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Article history: This article reviews the advances in the materials selection for applications in structures and engines of
Received 16 June 2012 current and future supersonic aircrafts. A brief overview of configuration design of the supersonic air-
Accepted 1 October 2012 crafts is first given; which also includes techniques to improve configuration design for future supersonic
Available online 25 October 2012
aircrafts. The operating and ambient environmental conditions during supersonic flight and the resulting
material requirements have been discussed; and consequently various aerospace aluminum alloys, tita-
Keywords: nium alloys, superalloys, and composites have been recommended. Finally, a new materials-selection
Materials selection
chart is presented that would enable aerospace designers to select appropriate materials for application
Aerospace aluminum alloys
Superalloys
in high-performance current and future supersonic/hypersonic aircrafts.
Composites Ó 2012 Elsevier Ltd. All rights reserved.
Configuration design
Supersonic aircrafts
1. Introduction when a plane is traveling faster than the speed of sound [6]. This
is why; almost all the supersonic aircrafts designed to-date are mil-
Supersonic aircrafts are capable of flying at speeds greater than itary aircraft; which are mainly made of lightweight carbon-fiber
750 mi/h (1207 km/h) but less than 2000 mi/h (3219 km/h), and reinforced polymer (CFRP) composite materials possessing high
the Mach number M is greater than one, 1 < M < 4. The design of a specific strength, fatigue strength, corrosion-resistance, and rea-
supersonic aircraft and its materials selection must be based on sonably high creep strength [7,8]. Another practical requirement
sound engineering principles and practices since a small mistake in the aerospace composites is their ability to be repaired when
in the design of the aircraft’s fuselage, skeleton, wing, or any critical the skin of the aircraft panel becomes disbonded [9]. In addition
part could be fatal. The important material selection considerations to military aircrafts, CFRP are used in SCT aircrafts; for instance,
in the design of a supersonic aircraft include: specific strength much of the fuselage of the new Boeing 787 Dreamliner and Airbus
(strength-to-weight ratio), tensile mechanical properties, fatigue A350 XWB are composed of CFRP. The physic of supersonic flow and
strength, low-speed impact strength, fracture toughness, notch sen- its design are completely different from that of subsonic flow, about
sitivity, fabricability, and resistances to crack propagation, stress as great as the difference between civil and military aircraft. The
corrosion, and exfoliation corrosion [1–3]. Another material require- unique features of supersonic aircraft design includes variable-
ment, directly related to the supersonic aircraft’s design is the resis- swept/high-swept/delta-wing and thinner wing, canard, more slen-
tance to creep since long-term operation at Mach 3.5 may heat up der fuselage, area ruling, sonic boom, more power-full propulsion
the structure of the aircraft to a temperature around 300 °C [4,5]. system, variable engine air intake, and the like. Supersonic laminar
One of the initial designs of the supersonic transport (SST) air- flow also looks very interesting, especially for small aircraft.
craft: Concorde was based on the selection of aluminum alloy as Although maintenance of laminar flow in a realistic operational
the basic structural material; this material selection was closely environment has yet to be demonstrated, this concept remains very
linked to the choice of Mach 2 as the design cruise speed. However, promising. A near term, environmentally acceptable supersonic
almost every country has rejected Concorde due to its sonic boom business aircraft based on this technology with efficient subsonic
and possibility depletion of ozone due to the pollutants in the en- overland flight appears quite feasible [10,11].
gine’s exhaust. Sonic boom is the ‘‘thunder-like’’ noise produced
2. Current and future configuration designs
⇑ Corresponding author. Tel.: +966 554130411.
