specimens which did
not break
vertical-up E 8018-C1 low-hydrogen
electrode was good. No difficulties
were encountered. A weaving tech-
nique was employed to deposit the procedure that exceeded the require- the weld zone of interest, a special
filler metal. ments of both Canadian Standards weld bead is placed parallel to the
For the Kobe LB-86VU vertical-down Association (CSA) Z184 and API 1104. long coupon axis and perpendicular to
low-hydrogen electrode, it was neces- The radiographs were sent to Climax the longitudinal axis of the weld to be
sary to deposit stringer passes w i t h no for inspection and to a qualified non- tested. This second weld is deposited
weaving of the electrode in order to destructive testing technician for ac- using a hardfacing type electrode and
keep the welding arc ahead of the tual interpretation. The pipes were serves as a crack starter into the zone
molten flux. This resulted in a number sectioned after the completion of to be tested. This brittle weld bead is
of stringers being used to weld the radiographic examination and half of notched transversely, thus assuring the
joint rather than a large flowing pud- the material sent to Climax and half to precise location of fracture initiation.
dle as with the vertical-up process. an electrode manufacturer for testing. Successive tests were made at the
Electrode travel speed varied by about The f o l l o w i n g tests were performed by three temperatures of interest. After
a factor of four between the two pro- the electrode manufacturer: impact loading, if the crack extends
cesses. The time required to complete Transverse weld metal tensile the full w i d t h of the coupon, the sam-
the weld was about the same, howev- tests. ple fails the test. If the crack is arrested
er, as the Kobe weld required 11 passes Drop weight tests. before extending completely across
and the E 8018-C1 weld required only Transverse root and face bend the specimen, the sample passes the
t w o (three passes were required for tests. test.
the 10-12 o'clock positions). Nick break tests. The temperature above which fail-
Although the pipeline company per- Charpy V-notch test in weld met- ure will not occur is called the nilduc-
sonnel making the welds had not used al. tility transition (NDT) temperature. It
the vertical-down type electrodes Chemical analysis of weld metal. is desired that the NDT temperature
prior to this trial, they seemed to The following tests were performed be lower than the service temperature.
adjust to the required procedures by Climax: The NDT temperature concept is app-
quickly and experienced what seemed Transverse base metal tensile licable to ferritic steels and has been
at the time to be only minor difficul- test. correlated to service performance of
ties. One such difficulty was the meth- Charpy V-notch tests of HAZ, root pressure vessels. A NDT temperature
od used to start the welding arc. Usual and fill passes. lower than the service temperature of
cellulosic electrode welding practice is Crack opening displacement the steel implies a certain degree of
to strike the electrode tip in the joint (COD) tests of HAZ, root and fill notch toughness at the service temper-
and then quickly draw it back, thus passes. ature.
forming the welding arc across the Metallographic examination. Nick-Break Test. This test is de-
gap. When this technique was used for Microhardness determination. scribed in API Specification 1104. The
the Kobe electrodes, severe porosity Base metal implant tests. specimen (Fig. 2) is approximately 230
was encountered. It was f o u n d , after All toughness tests were performed mm (9 in.) long, 25 mm (1 in.) wide by
the weld was almost complete, that a at temperatures of - 4 C ( + 25F), the pipe thickness. The weld is cen-
better technique was to bring the elec- - 2 3 C (-10F) or - 5 1 C (-60F). tered transverse to the coupon.
trode tip near the surface of the joint Tests performed at 51 C were for A small notch is saw cut into each
but w i t h o u t actually touching it. A information purposes only and are not edge of the coupon 3 mm (% in.) deep.
special tip material on each electrode required by the Foothills specifica- This notch locates the crack initiation
facilitated arc initiation with a small tions. point. The specimen is then broken by
tip-to-work distance. Large distances Drop Weight Test. The testing and either pulling in a tensile machine, by
caused insufficient shielding action evaluation was performed in accor- supporting the ends and striking the
and resulted in porosity. dance with ASTM E 208-69. The test center or by supporting one end and
uses a small coupon 50 x 127 mm striking the other end w i t h a hammer.
