PDA-280nm 20CU 5US 650 15

Results (System
(09/05/2018
01:09:14 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.412 17347 2.24 3796 14.67
1.535 5871 0.76 1462 5.65
1.750 21578 2.79 2141 8.27
1.890 16225 2.10 1703 6.58
2.188 23403 3.03 2501 9.66
2.950 615067 79.58 10096 39.01
6.557 1524 0.20 109 0.42
10.197 71852 9.30 4073 15.74

Totals
772867 100.00 25881 100.00

20CU 5US 650 30

PDA-280nm
Results (System
(09/05/2018
01:40:55 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.412 9596 1.02 1836 7.60
1.552 4452 0.48 1134 4.70
1.748 37895 4.04 2323 9.62
2.938 756989 80.78 11547 47.82
10.140 128142 13.67 7306 30.26

Totals
937074 100.00 24146 100.00

20CU 5US 650 45

PDA-280nm
Results (System
(09/05/2018
01:40:55 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.412 9596 1.02 1836 7.60
1.552 4452 0.48 1134 4.70
1.748 37895 4.04 2323 9.62
2.938 756989 80.78 11547 47.82
10.140 128142 13.67 7306 30.26

Totals
937074 100.00 24146 100.00

20CU 5US 650 60

PDA-280nm
Results (System
(09/05/2018
02:12:26 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.408 25672 1.76 5415 7.79
1.545 5314 0.36 1181 1.70
1.757 43151 2.96 2469 3.55
2.062 13608 0.93 2176 3.13
2.917 477104 32.72 11250 16.19
3.195 267806 18.37 11118 16.00
10.202 625328 42.89 35848 51.59
10.795 87 0.01 28 0.04

Totals
1458070 100.00 69485 100.00

20CU 5US 650 90

PDA-280nm
Results (System
(09/05/2018
02:28:12 a.m.)
(Original))
 Retention Time Area Area % Height Height %
1.410 13346 0.98 2731 5.28
1.543 6228 0.46 1287 2.49
1.747 35848 2.62 2270 4.39
2.148 36172 2.65 3373 6.52
2.895 742050 54.31 11462 22.15
10.143 532667 38.99 30617 59.17

Totals
1366311 100.00 51740 100.00

20CU 5US 650 120

PDA-280nm
Results (System
(09/05/2018
02:44:03 a.m.)
(Original))
Retention Time Area Area % Height Height %
 1.407 46267 3.01 9707 14.45
1.532 10636 0.69 2158 3.21
1.750 48583 3.16 2973 4.42
2.067 19611 1.28 2567 3.82
2.918 747283 48.66 11528 17.16
9.610 477 0.03 53 0.08
10.137 662966 43.17 38204 56.86

Totals
1535823 100.00 67190 100.00

20CU 5US 650 180

PDA-280nm
Results (System
(09/05/2018
02:59:48 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.410 24445 2.11 5205 9.37
 1.540 9089 0.79 1783 3.21
1.717 41208 3.56 2546 4.58
2.067 17136 1.48 2465 4.44
2.877 485516 41.97 11443 20.59
3.163 303539 26.24 16085 28.94
10.095 275940 23.85 16050 28.88

Totals
1156873 100.00 55577 100.00

20CU 5US 650 240

PDA-280nm
Results (System
(09/05/2018
03:15:36 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.418 20676 2.26 4280 15.46
1.513 23669 2.59 3775 13.64
1.680 67633 7.40 3952 14.27
 2.070 21098 2.31 2705 9.77
2.877 758076 82.90 11686 42.21
10.130 23323 2.55 1288 4.65

Totals
914475 100.00 27686 100.00

50CU 5US 500 300

PDA-280nm
Results (System
(08/05/2018
01:24:03 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.502 340578 20.25 39274 23.68
1.653 87582 5.21 18232 10.99
1.740 96198 5.72 16594 10.00
1.902 154361 9.18 23544 14.20
 2.123 94301 5.61 12361 7.45
2.645 283825 16.88 12518 7.55
2.757 69906 4.16 12344 7.44
2.877 210562 12.52 12739 7.68
3.155 257954 15.34 10805 6.51
4.143 8439 0.50 911 0.55
5.478 66274 3.94 5885 3.55
10.047 11856 0.70 652 0.39

Totals
1681836 100.00 165859 100.00

20CU 5US 650 360

PDA-280nm
Results (System
(09/05/2018
03:47:09 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.413 4738 0.53 1093 6.32
1.550 5002 0.56 1241 7.18
1.758 38067 4.26 2681 15.51
2.903 846357 94.65 12254 70.90
13.823 64 0.01 15 0.09
 Totals
894228 100.00 17284 100.00

20CU 5US 650 0

PDA-280nm
Results (System
(09/05/2018
01:09:14 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.412 17347 2.24 3796 14.67
1.535 5871 0.76 1462 5.65
1.750 21578 2.79 2141 8.27
1.890 16225 2.10 1703 6.58
2.188 23403 3.03 2501 9.66
2.950 615067 79.58 10096 39.01
6.557 1524 0.20 109 0.42
 10.197 71852 9.30 4073 15.74

Totals
772867 100.00 25881 100.00

SC
PDA-280nm
Results (System
(09/05/2018
12:53:29 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.408 17966 3.42 3639 10.13
1.503 8353 1.59 2112 5.88
1.677 30159 5.75 4162 11.58
1.788 29763 5.67 3879 10.80
1.992 54783 10.44 3928 10.93
2.183 41778 7.96 3717 10.35
2.437 51048 9.73 4134 11.51
2.573 33885 6.46 3909 10.88
2.750 217074 41.36 4183 11.64
8.757 40089 7.64 2265 6.30
 Totals
524898 100.00 35928 100.00

