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FILRTATION
Submitted by:
SANTOS, Amabelle C.
VALDEZ, Loisroi R.
Submitted to:
FILTRATION 1
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
TABLE OF CONTENTS
Filtration 3
History 4
Applications 6
Classification of Filtration Equipment 9
According to Driving Forces 9
According to filtration mechanism 12
According to process goal or objective 14
EQUIPMENT 17
Top suspended centrifuge 17
Continuous centrifugal separator 20
Rapid Sand Filter 23
Slow Sand Filter 28
Liquid Clarification 33
Cartridge Filtration 34
Bag Filter 38
Crossflow Filtration 44
Filter Pore Size 47
Discontinuous Pressure Filters 53
Discontinuous Vacuum Filters 57
Filter Press 63
Rotary Vacuum Drum Filter 70
References 75
FILTRATION 2
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
FILTRATION
Filtration is the removal of solid particles from a fluid by passing the fluid
through a filtering medium, or septum, on which the solids are deposited.
Industrial filtrations range from simple staining to highly complex separation.
The fluid may be a liquid or gas; the valuable stream from the filter may be the
fluid, or the solids or both.
FILTRATION 3
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Basic Operation: Slurry mixture enters the inlet pipe and will pass through
several layers of filters. Small particles will only pass on the filters depending on
the type and size of the pores of the filter. Liquid passed through all series of
filter are drained at the outlet pipe. Large particles will be deposited on the
surface of the filters and may form cake. This cake formation may be drained by
cleaning or by other methods.
HISTORY
During the 19th and 20th centuries, water filters for domestic water
production were generally divided into slow sand filters and rapid sand filters
(also called mechanical filters and American filters). While there were many
small-scale water filtration systems prior to 1800, Paisley, Scotland is generally
acknowledged as the first city to receive filtered water for an entire town. The
Paisley filter began operation in 1804 and was an early type of slow sand filter.
Throughout the 1800s, hundreds of slow sand filters were constructed in the UK
and on the European continent. An intermittent slow sand filter was constructed
and operated at Lawrence, Massachusetts in 1893 due to continuing typhoid
FILTRATION 4
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
fever epidemics caused by sewage contamination of the water supply. The first
continuously operating slow sand filter was designed by Allen Hazen for the city
of Albany, New York in 1897. The most comprehensive history of water filtration
was published by Moses N. Baker in 1948 and reprinted in 1981.
Rapid Sand Filtration
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
APPLICATION
On an industrial scale, filtration is used by the oil, gas, food and beverage,
and among others. Municipalities use filtration techniques when treating sewage
and purifying water.
Filtration cleans up river streams or other water streams. Furnaces use filtration
to prevent the furnace elements from fouling with particulates. Pneumatic
conveying systems often employ filtration to stop or slow the flow of material that
is transported, through the use of a baghouse.
In Water Treatment
FILTRATION 6
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
The most common type of filter is a rapid sand filter. Water moves vertically
through sand which often has a layer of activated carbon or anthracite coal above
the sand. The top layer removes organic compounds, which contribute to taste
and odor. The space between sand particles is larger than the smallest
suspended particles, so simple filtration is not enough. Most particles pass
through surface layers but are trapped in pore spaces or adhere to sand
particles.
In Oil Refinery
This means that any emulsion of oil and water will have to be broken before
final oil/water separation. For safety’s sake, a microfilter may be used at the well
head, although the flow rates will be high, and the filters will have to be
automatically (or easily manually) cleaned.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
In Gas Treatment
Natural gas produced in association with crude oil will not normally
present a filtration problem - from solids at least, although it may need
separation from oil or water droplets. However, there is nowadays an increasing
need for the injection of gases into underground strata, to improve oil production
rates. Increasingly this is done directly into the rock formation, either as an
enhanced oil recovery process or as a sequestration method for carbon dioxide
disposal.
The direct injection of gases will require that they be free from suspended solids,
possibly down to the same size level as is the case for water injection, namely
around 2μm. This will be done in the same sort of filters as are used for engine
intakes, using V-block minipleat filter panels, for example.
In Food Industy
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Ultrafiltration (UF). The ultrafiltration (UF) membrane separates the feed (e.g.
skim milk) into two streams, allowing water, dissolved salts, lactose, and acids
to pass through it in either direction, while retaining (and thereby concentrating)
proteins and fat.
Microfiltration (MF). Microfiltration uses the most open type of membrane, which
is used to separate bacteria, spores, and fat globules from the stream, and for
fractionation of skim milk.