( 2 x 5 in.) by the pipe thickness pic- For this investigation, the specimens
Evaluation of Welds were broken by pulling in a tensile test
tured in Fig. 1. The coupon is tested in
Following completion of the girth three point bending applying a 400 | machine.
welds, the complete circumference of (300 ft-lb) impact load. O n the tension The requirement of the test is that
all welds was radiographed using a face of the coupon and located over the exposed surfaces of each specimen
4 0 - s l FEBRUARY 1980
Table 5-Results of Radiographic Analysis of Pipe Welds
72-78 Yes
78-84 Yes
84-96 Incomplete fusion No
102-108 Yes
Weld 4 108-114 Yes
E70S-1B/LB-86VU 120-126 Incomplete penetration No
132-138 Yes
138-144 Yes
Table 6-Test Results for Drop Weight, Bend and Nick-Break TestsTesting and Evaluation According to API 1104
1 8010/8010 Pass Pass Pass Pass Fail Pass Pass Pass Pass
2 E70S-1B/8010 Pass Pass Fail Fail Pass Pass Pass Pass Pass
3 E70S-1B/ Pass Pass Pass Pass Pass Pass Pass Pass Pass
8018-C1
4 E70S-1B/ Pass Pass Fail Pass Pass Pass Fail Fail Pass
Kobe LB-86VU
WELDING R E S E A R C H S U P P L E M E N T I 41-s
TEMPERATURE, F TEMPERATURE, F
-40 -20 +20 -60 -40 -20 +20
140 .140
T-
180 - 180-
~~i 1
\
Coarse Grained HAZ A Coarse Grained HAZ
160 - 120 160- 120
Weld Metal D = Weld Metal
140 - Root and Hot Pass 140- O - Root and Hot Pass
100 100
0 = Average of Weld Metal 0 = Average of Weld Metal
120 - Samples Tested by an 120- Samples Tested by an
Electrode Manufacturer 80 T Electrode Manufacturer 80
100 - 100-
80 - -- 60 5 80- '60 S
A cc
Ui
60 - at 60-
*
40 - 8 40- 40 5
40
20 -
e 20-
20
- 20
0
0
1UU 1 1 1 A 1 i 1 1 i i 1
" A
A
80 - 80 _
0
cu A a
- . - 8-
| 60
40 9 o
ID
2 o
o B 40 o
ID cc A D
20 A - ID O
D O
20
n Al 1
-40
i
-20
i 1
-10
a 1 1 1
-50 30 -30
TEMPERATURE, C
0
TEMPERATURE, C
Fig- 4Results of Charpy V-notch tests performed by Climax on fill Fig. 5Results of Charpy V-notch tests performed by Climax on fill
and root passes and in the HAZ, weld 1, E8010/E8010 and root passes and in the HAZ, weld 2, E70S-1B/E8010
TEMPERATURE, F TEMPERATURE, F
-60 -40 -20 0 +20 -20
140 140
1 1 1 i 1 i i r
180 180
A = Coarse Gra ned HAZ A = Coarse Grained HAZ
120
160 = Weld Metal - 120 160
D = Weld Metal
140 0 ' Root and Hot Pass 140 O = Root and Hot Pass
100 100
o =Average of Weld Metal A O = Average of Weld Metal
i?n Samples Te ted by an 120 Samples Tested by an
Electrode Manufacturer
^ 80 Electrode Manufacturer
O 100
A - 100
80 fj_ _60 80
tt.