E-mail addresses: drzainulhuda@hotmail.com (Z. Huda), eprasetyo@kfupm. Prior to reviewing the progress in materials selection for super-
edu.sa (P. Edi). sonic aircrafts, a brief overview of the configuration design for
0261-3069/$ - see front matter Ó 2012 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.matdes.2012.10.001
Z. Huda, P. Edi / Materials and Design 46 (2013) 552–560 553
represents about 60,000 flight hours [19]. A substantial portion of K ¼ K IC ¼ YrðpaÞ1=2 ð5Þ
this flight cycle will be under supersonic cruise conditions at
speeds between Mach 2 and Mach 2.4. where K is stress intensity factor, KIC is plane strain fracture tough-
ness, r is the stress acting in a direction normal to the major axis of
3.1.2. Loading conditions and design relationships a central crack of length 2a (or an edge crack of length a) in the
An aircraft’s structure is subjected to the following types of component, and Y is geometric compliance function describing
loading during flight: (a) tension, (b) compression (that may cause the geometry of the structural component. In order to achieve a safe
two failure modes: yielding and buckling), (c) bending, and (d) tor- design, material’s fracture toughness must be so selected as to en-
sion. For supersonic application, the minimum weight of aircraft sure K < KIC (for preventing crack propagation).
(strength allied to lightness or specific strength) is an important In view of the stringent operating conditions in supersonic
factor in material selection. It is, therefore, important to consider flight, it is important to select a combination of high-performance
design relationships involving weight of aircraft for selecting a aluminum alloys, titanium alloys and polymer matrix composites
material. These design relationships are given for each type of in the aircraft structure. Aluminum alloys are light, yet strong; tita-
loading as follows [20]. nium alloys have a great thermal stability, strength, and corrosion-
resistance; while polymer matrix composites have excellent
3.1.2.1. Tension and its design equation. Under a certain tensile load stiffness, lightness and heat resistance (see sub-sections 3.2.1
until the yield limit is reached, the applied stress on a structural and 3.2.2). The design of future high-speed supersonic aircrafts
part (e.g. fuselage of the aircraft) should be considered in relation or the hypersonic aircrafts are imposing larger restrictions on the
to its weight (W). When the interest is to compare specific materials selection; and demand adequate quantification of mate-
strengths of two materials: (a) and (b), the relationship may be ex- rial behavior and performance during different flight conditions. In
pressed as follows: particular, the erosion due to weather conditions and other present
particles such as hydrometeors; rain, hail and ice, as well as sand,
ðW ðaÞ =W ðbÞ Þ ¼ ½ðqðaÞ ryðbÞ Þ=ðqðbÞ ryðaÞ Þ ð1Þ volcanic ash and dust resulting from residues in the atmosphere
are eminent as hazardous on the structure of a flying vehicle and
where W(a) is weight of a structural member using material (a), W(b)
may adversely influence the lifecycle of the structure [15].
is weight of the structural member using material (b), q(a) is density
Materials Selection Charts (e.g. Ashby chart) should be referred
of material (a), q(b) is density of material (b), ry(a) is yield strength of
to select materials for structural parts of a supersonic aircraft
material (a), and ry(b) is yield strength of material (b).
[24,25]. An Ashby plot useful for a stiff, light part (of an aircraft)
would have Young’s modulus on one axis and density on the other
3.1.2.2. Compression and its design equation. Under compression, an
axis, with one data point on the graph for each candidate material.
aircraft part may fail by buckling; thus an important design
On such a plot, it is easy to find not only the material with the high-
requirement is a high stiffness (Young’s modulus, E) of the mate-
est stiffness or that with the lowest density, but that with the best
rial. By comparison of two materials (a) and (b), the following com-
ratio (E/q). Traditional Materials Selection Charts are usually 2-
pression relationship is useful to the supersonic aircraft designer:
dimensional; and hence are not really robust for design of ad-
ðW ðaÞ =W ðbÞ Þ ¼ ðqðaÞ =qðbÞ Þ½ðEðbÞ =EðaÞ Þ1=3 ð2Þ vanced supersonic aircrafts. Recently (2011), Ashby has reported
the development of an advanced 3-dimensional Materials Selec-
where the symbols have their usual meanings. tion Chart that takes into consideration Young’s modulus-Den-
sity-Fracture Strength simultaneously on the single chart [26];
3.1.2.3. Bending and design equation. Under bending, both tensile this chart enables a designer to accurately and efficiently select
and compressive stresses act on a structural member (e.g. wing materials for design of advanced supersonic aircrafts.