GRAVITY FILTRATION
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
PRESSURE FILTRATION
Ex. Plate and Frame Filter Press, Shell and Leaf Filters
FILTRATION 10
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
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Vacuum Filtration
Suction filtration is a
filtration technique which
allows for a greater rate of
filtration. Whereas in normal
filtration gravity provides the
force which draws the liquid
through the filter paper, in
suction filtration a pressure
gradient performs this
function. This has the advantage of offering a variable rate depending on the
strength of the pump being used to extract air from the Büchner flask. Care
must be taken not to use such a strong vacuum that the filter paper rips (in
which case all the solid will be lost back into the solvent) or in extreme cases the
glass flask breaks. Suction filtration is used in recrystallisation experiments.
CENTRIFUGATION
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
the centrifuge, an oil driven rotor spins at high speeds of up to 7000 rpm. The
resulting gravitational force draws any particles outwards while the purified
substance passes back into your machinery. This way, soot and other
contaminants are continually removed during normal engine operation.
Cake filtration
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
time that a filter unit can be operational. It can be a continuous process, unlike
batch-wise dead-end filtration.
This type of filtration is typically selected for feeds containing a high proportion
of small particle size solids (where the permeate is of most value) because solid
material can quickly block (blind) the filter surface with dead-end filtration.
Industrial examples of this include the extraction of
soluble antibiotics from fermentation liquors.
Depth filtration
Depth filters are the variety of filters that use a porous filtration medium to
retain particles throughout the medium, rather
than just on the surface of the medium. These
filters are commonly used when the fluid to be
filtered contains a high load of particles because,
relative to other types of filters, they can retain a large mass of particles before
becoming clogged.
Depth filtration typified by multiple porous layers with depth are used to capture
the solid contaminants from the liquid phase. Due to the tortuous and channel-
like nature of the filtration medium, the particles are retained throughout the
medium within its structure, as opposed to on the surface. Depth filters pose the
added advantage that they are able to attain a high quantity of particles without
compromising the separation efficiency. Depth filters are commonly
characterised by the sand filter and have the ability to be used with substantially
higher filter rates than in other designs. It is these characteristics that have
cemented the use and popularity of depth filters as an effective medium for
separation. With ongoing advances in process technologies depth filter designs
are continuously adapting and improving to meet the needs of industry.
FILTRATION 13
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
The process goal of filtration may be dry solids (the cake is the product of value),
clarified liquid (the filtrate is the product of value), or both. Good solids recovery
is best obtained by cake filtration, while clarification of the liquid is accomplished
by either depth or cake filtration.
CAKE FILTRATION
A filter cake is formed by the substances that are retained on a filter. The filter
cake grows in the course of filtration, becomes "thicker" as particulate matter is
being retained. However, cake filtration in terms of process goal or objective
mainly focuses on the cake as its product. An example is the process of Miscella
Filtration for oils.
CLARIFYING FILTRATION
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
the flow channels, where they reduce the effective diameter of the channels but
usually do not block them completely.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
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Solution that is
directed to the
membrane surface
is called the feed.
Solution that
passes along the
membrane surface
and back to the
feed reservoir is
the retentate. This
solution is usually pumped back to the feed reservoir and recirculated. Solution
that passes across the membrane is the permeate.
FILTRATION 16
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
EQUIPMENT
PARTS
1. Motor – it holds the vertical shaft that holds and spins the basket during
the process.
2. Feed Inlet - entrance of the slurry mixture.
3. Liquor Outlet – exit of the liquid or the filtrate.
4. Screen or Filter – the medium to filter solids from liquid or liquid to liquid.
5. Perforated Basket – a wall that has holes in it that enables the filtrate to
escape from the solids, which then stops at the casing.
6. Casing – is a wall that prevents the filtrate to escape from the sides. The
casing also provides guide in where the solids it to be discharged.
7. Wash Inlet – solvent or water discharge that will help to dissolve the
remaining soluble components in the cake.
FILTRATION 17
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
8. Adjustable Unloader Knife – this cuts the cake formation in the lining of
the filter. It removes the cake and drops it into the solid discharge outlet.
MECHANISM
Feed slurry enters the rotating basket through an inlet pipe or chute.
Liquor drains through the filter medium into the casing and out a discharge pipe:
the solids form a cake 50 to 150 mm (2 – 6 in.) thick in the basket. Wash liquid
may be sprayed through the solids to remove soluble material. The cake is then
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
spun as dry as possible, sometimes at a higher speed than during the loading
and washing steps. The motor is shut off and the basket nearly stopped by means
of a brake. With the basket slowly turning at perhaps 30 – 50 rpm, the solids are
discharged by cutting them out with an unloader knife, which peels off the filter
medium and drops it through an opening in the basket floor. The filter medium
is rinsed clean, the motor turned on, and the cycle repeated.