60 60
D 40 40
D
0 40
40
20
A - 20 20
20
1 I 1 i 1 0 0
too 1 1 1 1 00 - 1 1 1 A 1 1 A -
A
A
80 A oO A A -
D
60 60 - n-
1 o -
40 A 40 8-
1
o
0 O
20 20 O
ID
O -
n D
i i 1 0 1 1 1 1 I
-30 -20 -40 -30
TEMPERATURE, TEMPERATURE, C
Fig. 6Results of Charpy V-notch tests performed by Climax on fill Fig. 7-Results of Charpy V-notch tests performed by Climax on fill
and root passes and in the HAZ, weld 3, E70S-1B/E8018-C1 and root passes and in the HAZ, weld 4, E70S-1B/Kobe LB-
86V U
the crack tip opening displacement whose ductility does not permit plane this notch was extended an additional
(COD) at the test temperature by strain (K lc ) testing. 1 to 2 mm (0.04 to 0.08 in.). The
using a published theoretical equa- For this investigation, specimens precracking load minima and maxima
tion, which is also included in Fig. 3. were initially notched in the area of were 66 N (15 Ibf) and 8385 N (1885
The C O D value is obtained from an interest using an EDM. The depth of Ibf) for heat-affected zone (HAZ)
extension of linear elastic fracture this notch was 2 mm (0.079 in.). By areas and 71 N (16 Ibf) and 8830 N
mechanics and applies to materials fatigue precracking each specimen, (1985 Ibf) for the weld areas. The total
4 2 - s l FEBRUARY 1980
Table 8-Results of Charpy V-Notch (CVN) Tests Performed by an Electrode Manufacturer, Five Samples Tested, At Each Temperature, )
(ft-lb)
Testir g temperature
W e l d num ber,
consumaf )les Test location - 4 C ( + 25F) - 2 3 C (-10F) - 5 1 C (-60F)
'"Porosity.
""Lack of fusion.
" ' D u p l i c a t e specimen exceeded 0.15 m m (0.006 in.) reference value.
length of precracking was determined at the root of the notch. A relatively guide is used to control travel speed.
after C O D testing by fracturing the high cracking susceptibility w o u l d By this method, the heat input is held
samples and measuring the actual mean that, using the shielded metal within about 8% of the average value.
crack length. ate process, welding of the steel w o u l d The welding parameters used are given
The bend test fixture satisfies the be difficult due to a high tendency for in Table 4.
requirements of ASTM E 399 for frac- hydrogen assisted cracking. The welded surface of the implant
ture mechanics testing. The specimen, For this investigation, the implant test assembly was placed in water
clip gauge and bend test fixture were test was performed as follows. Cylin- exactly 2 min after the test weld was
immersed in a tank containing metha- drical specimens 5.6 mm (0.22 in.) in completed and held in contact w i t h
nol and solid carbon dioxide which diameter were machined w i t h axes water for 4 min. The test assembly was
was used to maintain the test temper- transverse to the original rolling direc- removed from the water 6 min after
ature. tion. One end of each specimen was completion of the test weld and
Implant Test. The implant test3 is threaded to apply a load after welding. loaded in a modified creep testing
frequently used to evaluate the hy- A helical notch was machined at the machine 10 min after completion of
drogen assisted or cold cracking sus- other end of each specimen using a the test weld. Welded specimens of
ceptibility of steels. In this test, a special carbide cutting tool. The notch each steel were subjected to various
notched bar is incorporated into a radius and effective cross-sectional loads for 1000 min or until failure
weldment in such a way that the mate- area were measured w i t h the aid of an occurred. The critical stress was deter-
rial at the root of the notch is raised to optical comparator. Only those speci- mined graphically. The applied stress
a temperature approaching the fusion mens having a root radius of approxi- was plotted against log time to failure,
point of the steel. During the welding mately 0.008 mm (0.0003 in.) were used and the lower limit of the scatter band
process, hydrogen is introduced into for implant testing. that asymptotically approached a hori-
the weldment from the cellulosic elec- In the test, the notched end of the zontal line was taken as the critical
trode used to make the deposit. Subse- specimen is inserted into a hole drilled stress.
quent loading of the test bar simulates in a 14.5 mm (0.57 in.) thick mild steel Other Tests. The transverse weld
weld restraint which can lead to plate. The test weld is then deposited tensile tests, base metal tensile tests
delayed cracking. This delayed crack- d o w n the center of the plate, fusing in and bend tests were conducted
ing apparently results from hydrogen the notched end of the specimen. The according to API Specification 1104.
assisted propagation of cracks initiated test weld is deposited manually but a For metallographic examination, se-
4 4 - s l FEBRUARY 1980
Based upon this value virtually all of DISTANCE (X1000), INCHES
the specimens "passed." For many of 40 20 0 20 40 60 80 100 120 140
the various weldment/temperature
combinations, t w o tests were per-
formed. This was especially true if the
first measured C O D value was less
than 0.15 mm (0.006 in.). Due to a lack
of materials, duplicate tests were not
possible at all temperatures.