20CV 5US 500 SC

PDA-280nm
Results (System
(09/05/2018
09:51:35 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.122 1294 0.14 534 0.87
1.292 58004 6.27 4630 7.50
1.503 16241 1.75 2780 4.50
1.675 40376 4.36 3511 5.69
1.870 15415 1.67 2607 4.22
1.990 30881 3.34 2514 4.07
2.222 8065 0.87 1285 2.08
2.400 10558 1.14 826 1.34
2.737 2202 0.24 279 0.45
2.843 11816 1.28 423 0.69
3.210 17963 1.94 878 1.42
 8.655 711677 76.89 41384 67.06
11.978 1131 0.12 59 0.10

Totals
925623 100.00 61710 100.00

20CV 5US 500 15

PDA-280nm
Results (System
(09/05/2018
10:23:14 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.410 16001 1.47 3437 6.39
1.543 8234 0.76 1763 3.28
1.735 41414 3.81 2382 4.43
2.065 15346 1.41 2221 4.13
2.755 243490 22.41 8499 15.79
2.877 301526 27.75 8528 15.85
10.142 460397 42.38 26980 50.14

Totals
1086408 100.00 53810 100.00
20CV 5US 500 30

PDA-280nm
Results (System
(09/05/2018
10:39:01 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.408 25680 2.37 5288 11.09
1.525 10388 0.96 2049 4.30
1.705 18217 1.68 2192 4.60
1.838 22522 2.08 2273 4.77
2.067 12513 1.16 2055 4.31
2.723 568841 52.59 8896 18.65
10.100 423350 39.14 24915 52.24
10.693 112 0.01 23 0.05

Totals
1081623 100.00 47691 100.00
20CV 5US 500 45

PDA-280nm
Results (System
(09/05/2018
10:54:53 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.412 20314 2.01 4346 8.39
1.522 10308 1.02 2090 4.03
1.703 26032 2.57 2332 4.50
1.878 15755 1.56 2046 3.95
2.068 13745 1.36 2103 4.06
2.748 260022 25.68 8988 17.35
2.873 313137 30.92 8993 17.36
9.647 289 0.03 38 0.07
10.160 353034 34.86 20868 40.28

Totals
1012636 100.00 51804 100.00
20CV 5US 500 60

PDA-280nm
Results (System
(09/05/2018
11:10:45 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.418 18357 1.76 3811 5.09
1.518 26136 2.50 4375 5.85
1.682 34653 3.31 3665 4.90
1.845 37705 3.61 4290 5.73
2.065 20389 1.95 3036 4.06
2.618 295716 28.29 11320 15.13
2.847 79166 7.57 9562 12.78
2.987 69028 6.60 9243 12.35
3.150 206488 19.75 10266 13.72
10.105 257776 24.66 15247 20.38

Totals
1045414 100.00 74815 100.00
20CV 5US 500 90

PDA-280nm
Results (System
(09/05/2018
11:26:31 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.418 24441 2.52 4936 9.77
1.522 33780 3.48 5487 10.86
1.678 48945 5.05 4936 9.77
1.843 39775 4.10 4193 8.30
2.068 22874 2.36 3622 7.17
2.688 307053 31.66 10001 19.79
2.812 365929 37.74 9908 19.60
10.010 126908 13.09 7463 14.76

Totals
969705 100.00 50546 100.00
20CV 5US 500 120

PDA-280nm
Results (System
(09/05/2018
11:42:18 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.163 1859 0.19 166 0.34
1.427 28315 2.93 5981 12.25
1.523 54538 5.65 8204 16.80
1.687 103746 10.74 5506 11.27
2.063 31910 3.30 3494 7.15
2.788 294901 30.54 10240 20.97
2.877 365952 37.90 10245 20.98
9.657 1135 0.12 75 0.15
10.147 83321 8.63 4932 10.10

Totals
965677 100.00 48843 100.00
20CV 5US 500 180

PDA-280nm
Results (System
(09/05/2018
11:58:04 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.522 99333 10.94 10707 24.82
1.668 134374 14.79 8049 18.66
2.068 30016 3.30 3629 8.41
2.817 292117 32.16 10137 23.50
2.897 347981 38.31 10152 23.54
4.237 3079 0.34 387 0.90
12.277 1475 0.16 72 0.17

Totals
908375 100.00 43133 100.00
20CV 5US 500 240

PDA-280nm
Results (System
(10/05/2018
12:13:51 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.417 17997 2.54 3326 18.70
1.530 9776 1.38 2286 12.85
1.752 38210 5.40 2099 11.80
2.890 637789 90.12 9850 55.37
9.677 3956 0.56 228 1.28

Totals
707728 100.00 17789 100.00
20CV 5US 500 300

PDA-280nm
Results (System
(10/05/2018
12:29:37 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.413 16939 2.94 3155 20.45
1.530 5902 1.02 1612 10.45
1.752 19768 3.43 1627 10.55
2.905 533210 92.42 8968 58.13
9.670 1136 0.20 65 0.42

Totals
576955 100.00 15427 100.00
20CV 5US 500 360

PDA-280nm
Results (System
(10/05/2018
12:45:24 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.415 10743 1.44 2223 13.76
1.532 4446 0.59 1337 8.27
1.758 38304 5.12 2263 14.01
2.873 694542 92.85 10335 63.96

Totals
748035 100.00 16158 100.00
20CV 5US 500 sc

PDA-280nm
Results (System
(09/05/2018
09:51:35 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.122 1294 0.14 534 0.87
1.292 58004 6.27 4630 7.50
1.503 16241 1.75 2780 4.50
1.675 40376 4.36 3511 5.69
1.870 15415 1.67 2607 4.22
1.990 30881 3.34 2514 4.07
2.222 8065 0.87 1285 2.08
2.400 10558 1.14 826 1.34
2.737 2202 0.24 279 0.45
2.843 11816 1.28 423 0.69
3.210 17963 1.94 878 1.42
8.655 711677 76.89 41384 67.06
11.978 1131 0.12 59 0.10