APPLICATION
FILTRATION 19
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
A continuous centrifugal
separator is a continuous type
centrifuge rotating on a vertical axis
and can be used for a 2-phase
liquid/solid separation or a 3-phase
liquid/liquid/solid separation. Usually
used when there are fines or soft solids
approximately 1% -10% by volume.
Separation takes place in the bowl
assembly. The feed to the centrifuge is
continuous and not interrupted.
A continuous centrifugal
separator for coarse crystals is the
reciprocating conveyor centrifuge. The gentle acceleration of the feel slurry and
deceleration of the discharged solids minimize breakage of the crystals.
Multistage units that minimize the distance of travel of the crystals in each stage
are used with solid cakes that do not “convey” properly in a single-stage machine.
Reciprocating centrifuges are made with baskets ranging in diameter from 300
to 1200 mm (12 to 48 in.). They dewater and wash 0.3 to 0.25 tons/h of solids
containing no more than 10 percent by weight of materials finer than 100- mesh.
FILTRATION 20
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
PARTS
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
MECHANISM
Feed enters the small end of the funnel from a stationary pipe at the axis
of rotation of the basket. It travels toward the large end of the funnel, gaining
speed as it goes, and when it spills off the funnel onto the wall of the basket, it
is moving in the same direction as wall and at very nearly the same speed. Liquor
flows through the basket wall, which may be covered with a woven metal cloth.
A layer of crystals 25 to 75 mm (1 to 3 in,) thick is formed. This layer is removed
over the filtering surface by a reciprocating pusher. Each stroke of the pusher
moves the crystals a few inches toward the lip of the basket; on the return stroke
a space is opened on the filtering surface in which more cake can be deposited.
When the crystals reach the lip of the basket, they fly outward into a large casing
and drop into a collector chute. Filtrate and any was liquid that is sprayed on
the crystals during their travel leave the casing through separate outlets.
APPLICATION
After crystallization the drugs are separated from the mother liquor by
centrifugation. For example traces of mother liquor is separated from aspirin
crystals by centrifugation method. During manufacturing they remain in
colloidal dispersion in water. By normal methods of filtration it is difficult to
separate the colloid particles. In those cases centrifugal methods are used.
Insulin is purified from other precipitates of protein materials by centrifugation.
FILTRATION 22
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
The first modern rapid sand filtration plant was designed and built
by George W. Fuller in Little Falls, New Jersey. Fuller's filtration plant went into
operation in 1920 and its success was responsible for the change to this
technology in the U.S Rapid sand filters were widely used in large municipal
water systems by the 1920s, because they required smaller land areas compared
to slow sand filters.
FILTRATION 23
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
FILTRATION 24
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
FILTRATION 25
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
The cost of energy required to operate a rapid sand filter and the costs for
treatment of generated sludge during backwashing may add significant costs
(UNEP 1998). Although operation is usually conducted automatically, frequent
inspection by a well-educated worker is necessary to ensure proper treatment.
Maintenance costs will include repairs of the filters and replacement of
equipment. In general, construction, operation and maintenance costs for rapid
sand filters are significantly higher than costs for slow sand filters (UNEP 1998).
FILTRATION 26
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
ADVANTAGES
DISADVANTAGES
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Slow sand filtration has been an effective water treatment process for
preventing the spread of gastrointestinal diseases for over 150 years, having been
used first in Great Britain and later in other European countries (LOGSDON
2002). SFFs are still used in London and were relatively common in Western
Europe until recently and are still common elsewhere in the world. The move
away from slow sand filtration in industrialized countries has largely been a
function of rising land prices and labour costs, which increased the cost
FILTRATION 28
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
of SSF produced water. Where this is not the case, SSFs still represent a cost-
effective method for water treatment (WHO n.y.). Since these conditions prevail
in many developing countries, it is a very promising technique for water
purification and, therefore, the development of a sustainable water system.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
of the SSF is equivalent to the bio-sand filtration. While the former is applied to
semi-centralised water treatment, the latter mainly serves household purposes.
Structure
Once a SSF facility is built, only clean sand is required for occasional
replacement. The sand layers are put in gradually according to their grain sizes:
rather coarse grains at the bottom and fine grains at the top. The sand-bed is
usually covered with one meter of supernatant water (LOGSDON 2003). As the
process of biological filtration requires a fair amount of time in order to purify
the water sufficiently, SSFs usually operate at slow flow rates between 0.1 – 0.3
m3/h per square metre of surface (WHO n.y.). The water thus remains in the
space above the medium for several hours and larger particles are allowed to
separate and settle (see also sedimentation). It then passes through the sand-
bed where it goes through a number of purification processes (HUISMAN 1974).