of aircraft); thus the following relationship should be applied when Today’s aerospace designers are expected to efficiently select
comparing two materials: materials for application in different parts of the aircraft to be de-
ðW ðaÞ =W ðbÞ Þ ¼ ðqðaÞ =qðbÞ Þ½ryðbÞ =ryðaÞ 1=2 ð3Þ signed. A remarkable progress in this regard has been made
through the development of computer-based and web-based
where the symbols have the same meanings as mentioned in Eq. (1). materials-selection systems; these IT-based systems (e.g. CES Selec-
tor) enable an aerospace designer to efficiently select materials for
3.1.2.4. Torsion and design equation. Airframe construction involves current and future supersonic aircrafts [27–29].
tubes; which is subjected to torsional stresses. Under torsion, the
relationship between two materials may be expressed as follows: 3.2.1. Materials selection for structures for speeds up to 2.0 Mach
ðW ðaÞ =W ðbÞ Þ ¼ ðqðaÞ sðbÞ =qðbÞ sðaÞ Þ ð4Þ Usually the temperatures on a supersonic transport aircraft
(SSTA) flying at about 1.8 Mach speed are below 100 °C so both
where s(a) and s(a) are torques acting on materials (a) and (b), the aluminum and CFRP composites laminates can be selected to
respectively. build the fuselage of SST aircrafts. As regards the complexity of fab-
Eqs. (1)–(4) enable an aerospace designer to select a material for rication and its cost, aerospace aluminum alloys should be pre-
a specific aircraft structural part keeping in view the type of load- ferred over composites for SCTAs flying at speeds up to 1.8 Mach.
ing acting on it. Although Eqs. (1)–(4) provide useful design rela- The design of solution heat treatment of the aerospace Al alloys
tionships in material selection for design of an aircraft, they do play an important role is strengthening the alloys for supersonic
not fulfill complete design requirements; the latter requires appli- applications [30]. The heat-treated aluminum alloys: 2024-T81,
cation of fracture mechanics (design philosophy) which is illus- T6, T62, or T81 are suitable for extruded members. In particular,
trated in Section 3.2. the alloys: 2014-T6, 2024, and 2618-T61 can be employed for
forged products located in the heat-affected areas of aircraft.
3.2. Materials selection for structure Table 1 enables an aerospace designer to select some aerospace
aluminum alloys for supersonic applications at speeds up to 2.0
The materials selection in safe design for a structural compo- Mach [31,32].
nent of a supersonic aircraft requires application of design philoso- It is evident from the data in Table 1 that although the 2219-T87
phy relationship, as follows [21–23]: aluminum alloy is easy-to-fabricate (10% elongation at break), its
Z. Huda, P. Edi / Materials and Design 46 (2013) 552–560 555
Table 1 Table 2
Densities and tensile mechanical properties of some aluminum alloys for application Aircraft skin temperatures at various speeds.
in SCT aircrafts [31,32].
Speed (Mach number) Skin temperature (°C)
Alloy Density Yield UTS Elongation
2.0 100
(g/cm3) strength (MPa) at
2.5 150
(MPa) break (%)
3.0 200
2024-T81 2.78 450 485 6 3.5 300
2024-T86 2.78 440 515 6 4.0 370
2090-T83 2.59 483 520 5
2219-T87 2.84 393 476 10
8090-T651 2.53 360 465 6.2
7075-T6 2.81 505 575 11 Table 3
New type 2-mm n/a 424 555 12.3 Tensile mechanical properties of three classes of CFRP composites.
Al–Zn–Mg–Sc–Zr alloy
Tensile mechanical Standard Intermediate High
properties modulus modulus modulus CFRP
CFRP CFRP
low yield strength restricts its use for modern supersonic applica- Tensile strength 3450– 3450–6200 MPa 3450–5520 MPa
tions even below 2.0 Mach. However, the easy-to-fabricate 7075- 4830 MPa
T6 alloy and the new (heat-treated) type 2-mm Al–Zn–Mg–Sc–Zr Young’s modulus (E) 220–241 GPa 290–297 GPa 345–448 GPa
alloy (with the highest (12%) elongation at break) have promising Elongation at break 1.5–2.2% 1.3–2.0% 0.7–1.0%
Fig. 3. Predicted equilibrium skin temperatures for Mach 2.2 and 2.4 SCT aircrafts.