Totals
925623 100.00 61710 100.00
PDA-280nm
Results (System
(04/05/2018
11:33:42 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.397 4056 0.22 672 0.67
1.503 5437 0.29 1593 1.60
1.678 55251 2.98 3210 3.22
2.027 31673 1.71 2998 3.01
2.273 24824 1.34 2450 2.46
2.350 49759 2.69 2461 2.47
2.757 22770 1.23 2432 2.44
2.903 14730 0.80 2471 2.48
3.003 29968 1.62 2572 2.58
3.223 68365 3.69 2625 2.63
8.668 1544140 83.42 76140 76.43

Totals
1850973 100.00 99624 100.00
50CU 5US 500 0 2

PDA-280nm
Results (System
(07/05/2018
11:01:35 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.408 9354 0.37 1885 1.40
1.528 6585 0.26 1072 0.80
1.712 19953 0.79 2293 1.71
1.845 14157 0.56 2123 1.58
2.668 315842 12.47 9953 7.41
2.843 167174 6.60 9713 7.23
3.112 167201 6.60 8145 6.06
3.703 33968 1.34 2399 1.79
5.468 10556 0.42 490 0.36
6.503 14178 0.56 142 0.11
7.143 714 0.03 69 0.05
10.017 1773353 70.01 96104 71.51

Totals
2533035 100.00 134388 100.00
50CU 5US 500 15 2

PDA-280nm
Results (System
(07/05/2018
11:17:24 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.417 6067 0.20 1385 0.75
1.527 17581 0.58 2553 1.38
1.703 30518 1.01 3025 1.63
1.950 23968 0.79 2706 1.46
2.120 43570 1.44 5430 2.93
2.680 256126 8.49 10377 5.60
2.747 43424 1.44 10364 5.59
2.813 77632 2.57 10379 5.60
2.958 316241 10.48 9838 5.31
5.412 344267 11.41 28501 15.37
6.602 16514 0.55 238 0.13
6.805 671 0.02 96 0.05
9.973 1841189 61.01 100511 54.21

Totals
3017768 100.00 185403 100.00
50CU 5US 500 30 2

PDA-280nm
Results (System
(07/05/2018
11:33:17 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.418 5628 0.20 1273 0.68
1.535 25744 0.92 3594 1.92
1.710 35344 1.27 3473 1.86
1.948 28671 1.03 3180 1.70
2.118 66363 2.38 10061 5.39
2.717 251450 9.01 11019 5.90
2.770 37400 1.34 11021 5.90
2.843 93905 3.37 11176 5.98
2.997 252993 9.07 10187 5.45
3.573 76324 2.74 4256 2.28
5.460 387469 13.89 33807 18.10
7.897 547 0.02 39 0.02
9.103 1919 0.07 130 0.07
10.023 1526323 54.70 83589 44.74
10.737 44 0.00 16 0.01

Totals
2790124 100.00 186821 100.00
50CU 5US 500 45

PDA-280nm
Results (System
(07/05/2018
11:49:08 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.527 43150 1.71 4573 2.76
1.682 46771 1.86 4374 2.64
1.948 34636 1.38 3803 2.29
2.118 63394 2.52 8377 5.05
2.688 316434 12.56 11556 6.96
2.810 92034 3.65 11378 6.85
2.963 221207 8.78 10575 6.37
3.398 44447 1.76 5744 3.46
3.545 81983 3.26 4513 2.72
5.417 453338 18.00 39479 23.78
7.835 1292 0.05 74 0.04
8.257 63 0.00 9 0.01
9.070 2416 0.10 147 0.09
9.427 1230 0.05 88 0.05
9.975 1116038 44.31 61298 36.93

Totals
2518433 100.00 165988 100.00
50CU 5US 500 60

PDA-280nm
Results (System
(08/05/2018
12:04:54 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.533 56990 2.38 6274 4.12
1.718 52324 2.18 4868 3.20
1.950 44737 1.87 5029 3.30
2.118 92284 3.85 14545 9.56
2.705 320509 13.36 11881 7.81
2.835 358521 14.95 11608 7.63
3.573 74322 3.10 4232 2.78
5.468 510175 21.27 44753 29.40
9.097 1924 0.08 131 0.09
10.030 886625 36.97 48875 32.11

Totals
2398411 100.00 152196 100.00
50CU 5US 500 90

PDA-280nm
Results (System
(08/05/2018
12:20:46 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.532 89053 3.78 9588 5.71
1.675 86636 3.67 8108 4.83
1.878 30715 1.30 5994 3.57
1.947 33487 1.42 6195 3.69
2.063 50445 2.14 5780 3.44
2.710 468108 19.85 12801 7.62
2.987 101494 4.30 11924 7.10
3.148 165560 7.02 12371 7.37
3.437 45076 1.91 6133 3.65
3.577 91370 3.87 5152 3.07
5.467 560309 23.76 48949 29.15
10.028 635955 26.97 34950 20.81

Totals
2358208 100.00 167945 100.00
50CU 5US 500 120

PDA-280nm
Results (System
(08/05/2018
12:36:38 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.535 103250 4.47 11480 6.42
1.672 60995 2.64 10126 5.66
1.747 89765 3.89 9744 5.45
1.947 43892 1.90 7669 4.29
2.062 53770 2.33 6954 3.89
2.325 128487 5.57 13718 7.67
2.615 196100 8.50 13674 7.65
2.782 192550 8.34 13570 7.59
2.985 151749 6.58 14309 8.00
3.140 328733 14.25 12555 7.02
4.123 10615 0.46 1009 0.56
5.465 402329 17.43 34599 19.35
6.492 10702 0.46 197 0.11
8.897 3127 0.14 140 0.08
10.033 526537 22.82 28856 16.14
12.132 5018 0.22 169 0.09