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
The water requires some kind of physical pressure in order to pass the
drag created by the sand layers. In terms of construction, two different types are
feasible. The pressure can be built up either by pumps or gravity. While pump
systems need some type of engine and a more elaborate construction, gravity
systems work without any highly technological means (HUISMAN 1974).
Operational costs are incurred almost solely from the cleaning of the filter
beds. No chemicals or other materials are needed for the process. No compressed
air, mechanical stirring, or high-pressure water is needed for backwashing.
There is thus a saving not only in the provision of plant but also in the cost of
fuel or electricity (HUISMAN 1974).
At a Glance
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
ADVANTAGES
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
DISADVANTAGES
• Minimal quality and constant flow of fresh water required: turbidity (<10-
20 NTU) and low algae contamination. Otherwise, pre-treatment may be
necessary
• Cold temperatures lower the efficiency of the process due to a decrease in
biological activity
• Loss of productivity during the relatively long filter skimming and ripening
periods
• Very regular maintenance essential; some basic equipment or ready-made
test kits required to monitor some physical and chemical parameters
• Possible need for changes in attitude (belief that water that flows through
a green and slimy filter is safe to drink without the application of
chemicals), Chemical compounds (e.g. fluorine) are not removed
• Natural organic matter and other DBPs precursors not removed (may be
formed if chlorine is applied for final disinfection)
• May require electricity
• Requirement of a large land area, large quantities of filter media and
manual labor for cleaning, Low filtration rate
Liquid Clarification
Clarifiying filters for liquids include the gravity-bed filters for water treatment
and a variety of cartridge filters. Some cake filters, especially tank filters and
precoat filters are also used extensively for clarification. In a batch unit, the
filtration rate and soilds removal efficiency are typicallt almost constant for a
considerable period of operation, but eventually the soild content of the effluent
rises to an unacceptable value and backwashing of the filter becomes necessary.
FILTRATION 33
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
CARTRIDGE FILTRATION
Cartridge filters are a very important means of effecting a clarification and have
found use in a wide variety of industries. Advances in membrane manufacture
have enabled cartridge suppliers to use filtration media capable of retaining all
particulates down to 0.1 μm in diameter, and with significant removal of colloidal
material below this size. Cartridge filters can be classified into three groups:
depth, surface and edge, with additional subdivision.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
top of the casing. Solids are trapped between the disks and remain in the filter.
Periodically, the accumulated solids must be dislodged from the cartridge.
Advantages Disadvantages
Save on water – no backwashing can More air pressure when compressed.
result in saving thousands of litres
per year.
Low maintenance – most only need More difficult of reverse air.
cleaning once or twice per season.
Easy to install. There is less plumbing Less choice of filter material.
required because there is no
backwash piping required.
They generally take up less room. Not be as efficient when filtering larger
particulate at higher concentrations.
Cartridge filters are generally
regarded as filtering down to 30
microns. However, over a short period
of time they can be filtering down to
5-10 micron.
Very effective against very small
contaminants, at a concentration of
less than 50 ppm.
FILTRATION 35
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Gas Cleaning
Filters for gas cleaning include pad filters for atmospheric dust and granular
beds and bag filters for process dusts. Air is cleaned by passing it through pads
of cellulose pulp, cotton, felt, glass fiber or metal screening; the pad material
may be dry or coated with a viscous oil to act as a dust holder. For light duty the
pads are disposable but in large-sclae gas ceaning they are frequently rinsed and
recoated with oil.
Granular bed filters contain stationary or moving beds of granules. A bag filter
contains one or more large bags of felt or thin woven fabric, mounted inside a
metal housing. Dust-laden gas usually enters the bag at the bottom and passes
outward, leaving the dust behind. Efficiencies are typically 99% even with
exteremmely fine partciles – far finer than the openings in the bag material.
FILTRATION 36
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
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• Principle of Clarification
If the solid particles being removed completely plug the pores of the filter
medium and the rate of plugging is constant with time, the mechanism is known
as dierct sieving. Direct sieving is rarely encountered. Much more commonly the
particles partially block the pores, giving a gradual reduction in pore size; this is
called standard blocking.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
BAG FILTER
A baghouse (BH, B/H), bag filter (BF) or fabric filter (FF) is an air pollution
control device that removes particulates out of air or gas released from
commercial processes. Power plants, steel mills, pharmaceutical producers, food
manufacturers, chemical producers and other industrial companies often use
baghouses to control emission of air pollutants. Baghouses came into
widespread use in the late 1970s after the invention of high-temperature fabrics
(for use in the filter media) capable of withstanding temperatures over 350 °F.