temperature capabilities; and hence they are recommended for effects of supersonic speed on the stringent requirements for mate-
speeds above 3.5 Mach. The phthalonitrile resin system (graphite rials selection for high-speed supersonic aircrafts in the preceding
fiber-phthalonitrile composite) developed (2002) at the Naval Re- sub-section, the material selection tool: Weighted Relative Property
search Laboratory, Washington DC, USA, has the ability to survive Rating Procedure is now applied for selecting material for the wing
elevated temperature exposures up to 371 °C (700 °F) for extended of a military aircraft. Although, this procedure relies on selecting a
periods of time [39]. This is in contrast to the epoxy-based systems material with the highest overall rating, the aerospace designers
used in the Naval aircraft that, depending on the moisture content must also consider use of alternative material if speeds do not ex-
of the resin, lose their rigidity or shear strength as temperatures ceed a specified limit. This materials-selection philosophy is illus-
approach 150 °C (302 °F). For the short exposures times typical of trated in Table 4. In this Weighted Relative Property Rating
missile applications, high-temperature tension tests demonstrated procedure for materials selection, only metals have been consid-
that graphite fiber composites fabricated using the phthalonitrile ered because composites do not have a sharp yield point (ry). In
resin system can retain their tensile strength to temperatures Table 4, the weighting factors have been allocated as follows: 10
approaching 538 °C (1000 °F). Epoxy-based graphite fiber-rein- for mechanical properties, 20 for temperature resistance (if speed
forced composites, by comparison, start to lose their tensile of aircraft is as high as Mach 4.0), and unity for cost.
strength rapidly at temperatures around 260 °C (500 °F) for similar The analysis of data in Table 4 indicates that stainless steel
short time exposures (Fig. 5). It is evident from Fig. 5 that the ulti- should be the optimum choice for the specific application. How-
mate tensile strength (UTS) of graphite–epoxy drops nearly 50% at ever, an aerospace designer must not overlook the outstanding cor-
316 °C. On the other hand, the graphite–phthalonitrile does not rosion-resistance capability and low density of titanium alloy;
suffer significant degradation until temperatures are above which should be preferred if the speeds of the supersonic aircraft
482 °C; this is why this material is specially recommended for does not exceed 3.0 Mach.
application in nose and around wings of the supersonic aircraft In fact, a combination of stainless steel (or composite), titanium
for speeds around 3.5 Mach. alloy, and high-temperature aluminum alloy (e.g. 2650-T8) can be
selected for the wings of the military aircrafts. This materials-
selection recommendation is justified in view of the wide differ-
3.2.2.1. A material-selection tool/philosophy applied to wing of a ence of temperatures to which the wing is heated up during the
military aircraft. Having established the quantitative aspects the supersonic flight (see Fig. 6).
Z. Huda, P. Edi / Materials and Design 46 (2013) 552–560 557
Table 4
Weighted relative property rating procedure for selecting a material for wing of a fighter aircraft.
Material ry/q (KIC/ry)2 (mm) E1/3/q Temp. limit (°C) Cost (£/ton) Overall rating [10A + 10B + 10C + 20D+(1 E)]/51
Abs. Rel. = A Abs. Rel. = B Abs. Rel. = C Abs. Rel. = D Abs. Rel. = E
Al alloy 1 130 0.64 16.5 1.00 1.50 1.0 150 0.38 13.100 0.134 0.683
Al alloy 2 204 1.00 2.1 0.13 1.50 1.0 150 0.38 14.000 0.142 0.583
Ti alloy 196 0.96 4.6 0.27 1.06 0.71 300 0.75 98.000 1.000 0.674
Stainless steel 115 0.56 12.3 0.75 0.75 0.50 400 1.00 10.900 0.111 0.764
nickel-base and cobalt-base superalloys; which include: mechani- higher operating temperatures in aircraft engines [53]. This new
cally alloyed (MA) superalloys (e.g. MA6000), powder metallurgy materials (after full investigation) can be a potential candidate in
(P/M) superalloys (e.g. P/M IN-792), single crystal (SC) superalloys future supersonic aircrafts’ engines.