Totals
2307619 100.00 178769 100.00
50CU 5US 500 180

PDA-280nm
Results (System
(08/05/2018
12:52:23 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.513 341584 10.93 37918 13.23
1.658 212348 6.80 21636 7.55
1.895 154578 4.95 15741 5.49
2.115 255783 8.19 43208 15.08
2.315 115294 3.69 12928 4.51
2.432 139188 4.46 15348 5.36
2.592 125923 4.03 16225 5.66
2.707 94159 3.01 14931 5.21
2.812 446256 14.29 14665 5.12
3.530 108854 3.48 6238 2.18
4.078 15815 0.51 1563 0.55
5.377 757029 24.23 66506 23.20
7.010 203 0.01 16 0.01
7.363 152 0.00 15 0.01
9.050 422 0.01 36 0.01
9.937 356286 11.41 19633 6.85

Totals
3123874 100.00 286607 100.00
50CU 5US 500 240

PDA-280nm
Results (System
(08/05/2018
01:08:08 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.503 491785 21.20 44466 20.85
1.735 96406 4.16 17255 8.09
1.898 133860 5.77 15256 7.15
2.122 176061 7.59 27839 13.05
2.473 170688 7.36 12128 5.69
2.643 158459 6.83 14498 6.80
2.777 142927 6.16 13225 6.20
2.940 144082 6.21 13086 6.14
3.138 271101 11.69 11067 5.19
4.183 9423 0.41 1017 0.48
5.517 435078 18.75 38409 18.01
10.083 90141 3.89 5025 2.36

Totals
2320011 100.00 213271 100.00
50CU 5US 500 300

PDA-280nm
Results (System
(08/05/2018
01:24:03 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.502 340578 20.25 39274 23.68
1.653 87582 5.21 18232 10.99
1.740 96198 5.72 16594 10.00
1.902 154361 9.18 23544 14.20
2.123 94301 5.61 12361 7.45
2.645 283825 16.88 12518 7.55
2.757 69906 4.16 12344 7.44
2.877 210562 12.52 12739 7.68
3.155 257954 15.34 10805 6.51
4.143 8439 0.50 911 0.55
5.478 66274 3.94 5885 3.55
10.047 11856 0.70 652 0.39

Totals
1681836 100.00 165859 100.00
50CU 5US 500 360

PDA-280nm
Results (System
(08/05/2018
01:39:49 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.507 168030 15.73 15681 30.38
1.660 108882 10.19 9072 17.58
1.950 29718 2.78 4400 8.53
2.757 345473 32.34 11223 21.74
2.840 416088 38.95 11236 21.77

Totals
1068191 100.00 51612 100.00
50CU 5US 500 SC

PDA-280nm
Results (System
(05/05/2018
12:09:37 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.480 12416 2.09 1470 15.29
2.497 580963 97.91 8144 84.71

Totals
593379 100.00 9614 100.00
50CU 5US 500 SC 2

PDA-280nm
Results (System
(07/05/2018
10:45:41 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.297 100549 4.22 7013 5.02
1.507 37969 1.60 5571 3.99
1.675 130714 5.49 7263 5.20
1.987 77705 3.26 6893 4.93
2.173 66657 2.80 6175 4.42
2.417 65001 2.73 5874 4.20
2.532 46395 1.95 5674 4.06
2.902 174112 7.32 7441 5.32
3.213 145278 6.10 4983 3.57
4.323 756 0.03 108 0.08
6.025 16495 0.69 632 0.45
7.863 1922 0.08 139 0.10
8.680 1514401 63.63 81809 58.54
12.030 1137 0.05 95 0.07
12.103 977 0.04 90 0.06

Totals
2380068 100.00 139760 100.00
50CU SI 500 0

PDA-280nm
Results (System
(08/05/2018
09:43:22 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.407 18413 0.77 2160 1.81
1.543 5107 0.21 1133 0.95
1.708 31597 1.32 2096 1.76
2.732 284348 11.90 8707 7.30
2.857 286027 11.97 8671 7.27
3.748 31503 1.32 2189 1.84
10.058 1731338 72.45 94228 79.02
13.590 1275 0.05 55 0.05

Totals
2389608 100.00 119239 100.00
50CU SI 500 15

PDA-280nm
Results (System
(08/05/2018
09:59:08 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.405 4009 0.17 824 0.73
1.542 4669 0.20 1065 0.95
1.740 28816 1.24 2072 1.84
2.858 428404 18.50 9578 8.53
3.158 238797 10.31 10346 9.21
4.458 482 0.02 66 0.06
5.502 13836 0.60 1222 1.09
7.198 3479 0.15 253 0.23
10.085 1592781 68.77 86812 77.30
13.588 622 0.03 41 0.04
13.850 135 0.01 26 0.02

Totals
2316030 100.00 112305 100.00
50CU SI 500 30

PDA-280nm
Results (System
(08/05/2018
10:14:58 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.407 5709 0.27 1078 1.04
1.542 5074 0.24 1212 1.17
1.748 29803 1.38 2210 2.14
2.733 290648 13.50 9717 9.40
2.863 384231 17.84 9811 9.49
5.502 16403 0.76 1452 1.41
10.093 1421245 66.01 77821 75.31
10.795 123 0.01 30 0.03