Most baghouses use long, cylindrical bags (or tubes) made of woven or felted
fabric as a filter medium. (For applications where there is relatively low dust
loading and gas temperatures are 250 °F or less, pleated, nonwoven cartridges
are sometimes used as filtering media instead of bags.) Dust-laden gas or air
enters the baghouse through hoppers (large funnel-shaped containers used for
storing and dispensing particulate) and is directed into the baghouse
compartment. The gas is drawn through the bags, either on the inside or the
outside depending on cleaning method, and a layer of dust accumulates on the
filter media surface until air can no longer move through it. When sufficient
pressure drop (delta P) occurs, the cleaning process begins. Cleaning can take
place while the baghouse is online (filtering) or is offline (in isolation). When the
compartment is clean, normal filtering resumes.
Types of Baghouses
• Mechanical shakers
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College of Engineering and Technology
Department of Chemical Engineering
In reverse-air baghouses, the bags are fastened onto a cell plate at the
bottom of the baghouse and suspended from an adjustable hanger frame
at the top. Dirty gas flow normally enters the baghouse and passes
through the bag from the inside, and the dust collects on the inside of the
bags.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
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the dust cake to crack and fall into the hopper below. At the end of the
cleaning cycle, reverse airflow is discontinued, and the compartment is
returned to the main stream.
The flow of the dirty gas helps maintain the shape of the bag. However, to
prevent total collapse and fabric chafing during the cleaning cycle, rigid
rings are sewn into the bags at intervals.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
This cleaning system works with the help of digital sequential timer
attached to the fabric filter. this timer indicates the solenoid valve to
inject the air to the blow pipe.
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College of Engineering and Technology
Department of Chemical Engineering
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Advantages Disadvantages
It is simple, continuous cleaning, has a high resistance which is about
resistance stability, high filtration 600-1200P
speed, no internal moving parts,
simple design and other
characteristics, is a high
performance bag filter.
High removal efficiency can trap It is easy to stoppage the bags and
more dust 0.3UM so dusty gas the operating life is about 3 to 5
purification to 15mg / m3 or less. years.
can capture electrostatic
precipitator dust is difficult to
recover, and to some extent,
nitrites, sulfides and other
compounds can be collected
changes in load adaptability,
especially suitable trapping fine
dry dust, collect dry dust to
facilitate the handling and
recycling.
baghouse collection containing
explosive or dusty gas with a spark
higher security.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
CROSSFLOW FILTRATION
Cross flow filtration (CFF, also known as tangential flow filtration TFF) is a
filtration technique in which the starting solution passes tangentially along the
surface of the filter. A pressure difference across the filter drives components
that are smaller than the pores through the filter. Components larger than the
filter pores are retained and pass along the membrane surface, flowing back to
the feed reservoir.
Solution that is directed to the membrane surface is called the feed. Solution
that passes along the membrane surface and back to the feed reservoir is the
retentate. This solution is usually pumped back to the feed reservoir and
recirculated. Solution that passes across the membrane is the permeate.
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College of Engineering and Technology
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System Configuration
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• A retentate pump may be used to maintain and control flow of retentate back
into the feed reservoir.
• A permeate pump may be used to control flow of permeate from the filter. The
permeate pump, if used, should not create negative pressure on the permeate
side of the filter (i.e., the pump flow rate must be less than the spontaneous
permeate flux).
Filter Configurations
Cartridge filters (often called hollow fiber filters): the membrane forms a set
of parallel hollow fibers. The feed stream passes through the lumen of the fibers
and the permeate is collected from outside the fibers. Cartridges are
characterized in terms of fiber length, lumen diameter and number of fibers, as
well as filter pore size.
Cassette filters: several flat sheets of membrane are held apart from each other
and from the cassette housing by support screens. The feed stream passes into
the space between two sheets and permeate is collected from the opposite side
of the sheets. Cassettes are characterized in terms of flow path length and
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channel height, as well as membrane pore size. The channel height is determined
by the thickness of the support screen
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➢ Microfiltration filters
Filters with pore sizes of 0.1 μm and larger are classified as microfilters.
In CFF applications the pore size is usually in the range 0.1 to 1 μm.
These membranes are used for separation of cultured cells from the
growth medium (broth), as well as for removal of particulate material in
numerous biopharmaceutical processes.