Microhardness Test
A graphical plot of Vickers hardness
vs. relative position in the weldment is
shown in Fig. 8. It compares the five
areas of interest in this investigation. It
should be noted that a 1 kg (2.2 lb)
load was used for the microhardness
tests, as has been the practice at Cli-
max. The Foothills specification calls
for a 0.5 kg (1.1 lb) load and requires
that no area should have a microhard-
ness greater than 350 HV0.5.
The maximum hardness for all welds
was well below the allowed maximum
so that the differences in loads should
not be significant. The base metal
hardness of the X-70 pipe was about
214 HV1. Thus it may be seen that the
traverse did not go completely out of
the HAZ and into the base metal;
however, the area of maximum hard-
ness was crossed.
Implant Test
The lowest applied stress (critical
stress) that resulted in the failure of an
implant specimen was 220 MPa (32
ksi)Fig. 9. This implies a CS/UTS ratio 1.0 0.5 0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0
of 0.34. F N
LINE DISTANCE, mm
This value is somewhat lower than
that obtained for pipeline steels of Fig. 8Microhardness of weld and HAZ
similar composition. However, it is sig-
nificant to note that even w i t h this made using the same electrode. The
value, no hydrogen assisted cracking Figure 11 shows the structure of the microstructure is the same.
was detected, even though no pre- root pass made using the 8010 elec- Figure 13 shows the structure of the
heating of the pipes was performed. trode. It consists of a very fine poly- weld made using the 8018-C1 elec-
Since usual field practice is to preheat gonal ferrite w i t h pearlite. Figure 12 trode. It is mainly acicular ferrite and
prior to welding, hydrogen assisted shows the structure of the fill passes polygonal ferrite w i t h scattered mar-
cracking should not be a problem with
the low-carbon M o - N b steel.
300 r -ii i i i 111 1 1i i i i 111 1 1 |
40
Metallography
Photomicrographs of the weldments
are shown in Figs. 10 to 15. Figure 10
shows the microstructure of the M o -
Nb X-70 pipe steel. It consists of a Vo-
mixture of polygonal ferrite, pearlite
and upper bainite. A large fraction of 200
the ferrite has been deformed by con-
trolled rolling of the pipe skelp below 0
the Ar, temperature. This controlled
rolling procedure results in a rounded
stress-strain curve w i t h an appreciable - 20
work hardening rate, so that the
formed pipe has a higher yield
strength than the skelp. This offsets I 1 I I I I I I
-I I I I
the loss in yield strength due to the 10 100 1000
Bauschinger effect that occurs during TIME TO FAILURE, MINUTES
testing of a flattened API tensile speci- Fig. 9Implant test results
W E L D I N G RESEARCH S U P P L E M E N T I 45-s
^58
Jf--, . - / tr f. t, '-t>
^T'* j v ' ^ -* ' ' ^ ^ '"^* - ... ;
> ^ *
4^
^
m
**
?
. > . ; > i ' 2*
'-rt'"
wii
^ 'J*,' 7%
.V "
-i8..
<f. v'. \ \'iS- v *> -'^'"Vi' v.c
tensite islands. Figure 14 shows the ers. However, the results of the radio- welds were completed and the radio-
structure of the weld made using the graphs and examination of selected graphs interpreted.
Kobe electrode. It consists of acicular samples obtained from several sets of Because of these weld quality prob-
ferrite with small martensite islands. tests indicate that the welds were not lems, which w o u l d not exist if proper
Figure 15 shows the microstructure of of o p t i m u m quality. It became appar- training time were available, the
the E70S-1B used for the G M A W root ent that a welder required a certain results of the mechanical tests may be
passes. This microstructure is predomi- amount of practice w i t h an unfamiliar too conservative. Thus, the CVN test
nately acicular ferrite w i t h many small consumable before his usual high level results at - 2 3 C (-10F) on the weld
martensite islands. A few round sili- of quality could be achieved. deposits should be interpreted w i t h
cate inclusions may be seen. These Unfortunately, the amount of prac- some flexibility. The above comment
inclusions may have reduced the tice required, in some cases, proved to should also be kept in mind when
toughness of this weld. be more than was available. This is considering the three bend tests, the
especially true for weldments 1, 2 and one nick-break and possibly the t w o
4. Weldment 3, the low-hydrogen ver- dropweight test failures at 51 C
Discussion ( - 6 0 F).