Totals
2153236 100.00 103331 100.00
50CU SI 500 45

PDA-280nm
Results (System
(08/05/2018
10:30:46 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.408 4157 0.18 953 0.89
1.540 4822 0.21 1169 1.09
1.738 27438 1.22 2062 1.92
2.717 316937 14.10 9935 9.25
2.847 384652 17.11 9984 9.30
5.452 21071 0.94 1861 1.73
10.040 1489196 66.24 81430 75.82

Totals
2248273 100.00 107394 100.00
50CU SI 500 90

PDA-280nm
Results (System
(08/05/2018
11:02:17 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.412 4612 0.21 837 0.81
1.537 6608 0.30 1522 1.47
1.717 25962 1.16 2067 2.00
1.955 10835 0.48 1679 1.62
2.135 19729 0.88 2553 2.47
2.870 654182 29.24 10231 9.88
5.555 36587 1.64 3243 3.13
10.153 1477787 66.05 81348 78.57
12.425 1000 0.04 51 0.05

Totals
2237302 100.00 103531 100.00
50CU SI 500 120

PDA-280nm
Results (System
(08/05/2018
11:18:08 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.410 8277 0.38 1696 1.47
1.538 6424 0.30 1563 1.36
1.705 16515 0.77 2003 1.74
1.837 10166 0.47 1689 1.47
1.950 10851 0.50 1697 1.47
2.142 18471 0.86 2144 1.86
2.908 419177 19.48 10320 8.96
3.203 219261 10.19 12090 10.50
3.812 31991 1.49 2403 2.09
5.610 41698 1.94 3756 3.26
10.215 1369374 63.63 75817 65.83

Totals
2152205 100.00 115178 100.00
50CU SI 500 180

PDA-280nm
Results (System
(08/05/2018
11:33:58 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.495 26170 1.14 3296 2.56
1.717 17526 0.76 1891 1.47
1.953 15100 0.66 1715 1.33
2.128 28632 1.24 3831 2.98
2.733 268485 11.66 10439 8.11
2.857 177570 7.71 10557 8.20
3.158 240529 10.45 10492 8.15
5.513 59947 2.60 5347 4.15
9.163 876 0.04 65 0.05
10.112 1467770 63.74 81120 63.00

Totals
2302605 100.00 128753 100.00
50CU SI 500 240

PDA-280nm
Results (System
(08/05/2018
11:49:50 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.505 28790 1.23 3807 3.10
1.708 15650 0.67 1717 1.40
1.955 15482 0.66 1898 1.55
2.123 30940 1.32 4455 3.63
2.712 273764 11.70 10734 8.74
2.845 428837 18.33 10859 8.84
5.458 99747 4.26 8922 7.27
9.105 1620 0.07 107 0.09
10.052 1444809 61.75 80285 65.38
10.857 60 0.00 18 0.01

Totals
2339699 100.00 122802 100.00
50CU SI 500 300

PDA-280nm
Results (System
(09/05/2018
12:05:42 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.507 37273 1.53 4672 3.49
1.713 18705 0.77 1972 1.47
1.955 21377 0.88 2598 1.94
2.122 40479 1.66 5709 4.26
2.705 291564 11.97 10964 8.18
2.832 354266 14.54 11092 8.28
3.545 77984 3.20 4107 3.07
5.458 115959 4.76 10387 7.75
10.052 1478347 60.69 82475 61.56

Totals
2435954 100.00 133976 100.00
50CU SI 500 360

PDA-280nm
Results (System
(09/05/2018
12:21:29 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.502 61393 2.46 7669 5.17
1.707 27174 1.09 2805 1.89
1.955 35170 1.41 3850 2.59
2.123 52143 2.09 7082 4.77
2.730 311101 12.45 11461 7.72
2.850 190168 7.61 11553 7.78
3.157 286473 11.46 12998 8.76
5.513 146380 5.86 13147 8.86
10.110 1389396 55.59 77868 52.46

Totals
2499398 100.00 148433 100.00
50CU SI 500 SC

PDA-280nm
Results (System
(08/05/2018
09:27:36 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.397 4026 0.33 724 1.01
1.498 3749 0.31 1076 1.49
1.687 38145 3.11 2996 4.16
1.977 21260 1.73 2503 3.48
2.190 15835 1.29 1957 2.72
2.410 7723 0.63 785 1.09
2.510 4372 0.36 603 0.84
2.737 5332 0.43 773 1.07
2.990 3113 0.25 356 0.49
3.215 14635 1.19 1437 2.00
4.250 178 0.01 10 0.01
6.053 26077 2.13 528 0.73
6.722 15740 1.28 321 0.45
8.640 1066060 86.94 57932 80.46

Totals
1226245 100.00 72001 100.00
50CU SI 500 SC2

PDA-280nm
Results (System
(07/05/2018
10:45:41 p.m.)
(Original))

Retention Time Area Area % Height Height %

1.297 100549 4.22 7013 5.02
1.507 37969 1.60 5571 3.99
1.675 130714 5.49 7263 5.20
1.987 77705 3.26 6893 4.93
2.173 66657 2.80 6175 4.42
2.417 65001 2.73 5874 4.20
2.532 46395 1.95 5674 4.06
2.902 174112 7.32 7441 5.32
3.213 145278 6.10 4983 3.57
4.323 756 0.03 108 0.08
6.025 16495 0.69 632 0.45
7.863 1922 0.08 139 0.10
8.680 1514401 63.63 81809 58.54
12.030 1137 0.05 95 0.07
12.103 977 0.04 90 0.06

Totals
2380068 100.00 139760 100.00
50CU SI 500 0
 PDA-280nm
Results (System
(08/05/2018
09:43:22 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.407 18413 0.77 2160 1.81
1.543 5107 0.21 1133 0.95
1.708 31597 1.32 2096 1.76
2.732 284348 11.90 8707 7.30
2.857 286027 11.97 8671 7.27
3.748 31503 1.32 2189 1.84
10.058 1731338 72.45 94228 79.02
13.590 1275 0.05 55 0.05

