SOP FOR DYE SEALING TEST FOR ANODIZED ALUMINIUM

OBJECTIVE & SIGNIFICANCE OF TEST:- The purpose of sealing an Anodic coating is to

close the pore structure of the anodic film & render the film inert. This is accomplished by
chemically changing the surface oxide structure through hydration with hot water & metallic based
sealing compounds. This sealing process useful for Non staining, Non absorbing, Non reacting, Non
corroding properties. To check the effectiveness of sealing process, dye sealing test is
recommended. It is test of ability of Anodized coating to absorb dyestuffs under specified
conditions.
CHEMICAL REAGENTS:- 1:3 Nitric Acid, Mercuric Blue Dye

PROCEDURE:-
1. Clean the Aluminum Anodized surface with tap running water to remove any dirt, dust etc.
2. Put 2 – 3 drops of 1:3 Nitric Acid on anodized surface with the help of glass rod for Etching
purpose. Wait for 2 minutes.
3. After 2 minutes, clean the anodized surface with tap running water.
4. Then put 2 – 3 drops of Mercuric blue dye on Etched surface with the help of glass rod and
allow it for 2 – 3 minutes for better penetration of dye.
5. Then again clean the test area with tap running water & wipe it with dry cloth & then observe
for any stain marks of dye remains on the surface by visually.
6. Acceptance Criteria – More than 90 % dye stain marks should get invisible.

DO’S & DON’T:-

1. Before the test clean the test specimen properly to remove any surface contaminations.
2. Use separate Glass rods for Nitric Acid & dye respectively.
3. Handle the dye carefully otherwise the dye stain marks on cloths will not be easily get
removed.

SAFETY PRACUATIONS:-
1. Use Rubber hand gloves and safety goggles while handling the Nitric Acid.
2. Diluted Nitric acid should be kept in air tight glass bottle with proper identification.