➢ Ultrafiltration filters
Ultrafiltration membranes have pore sizes in the range 20 to 100 nm, and
are generally characterized in terms of the nominal molecular weight
cutoff (NMWC), which is the molecular weight of the largest globular
protein that can pass through the membrane. NMWC values range from
1 to 100 kD (kiloDalton). These filters are used for concentrating and
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
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College of Engineering and Technology
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➢ Nanofiltration
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➢ Reverse Osmosis
Reverse Osmosis is based upon the fundamental pursuit for balance. Two fluids
containing different concentrations of dissolved solids that come in contact with
each other will mix until the concentration is uniform. When these two fluids are
separated by a semi permeable membrane (which lets the fluid flow through,
while dissolved solids stay behind), a fluid containing a lower concentration will
move through the membrane into the fluids containing a higher concentration
of dissolved solids. (Binnie e.a., 2002)
After a while the water level will be higher on one side of the membrane. The
difference in height is called the osmotic pressure.
By pursuing pressure upon the fluid column, which exceeds the osmotic
pressure, one will get a reversed effect. Fluids are pressed back through the
membrane, while dissolved solids stay behind in the column.
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College of Engineering and Technology
Department of Chemical Engineering
Using this technique, a larger part the salt content of the water can be removed.
Reverse osmosis can remove many types of dissolved and suspended species
from water, including bacteria, and is used in both industrial processes and the
production of potable water. The result is that the solute is retained on the
pressurized side of the membrane and the pure solvent is allowed to pass to the
other side. To be "selective", this membrane should not allow large molecules or
ions through the pores (holes), but should allow smaller components of the
solution (such as solvent molecules) to pass freely.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Filter press. A filter press contains a set of plates designed to provide a series
of chambers or compartments in which solids may collect. The plates are covered
with a filter medium such as canvas. Slurry is admitted to each compartment
under pressure; liquor passes through the canvas and out a discharge pipe,
leaving a wet cake of solids behind.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
to displace as much residual liquid as possible. The press is then opened, and
the cake of solids removed from the filter medium and dropped to a conveyor or
storage bin. In may filter presses these operations are carried out automatically.
Thorough washing in a filter press may take several hours, for the wash
liquid tends to follow the easiest paths and to bypass tightly packed parts of
cake. If the cake is less dense in some parts than in others, as is usually the
case, much of the wash liquid will be ineffective. If washing must be exceedingly
good, it may be best to reslurry a partly washed cake with a large volume of wash
liquid and refilter it or to use a shell-and-leaf filter, which permits more effective
washing than a plate-and-frame press.
Shell-and-leaf filters. For filtering under higher pressures than are possible in
a plate-and-frame press, to economize on labor, or where more effective washing
of the cake is necessary, a shell-and-leaf filter may be used. In the horizontal-
tank design, a set of vertical leaves is held on a retractable rack.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
The chambers are then opened hydraulically so that the belt may be moved
a distance somewhat greater than the length of one chamber. This action
discharges cake from both sides of the filter. At the same time, part of the belt
passes between spray nozzles for washing. After all the cake has been
discharged, the belt is stopped, the chambers are closed, and the filtration cycle
is repeated. All the steps are actuated automatically by impulses from a control
panel. Filter sizes range from 0.8m2 (8.6 ft2) to 31.5m2 (339 ft2). The overall
cycle is relatively short, typically 10 to 30 min, so that these filters can be used
in continuous processes.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Rotary-drum filter. The most common type of continuous vacuum filter is the
rotary-drum filter. A horizontal drum with slotted face turns at 0.1 to 2 r/min
in an agitated slurry trough. A filter medium, such as canvas, covers the face of
the drum, which is partly submerged in the liquid. Under the slotted cylindrical
face of the main drum is a second, smaller drum with a solid surface. Between
the two drums are radial partitions dividing the annular space into separate
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Consider the figure. It is just about to enter the slurry in the trough. As
it dips under the surface of the liquid, vacuum is applied through the rotary
valve. A layer of solids builds up on the face of panel as liquid is drawn through
the cloth into the compartment, through the internal pipe, through the valve,
and into a collecting tank. As the panel leaves the slurry and enters the washing
and drying zone, vacuum is applied to the panel from a separate system, sucking
wash liquid and air through the cake of solids. As shown in the figure, wash
liquid is drawn through the filter into a separate collecting tank. After the cake
of solids on the face of the panel has been sucked as dry as possible, the panel
leaves the drying zone, vacuum is cut off, and the cake is removed by scraping
it off with a horizontal knife known as a doctor blade. A little air is blown in
under the cake to belly out the cloth. This cracks the cake away from the cloth
and makes it unnecessary for the knife to scrape the drum face itself. Once the
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
cake is dislodged, the panel reenters the slurry and the cycle is repeated. The
operation of any given panel, therefore, is cyclic, but since some panels are in
each part of the cycle at all times, the operation of the filter as a whole is