Totals
2389608 100.00 119239 100.00

50CU SI 500 15

PDA-280nm
Results (System
 (08/05/2018
09:59:08 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.405 4009 0.17 824 0.73
1.542 4669 0.20 1065 0.95
1.740 28816 1.24 2072 1.84
2.858 428404 18.50 9578 8.53
3.158 238797 10.31 10346 9.21
4.458 482 0.02 66 0.06
5.502 13836 0.60 1222 1.09
7.198 3479 0.15 253 0.23
10.085 1592781 68.77 86812 77.30
13.588 622 0.03 41 0.04
13.850 135 0.01 26 0.02

Totals
2316030 100.00 112305 100.00

50CU SI 500 30

PDA-280nm
Results (System
(08/05/2018
 10:14:58 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.407 5709 0.27 1078 1.04
1.542 5074 0.24 1212 1.17
1.748 29803 1.38 2210 2.14
2.733 290648 13.50 9717 9.40
2.863 384231 17.84 9811 9.49
5.502 16403 0.76 1452 1.41
10.093 1421245 66.01 77821 75.31
10.795 123 0.01 30 0.03

Totals
2153236 100.00 103331 100.00

50CU SI 500 45

PDA-280nm
Results (System
(08/05/2018
10:30:46 p.m.)
 (Original))
Retention Time Area Area % Height Height %
1.408 4157 0.18 953 0.89
1.540 4822 0.21 1169 1.09
1.738 27438 1.22 2062 1.92
2.717 316937 14.10 9935 9.25
2.847 384652 17.11 9984 9.30
5.452 21071 0.94 1861 1.73
10.040 1489196 66.24 81430 75.82

Totals
2248273 100.00 107394 100.00

50CU SI 500 60

PDA-280nm
Results (System
(08/05/2018
10:46:32 p.m.)
(Original))
 Retention Time Area Area % Height Height %
1.410 7377 0.30 1520 1.26
1.538 4717 0.20 1248 1.03
1.712 29087 1.20 2075 1.72
1.950 9795 0.40 1731 1.43
2.870 450939 18.64 10433 8.63
3.175 233616 9.66 10152 8.40
5.557 30833 1.27 2749 2.27
9.243 776 0.03 57 0.05
10.150 1650950 68.25 90824 75.15
13.705 667 0.03 42 0.03
14.013 94 0.00 19 0.02

Totals
2418851 100.00 120850 100.00

50CU SI 500 90

PDA-280nm
Results (System
(08/05/2018
11:02:17 p.m.)
(Original))
Retention Time Area Area % Height Height %
 1.412 4612 0.21 837 0.81
1.537 6608 0.30 1522 1.47
1.717 25962 1.16 2067 2.00
1.955 10835 0.48 1679 1.62
2.135 19729 0.88 2553 2.47
2.870 654182 29.24 10231 9.88
5.555 36587 1.64 3243 3.13
10.153 1477787 66.05 81348 78.57
12.425 1000 0.04 51 0.05

Totals
2237302 100.00 103531 100.00

50CU SI 500 120

PDA-280nm
Results (System
(08/05/2018
11:18:08 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.410 8277 0.38 1696 1.47
 1.538 6424 0.30 1563 1.36
1.705 16515 0.77 2003 1.74
1.837 10166 0.47 1689 1.47
1.950 10851 0.50 1697 1.47
2.142 18471 0.86 2144 1.86
2.908 419177 19.48 10320 8.96
3.203 219261 10.19 12090 10.50
3.812 31991 1.49 2403 2.09
5.610 41698 1.94 3756 3.26
10.215 1369374 63.63 75817 65.83

Totals
2152205 100.00 115178 100.00

50CU SI 500 180

PDA-280nm
Results (System
(08/05/2018
11:33:58 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.495 26170 1.14 3296 2.56
1.717 17526 0.76 1891 1.47
 1.953 15100 0.66 1715 1.33
2.128 28632 1.24 3831 2.98
2.733 268485 11.66 10439 8.11
2.857 177570 7.71 10557 8.20
3.158 240529 10.45 10492 8.15
5.513 59947 2.60 5347 4.15
9.163 876 0.04 65 0.05
10.112 1467770 63.74 81120 63.00

Totals
2302605 100.00 128753 100.00

50CU SI 500 240

PDA-280nm
Results (System
(08/05/2018
11:49:50 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.505 28790 1.23 3807 3.10
1.708 15650 0.67 1717 1.40
1.955 15482 0.66 1898 1.55
 2.123 30940 1.32 4455 3.63
2.712 273764 11.70 10734 8.74
2.845 428837 18.33 10859 8.84
5.458 99747 4.26 8922 7.27
9.105 1620 0.07 107 0.09
10.052 1444809 61.75 80285 65.38
10.857 60 0.00 18 0.01

Totals
2339699 100.00 122802 100.00

50CU SI 500 300

PDA-280nm
Results (System
(09/05/2018
12:05:42 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.507 37273 1.53 4672 3.49
1.713 18705 0.77 1972 1.47
1.955 21377 0.88 2598 1.94
2.122 40479 1.66 5709 4.26
 2.705 291564 11.97 10964 8.18
2.832 354266 14.54 11092 8.28
3.545 77984 3.20 4107 3.07
5.458 115959 4.76 10387 7.75
10.052 1478347 60.69 82475 61.56

Totals
2435954 100.00 133976 100.00

50CU SI 500 360

PDA-280nm
Results (System
(09/05/2018
12:21:29 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.502 61393 2.46 7669 5.17
1.707 27174 1.09 2805 1.89
1.955 35170 1.41 3850 2.59
2.123 52143 2.09 7082 4.77
2.730 311101 12.45 11461 7.72
 2.850 190168 7.61 11553 7.78
3.157 286473 11.46 12998 8.76
5.513 146380 5.86 13147 8.86
10.110 1389396 55.59 77868 52.46