(e.g. TMS-75, Rene’N6, CMSX-lfl, etc.), directionally solidified (DS)
superalloy blades, Hastelloy X, Haynes 188, and the like [46–50]. 4.4. Thermal barrier coatings
4.3. Materials selection for hot sections of the engine for future For high-thrust current and future supersonic aircraft engines,
supersonic aircrafts advanced alloys with thermal barrier coating (TBC) and environ-
mental coatings are required for the combustor liners and turbine
An optimum choice for current aircraft-engine’s compressor- vanes and blades, and turbine and compressor disks [54]. A thermal
blades (operating around 600 °C) is a high-performance titanium barrier coating (TBC) is a multi-layer coating system that consists of
alloy; but they are not suitable for application in future high- an insulating ceramic outer layer (top coat) and a metallic inner
speed/hypersonic aircrafts-engines’ compressor blade since this layer (bond coat) between the ceramic and the substrate. The func-
component would operate at temperatures exceeding 600 °C tion of the ceramic topcoat is to insulate the metallic substrate from
thereby requiring superalloys to be used) However, superalloys high surface temperature; thereby lowering the components tem-
are heavy alloys with lower specific strength (strength-to-weight perature and reducing the oxidation and hot corrosion of bond coat-
ratio) as compared to titanium alloys. This difficulty in material ings, while simultaneously reducing cyclic thermal strains [54,55].
selection for future supersonic aircrafts can be overcome by select- A cost-effective method to apply an oxide TBC to the hot-sec-
ing titanium aluminides; which are attractive alternatives to tion components is by electrophoretic deposition (EPD). Fig. 9 illus-
superalloys for temperature applications in the range of 600– trates a typical EPD coating system in a high-pressure turbine
850 °C by virtue of their high strength-to-density ratio [51]. blade for an aircraft engine [56,57]. Recently, Kitazawa and co-
The future supersonic aircrafts would be designed with greater workers (2010) have reported that a temperature gradient of
turbine efficiency that would consequently demand materials (for 150 °C can be achieved by using a ceramic TBC (Y2O3–ZrO2 top-
the hot sections) with a higher temperature capability than current coat) on superalloy components [58].
nickel and cobalt alloys since thermal efficiency of a gas-turbine is
a direct function of the turbine inlet temperature (TIT). In this re- 4.4.1. A unique philosophy to extend component lifetimes of future
gard, Perepezko (2009) has proposed use of alloys with higher high-speed supersonic aircrafts
melting temperatures (>2500 °C) (such as molybdenum-based al- Future high-speed supersonic aircrafts’ engines would require
loys) for future advanced aircraft engines operating at higher tur- more energy-efficient ceramic thermal and environmental barrier
bine inlet temperatures (TIT > 1600 °C) [52]. This technological coatings (TEBCs) to protect engine hot-section components in the
challenge for future trend is also evident in Fig. 8; which illustrates harsh combustion environments, and to extend component life-
the development of advanced superalloys in the temperature times. Now, a unique aerospace-material philosophy is presented
capacity of the alloys since 1940. that can make TBCs more energy efficient for application in future
Fig. 9 not only focuses on current nickel-based superalloys for supersonic aircrafts. The supersonic aircrafts are exposed to ex-
aircraft engines’ applications, but also demonstrates the need for tremes in temperature (ranging from about 30 °C to 370 °C) dur-
developing new energy-efficient superalloys, such as Mo-based ing flight. In order to take advantage of the ground ambient
superalloys for achieving further technological gains. In view of operating condition. The temperature outside the aircraft at
the very high TIT in advanced engines, materials scientists must 55,000 feet is many degrees below 0 °C. This cold air can be
also endeavor to develop ceramic matrix composites with ade- exploited to take an engineering advantage, as follows. It is sug-
quate toughness for future energy-efficient supersonic-aircrafts’ gested to make a layer of no more than 2 cm before the ceramic
engines. In this regard, a good progress has been very recently coating of the TBC; which will have cold air in it. A machine will
(2012) been reported by Boyce; who has suggested potential for suck air from outside and will bring this air through the compres-
using ceramic with added aluminum in a superalloy to achieve sor section into this special coating in the combustor section of the
engine. The air will be released when it reaches a certain temper-
ature and after that ‘‘new’’ cold air will be sucked in. This way the
structural parts of the engine’s hot-sections will not suffer from
overheating and consequently they will ‘‘live’’ longer. Hence, the
outside part of the engine could be built with the same material
as the fuselage.