continuous.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Horizontal belt filter. When the feed contains coarse fast-settling particles of
solid, a rotary-drum filter works poorly or not at all. The coarse particles cannot
be suspended well in the slurry trough, and the cake that forms often will not
adhere to the surface of the filter drum. In this situation a top-fed horizontal
filter may be used. The moving belt filter shown is one of several types of
horizontal filter; it resembles a belt conveyor, with a transversely ridged support
or drainage belt carrying the filter cloth, which is also in the form of an endless
belt. Central opening the drainage belt slide over a longitudinal vacuum box,
into which the filtrate is drawn. Feed slurry flows onto the belt from a distributor
at one end of the unit; filtered and washed cake is discharged from the other.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Belt filters are especially useful in waste treatment, since the waste often
contains a very wide range of particle sizes. They are available in sizes from 0.6
to 5.5 m (2 to 18 ft) wide and 4.9 to 33.5 m (16 to 110 ft) long, with filtration
areas up to 110 m2 (1200 ft2). Some models are “indexing” belt filters, similar in
action to the Larox pressure filter described earlier; in these the vacuum Is
intermittently cut off and reapplied. The belt is moved forward half a meter or
so when the vacuum is off and is held stationary while vacuum is applied. This
avoids the difficulty of maintaining a good vacuum seal between the vacuum box
and a moving belt.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Filter press
The plates of a filter press may be square or circular, vertical or horizontal. Most
commonly the compartments for solids are formed by recesses in the faces of
molded polypropylene plates. In other designs, they are formed as in the plate-
and-frame press, in which square plates 6 to 78 in. (150 mm to 2m) on a side
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
alternate with open frames. The plates are ¼ to 2 in. (6 to 50mm) thick, the
frames ¼ to 8 in. (6 to 200 mm) thick. Plates and frames sit vertically in a metal
rack, with cloth covering the face of each plate, and are squeezed tightly together
by a screw or a hydraulic ram. Slurry enters at one end of the assembly of plates
and frames. It passes through a channel running lengthwise through one corner
of the assembly. Auxiliary channels carry slurry from the main inlet channel
into each frame. Here the solids are deposited on the cloth-covered faces of the
plates. Liquor passes through the cloth, down grooves or corrugations in the
plate faces, and out of the press.
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
is then said to be jammed. Wash liquid may then be admitted to remove soluble
impurities from the solids, after which the cake may be blown with steam or air
to displace as much residual liquid as possible. The press is then opened, and
the cake of solids removed from the filter medium and dropped to a conveyor or
storage bin. In may filter presses these operations are carried out automatically.
Thorough washing in a filter press may take several hours, for the wash
liquid tends to follow the easiest paths and to bypass tightly packed parts of
cake. If the cake is less dense in some parts than in others, as is usually the
case, much of the wash liquid will be ineffective. If washing must be exceedingly
good, it may be best to reslurry a partly washed cake with a large volume of wash
liquid and refilter it or to use a shell-and-leaf filter, which permits more effective
washing than a plate-and-frame press.
There are three main basic types of filter presses: plate and frame filter presses,
recessed plate and frame filter presses and automatic filter presses.
A plate and frame filter press is the most fundamental design, and many now
refer it as a "membrane filter plate". This type of
filter press consists of many plates and frames
assembled alternately with the supports of a pair
of rails. The presence of a centrifuge pump
ensures the remaining suspended solids do not
settle in the system, and its main function is to
deliver the suspension into each of the separating
chambers in the plate and frame filter. For each
of the individual separating chambers, there is one hollow filter frame separated
from two filter plates by filter cloths. The introduced slurry flows through a port
FILTRATION 65
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
in each individual frame, and the filter cakes are accumulated in each hollow
frame. As the filter cake becomes thicker, the filter resistance increases as well.
So when the separating chamber is full, the filtration process is stopped as the
optimum pressure difference is reached. The filtrate that passes through filter
cloth is collected through collection pipes and stored in the filter tank. Filter cake
(suspended solid) accumulation occurs at the hollow plate frame, then being
separated at the filter plates by pulling the plate and frame filter press apart. The
cakes then fall off from those plates and are discharged to the final collection
point. (Von Sperling, 2007)
Cake discharge can be done in many ways. For example: Shaking the plates
while they are being opened or shaking the cloths. A scraper can also be used,
by moving from one chamber to another and scraping the cake off the cloth. At
the end of each run, the cloths are cleaned using wash liquid and are ready to
start the next cycle. (Sutherland, K. 2008)
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Other industrial uses for automatic membrane filter presses include municipal
waste sludge dewatering, ready mix concrete water recovery, metal concentrate
recovery, and large-scale fly ash pond dewatering. (Tarleton, E. S. W. R., J. 2007)
Applications
Many specialized applications are associated with different types of filter press
that are currently used in various industries. Plate filter press is extensively used
in sugaring operations such as the production of maple syrup in Canada, since
it offers very high efficiency and reliability. According to M.Isselhardt,
"appearance can affect the value of maple syrup and customer's perception of
quality". This makes the raw syrup filtration process extremely crucial in
achieving desired product with high quality and appealing form, which again
suggested how highly appreciated filter press methods are in industry.