Totals
2499398 100.00 148433 100.00

50CU SI 500 SC

PDA-280nm
Results (System
(08/05/2018
09:27:36 p.m.)
(Original))
Retention Time Area Area % Height Height %
1.397 4026 0.33 724 1.01
1.498 3749 0.31 1076 1.49
1.687 38145 3.11 2996 4.16
1.977 21260 1.73 2503 3.48
2.190 15835 1.29 1957 2.72
2.410 7723 0.63 785 1.09
2.510 4372 0.36 603 0.84
 2.737 5332 0.43 773 1.07
2.990 3113 0.25 356 0.49
3.215 14635 1.19 1437 2.00
4.250 178 0.01 10 0.01
6.053 26077 2.13 528 0.73
6.722 15740 1.28 321 0.45
8.640 1066060 86.94 57932 80.46

Totals
1226245 100.00 72001 100.00

50CUV 5I500N 0

PDA-280nm
Results (System
(08/05/2018
02:11:59 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.408 8092 0.37 1504 1.61
1.537 4201 0.19 852 0.91
1.737 31320 1.43 2304 2.46
2.147 40731 1.86 3720 3.98
2.850 773191 35.34 12035 12.86
9.550 2271 0.10 158 0.17
10.023 1327980 60.70 72990 78.01
 Totals
2187786 100.00 93563 100.00

50CUV 5I500N 15

PDA-280nm
Results (System
(08/05/2018
02:27:44 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.407 8012 0.33 1548 1.52
1.538 2029 0.08 764 0.75
1.598 1497 0.06 669 0.66
1.742 29608 1.23 2253 2.21
2.865 808544 33.62 11617 11.40
10.033 1554955 64.66 85030 83.46

Totals
2404645 100.00 101881 100.00
50CUV 5I500N 30

PDA-280nm
Results (System
(08/05/2018
02:43:29 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.402 5392 0.23 1059 1.07
1.523 1646 0.07 543 0.55
1.598 1536 0.07 641 0.65
1.747 29239 1.25 2131 2.15
2.877 786619 33.54 11696 11.78
5.570 2013 0.09 155 0.16
10.080 1519162 64.77 83095 83.66

Totals
2345607 100.00 99320 100.00
50CUV 5I500N 45

PDA-280nm
Results (System
(08/05/2018
02:59:15 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.407 4043 0.12 667 0.21
1.515 6066 0.18 1171 0.37
1.747 30514 0.93 2226 0.70
2.315 157003 4.78 20176 6.38
2.865 407362 12.41 11869 3.75
3.167 1213948 36.97 198048 62.59
5.520 45108 1.37 3863 1.22
5.817 15343 0.47 1226 0.39
9.165 819 0.02 63 0.02
10.082 1402682 42.72 77047 24.35
13.588 879 0.03 48 0.02
 Totals
3283767 100.00 316404 100.00

50CUV 5I500N 60

PDA-280nm
Results (System
(08/05/2018
03:15:00 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.403 6590 0.25 1205 1.07
1.525 2157 0.08 677 0.60
1.598 1494 0.06 661 0.59
1.752 28726 1.11 2154 1.91
2.877 785315 30.38 11723 10.41
5.538 3132 0.12 276 0.25
9.175 903 0.03 55 0.05
10.072 1756895 67.96 95892 85.13

Totals
2585212 100.00 112643 100.00
50CUV 5I500N 90

PDA-280nm
Results (System
(08/05/2018
03:30:51 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.402 6689 0.27 1147 1.09
1.530 2441 0.10 752 0.72
1.600 1142 0.05 584 0.56
1.750 28810 1.18 2104 2.01
2.880 783942 32.14 11686 11.14
5.543 5816 0.24 514 0.49
9.558 2203 0.09 165 0.16
10.085 1608382 65.93 87931 83.84

Totals
2439425 100.00 104883 100.00
50CUV 5I500N 120

PDA-280nm
Results (System
(08/05/2018
03:46:37 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.405 6276 0.24 1119 0.99
1.540 4365 0.17 1096 0.97
1.750 23784 0.91 2159 1.92
2.850 825761 31.47 11762 10.45
5.445 6422 0.24 575 0.51
9.980 1757334 66.97 95849 85.15

Totals
2623942 100.00 112560 100.00
50CUV 5I500N 240

PDA-280nm
Results (System
(08/05/2018
04:18:13 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.408 8155 0.36 1557 1.49
1.542 4132 0.18 1139 1.09
1.750 24008 1.07 2061 1.97
2.850 536011 23.83 11907 11.37
3.137 271407 12.06 10802 10.31
5.490 7150 0.32 642 0.61
10.030 1398653 62.17 76624 73.14
10.688 119 0.01 27 0.03

Totals
2249635 100.00 104759 100.00
50CUV 5I500N 300

PDA-280nm
Results (System
(08/05/2018
04:34:05 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.408 4538 0.17 793 0.69
1.537 6566 0.25 1430 1.24
1.753 19231 0.72 2021 1.75
2.903 831344 31.11 11978 10.36
5.525 19497 0.73 1706 1.48
10.085 1791378 67.03 97639 84.49

Totals
2672554 100.00 115567 100.00
50CUV 5I500N 360

PDA-280nm
Results (System
(08/05/2018
04:47:28 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.408 4591 0.20 787 0.76
1.537 5819 0.25 1361 1.32
1.753 21790 0.94 2243 2.17
2.843 589556 25.41 12340 11.96
3.125 314889 13.57 11331 10.98
5.430 18965 0.82 1334 1.29
6.417 10928 0.47 142 0.14
 9.977 1353801 58.34 73662 71.38