Fig. 9. Illustration of a typical coating system in a high-pressure turbine blade. Clockwise, a TBC coated high-pressure turbine blade, view from top showing the cooling
systems; and schematic profile temperature, note the drop of temperature close to the blade surface due to the presence of a thin cooling air film [58].
Table 5
A new materials selection guide for designing current and future supersonic aircrafts.
Aircraft Current supersonic with cruise Current supersonic with cruise speed: 2.0–4.0 Mach Future hypersonic with cruise speed above 4.0 Mach
part speed up to 2.0 Mach
Possible material(s) to be selected Possible material(s) to be selected Possible material(s) to be selected
Structure Fuselage: Al: 2090-T651; 7075-T6; Fuselage: CFRP: PMR-15, PMR-11-55, or similar high- Fuselage: polyimides, BMIs, CEs, graphite fiber–
8090-T651 (nose) modulus composites; or new type 2-mm Al–Zn–Mg–Sc–Zr phthalonitrile, or FGM (ceramic–metal composite)
alloy
Skeleton: Ti–6Al–4V or other Ti Skeleton: high perf. Ti alloy Skeleton: titanium aluminides, or high perf. Ti
Wings: commercial grade CFRP Wings: CFRP: PMR-15, PMR-11-55, or similar composites; Alloy wings: mesh-protected CFRP, polyimides, BMIs,
or Ti alloy CEs, or stainless steel, or Ti alloy
Engine Compressor: Ti alloy Compressor: Ti–6Al–2Sn–4Zr–6Mo or similar Ti alloy Compressor: advanced Ti alloy
Combustor & Turbine TBC coated Combustor & turbine TBC coated Ni-base superalloys: SC Combustor & Turbine TEBC coated superalloys: Mo-
superalloys: SC alloys, DS blades; P/ alloys (TMS-75, Rene’N6, CMSX-lfl), MA superalloys; DS based superalloys; or aluminum-added ceramic
M IN-792 disc, and others blades; P/M IN-792 disc, or advanced alloys composite; or other advanced material
In order to select appropriate materials for various section of a (b) The materials-selection tool: Weighted Relative Property Rat-
supersonic aircraft, Table 5 should be referred keeping in view ing procedure, has been applied and appropriate recommen-
materials-properties data (see Figs. 4 and 5). For example, the dations have been made to use stainless steel, composites,
selection of CFRP for application in fuselage and wing of supersonic titanium alloy and high-temperature aluminum alloys in
aircrafts cruising at speeds 2–4 Mach and above (see Table 5) various structural parts of supersonic aircrafts.
should be made with reference to Figs. 4 and 5. Although Ni-base (c) Materials selection for engine components has also been
superalloys should be selected for the hot-section components of critically considered and appropriate recommendations
engines of current supersonic aircrafts, the selection of material have been made to use specific advanced superalloys and
for the hot section of future hypersonic aircrafts requires use of ad- titanium aluminides for current and future supersonic air-
vanced Mo-based superalloys or Al-added ceramic composite. crafts’ engines.
(d) A new aerospace-material philosophy has been presented
6. Conclusions that can make TBCs more energy efficient for application
in future supersonic aircrafts.
The materials selection in design of the structure and engine (e) A unique materials-selection chart/Table has also been
along with the configuration designs of current and next-genera- developed that enables an aerospace designers to select
tion supersonic aircrafts have been reviewed; and the following appropriate materials in design of current and future super-
conclusions have been drawn. sonic aircrafts cruising at speeds with various Mach number
ranges.
(a) It has been emphasized that an accurate understanding of
expected service conditions (including operating stresses
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