Filter medium
Typical cloth areas can range from 1 m2 or less on laboratory scale to 1000 m2 in
a production environment, even though plates can provide filter areas up to
2000 m2. Normally, plate and frame filter press can form up to 50 mm of cake
thickness, however, it can be push up to 200 mm for extreme cases. Recessed
plate press can form up to 32 mm of cake thickness. (Tarleton, E. S. W., R. J,
2007)
In the early days of press use in the municipal waste biosolids treatment
industry, issues with cake sticking to the cloth was problematic and many
treatment plants adopted less effective centrifuge or belt filter press
technologies. Since then, there have been great enhancements in fabric quality
and manufacturing technology that have made this issue obsolete. (Jingjin Filter
Cloth Manufacture and Quality Control) Unlike the USA, automatic membrane
filter technology is the most common method to dewater municipal waste
biosolids in Asia. Moisture is typically 10-15% lower and less polymer is
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Advantages Disadvantages
Large quantities
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
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Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
Consider the figure. It is just about to enter the slurry in the trough. As
it dips under the surface of the liquid, vacuum is applied through the rotary
valve. A layer of solids builds up on the face of panel as liquid is drawn through
the cloth into the compartment, through the internal pipe, through the valve,
and into a collecting tank. As the panel leaves the slurry and enters the washing
and drying zone, vacuum is applied to the panel from a separate system, sucking
wash liquid and air through the cake of solids. As shown in the figure, wash
liquid is drawn through the filter into a separate collecting tank. After the cake
of solids on the face of the panel has been sucked as dry as possible, the panel
leaves the drying zone, vacuum is cut off, and the cake is removed by scraping
it off with a horizontal knife known as a doctor blade. A little air is blown in
under the cake to belly out the cloth. This cracks the cake away from the cloth
and makes it unnecessary for the knife to scrape the drum face itself. Once the
cake is dislodged, the panel reenters the slurry and the cycle is repeated. The
operation of any given panel, therefore, is cyclic, but since some panels are in
each part of the cycle at all times, the operation of the filter as a whole is
continuous.
FILTRATION 71
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
FILTRATION 72
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
filters are 3 to about 40 mm (1/8 to 1 ½ in.) thick. Standard drum sizes range
from 0.3 m (1 ft) in diameter with a 0.3-m (1-ft) face to 3 m (10 ft) in diameter
with a 4.3-m (14-ft) face.
A rotary vacuum filter consists of a large rotating drum covered by a cloth. The
drum is suspended on an axial over a trough containing liquid/solids slurry with
approximately 50-80% of the screen area immersed in the slurry.
FILTRATION 73
Pamantasan ng Lungsod ng Maynila
College of Engineering and Technology
Department of Chemical Engineering
As the drum rotates into and out of the trough, the slurry is sucked on the
surface of the cloth and rotated out of the liquid/solids suspension as a cake.
When the cake is rotating out, it is dewatered in the drying zone. The cake is dry
because the vacuum drum is continuously sucking the cake and taking the
water out of it. At the final step of the separation, the cake is discharged as solids
products and the drum rotates continuously to another separation cycle.
Advantages Disadvantages
The variation of the drum speed Besides the drum, other accessories,
rotating can be used to control the for example, agitators and vacuum
cake thickness pump, are required.
The process can be easily modified The discharge cake contains residual
(pre-coating filter process) moisture
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Department of Chemical Engineering
REFERENCES
DIJK, J.C. van; OOMEN, J.H.C. (1978): Slow Sand Filtration for Community
Water Supply in Developing Countries. A Design and Construction Manual. (=
IRC Technical Paper Series, 11). The Hague: International Reference Centre for
Community Water Supply. URL [Accessed: 06.02.3012].
HUISMAN, L.; WOOD, W.E. (1974): Slow Sand Filtration. Geneva: World Health
Organisation (WHO). URL [Accessed: 06.02.2012].
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Department of Chemical Engineering
TWT (Editor) (n.y.): Components of an Open Rapid Sand Filter. The Water
Treatments (TWT). URL [Accessed: 21.02.2012].
WHO (Editor) (n.y.): Chapter 12: Water Treatment. In: WHO (Editor) (2009):
WHO Seminar Pack for Drinking Water Quality. . URL [Accessed: 07.02.2012].
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