Totals
2320339 100.00 103200 100.00

50CUV 5I500N SC

PDA-280nm
Results (System
(08/05/2018
01:56:06 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.405 7647 0.30 1261 1.12
1.540 3014 0.12 999 0.88
1.597 2972 0.11 1016 0.90
2.463 797641 30.82 12033 10.64
3.193 147585 5.70 9311 8.23
3.490 98329 3.80 4965 4.39
6.707 7901 0.31 560 0.50
8.618 2839 0.11 178 0.16
9.507 1519830 58.73 82748 73.18

Totals
2587758 100.00 113071 100.00
120 D

PDA-280nm
Results (System
(09/06/2018
01:34:26 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.423 476 0.01 117 0.03
1.543 3649 0.10 553 0.16
1.643 4303 0.12 964 0.27
1.755 8650 0.25 766 0.22
1.923 11821 0.34 999 0.28
2.277 2760497 79.38 301716 84.80
2.533 411418 11.83 36999 10.40
2.992 276730 7.96 13688 3.85

Totals
3477544 100.00 355802 100.00
150 D

PDA-280nm
Results (System
(09/06/2018
01:43:51 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.503 1489 0.04 320 0.10
1.585 8580 0.23 1384 0.44
1.875 2485980 67.45 229621 72.73
2.132 492915 13.37 39327 12.46
2.565 398774 10.82 20116 6.37
2.968 291660 7.91 24352 7.71
3.755 6286 0.17 582 0.18

Totals
3685684 100.00 315702 100.00
150 d (excelente)

PDA-280nm
Results (System
(09/06/2018
02:29:56 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.523 2080 0.07 347 0.13
1.620 4844 0.16 1068 0.39
1.770 8127 0.27 1567 0.57
1.985 2117179 70.75 202861 73.48
2.247 372856 12.46 32205 11.67
2.672 253306 8.47 15698 5.69
2.952 51619 1.73 6844 2.48
3.145 182298 6.09 15477 5.61

Totals
 2992309 100.00 276067 100.00

180 D

PDA-280nm
Results (System
(09/06/2018
01:52:48 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.427 374 0.01 102 0.03
1.645 6359 0.14 815 0.24
1.763 14641 0.31 565 0.17
2.288 2805420 60.03 269357 79.25
2.548 1846333 39.51 69058 20.32

Totals
4673127 100.00 339897 100.00
180 d (bien)

PDA-280nm
Results (System
(09/06/2018
02:08:44 a.m.)
(Original))
Retention Time Area Area % Height Height %
0.262 5892 0.12 2057 0.87
0.692 217987 4.35 22048 9.30
0.808 218335 4.36 22954 9.68
1.015 490260 9.79 50985 21.50
1.415 2832533 56.58 100088 42.21
2.158 1241009 24.79 39013 16.45

Totals
5006016 100.00 237145 100.00
180 d (excelente)

PDA-280nm
Results (System
(09/06/2018
02:35:19 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.528 2294 0.07 310 0.10
1.638 3371 0.10 789 0.25
1.785 8764 0.26 831 0.26
2.083 2264621 66.84 220655 69.20
2.340 386885 11.42 40409 12.67
2.558 102323 3.02 17283 5.42
2.772 334485 9.87 19330 6.06
3.100 89114 2.63 7525 2.36
3.440 196161 5.79 11748 3.68

Totals
 3388018 100.00 318880 100.00

210 D

PDA-280nm
Results (System
(09/06/2018
02:00:11 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.427 388 0.01 104 0.03
1.543 2887 0.06 428 0.12
1.647 3240 0.06 776 0.21
1.755 5814 0.12 504 0.14
1.923 7116 0.14 669 0.18
2.267 3112627 61.85 289769 78.81
2.522 1900407 37.76 75414 20.51

Totals
5032479 100.00 367664 100.00
210 d (bien)

PDA-280nm
Results (System
(09/06/2018
02:22:35 a.m.)
(Original))
Retention Time Area Area % Height Height %
0.072 13733 0.38 3169 1.44
0.487 57936 1.62 5861 2.66
0.828 333387 9.33 33390 15.16
1.097 347413 9.72 26836 12.18
1.402 1399167 39.14 77866 35.35
1.783 472928 13.23 36709 16.67
1.928 779984 21.82 25725 11.68
2.585 170064 4.76 10701 4.86

Totals
3574612 100.00 220257 100.00
210 d (excelente)

PDA-280nm
Results (System
(09/06/2018
02:40:33 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.427 41915 1.22 1454 0.60
1.637 22309 0.65 1990 0.82
1.757 37050 1.07 1666 0.68
2.280 2088387 60.57 183577 75.47
2.532 1258184 36.49 54554 22.43

Totals
3447845 100.00 243241 100.00
240 d (bien)

PDA-280nm
Results (System
(09/06/2018
02:14:29 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.517 1770 0.06 270 0.10
1.623 3745 0.12 918 0.34
1.773 6028 0.20 1211 0.45
1.987 2029517 67.28 187102 69.04
2.248 429147 14.23 38856 14.34
2.677 279291 9.26 17184 6.34
2.957 61733 2.05 8020 2.96
3.155 205256 6.80 17432 6.43
 Totals
3016487 100.00 270993 100.00

240 d (excelente)

PDA-280nm
Results (System
(09/06/2018
02:45:45 a.m.)
(Original))
Retention Time Area Area % Height Height %
1.423 41719 1.23 1481 0.66
1.637 22644 0.67 2052 0.92
1.755 43537 1.28 1780 0.79
2.313 1902525 56.14 164715 73.47
2.568 1378760 40.68 54172 24.16

Totals
3389185 100.00 224200 100.00