tical-up weld seemed to present few
Based upon the results of the tests welding difficulties judging by the Further improvements of welding
performed, weldments made using radiography results. W e l d 4, the Kobe consumables could be efficacious. The
any of the four consumable/process low-hydrogen vertical-down weld, ex- four consumables evaluated in this
variations w o u l d be suitable, for the hibited porosity problems due to the investigation were selected because
most part, for service at - 4 C ( + 25F) welder using an inappropriate starting these materials were readily available
as specified by Foothills. The reason and stopping procedure. and were of practical interest. Based
for qualifying this statement is due to The correct procedure was devel- upon the results of this study, other
the results of the bend and nick-break oped by trial and error, but this exper- consumables should be tested and
tests (both of which are more depen- imentation was conducted in the compared to see if they offer improve-
dent on operator technique than on weldment to be evaluated. Welds 1 ments in either ease of welding or
the consumables used). This service and 2, the cellulosic welds, were mechanical properties.
temperature applies to 98% of the intended to serve as a base for com- It was shown that the HAZ of the
Canadian portion of the pipeline. paring the other consumables. It M o - N b X-70 pipe exhibited acceptable
At - 2 3 C (-10F), the test results became apparent that, even though properties d o w n to at least 23C
were mixed. It is possible that the welders used similar cellulosic (10F)that is, the microhardness
increases in impact energy absorption electrodes in their work, the different was w i t h i n specification, the C O D val-
at this temperature may be achievable arc characteristics required a slightly ues generally exceeded 0.15 mm (0.006
w i t h o u t excessive efforts. Again, weld different method of manipulating the inches) even at - 5 1 C (-60F), and
quality should improve w i t h better electrode as the weld progressed. HAZ apparently is not a problem as
operator skill and also through the use Again, due to lack of material, the evidenced by the implant test and
of improved consumables. learning was obtained on the weld welding the pipe w i t h o u t preheat.
As stated previously, all personnel which was evaluated. The severity of Even though the actual weld deposits
making the welds were skilled w e l d - this problem was not evident until the examined in this study were not c o m -
4 6 - s l FEBRUARY 1980
pletely acceptable at - 2 3 C (-10F), Lines (Yukon) Ltd. specifications. References
the low-carbon M o - N b X-70 pipe It was found that all weldments met 1. Tither, G., and Lavite, M., "Beneficial
steel, as evidenced by the acceptable the requirements for service at - 4 C Stress-Strain Behavior of Moly-Columbium
HAZ toughness properties, appears to ( + 25F). While the X-70 pipe ex- Steel Line Pipe," Journal of Metals, Septem-
meet the requirements for Arctic pipe- ceeded the lower temperature require- ber 1975, pp. 15-23.
lines. ments, the weld deposits showed 2. "Methods for Crack Opening Dis-
placement (COD) Testing," British Stan- Q-
mixed results at - 2 3 C (-10F). These O
welds w o u l d probably pass all require- dards Institution, DD 99:1972.
Conclusions 3. Granjon, H., "The Implants Method
ments at - 2 3 C (-10F) if w e l d q u a l i t y
for Studying the Weldability of High
Extensive testing was performed on were optimized. It w o u l d appear, Strength Steels," Metal Construction, (11),
a series of M o - N b X-70 steel pipe however, that better welding tech- Nov. 1969, pp. 505-515.
weldments made using SMA and GMA niques and/or consumables should be X
4. "Specification for High Strength Steel
welding techniques and four electrode investigated aiming to come up w i t h Line Pipe 457 mm (18 inches) and Larger in o
combinations. The evaluation criteria improved weld performance at 23C Diameter," Number P-100, July 14, 1978, <
were the API 1104 and Foothills Pipe (-10F). Foothills Pipe Lines (Yukon) Ltd. LU
lf>
LU
Full details are contained in the tentative program for the 61st
Annual Meeting technical sessions program that appeared in
the December 1979 issue of the Welding Journal.
W E L D I N G RESEARCH S U P P L E M E N T I 47-s